#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:42:55 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181280 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/58/2235884.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235884_Fobs loop_ _publ_author_name 'Cukrowski, Ignacy' 'Adeyinka, Adedapo S.' 'Liles, David C.' _publ_section_title ; 3,6-Diazaoctane-1,8-diaminium diiodide ; _journal_coeditor_code JJ2132 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2387 _journal_volume 68 _journal_year 2012 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 8.1253 _cell_length_b 8.6138 _cell_length_c 18.9368 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.6401 _cod_data_source_file jj2132Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' up1110 (S_17) in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 311.51 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10968.07 11260.86 235.27 o 4 0 0 34441.05 32329.47 683.00 o 6 0 0 15202.22 15267.86 391.32 o 8 0 0 562.47 546.46 30.30 o 10 0 0 7871.95 7811.77 361.43 o 12 0 0 842.68 781.09 88.95 o 2 1 0 95843.79 82241.53 1452.89 o 4 1 0 8865.66 8413.35 151.14 o 6 1 0 5430.61 5345.02 135.80 o 8 1 0 8898.34 9252.91 249.60 o 10 1 0 121.26 126.50 26.73 o 12 1 0 1630.62 1548.59 77.98 o 0 2 0 672.14 581.78 16.22 o 2 2 0 304.30 325.20 6.73 o 4 2 0 2933.79 2903.74 48.75 o 6 2 0 1074.60 1152.49 30.43 o 8 2 0 10.91 17.14 18.64 o 10 2 0 274.90 232.67 31.72 o 12 2 0 16.06 -6.79 53.86 o 2 3 0 17038.55 16476.71 243.87 o 4 3 0 5736.04 5895.14 119.89 o 6 3 0 1444.17 1445.58 50.54 o 8 3 0 4276.29 4407.23 104.37 o 10 3 0 0.53 -2.29 37.42 o 12 3 0 298.09 250.64 68.82 o 0 4 0 62237.46 52901.66 1600.63 o 2 4 0 15646.34 15529.84 349.12 o 4 4 0 15646.25 15331.62 376.72 o 6 4 0 18390.02 19049.54 455.96 o 8 4 0 1273.91 1320.87 36.63 o 10 4 0 5230.47 5358.18 231.77 o 12 4 0 154.09 131.62 60.91 o 2 5 0 33904.67 31370.19 1082.71 o 4 5 0 18894.76 18863.05 462.38 o 6 5 0 6205.57 6675.05 198.48 o 8 5 0 7822.45 8411.53 313.64 o 10 5 0 0.25 5.61 35.40 o 0 6 0 11356.07 10795.73 556.84 o 2 6 0 705.69 583.38 20.67 o 4 6 0 7991.91 8540.41 276.56 o 6 6 0 3242.52 3352.23 404.09 o 8 6 0 95.37 109.00 32.65 o 10 6 0 834.33 806.66 60.75 o 2 7 0 68.62 68.45 17.25 o 4 7 0 343.73 323.17 32.09 o 6 7 0 9.71 12.09 36.28 o 8 7 0 70.57 75.83 48.40 o 10 7 0 0.38 -6.92 55.54 o 0 8 0 10214.06 10406.03 525.93 o 2 8 0 1638.99 1612.01 45.34 o 4 8 0 4545.60 4662.57 167.45 o 6 8 0 2352.26 2217.00 90.95 o 8 8 0 77.11 88.38 53.55 o 10 8 0 794.13 736.95 68.93 o 2 9 0 11518.50 11841.09 417.57 o 4 9 0 4136.27 4082.41 154.05 o 6 9 0 1469.26 1568.62 70.42 o 8 9 0 2092.68 2095.05 129.45 o 0 10 0 4917.19 5271.71 314.22 o 2 10 0 419.43 424.23 44.95 o 4 10 0 2358.48 2452.62 112.63 o 6 10 0 2522.69 2348.93 120.87 o 8 10 0 152.16 172.61 70.60 o 2 11 0 185.18 191.97 62.64 o 4 11 0 120.88 122.47 46.77 o 6 11 0 98.41 128.51 64.56 o 0 12 0 523.15 628.55 79.61 o 2 12 0 51.44 26.26 50.67 o 4 12 0 200.25 197.04 66.21 o 2 13 0 1401.13 1508.04 87.66 o 1 1 1 29.14 55.42 4.67 o 2 1 1 34090.10 32947.25 359.07 o 3 1 1 17091.07 17397.02 179.80 o 4 1 1 5066.69 5135.29 70.66 o 5 1 1 113.75 133.54 7.03 o 6 1 1 3017.80 3049.00 41.93 o 7 1 1 4364.92 4510.65 81.44 o 8 1 1 4336.77 4442.56 74.30 o 9 1 1 732.41 663.44 17.21 o 10 1 1 63.23 62.47 18.80 o 11 1 1 145.59 121.59 37.28 o 12 1 1 529.17 472.16 42.22 o 