#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/59/2235900.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235900_Fobs loop_ _publ_author_name 'Huo, Yan-Ping' 'Nie, Xiao-Li' 'Fang, Xiao-Ming' _publ_section_title ; (E)-2-[2-(3-Fluorophenyl)ethenyl]quinolin-8-yl acetate ; _journal_coeditor_code LD2060 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2420 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.528 _cell_angle_gamma 90.000 _cell_length_a 17.6277 _cell_length_b 5.2641 _cell_length_c 16.0624 _exptl_crystal_F_000 640.00 _reflns_d_resolution_high 0.7806 _[local]_cod_data_source_file ld2060Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' YGZ in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 194.20 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 12.48 14.65 0.99 o 3 0 0 6968.91 7119.53 142.57 o 4 0 0 4908.17 4910.86 63.09 o 5 0 0 2777.91 2923.72 37.46 o 6 0 0 4803.94 4831.04 61.63 o 7 0 0 2.48 4.49 0.62 o 8 0 0 11088.77 12130.38 178.66 o 9 0 0 2568.59 3050.63 39.42 o 10 0 0 1800.41 1799.11 30.47 o 11 0 0 1164.66 1260.14 18.80 o 13 0 0 0.14 1.44 0.85 o 14 0 0 80.90 68.53 3.35 o 15 0 0 4.41 6.46 1.22 o 16 0 0 382.24 333.78 6.16 o 17 0 0 711.42 623.73 10.08 o 18 0 0 0.34 13.18 2.57 o 19 0 0 225.07 211.10 8.00 o 20 0 0 40.59 57.42 2.57 o 21 0 0 35.77 40.88 2.34 o 22 0 0 2.57 3.88 1.62 o 1 1 0 1408.10 1507.11 20.15 o 2 1 0 6366.78 6152.76 95.04 o 3 1 0 333.58 379.76 4.40 o 4 1 0 979.31 928.03 10.12 o 5 1 0 221.75 248.91 6.16 o 6 1 0 466.33 414.84 3.77 o 7 1 0 442.95 436.98 4.54 o 8 1 0 859.85 905.20 8.79 o 9 1 0 198.47 187.71 3.84 o 10 1 0 236.33 184.62 2.50 o 11 1 0 26.78 27.42 0.97 o 12 1 0 183.32 164.14 2.46 o 13 1 0 11.41 12.54 0.94 o 14 1 0 59.91 66.20 1.61 o 15 1 0 23.41 18.29 1.08 o 16 1 0 81.28 77.73 1.83 o 17 1 0 2.33 1.42 0.82 o 18 1 0 267.34 252.27 3.77 o 19 1 0 7.41 6.06 2.16 o 20 1 0 2.26 0.75 1.11 o 21 1 0 114.89 106.94 2.86 o 0 2 0 164.92 160.11 4.09 o 1 2 0 176.59 151.82 2.80 o 2 2 0 555.54 583.73 8.49 o 3 2 0 36.14 14.13 0.88 o 4 2 0 7.96 2.75 0.86 o 5 2 0 1236.91 1327.20 17.77 o 6 2 0 0.71 2.22 0.83 o 7 2 0 309.50 283.49 3.84 o 8 2 0 387.65 354.96 4.65 o 9 2 0 474.49 462.76 6.69 o 10 2 0 33.62 43.11 1.39 o 11 2 0 51.33 43.16 1.42 o 12 2 0 16.43 