#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/59/2235928.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235928_Fobs loop_ _publ_author_name 'Saphu, Watcharin' 'Chanthee, Songwuit' 'Chainok, Kittipong' 'Harding, David J.' 'Pakawatchai, Chaveng' _publ_section_title ; trans-Bis(nitrato-\kO)bis(1,10-phenanthroline-\k^2^N,N')manganese(II) ; _journal_coeditor_code NG5277 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1026 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.387 _cell_angle_gamma 90.000 _cell_length_a 11.6191 _cell_length_b 15.1164 _cell_length_c 13.4526 _exptl_crystal_F_000 1100.00 _reflns_d_resolution_high 0.7557 _[local]_cod_data_source_file ng5277Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' [Mn(phen)2(NO3)2]' _shelx_refln_list_code 4 _shelx_f_calc_maximum 432.48 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 30866.75 33331.46 367.02 o 4 0 0 7877.52 7765.70 90.33 o 6 0 0 772.22 758.58 15.29 o 8 0 0 22.85 42.85 5.72 o 10 0 0 686.30 653.40 36.62 o 12 0 0 167.28 121.13 17.48 o 14 0 0 0.68 7.58 13.47 o 1 1 0 30995.95 33507.77 249.48 o 3 1 0 190.49 202.77 4.29 o 5 1 0 2557.37 2441.84 23.70 o 7 1 0 51.48 48.30 3.82 o 9 1 0 1630.25 1560.05 21.56 o 11 1 0 86.05 78.64 10.94 o 13 1 0 175.94 181.23 15.14 o 2 2 0 16909.12 19528.81 153.16 o 4 2 0 3896.60 3768.88 33.42 o 6 2 0 5291.33 5572.54 49.25 o 8 2 0 1634.95 1591.68 60.30 o 10 2 0 226.31 217.11 11.79 o 12 2 0 230.42 247.77 16.59 o 14 2 0 122.39 113.29 13.59 o 1 3 0 3543.27 3874.76 34.86 o 3 3 0 3205.19 3383.77 30.04 o 5 3 0 683.51 646.08 9.06 o 7 3 0 1611.31 1587.00 17.80 o 9 3 0 1211.95 1152.69 15.63 o 11 3 0 58.60 51.87 9.38 o 13 3 0 125.71 127.13 13.41 o 0 4 0 14154.82 15814.75 295.91 o 2 4 0 3691.55 4181.41 36.07 o 6 4 0 2307.84 2336.95 24.69 o 8 4 0 1686.16 1611.51 20.95 o 10 4 0 605.82 561.07 16.82 o 12 4 0 129.95 136.63 13.61 o 14 4 0 4.65 -5.87 8.66 o 1 5 0 551.54 531.98 9.49 o 3 5 0 4186.79 4286.54 38.11 o 5 5 0 1446.79 1537.88 21.06 o 7 5 0 1730.35 1681.24 20.62 o 9 5 0 1404.57 1369.94 20.50 o 11 5 0 68.14 71.22 10.23 o 13 5 0 3.63 7.56 8.84 o 0 6 0 4297.20 4689.60 133.48 o 2 6 0 1464.79 1400.51 15.58 o 4 6 0 4088.91 4513.54 41.20 o 6 6 0 54.62 77.10 5.14 o 8 6 0 11.60 11.20 4.04 o 10 6 0 378.24 378.83 17.06 o 12 6 0 353.50 321.49 18.89 o 14 6 0 19.48 36.99 10.34 o 1 7 0 134.18 126.03 6.26 o 3 7 0 2580.79 2856.54 28.21 o 5 7 0 170.85 185.69 6.72 o 7 7 0 2.07 6.56 3.81 o 9 7 0 8.16 7.93 4.67 o 11 7 0 373.45 360.83 17.43 o 13 7 0 3.27 21.29 9.32 o 0 8 0 8.43 5.44 6.80 o 2 8 0 76.88 100.06 5.07 o 4 8 0 729.67 752.67 16.71 o 6 8 0 65.66 65.17 5.53 o 8 8 0 270.45 279.57 9.59 o 10 8 0 24.85 22.10 7.25 o 12 8 0 19.64 38.97 9.18 o 1 9 0 212.20 235.28 11.35 o 3 9 0 353.65 362.27 8.50 o 5 9 0 