0 2 1 48007.11 41402.84 810.26 o 1 2 1 43033.44 39515.38 553.75 o 2 2 1 2359.82 2255.75 23.34 o 3 2 1 65.88 49.84 3.88 o 4 2 1 33153.36 32996.32 426.65 o 5 2 1 14360.29 14663.74 203.03 o 6 2 1 19261.52 19785.63 287.50 o 7 2 1 534.33 527.78 13.84 o 8 2 1 384.52 363.42 15.37 o 9 2 1 1947.96 2008.45 49.96 o 10 2 1 4104.93 4137.07 99.40 o 11 2 1 1317.38 1290.44 41.66 o 12 2 1 286.28 257.10 43.40 o 1 3 1 17774.00 16871.03 217.40 o 2 3 1 30477.16 28467.13 285.00 o 3 3 1 14770.31 14616.06 185.08 o 4 3 1 15779.81 15986.38 230.28 o 5 3 1 42.77 50.54 7.66 o 6 3 1 5336.73 5519.47 86.15 o 7 3 1 3593.75 3773.02 69.22 o 8 3 1 8879.21 8990.87 163.45 o 9 3 1 1108.86 1161.88 27.00 o 10 3 1 6.25 -14.97 26.55 o 11 3 1 206.80 213.08 31.39 o 12 3 1 821.35 749.67 45.87 o 0 4 1 5031.72 4481.80 158.82 o 1 4 1 2548.87 2355.13 45.28 o 2 4 1 2435.45 2479.89 43.88 o 3 4 1 2545.16 2778.55 42.28 o 4 4 1 1794.81 1781.10 28.59 o 5 4 1 1105.94 1154.32 20.41 o 6 4 1 2171.83 2228.09 34.92 o 7 4 1 390.23 400.30 13.93 o 8 4 1 291.91 299.92 15.06 o 9 4 1 225.87 197.04 18.34 o 10 4 1 566.15 594.68 31.80 o 11 4 1 110.02 111.22 31.39 o 12 4 1 5.83 12.66 43.19 o 1 5 1 464.62 469.20 21.46 o 2 5 1 2666.29 2644.87 50.49 o 3 5 1 1405.32 1357.10 28.85 o 4 5 1 492.69 531.12 17.09 o 5 5 1 22.70 32.16 12.82 o 6 5 1 203.87 231.56 16.34 o 7 5 1 297.02 324.48 15.76 o 8 5 1 615.85 632.54 18.55 o 9 5 1 95.61 128.88 27.25 o 10 5 1 36.99 45.66 29.96 o 11 5 1 0.81 -6.65 34.98 o 0 6 1 18934.40 18564.02 603.89 o 1 6 1 7497.30 7580.29 167.69 o 2 6 1 911.76 822.35 21.46 o 3 6 1 610.96 628.50 15.32 o 4 6 1 8734.88 9164.34 167.14 o 5 6 1 3936.36 3982.19 77.70 o 6 6 1 5106.95 5238.75 144.15 o 7 6 1 478.97 434.79 17.39 o 8 6 1 40.66 35.58 22.15 o 9 6 1 837.50 850.83 36.68 o 10 6 1 1569.89 1566.31 60.40 o 11 6 1 357.73 352.90 47.66 o 1 7 1 3124.98 3163.50 67.01 o 2 7 1 18017.17 17361.33 342.26 o 3 7 1 6830.07 6766.31 127.03 o 4 7 1 2831.89 2776.43 60.64 o 5 7 1 362.23 277.98 22.95 o 6 7 1 2438.06 2481.98 68.51 o 7 7 1 2853.61 3094.56 117.53 o 8 7 1 3412.78 3640.15 100.13 o 9 7 1 481.44 486.61 38.76 o 10 7 1 181.83 175.16 46.26 o 0 8 1 9573.83 10287.59 332.10 o 1 8 1 1424.76 1418.93 36.52 o 2 8 1 497.13 450.34 20.09 o 3 8 1 148.60 153.59 14.79 o 4 8 1 2939.06 2915.65 84.02 o 5 8 1 2574.56 2605.07 74.83 o 6 8 1 1040.07 1020.68 45.30 o 7 8 1 261.82 274.18 33.84 o 8 8 1 42.40 50.15 34.78 o 9 8 1 485.01 485.61 47.15 o 10 8 1 626.89 656.84 51.35 o 1 9 1 2.04 19.81 22.59 o 2 9 1 185.44 156.16 15.15 o 3 9 1 101.30 75.93 17.66 o 4 9 1 2.86 31.68 25.80 o 5 9 1 32.13 23.35 30.20 o 6 9 1 1.47 9.25 33.27 o 7 9 1 23.85 27.08 34.90 o 8 9 1 2.02 -10.70 39.71 o 9 9 1 0.03 13.35 49.07 o 0 10 1 1322.51 1376.35 55.66 o 1 10 1 543.22 611.99 29.48 o 2 10 1 192.84 169.04 30.44 o 3 10 1 77.46 81.53 26.92 o 4 10 1 765.18 817.48 38.18 o 5 10 1 426.16 434.53 34.68 o 6 10 1 683.22 637.59 39.09 o 7 10 1 158.98 156.58 40.89 o 8 10 1 13.87 19.95 45.26 o 1 11 1 702.26 781.60 43.21 o 2 11 1 2130.93 2282.24 71.50 o 3 11 1 1485.62 1503.35 55.12 o 4 11 1 1021.03 1085.95 45.69 o 5 11 1 0.92 26.27 36.00 o 6 11 1 504.77 528.86 44.97 o 7 11 1 336.23 347.10 44.64 o 0 12 1 1644.70 1768.56 95.96 o 1 12 1 681.39 731.18 43.60 o 2 12 1 248.81 276.75 42.76 o 3 12 1 106.66 110.08 41.00 o 4 12 1 705.30 771.91 63.11 o 5 12 1 650.46 677.25 46.37 o 1 13 1 23.39 21.71 47.55 o 2 13 1 275.54 304.80 50.67 o 3 