15.99 1.15 o 13 2 0 218.58 208.00 3.54 o 14 2 0 43.40 43.80 1.60 o 15 2 0 28.56 23.21 1.33 o 16 2 0 107.40 102.63 2.48 o 17 2 0 37.59 40.68 1.80 o 18 2 0 102.54 97.18 2.55 o 19 2 0 28.94 24.86 2.75 o 20 2 0 0.84 0.42 1.16 o 21 2 0 0.26 -0.12 1.56 o 1 3 0 373.71 430.23 6.90 o 2 3 0 375.94 392.27 6.41 o 3 3 0 413.63 489.46 7.70 o 4 3 0 98.08 103.67 3.35 o 5 3 0 688.07 789.56 11.67 o 6 3 0 1317.56 1544.76 17.18 o 7 3 0 270.38 226.32 3.46 o 8 3 0 12.72 9.81 1.03 o 9 3 0 280.84 277.75 4.14 o 10 3 0 81.42 91.02 2.13 o 11 3 0 2373.01 2234.46 24.66 o 12 3 0 4.69 5.66 1.62 o 13 3 0 117.13 132.09 5.20 o 14 3 0 1795.10 1842.22 20.94 o 15 3 0 140.63 142.18 3.14 o 16 3 0 663.51 664.45 8.89 o 17 3 0 193.85 187.25 3.78 o 18 3 0 43.59 45.64 1.97 o 19 3 0 35.94 40.16 1.96 o 0 4 0 68.97 65.18 3.16 o 1 4 0 73.70 89.18 4.41 o 2 4 0 31.10 40.34 1.82 o 3 4 0 7.85 6.92 1.71 o 4 4 0 120.55 129.52 3.25 o 5 4 0 3.31 2.18 1.13 o 6 4 0 5.45 6.05 1.86 o 7 4 0 248.19 254.08 4.08 o 8 4 0 85.03 84.15 2.16 o 9 4 0 187.84 189.22 3.41 o 10 4 0 3.62 4.06 1.04 o 11 4 0 0.01 -0.73 0.92 o 12 4 0 0.46 -0.02 0.99 o 13 4 0 60.96 62.16 2.26 o 14 4 0 13.80 14.15 3.41 o 15 4 0 152.91 144.48 5.04 o 16 4 0 52.71 48.97 2.55 o 17 4 0 36.94 36.00 3.20 o 1 5 0 118.72 117.95 3.42 o 2 5 0 72.57 71.12 2.67 o 3 5 0 1.59 3.63 1.42 o 4 5 0 57.75 55.11 2.68 o 5 5 0 17.93 12.14 2.46 o 6 5 0 26.21 24.97 1.84 o 7 5 0 143.50 140.28 5.57 o 8 5 0 23.51 27.52 2.05 o 9 5 0 33.95 30.40 2.04 o 10 5 0 35.81 39.61 2.26 o 11 5 0 1.91 3.22 2.29 o 12 5 0 4.51 1.50 1.61 o 13 5 0 63.59 63.90 2.92 o 14 5 0 5.35 3.61 2.27 o 0 6 0 107.09 117.04 5.32 o 1 6 0 13.84 15.84 2.15 o 2 6 0 53.96 58.69 2.80 o 3 6 0 9.29 13.94 2.08 o 4 6 0 123.11 125.91 3.93 o 5 6 0 229.53 257.07 8.17 o 6 6 0 0.06 -1.59 1.59 o 7 6 0 12.40 12.69 2.20 o 8 6 0 10.29 12.63 2.10 o 9 6 0 5.78 2.38 2.46 o 10 6 0 5.86 7.85 2.72 o -22 1 1 2.29 1.32 1.28 o -21 1 1 13.23 17.28 1.67 o -20 1 1 0.64 0.35 1.06 o -19 1 1 0.33 0.50 1.44 o -18 1 1 0.33 -0.03 0.95 o -17 1 1 40.96 34.08 1.50 o -16 1 1 141.82 125.39 2.97 o -15 1 1 19.70 18.00 1.14 o -14 1 1 94.78 86.13 4.40 o -13 1 1 8.09 9.02 0.84 o -12 1 1 30.86 26.24 0.98 o -11 1 1 86.43 86.86 4.01 o -10 1 1 892.59 937.26 13.74 o -9 1 1 20.44 10.95 0.77 o -8 1 1 568.06 664.36 7.69 o -7 1 1 123.38 87.29 2.08 o -6 1 1 981.97 974.83 10.76 o -5 1 1 796.60 778.41 8.62 o -4 1 1 0.01 0.43 0.29 o -3 1 1 54.37 38.78 0.71 o -1 1 1 1401.32 1471.22 16.05 o 0 1 1 231.80 307.95 3.69 o 1 1 1 4458.42 5000.72 155.23 o 2 1 1 1924.84 2061.62 22.46 o 3 1 1 5828.81 5824.82 139.30 o 4 1 1 239.35 267.92 2.85 o 5 1 1 194.78 196.16 1.97 o 6 1 1 35.22 40.97 0.88 o 7 1 1 1147.23 1105.03 17.82 o 8 1 1 4.37 4.29 0.53 o 9 1 1 1199.38 1325.58 15.61 o 10 1 1 324.82 320.94 3.75 o 11 1 1 217.81 200.07 2.72 o 12 1 1 394.12 424.48 4.86 o 13 1 1 77.47 77.63 1.68 o 14 1 1 226.61 226.66 3.23 o 15 1 1 79.01 73.65 1.75 o 16 1 1 28.27 24.34 1.19 o 17 1 1 4.36 3.47 0.91 o 18 1 1 83.25 81.47 2.00 o 19 1 1 193.61 203.62 3.40 o 20 1 1 54.12 56.84 1.84 o 21 1 1 32.64 37.56 1.87 o -21 2 1 28.61 44.91 2.03 o -20 2 1 26.33 30.15 1.69 o -19 2 1 9.00 6.78 1.30 o -18 2 1 8.71 10.47 1.40 o -17 2 1 121.80 122.29 2.81 o -16 2 1 45.90 47.31 1.74 o -15 2 1 33.97 28.99 1.40 o -14 2 1 23.90 26.94 1.36 o -13 2 1 402.61 384.09 5.43 o -12 2 1 745.37 708.02 8.68 o -11 2 1 3.39 1.11 0.70 o -10 2 1 128.32 106.92 2.13 o -9 2 1 53.30 35.64 1.21 o -8 2 1 15.56 15.25 0.86 o -7 2 1 244.68 244.58 3.40 o -6 2 1 12.50 11.04 0.72 o -5 2 1 483.16 574.44 6.73 o -4 2 1 95.41 69.05 1.75 o -3 2 1 215.99 233.29 3.93 o -2 2 1 1452.30 1558.24 21.11 o -1 2 1 127.50 90.66 1.97 o 1 2 1 244.91 292.71 14.39 o 2 2 1 1113.12 1280.66 24.83 o 3 2 1 2139.88 2312.70 43.70 o 4 2 1 12.32 9.79 1.30 o 7 2 1 55.87 56.22 1.34 o 8 2 1 167.62 123.69 2.12 o 9 2 1 86.92 87.68 1.45 o 10 2 1 404.51 423.67 10.05 o 11 2 1 7.79 9.58 0.98 o 12 2 1 86.05 95.91 2.22 o 13 2 1 600.99 610.85 7.84 o 14 2 1 240.12 227.44 3.83 o 15 2 1 74.06 75.88 3.13 o 16 2 1 21.84 20.07 1.69 o 17 2 1 58.73 60.20 2.45 o 18 2 1 0.70 0.05 1.05 o 19 2 1 41.59 44.64 1.87 o 20 2 1 19.52 22.02 1.57 o -20 3 1 9.28 13.32 2.07 o -19 3 1 145.76 163.13 3.63 o -18 3 1 4.78 1.24 1.22 o -17 3 1 6.06 6.71 1.79 o -16 3 1 551.73 579.71 8.00 o -15 3 1 527.30 503.36 7.76 o -14 3 1 3.50 6.62 1.23 o -13 3 1 115.23 110.28 2.54 o -12 3 1 9.74 9.74 1.24 o -11 3 1 2595.49 2580.18 28.19 o -10 3 1 43.98 35.17 1.53 o -9 3 1 32.81 36.91 1.37 o -8 3 1 287.10 326.81 4.58 o -7 3 1 276.07 252.56 3.74 o -6 3 1 1148.78 