13 1 129.40 146.83 51.04 o 2 0 2 4254.31 4480.95 65.22 o 3 0 2 4153.40 4226.21 58.01 o 4 0 2 4932.76 4995.32 79.12 o 5 0 2 71680.60 70561.82 1310.10 o 6 0 2 1800.69 1815.17 31.97 o 7 0 2 5567.35 5670.32 135.28 o 8 0 2 54.27 51.27 16.75 o 9 0 2 7316.25 7212.46 190.30 o 10 0 2 568.61 579.02 34.44 o 11 0 2 2533.12 2391.03 119.10 o 12 0 2 103.50 78.38 55.48 o 1 1 2 12230.72 12787.91 152.42 o 2 1 2 9401.78 9370.25 102.66 o 3 1 2 51988.60 50376.99 526.52 o 4 1 2 968.64 968.76 14.55 o 5 1 2 474.86 537.04 10.55 o 6 1 2 336.17 355.45 9.54 o 7 1 2 14812.84 14969.81 246.18 o 8 1 2 384.27 394.55 14.47 o 9 1 2 2524.96 2439.07 53.55 o 10 1 2 19.79 20.26 17.93 o 11 1 2 689.48 640.14 35.91 o 12 1 2 228.74 211.75 40.26 o 0 2 2 9744.26 9422.58 195.19 o 1 2 2 5811.69 5848.51 72.59 o 2 2 2 927.69 989.02 10.74 o 3 2 2 139.71 158.48 6.24 o 4 2 2 187.65 195.02 6.23 o 5 2 2 1142.98 1222.27 17.58 o 6 2 2 12.04 20.52 8.69 o 7 2 2 28.11 37.13 9.03 o 8 2 2 18.09 30.31 11.22 o 9 2 2 250.87 238.95 15.43 o 10 2 2 35.32 48.03 20.33 o 11 2 2 88.05 91.52 31.87 o 12 2 2 11.90 -13.50 41.67 o 1 3 2 7660.36 7324.77 81.72 o 2 3 2 208.06 205.06 9.41 o 3 3 2 13031.73 12811.90 162.72 o 4 3 2 2602.88 2803.27 54.29 o 5 3 2 2.43 9.80 6.02 o 6 3 2 276.95 295.77 11.26 o 7 3 2 2948.08 3042.69 46.44 o 8 3 2 86.06 102.57 13.18 o 9 3 2 922.39 921.34 24.70 o 10 3 2 4.95 -1.04 21.94 o 11 3 2 153.41 143.67 27.29 o 12 3 2 76.52 53.55 39.41 o 0 4 2 5821.63 5374.43 185.57 o 1 4 2 36108.85 32506.45 450.06 o 2 4 2 1140.33 1183.43 18.25 o 3 4 2 11271.44 11726.75 188.98 o 4 4 2 1772.55 1773.65 39.29 o 5 4 2 26306.08 26965.42 413.44 o 6 4 2 1335.67 1398.71 25.26 o 7 4 2 2183.94 2363.85 41.13 o 8 4 2 73.95 71.75 13.86 o 9 4 2 2254.32 2258.26 52.77 o 10 4 2 377.95 346.82 29.22 o 11 4 2 2384.40 2450.55 102.67 o 12 4 2 38.85 39.64 55.15 o 1 5 2 18933.07 18455.15 334.98 o 2 5 2 4302.98 4232.89 61.24 o 3 5 2 31908.89 30899.95 522.42 o 4 5 2 824.07 827.28 18.89 o 5 5 2 23.03 55.00 15.54 o 6 5 2 199.54 231.14 18.56 o 7 5 2 9995.04 10198.93 200.12 o 8 5 2 1049.71 1079.66 27.84 o 9 5 2 3013.37 3047.78 85.32 o 10 5 2 3.68 7.45 30.26 o 11 5 2 361.83 391.62 39.50 o 0 6 2 1579.45 1467.70 42.92 o 1 6 2 8397.27 8353.73 170.46 o 2 6 2 113.13 103.21 9.86 o 3 6 2 144.17 163.48 10.19 o 4 6 2 151.44 196.45 14.48 o 5 6 2 4940.82 4953.12 103.86 o 6 6 2 471.38 473.50 21.40 o 7 6 2 369.28 335.77 17.85 o 8 6 2 40.21 39.47 21.37 o 9 6 2 1356.82 1306.32 43.45 o 10 6 2 173.73 171.18 35.94 o 11 6 2 403.10 404.54 47.78 o 1 7 2 215.73 221.66 16.70 o 2 7 2 91.84 93.88 11.12 o 3 7 2 169.85 190.26 13.65 o 4 7 2 2.37 -5.53 15.16 o 5 7 2 3.78 -3.59 22.67 o 6 7 2 17.61 26.65 20.60 o 7 7 2 16.63 27.32 25.07 o 8 7 2 0.16 15.82 21.91 o 9 7 2 46.41 55.16 42.33 o 10 7 2 0.61 6.84 45.45 o 0 8 2 1616.16 1662.12 61.87 o 1 8 2 5137.96 5173.25 115.16 o 2 8 2 93.95 89.66 12.45 o 3 8 2 434.29 452.45 16.80 o 4 8 2 68.01 67.22 18.10 o 5 8 2 4948.51 5237.90 134.01 o 6 8 2 300.04 282.20 28.10 o 7 8 2 658.66 613.23 39.37 o 8 8 2 18.05 14.03 32.49 o 9 8 2 892.70 892.61 45.94 o 10 8 2 149.53 133.04 47.25 o 1 9 2 3487.43 3663.89 96.58 o 2 9 2 852.05 792.02 29.04 o 3 9 2 7863.62 8317.95 207.92 o 4 9 2 340.51 356.48 29.87 o 5 9 2 10.04 17.67 29.94 o 6 9 2 96.35 96.13 33.73 o 7 9 2 3909.43 4202.86 153.95 o 8 9 2 384.20 369.92 49.35 o 9 9 2 1134.17 1061.14 51.77 o 0 10 2 375.01 355.88 38.73 o 1 10 2 4224.88 