1170.44 13.26 o -5 3 1 1324.13 1393.32 19.48 o -4 3 1 5.11 5.54 0.97 o -3 3 1 1302.87 1523.95 24.87 o -2 3 1 759.30 778.37 11.45 o -1 3 1 589.23 672.59 14.15 o 0 3 1 63.06 79.10 3.28 o 1 3 1 317.35 317.37 5.40 o 2 3 1 15.30 8.33 3.76 o 3 3 1 6.79 1.40 1.25 o 4 3 1 65.42 55.54 1.84 o 5 3 1 465.13 484.88 7.70 o 6 3 1 108.18 119.19 2.84 o 7 3 1 1.74 1.50 0.72 o 8 3 1 256.19 284.14 4.18 o 9 3 1 1.04 0.32 0.75 o 10 3 1 16.70 16.56 1.92 o 11 3 1 43.71 44.77 1.69 o 12 3 1 234.33 223.31 3.79 o 13 3 1 42.94 42.23 1.72 o 14 3 1 633.16 653.72 8.57 o 15 3 1 26.03 25.57 1.96 o 16 3 1 105.42 113.05 2.83 o 17 3 1 53.98 53.85 2.09 o 18 3 1 3.32 3.17 3.39 o 19 3 1 1.98 0.33 1.56 o -18 4 1 3.26 4.75 1.90 o -17 4 1 18.59 17.01 4.78 o -16 4 1 143.06 145.76 4.18 o -15 4 1 2.54 1.15 1.49 o -14 4 1 96.45 96.38 3.23 o -13 4 1 135.77 143.63 4.24 o -12 4 1 2.67 2.20 1.30 o -11 4 1 12.27 10.57 2.12 o -10 4 1 67.12 64.01 2.43 o -9 4 1 42.11 37.56 2.68 o -8 4 1 142.79 145.17 2.85 o -7 4 1 335.34 323.98 5.35 o -6 4 1 75.81 78.00 2.02 o -5 4 1 62.94 67.36 2.33 o -4 4 1 377.89 385.30 8.49 o -3 4 1 138.80 139.56 3.39 o -2 4 1 472.31 501.75 8.28 o -1 4 1 21.41 16.87 1.43 o 0 4 1 48.66 44.32 2.25 o 1 4 1 285.47 292.24 7.59 o 2 4 1 71.43 80.67 3.46 o 3 4 1 9.89 8.06 1.28 o 4 4 1 25.17 20.47 1.51 o 5 4 1 51.06 39.92 1.88 o 6 4 1 0.53 -0.51 1.51 o 7 4 1 456.07 443.02 6.14 o 8 4 1 0.93 2.05 0.93 o 9 4 1 178.60 167.58 3.20 o 10 4 1 70.76 70.88 2.06 o 11 4 1 50.28 45.66 1.74 o 12 4 1 31.05 30.04 1.55 o 13 4 1 17.18 17.90 2.22 o 14 4 1 7.35 5.99 1.57 o 15 4 1 218.21 216.08 5.09 o 16 4 1 20.10 27.70 2.85 o 17 4 1 44.28 44.97 3.54 o -15 5 1 17.93 23.53 3.39 o -14 5 1 0.46 -0.41 1.65 o -13 5 1 17.98 17.04 2.14 o -12 5 1 32.36 30.96 3.69 o -11 5 1 11.01 14.22 2.08 o -10 5 1 19.52 22.19 1.83 o -9 5 1 0.99 0.47 1.34 o -8 5 1 2.25 1.85 1.39 o -7 5 1 67.52 64.92 2.64 o -6 5 1 21.76 21.01 1.90 o -5 5 1 1.16 -0.41 1.60 o -4 5 1 257.10 274.21 5.70 o -3 5 1 1.57 1.20 1.34 o -2 5 1 187.82 199.16 4.64 o -1 5 1 147.54 164.01 4.10 o 0 5 1 9.11 9.17 2.23 o 1 5 1 93.37 104.32 3.25 o 2 5 1 552.01 610.90 10.19 o 3 5 1 0.85 1.56 2.07 o 4 5 1 49.56 43.28 3.70 o 5 5 1 0.29 -1.20 1.20 o 6 5 1 5.64 4.78 1.50 o 7 5 1 124.33 107.66 3.36 o 8 5 1 6.12 3.16 1.42 o 9 5 