4646.20 129.54 o 2 10 2 127.60 122.16 27.90 o 3 10 2 489.15 513.14 33.97 o 4 10 2 286.24 291.69 29.77 o 5 10 2 2559.03 2550.68 89.13 o 6 10 2 157.46 168.83 36.05 o 7 10 2 147.11 151.73 41.03 o 8 10 2 17.57 18.32 42.20 o 1 11 2 309.77 313.14 33.86 o 2 11 2 11.49 2.79 32.93 o 3 11 2 392.00 378.53 33.71 o 4 11 2 35.55 57.21 35.21 o 5 11 2 19.31 23.47 38.51 o 6 11 2 57.03 86.63 41.91 o 7 11 2 29.08 45.54 45.79 o 0 12 2 167.12 189.01 50.96 o 1 12 2 287.63 334.09 39.73 o 2 12 2 8.31 -4.67 41.24 o 3 12 2 8.52 -2.01 40.34 o 4 12 2 5.69 24.16 49.50 o 5 12 2 266.77 259.56 42.95 o 1 13 2 425.73 456.72 47.34 o 2 13 2 146.80 165.34 50.04 o 3 13 2 1099.19 1297.34 140.87 o 1 1 3 27765.28 27248.07 304.54 o 2 1 3 12087.76 12014.62 351.81 o 3 1 3 26502.34 26406.47 273.95 o 4 1 3 135.24 120.23 4.50 o 5 1 3 399.08 417.69 11.23 o 6 1 3 81.99 94.01 7.30 o 7 1 3 6898.13 7033.75 106.46 o 8 1 3 173.09 194.61 12.31 o 9 1 3 1747.33 1731.51 53.07 o 10 1 3 1.14 13.43 19.99 o 11 1 3 619.67 567.22 31.85 o 12 1 3 150.49 148.68 42.61 o 0 2 3 10859.66 10550.58 208.79 o 1 2 3 97036.83 86489.34 1806.81 o 2 2 3 10.53 26.74 3.44 o 3 2 3 4132.10 4005.19 48.26 o 4 2 3 5500.13 5723.61 71.43 o 5 2 3 31443.53 31434.48 494.32 o 6 2 3 2534.78 2691.23 38.80 o 7 2 3 2811.66 2898.93 50.13 o 8 2 3 22.53 21.49 11.10 o 9 2 3 5512.45 5634.02 113.07 o 10 2 3 603.36 564.84 23.21 o 11 2 3 2866.96 2779.61 88.31 o 12 2 3 42.97 29.77 41.69 o 1 3 3 29242.42 27215.40 378.88 o 2 3 3 3130.43 2927.56 35.34 o 3 3 3 43494.20 42400.10 551.96 o 4 3 3 3433.75 3552.37 93.73 o 5 3 3 11.08 19.39 6.87 o 6 3 3 731.11 743.87 14.96 o 7 3 3 9984.20 10677.95 184.56 o 8 3 3 1371.74 1358.95 34.58 o 9 3 3 2542.23 2628.45 79.69 o 10 3 3 8.08 -2.08 24.26 o 11 3 3 643.88 613.79 33.64 o 12 3 3 178.28 153.43 40.11 o 0 4 3 1562.03 1392.89 57.88 o 1 4 3 5963.47 5573.55 116.34 o 2 4 3 870.96 873.92 15.78 o 3 4 3 1183.42 1335.34 39.74 o 4 4 3 163.09 161.41 11.89 o 5 4 3 5058.54 5345.44 124.27 o 6 4 3 147.42 166.86 11.17 o 7 4 3 81.40 91.36 13.20 o 8 4 3 67.59 72.51 19.31 o 9 4 3 253.29 260.75 22.58 o 10 4 3 109.45 95.37 26.76 o 11 4 3 524.72 476.36 34.52 o 12 4 3 5.31 17.93 48.81 o 1 5 3 1141.52 1049.76 24.96 o 2 5 3 37.13 41.61 6.09 o 3 5 3 3197.45 3192.56 55.30 o 4 5 3 806.70 815.85 17.57 o 5 5 3 243.89 223.67 14.95 o 6 5 3 0.32 -3.51 16.40 o 7 5 3 1015.68 974.28 23.39 o 8 5 3 150.00 146.41 21.45 o 9 5 3 147.00 134.17 23.47 o 10 5 3 62.64 59.80 30.45 o 11 5 3 89.42 87.55 40.80 o 0 6 3 1666.92 1600.98 54.94 o 1 6 3 17005.76 16742.45 323.50 o 2 6 3 629.59 582.75 14.71 o 3 6 3 159.62 162.61 13.43 o 4 6 3 857.51 900.89 22.57 o 5 6 3 13475.98 13612.90 276.96 o 6 6 3 1089.65 1119.80 29.90 o 7 6 3 671.73 650.32 21.23 o 8 6 3 76.92 88.58 21.27 o 9 6 3 1989.32 1895.55 61.46 o 10 6 3 286.88 294.57 40.59 o 11 6 3 974.89 911.28 46.04 o 1 7 3 5026.54 5138.09 118.91 o 2 7 3 2546.10 2471.49 49.14 o 3 7 3 20716.58 20706.77 485.51 o 4 7 3 454.33 434.35 19.97 o 5 7 3 210.79 169.46 19.50 o 6 7 3 588.96 576.28 23.42 o 7 7 3 6851.42 7269.47 183.02 o 8 7 3 432.98 432.17 24.76 o 9 7 3 1083.24 1109.89 44.51 o 10 7 3 44.30 63.74 42.91 o 0 8 3 1750.15 1645.49 60.78 o 1 8 3 4404.93 4394.37 106.18 o 2 8 3 189.43 182.24 13.46 o 3 8 3 232.90 285.02 19.51 o 4 8 3 341.86 303.34 21.95 o 5 8 3 5678.75 5931.05 183.81 o 6 8 3 91.43 102.88 27.42 o 7 8 3 375.76 325.65 30.31 o 8 8 3 24.76 46.70 35.31 o 9 8 3 1053.30 1053.98 47.98 o 10 8 3 88.62 122.85 47.61 o 1 9 3 36.55 36.51 22.83 o 2 9 3 2.63 2.15 20.51 o 3 9 3 9.55 30.95 19.14 o 4 9 3 15.44 21.50 21.32 o 5 9 3 0.66 7.82 30.33 o 6 9 3 1.97 -0.18 30.99 o 7 9 3 169.09 206.34 39.02 o 8 9 3 40.74 36.87 40.35 o 9 9 3 10.41 24.54 42.44 o 0 10 3 610.82 629.39 47.10 o 1 10 3 1895.25 2023.45 72.52 o 2 10 3 74.07 87.90 23.05 o 3 10 3 70.89 81.17 27.02 o 4 10 3 104.31 104.34 28.73 o 5 10 3 1139.75 1083.75 43.92 o 6 10 3 3.31 -2.79 38.55 o 7 10 3 62.80 52.16 40.18 o 8 10 3 1.67 -8.90 45.31 o 1 11 3 1799.13 1833.38 64.34 o 2 11 3 301.22 326.42 34.61 o 3 11 3 3215.58 3332.81 122.06 o 4 11 3 125.37 101.56 37.90 o 5 11 3 6.74 -6.28 36.18 o 6 11 3 88.58 100.98 39.21 o 7 11 3 1001.18 980.07 53.98 o 0 12 3 231.44 226.01 51.39 o 1 12 3 1712.02 1868.26 76.25 o 2 12 3 27.37 20.58 36.27 o 3 12 3 337.44 392.49 50.55 o 4 12 3 77.71 88.34 39.66 o 5 12 3 1201.19 1176.89 55.20 o 1 13 3 186.58 190.49 42.82 o 2 13 3 63.93 57.49 54.26 o 1 0 4 24699.25 25407.37 407.46 o 2 0 4 14889.97 15097.50 241.36 o 3 0 4 2217.60 2260.11 42.88 o 4 0 4 27064.18 26192.96 402.87 o 5 0 4 17460.85 17588.96 321.58 o 6 0 4 10999.20 11049.58 243.29 o 7 0 4 1572.59 1704.85 37.82 o 8 0 4 658.70 571.84 35.75 o 9 0 4 2394.53 2342.85 69.23 o 10 0 4 4135.73 4513.97 165.81 o 11 0 4 918.76 914.17 49.06 o 12 0 4 600.24 551.35 68.55 o 1 1 4 2874.42 3150.39 34.01 o 2 1 4 39786.31 38922.23 425.10 o 3 1 4 14190.71 14319.17 152.07 o 4 1 4 9024.80 8999.15 112.52 o 5 1 4 111.30 123.47 6.16 o 6 1 4 4467.70 4508.57 76.60 o 7 1 4 6803.36 6995.20 113.57 o 8 1 4 5528.93 5542.57 162.65 o 9 1 4 1237.53 1154.49 24.92 o 10 1 4 74.78 64.90 23.83 o 11 1 4 152.13 135.28 29.46 o 12 1 4 927.78 842.63 45.75 o 0 2 4 1392.37 1377.89 29.02 o 1 2 4 134.11 150.18 3.55 o 2 2 4 21.97 20.03 3.15 o 3 2 4 1534.74 1648.26 24.76 o 4 2 4 724.00 703.22 20.36 o 5 2 4 2244.03 2329.32 33.27 o 6 2 4 1144.54 1194.00 19.00 o 7 2 4 99.93 88.21 10.05 o 8 2 4 23.18 20.81 10.84 o 9 2 4 293.03 316.86 22.65 o 10 2 4 259.48 235.45 23.79 o 11 2 4 0.64 -9.92 30.03 o 12 2 4 1.67 4.26 49.19 o 1 3 4 6804.21 6673.11 78.67 o 2 3 4 8020.16 7860.38 86.73 o 3 3 4 2244.06 2179.49 50.04 o 4 3 4 3626.96 3682.75 56.80 o 5 3 4 241.13 254.54 10.59 o 6 3 4 1913.02 1950.03 33.97 o 7 3 4 1167.83 1155.93 31.98 o 8 3 4 1644.64 1666.46 49.77 o 9 3 4 838.29 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42.26 o 4 4 8 2837.63 2908.95 45.95 o 5 4 8 19156.40 19963.33 399.91 o 6 4 8 1068.03 1075.78 22.96 o 7 4 8 1836.90 1903.24 39.92 o 8 4 8 10.47 6.02 18.84 o 9 4 8 2839.66 2820.42 72.14 o 10 4 8 341.62 351.71 30.83 o 11 4 8 1437.42 1416.38 55.20 o 1 5 8 10650.03 10924.58 173.93 o 2 5 8 3537.40 3504.77 79.72 o 3 5 8 19761.87 19583.23 319.67 o 4 5 8 794.10 762.42 24.50 o 5 5 8 131.45 97.38 7.31 o 6 5 8 665.15 608.22 23.34 o 7 5 8 7599.48 8013.94 175.14 o 8 5 8 605.48 570.07 23.70 o 9 5 8 1956.72 1919.11 56.49 o 10 5 8 20.25 58.30 28.61 o 11 5 8 528.08 503.16 41.52 o 0 6 8 792.02 737.71 22.67 o 1 6 8 4869.81 4900.77 99.77 o 2 6 8 66.14 68.39 12.91 o 3 6 8 2011.85 2014.69 57.24 o 4 6 8 548.56 528.95 18.43 o 5 6 8 3558.62 3632.81 71.36 o 6 6 8 180.41 197.83 20.01 o 7 6 8 443.65 408.16 23.88 o 8 6 8 16.70 25.71 22.49 o 9 6 8 450.80 468.90 31.45 o 10 6 8 70.93 101.00 39.84 o 1 7 8 13.38 21.71 15.68 o 2 7 8 3.02 7.45 13.68 o 3 7 8 26.92 37.00 15.61 o 4 7 8 2.67 9.64 16.51 o 5 7 8 