1 54.32 57.16 2.51 o 10 5 1 20.68 20.39 1.93 o 11 5 1 18.54 21.63 2.98 o 12 5 1 10.97 11.87 2.64 o 13 5 1 69.95 77.50 4.24 o 14 5 1 15.69 22.74 2.83 o -10 6 1 42.21 46.08 3.87 o -9 6 1 0.01 -1.59 1.59 o -8 6 1 1.63 -2.05 2.05 o -7 6 1 0.27 -1.49 1.49 o -6 6 1 1.11 -0.93 2.33 o -5 6 1 695.12 695.19 19.12 o -4 6 1 104.20 110.72 3.74 o -3 6 1 34.47 32.96 2.40 o -2 6 1 80.01 81.57 3.25 o -1 6 1 8.78 6.63 1.79 o 0 6 1 3.56 3.35 1.64 o 1 6 1 154.63 162.93 4.46 o 2 6 1 15.89 26.34 2.45 o 3 6 1 722.67 777.15 12.91 o 4 6 1 16.31 18.01 2.94 o 5 6 1 211.02 226.24 5.84 o 6 6 1 134.49 113.68 3.71 o 7 6 1 16.75 21.89 3.31 o 8 6 1 0.13 -0.74 2.20 o 9 6 1 17.16 23.38 3.54 o -22 0 2 0.36 0.63 1.82 o -21 0 2 23.47 18.54 2.64 o -20 0 2 2.01 9.34 1.60 o -19 0 2 419.88 379.09 7.12 o -18 0 2 280.47 276.59 5.62 o -17 0 2 847.20 823.81 15.11 o -16 0 2 426.57 376.00 8.71 o -15 0 2 243.28 207.95 4.36 o -14 0 2 196.25 204.72 6.57 o -13 0 2 571.87 590.06 9.12 o -12 0 2 94.74 91.02 2.40 o -11 0 2 1851.44 1916.92 25.45 o -10 0 2 140.91 192.83 3.60 o -9 0 2 716.35 937.74 17.76 o -8 0 2 732.27 840.43 9.39 o -7 0 2 1521.61 1343.33 22.57 o -6 0 2 188.74 195.05 2.68 o -5 0 2 2672.02 2873.65 30.40 o -4 0 2 1240.39 1210.63 13.13 o -3 0 2 7064.67 6858.36 114.65 o -2 0 2 4214.86 4108.19 77.65 o -1 0 2 6725.04 6471.22 124.61 o 0 0 2 1159.18 1346.51 26.50 o 1 0 2 0.56 18.74 0.46 o 2 0 2 3889.72 4056.14 43.34 o 3 0 2 858.35 733.24 8.01 o 4 0 2 5266.85 5542.02 84.13 o 5 0 2 4760.42 4574.66 58.35 o 6 0 2 175.97 177.56 2.87 o 7 0 2 1202.95 982.09 22.85 o 8 0 2 301.47 265.19 3.42 o 9 0 2 756.10 886.10 9.96 o 10 0 2 310.29 364.60 6.42 o 11 0 2 87.72 61.56 1.91 o 12 0 2 0.70 2.19 0.87 o 13 0 2 43.34 39.74 1.78 o 14 0 2 1.31 3.12 1.06 o 15 0 2 188.27 166.74 3.81 o 16 0 2 2.78 2.29 1.14 o 17 0 2 86.90 78.27 2.70 o 18 0 2 76.22 66.07 2.58 o 19 0 2 65.22 66.21 2.65 o 20 0 2 53.65 53.42 5.01 o 21 0 2 6.58 7.51 1.84 o -22 1 2 3.40 2.10 1.34 o -21 1 2 0.61 -1.03 1.03 o -20 1 2 4.56 2.26 1.09 o -19 1 2 20.29 17.38 1.54 o -18 1 2 1.33 -0.44 0.92 o -17 1 2 44.75 41.63 1.61 o -16 1 2 143.09 120.12 2.60 o -15 1 2 12.20 12.41 1.17 o -14 1 2 21.73 23.45 1.23 o -13 1 2 0.71 0.63 0.67 o -12 1 2 49.33 41.15 1.33 o -11 1 2 43.53 30.08 2.81 o -10 1 2 491.42 589.53 