9.87 1.31 17.90 o 6 7 8 21.79 17.41 22.38 o 7 7 8 177.28 162.86 25.26 o 8 7 8 24.50 35.27 26.44 o 9 7 8 90.92 96.07 33.13 o 10 7 8 7.55 4.78 40.50 o 0 8 8 473.58 477.43 31.06 o 1 8 8 3695.17 3742.35 92.93 o 2 8 8 41.04 43.12 19.19 o 3 8 8 1319.05 1280.03 31.48 o 4 8 8 560.54 538.27 24.36 o 5 8 8 2999.38 2886.34 75.81 o 6 8 8 283.77 295.23 31.37 o 7 8 8 578.71 537.88 34.61 o 8 8 8 2.70 24.89 29.55 o 9 8 8 387.61 339.69 36.96 o 1 9 8 3713.46 3898.52 104.75 o 2 9 8 888.90 967.68 36.00 o 3 9 8 6035.16 6128.34 175.99 o 4 9 8 193.72 193.97 25.28 o 5 9 8 4.54 5.99 23.45 o 6 9 8 176.97 184.74 30.64 o 7 9 8 1824.13 1809.17 65.39 o 8 9 8 215.15 200.59 34.68 o 0 10 8 695.33 682.96 48.94 o 1 10 8 2122.88 2261.53 69.16 o 2 10 8 13.34 30.07 25.96 o 3 10 8 207.82 186.06 24.83 o 4 10 8 216.87 241.22 26.53 o 5 10 8 2513.16 2647.56 90.40 o 6 10 8 101.48 110.21 35.47 o 7 10 8 167.99 192.42 49.06 o 1 11 8 20.64 30.32 27.07 o 2 11 8 86.66 102.77 29.13 o 3 11 8 324.27 354.32 42.65 o 4 11 8 0.07 7.88 36.42 o 5 11 8 0.11 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4586.31 77.27 o 5 3 9 119.71 121.81 11.35 o 6 3 9 3402.75 3589.73 95.69 o 7 3 9 2452.07 2447.32 58.85 o 8 3 9 3469.70 3782.30 81.46 o 9 3 9 607.28 614.52 24.16 o 10 3 9 84.94 91.55 27.55 o 11 3 9 231.33 207.74 28.85 o 0 4 9 3495.80 3263.41 102.21 o 1 4 9 2035.63 2009.73 55.56 o 2 4 9 243.76 246.24 7.40 o 3 4 9 65.71 73.12 7.19 o 4 4 9 3497.26 3527.56 69.62 o 5 4 9 679.10 722.12 19.04 o 6 4 9 799.35 820.00 21.98 o 7 4 9 18.43 37.38 17.47 o 8 4 9 15.17 4.23 20.63 o 9 4 9 112.84 119.77 23.85 o 10 4 9 221.90 212.86 27.76 o 11 4 9 140.17 166.35 41.83 o 1 5 9 17.61 19.90 11.03 o 2 5 9 1851.61 1791.00 38.71 o 3 5 9 1083.01 1075.49 26.39 o 4 5 9 265.77 243.90 13.32 o 5 5 9 384.10 378.14 18.45 o 6 5 9 175.94 177.80 19.50 o 7 5 9 239.45 200.63 18.74 o 8 5 9 445.38 444.33 23.22 o 9 5 9 1.29 2.03 25.60 o 10 5 9 14.73 23.14 28.56 o 11 5 9 99.24 99.08 46.70 o 0 6 9 10601.07 10421.97 250.69 o 1 6 9 3817.55 3847.45 72.38 o 2 6 9 1737.48 1634.63 32.37 o 3 6 9 12.01 6.97 13.14 o 4 6 9 4994.51 4994.53 108.23 o 5 6 9 3100.59 2955.73 69.11 o 6 6 9 3197.41 3200.60 83.57 o 7 6 9 215.34 197.29 22.70 o 8 6 9 172.68 159.23 26.85 o 9 6 9 673.84 613.95 31.99 o 10 6 9 1009.09 946.69 37.11 o 1 7 9 1438.04 1388.56 29.65 o 2 7 9 7768.16 7997.01 198.65 o 3 7 9 4511.00 4631.86 92.06 o 4 7 9 5237.09 5225.98 115.07 o 5 7 9 30.93 19.25 16.56 o 6 7 9 1772.28 1804.24 50.52 o 7 7 9 1647.06 1750.90 52.40 o 8 7 9 2379.74 2477.86 71.96 o 9 7 9 321.10 339.70 36.08 o 10 7 9 1.66 12.80 36.77 o 0 8 9 2787.75 2746.52 114.03 o 1 8 9 1414.40 1429.67 39.51 o 2 8 9 438.73 440.25 18.89 o 3 8 9 28.63 30.98 19.36 o 4 8 9 1938.83 1915.48 52.43 o 5 8 9 1133.11 1176.25 31.46 o 6 8 9 1881.67 1916.32 74.08 o 7 8 9 59.41 38.59 30.39 o 8 8 9 112.12 142.52 30.96 o 9 8 9 244.40 218.51 33.61 o 1 9 9 7.77 3.37 25.57 o 2 9 9 97.48 89.63 20.59 o 3 9 9 2.68 6.89 21.95 o 4 9 9 2.69 14.55 22.60 o 5 9 9 2.76 1.49 25.74 o 6 9 9 3.90 -1.31 28.74 o 7 9 9 115.67 127.09 31.35 o 8 9 9 30.39 51.82 34.69 o 0 10 9 733.48 752.37 65.00 o 1 10 9 794.98 802.77 40.11 o 2 10 9 193.15 186.97 25.85 o 3 10 9 21.81 37.56 25.87 o 4 10 9 595.07 587.84 30.86 o 5 10 9 123.39 112.45 33.60 o 6 10 9 465.84 449.28 43.83 o 7 10 9 3.10 -9.95 55.21 o 1 11 9 387.56 353.74 30.79 o 2 11 9 2225.66 2262.78 75.08 o 3 11 9 755.14 717.07 34.22 o 4 11 9 515.59 482.11 38.15 o 5 11 9 2.14 -5.35 40.78 o 6 11 9 223.39 208.58 48.71 o 0 12 9 1878.92 1973.51 105.96 o 1 12 9 378.94 401.36 36.18 o 2 12 9 35.43 23.10 41.26 o 3 12 9 43.65 57.92 42.14 o 4 12 9 595.55 635.05 52.30 o 0 0 10 40623.14 38803.49 775.69 o 1 0 10 2157.38 2261.05 55.61 o 2 0 10 5537.59 5742.51 151.01 o 3 0 10 1.40 12.15 6.51 o 4 0 10 23153.21 23443.12 482.71 o 5 0 10 37.61 41.23 14.14 o 6 0 10 19715.66 20488.38 566.34 o 7 0 10 309.86 271.85 22.11 o 8 0 10 620.06 583.23 40.01 o 9 0 10 41.92 48.41 29.68 o 10 0 10 4604.15 4284.92 197.06 o 11 0 10 62.70 38.35 43.53 o 1 1 10 285.87 279.09 6.73 o 2 1 10 27983.84 28186.99 331.00 o 3 1 10 86.89 113.46 6.16 o 4 1 10 9822.81 10255.63 177.80 o 5 1 10 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6.43 21.62 13.01 o 6 4 10 7523.66 7966.55 169.38 o 7 4 10 7.54 2.50 18.91 o 8 4 10 163.36 152.19 23.76 o 9 4 10 99.30 95.68 22.45 o 10 4 10 2469.49 2422.19 71.53 o 11 4 10 2.59 -0.33 34.75 o 1 5 10 42.43 45.00 9.54 o 2 5 10 23979.62 23464.44 511.32 o 3 5 10 0.08 13.11 9.55 o 4 5 10 5803.23 5825.91 113.24 o 5 5 10 70.64 75.80 15.41 o 6 5 10 3108.43 3225.50 84.66 o 7 5 10 17.35 24.41 18.76 o 8 5 10 5012.66 5238.66 143.19 o 9 5 10 4.92 7.03 27.09 o 10 5 10 58.56 58.00 31.03 o 0 6 10 7299.02 7201.81 186.03 o 1 6 10 4.91 9.18 12.85 o 2 6 10 1271.06 1326.96 29.36 o 3 6 10 80.40 64.31 15.63 o 4 6 10 1961.57 2010.03 41.45 o 5 6 10 1.41 -4.46 16.67 o 6 6 10 2003.52 2039.21 102.70 o 7 6 10 17.20 15.03 20.37 o 8 6 10 225.51 223.12 25.73 o 9 6 10 10.02 11.55 28.99 o 10 6 10 856.77 849.57 41.11 o 1 7 10 2.02 -8.44 14.81 o 2 7 10 249.55 245.17 17.03 o 3 7 10 2.02 -2.55 16.08 o 4 7 10 40.58 36.95 15.72 o 5 7 10 19.02 13.57 18.46 o 6 7 10 1.73 5.39 22.34 o 7 7 10 3.21 2.16 28.01 o 8 7 10 1.36 2.45 27.66 o 9 7 10 3.37 -4.27 32.36 o 0 8 10 5530.99 5738.96 210.22 o 1 8 10 80.36 83.65 21.96 o 2 8 10 906.62 866.50 24.76 o 3 8 10 2.71 6.94 17.39 o 4 8 10 1729.31 1694.41 43.75 o 5 8 10 31.56 40.56 20.35 o 6 8 10 1957.79 1888.13 58.56 o 7 8 10 1.34 5.33 28.39 o 8 8 10 83.00 82.50 29.89 o 9 8 10 18.28 28.46 35.05 o 1 9 10 20.85 22.45 23.61 o 2 9 10 5434.10 5697.19 166.14 o 3 9 10 5.48 8.88 24.00 o 4 9 10 2167.41 2098.07 62.20 o 5 9 10 5.86 7.52 24.54 o 6 9 10 1072.02 1114.74 41.33 o 7 9 10 1.27 3.64 34.69 o 8 9 10 2195.28 2103.63 66.07 o 0 10 10 4175.16 4691.64 293.69 o 1 10 10 6.17 10.46 28.65 o 2 10 10 358.87 322.34 27.10 o 3 10 10 15.36 14.18 28.04 o 4 10 10 1576.74 1583.20 54.23 o 5 10 10 43.54 32.10 29.93 o 6 10 10 910.24 816.71 45.15 o 7 10 10 1.98 -5.22 42.68 o 1 11 10 70.61 69.82 28.27 o 2 11 10 348.45 336.35 30.46 o 3 11 10 6.27 6.51 29.51 o 4 11 10 28.24 14.11 42.51 o 5 11 10 0.38 6.27 41.65 o 0 12 10 462.94 549.74 65.21 o 1 12 10 13.07 19.19 35.35 o 2 12 10 70.18 88.85 44.64 o 3 12 10 1.49 9.83 42.39 o 1 1 11 4296.88 4486.85 51.48 o 2 1 11 7465.37 7575.03 100.81 o 3 1 11 5880.22 6130.36 82.71 o 4 1 11 3984.91 4069.02 96.31 o 5 1 11 47.03 37.75 8.67 o 6 1 11 2229.33 2310.51 41.68 o 7 1 11 1228.37 1234.24 29.86 o 8 1 11 2232.75 2327.12 76.34 o 9 1 11 349.20 328.30 23.28 o 10 1 11 80.68 93.73 25.22 o 11 1 11 61.82 78.02 38.12 o 0 2 11 21145.54 20910.86 359.06 o 1 2 11 6316.76 6385.21 111.18 o 2 2 11 3701.99 3823.56 74.72 o 3 2 11 2502.36 2647.67 50.35 o 4 2 11 12330.52 12495.66 246.59 o 5 2 11 11320.26 11876.22 221.49 o 6 2 11 7789.21 8041.74 165.38 o 