7.12 o -9 1 2 499.34 498.63 6.06 o -8 1 2 1283.26 1424.03 15.57 o -7 1 2 660.15 670.26 6.60 o -6 1 2 142.55 107.83 1.42 o -5 1 2 700.08 691.92 6.69 o -4 1 2 397.00 447.68 4.43 o -3 1 2 327.04 399.72 3.97 o -2 1 2 536.83 637.84 7.07 o -1 1 2 8401.21 8809.84 95.15 o 0 1 2 2851.14 3039.30 32.80 o 1 1 2 1317.47 1466.41 13.88 o 2 1 2 15158.99 15783.37 130.00 o 3 1 2 8945.58 9158.83 98.75 o 4 1 2 474.12 455.90 4.59 o 5 1 2 166.67 150.55 1.48 o 6 1 2 141.93 120.40 1.94 o 7 1 2 46.70 38.02 0.67 o 8 1 2 836.20 784.34 7.63 o 9 1 2 593.68 648.68 5.84 o 11 1 2 5.15 3.81 0.64 o 12 1 2 578.85 611.06 6.56 o 13 1 2 124.30 102.98 1.95 o 14 1 2 328.53 292.08 3.86 o 15 1 2 15.58 16.82 1.07 o 16 1 2 15.78 17.95 1.16 o 17 1 2 33.75 30.44 1.33 o 18 1 2 170.23 180.80 3.11 o 19 1 2 1.17 1.76 1.00 o 20 1 2 27.35 24.65 1.51 o 21 1 2 83.47 88.73 2.32 o -21 2 2 196.18 257.01 4.77 o -20 2 2 39.02 47.39 1.95 o -19 2 2 0.99 3.99 1.17 o -18 2 2 1.90 1.15 1.04 o -17 2 2 26.97 22.06 1.37 o -16 2 2 0.05 0.42 1.01 o -15 2 2 589.33 576.17 7.62 o -14 2 2 257.62 251.45 4.05 o -13 2 2 1968.79 1912.50 21.28 o -12 2 2 1588.09 1504.40 16.93 o -11 2 2 42.77 49.27 1.48 o -10 2 2 37.35 31.71 1.19 o -9 2 2 1.46 0.32 0.57 o -8 2 2 10.29 13.09 0.97 o -7 2 2 275.82 304.32 4.70 o -6 2 2 350.79 337.92 4.30 o -5 2 2 361.42 373.39 4.61 o -4 2 2 1121.09 1217.33 13.67 o -3 2 2 86.86 81.45 3.83 o -2 2 2 8.62 20.38 0.77 o -1 2 2 705.82 704.79 8.22 o 0 2 2 1298.50 1418.18 19.25 o 1 2 2 49.84 42.45 2.64 o 2 2 2 1039.13 1314.66 14.69 o 3 2 2 3.84 6.84 0.69 o 4 2 2 5169.02 5790.92 62.01 o 5 2 2 1272.37 1467.92 14.13 o 6 2 2 379.89 397.24 3.86 o 7 2 2 47.27 43.40 0.98 o 8 2 2 214.32 223.86 3.14 o 9 2 2 525.76 489.31 5.21 o 11 2 2 102.59 108.73 2.83 o 12 2 2 874.30 911.49 13.34 o 13 2 2 2313.34 2413.70 32.32 o 14 2 2 466.62 466.89 8.71 o 15 2 2 10.01 9.10 1.23 o 16 2 2 25.92 22.75 1.36 o 17 2 2 49.98 47.84 1.89 o 18 2 2 8.33 5.98 1.24 o 19 2 2 114.80 131.66 7.35 o 20 2 2 26.34 23.87 3.24 o -20 3 2 53.59 68.13 2.94 o -19 3 2 34.87 42.53 2.39 o -18 3 2 42.66 46.67 1.95 o -17 3 2 82.46 75.17 2.47 o -16 3 2 145.07 153.18 3.26 o -15 3 2 7.37 5.66 1.23 o -14 3 2 342.52 356.73 5.37 o -13 3 2 42.80 37.95 1.64 o 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