7 2 11 937.10 913.86 29.55 o 8 2 11 243.18 219.73 20.68 o 9 2 11 1119.05 1035.06 31.09 o 10 2 11 2032.43 1899.74 48.89 o 11 2 11 559.61 514.87 36.43 o 1 3 11 1533.43 1398.97 36.55 o 2 3 11 16246.04 16023.47 311.31 o 3 3 11 8712.90 8865.34 165.94 o 4 3 11 3989.41 4108.56 91.25 o 5 3 11 202.88 195.78 12.61 o 6 3 11 2019.17 2130.21 43.46 o 7 3 11 4582.49 4715.15 91.81 o 8 3 11 3989.35 3991.74 98.88 o 9 3 11 643.74 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810.04 42.23 o 3 1 25 16.34 15.89 37.15 o 4 1 25 405.08 449.61 42.50 o 5 1 25 2.32 20.54 59.92 o 6 1 25 97.39 113.18 67.07 o 0 2 25 3451.26 3316.88 217.81 o 1 2 25 61.29 42.27 26.22 o 2 2 25 425.71 460.07 36.95 o 3 2 25 6.55 7.62 35.20 o 4 2 25 710.86 702.89 48.34 o 5 2 25 3.24 27.49 60.71 o 6 2 25 663.58 691.41 65.50 o 1 3 25 73.31 92.67 31.45 o 2 3 25 1923.90 1953.50 74.22 o 3 3 25 4.04 -4.16 39.75 o 4 3 25 396.80 410.71 45.87 o 5 3 25 18.51 39.54 55.56 o 6 3 25 203.04 151.93 86.19 o 0 4 25 268.05 298.90 57.04 o 1 4 25 0.91 -10.22 35.40 o 2 4 25 6.39 7.19 30.55 o 3 4 25 85.79 48.40 37.69 o 4 4 25 247.24 249.63 62.99 o 5 4 25 3.16 0.82 65.30 o 1 5 25 2.34 -0.06 46.56 o 2 5 25 153.62 142.50 36.28 o 3 5 25 2.40 -5.51 43.69 o 4 5 25 38.48 47.23 50.89 o 0 6 25 1070.13 1230.01 134.70 o 1 6 25 9.85 1.55 57.18 o 2 6 25 193.48 193.92 48.78 o 3 6 25 0.03 -0.49 47.06 o 0 0 26 202.53 222.64 54.92 o 1 0 26 619.65 550.89 50.89 o 2 0 26 120.05 111.41 42.07 o 3 0 26 32.27 21.27 96.14 o 4 0 26 788.19 852.85 113.22 o 5 0 26 639.44 582.44 86.81 o 1 1 26 119.17 106.14 33.67 o 2 1 26 404.47 445.79 39.08 o 3 1 26 472.20 463.00 45.26 o 4 1 26 351.25 364.49 50.81 o 5 1 26 2.98 33.84 55.85 o 0 2 26 155.42 180.56 50.30 o 1 2 26 7.73 3.63 28.17 o 2 2 26 4.11 -13.09 31.87 o 3 2 26 0.64 18.24 51.57 o 4 2 26 7.32 2.49 47.79 o 5 2 26 28.18 30.89 44.11 o 1 3 26 61.87 55.39 35.09 o 2 3 26 186.05 167.93 36.23 o 3 3 26 179.58 148.38 44.47 o 4 3 26 89.56 126.89 48.60 o 5 3 26 2.46 39.58 58.60 o 0 4 26 779.65 755.76 59.21 o 1 4 26 403.92 411.93 48.32 o 2 4 26 1.08 1.46 37.33 o 3 4 26 39.96 39.55 40.59 o 4 4 26 605.24 616.04 54.70 o 1 5 26 240.61 245.23 51.60 o 2 5 26 711.06 712.61 52.66 o 3 5 26 353.75 333.08 43.47 o 0 6 26 288.88 241.24 127.35 o 1 6 26 107.25 87.55 50.43 o 2 6 26 50.68 53.91 125.31 o 1 1 27 432.37 452.07 43.95 o 2 1 27 14.41 30.72 47.17 o 3 1 27 420.02 438.53 43.46 o 4 1 27 27.52 47.44 63.92 o 5 1 27 2.34 11.81 69.02 o 0 2 27 169.06 204.74 67.74 o 1 2 27 678.11 669.60 45.70 o 2 2 27 76.70 93.94 37.70 o 3 2 27 269.97 259.95 47.76 o 4 2 27 6.88 1.17 47.71 o 1 3 27 199.67 173.25 47.38 o 2 3 27 99.60 99.16 43.71 o 3 3 27 796.74 840.56 60.83 o 4 3 27 3.42 15.82 46.24 o 0 4 27 45.25 41.83 64.37 o 1 4 27 146.59 153.77 42.06 o 2 4 27 18.46 16.48 46.95 o 3 4 27 2.24 0.92 44.55 o 1 5 27 9.57 -11.20 41.97 o 2 5 27 0.08 8.61 87.91 o 1 0 28 1313.81 1398.78 125.92 o 2 0 28 26.10 23.51 73.14 o 3 0 28 57.51 109.60 111.54 o 4 0 28 124.86 106.49 87.77 o 1 1 28 287.36 236.56 59.36 o 2 1 28 161.67 139.85 50.32 o 3 1 28 455.41 413.85 60.06 o 0 2 28 114.54 75.02 108.84 o 1 2 28 3.48 64.94 47.96 o 2 2 28 7.88 2.78 53.19 o 3 2 28 0.12 -19.24 56.32 o 1 3 28 102.26 123.51 56.42 o 2 3 28 6.83 -16.19 51.38 o 0 4 28 149.02 124.46 66.13 o 1 4 28 571.27 575.69 54.01 o 1 1 29 9.32 32.23 104.15 o 2 1 29 108.83 152.52 78.94 o 0 2 29 638.97 548.42 86.96 o 1 2 29 56.25 45.03 51.07 o