1676.37 1648.30 20.92 o 7 9 0 117.60 131.86 7.32 o 9 9 0 0.85 6.71 5.41 o 11 9 0 0.27 4.72 7.09 o 13 9 0 1.33 18.10 11.54 o 0 10 0 2829.04 2874.29 63.53 o 2 10 0 451.70 442.06 11.12 o 4 10 0 1440.47 1352.32 18.42 o 6 10 0 126.90 117.77 7.32 o 8 10 0 1.70 2.12 5.24 o 10 10 0 29.87 45.38 13.26 o 12 10 0 6.67 21.39 10.90 o 1 11 0 3799.09 3425.63 138.62 o 3 11 0 3477.74 3384.92 35.11 o 5 11 0 1369.56 1295.91 18.99 o 7 11 0 162.75 176.23 9.19 o 9 11 0 150.60 187.63 12.58 o 11 11 0 32.25 52.01 11.45 o 0 12 0 2428.05 2375.09 59.55 o 2 12 0 37.48 26.20 7.58 o 4 12 0 872.97 867.74 19.77 o 6 12 0 656.82 603.89 14.24 o 8 12 0 893.23 820.09 19.44 o 10 12 0 77.74 98.68 10.47 o 1 13 0 1504.68 1526.00 32.83 o 3 13 0 449.45 452.24 15.76 o 5 13 0 529.66 535.40 16.42 o 7 13 0 782.62 690.74 16.29 o 9 13 0 211.26 227.70 16.57 o 11 13 0 58.40 60.59 18.83 o 0 14 0 3337.24 3123.46 75.49 o 2 14 0 2218.34 2075.08 35.36 o 4 14 0 1232.53 1236.27 30.88 o 6 14 0 514.20 507.30 18.51 o 8 14 0 105.07 115.16 14.11 o 10 14 0 44.06 74.81 14.57 o 1 15 0 1811.59 1645.54 36.69 o 3 15 0 642.31 651.75 23.21 o 5 15 0 330.52 339.10 23.21 o 7 15 0 61.17 83.10 10.00 o 9 15 0 127.56 170.17 17.32 o 0 16 0 1132.46 1083.15 115.02 o 2 16 0 805.63 799.73 26.39 o 4 16 0 775.70 781.25 25.56 o 6 16 0 320.62 316.46 26.92 o 8 16 0 187.48 231.22 22.90 o 1 17 0 834.30 790.54 26.27 o 3 17 0 662.99 653.80 38.28 o 5 17 0 108.33 119.87 15.26 o 7 17 0 43.71 39.53 13.07 o 0 18 0 276.28 277.39 29.92 o 2 18 0 39.11 40.44 11.66 o 4 18 0 4.75 17.13 9.64 o 6 18 0 26.75 42.40 11.52 o 1 19 0 145.65 152.63 17.25 o 3 19 0 61.13 51.68 12.07 o 0 20 0 52.80 65.59 17.65 o -15 1 1 3.37 57.11 32.06 o -13 1 1 10.45 24.60 8.72 o -11 1 1 49.74 63.97 8.22 o -9 1 1 101.02 114.10 7.51 o -7 1 1 2230.25 2350.97 24.47 o -5 1 1 20.43 13.84 2.30 o -3 1 1 294.78 247.33 4.40 o -1 1 1 3499.48 3763.77 35.98 o 1 1 1 217.63 220.29 3.81 o 3 1 1 51025.98 55751.31 432.68 o 5 1 1 3537.08 3770.62 34.34 o 7 1 1 211.42 236.37 6.74 o 9 1 1 319.02 325.18 9.79 o 11 1 1 2.25 10.05 8.92 o 13 1 1 1.00 16.78 8.81 o -14 2 1 22.91 60.74 11.08 o -12 2 1 0.13 12.99 7.51 o -10 2 1 52.66 55.91 6.64 o -8 2 1 76.50 98.85 4.75 o -6 2 1 1417.84 1448.41 15.41 o -4 2 1 357.93 400.03 8.58 o -2 2 1 833.86 807.08 8.83 o 0 2 1 1148.55 1250.54 14.65 o 2 2 1 9.06 18.38 1.97 o 4 2 1 4383.61 4233.23 37.26 o 6 2 1 43.53 51.56 3.66 o 8 2 1 771.49 797.00 12.82 o 10 2 1 14.53 7.50 6.70 o 12 2 1 4.91 17.89 8.24 o 14 2 1 2.57 -8.95 8.95 o -13 3 1 58.11 97.73 11.88 o -11 3 1 56.79 53.40 8.00 o -9 3 1 387.63 399.13 10.68 o -7 3 1 16.09 11.20 3.00 o -5 3 1 3953.72 3793.73 34.70 o -3 3 1 1692.03 1903.84 18.49 o -1 3 1 12000.57 13022.05 119.36 o 1 3 1 421.19 445.01 6.68 o 3 3 1 577.34 542.52 7.39 o 5 3 1 3475.37 3569.45 31.39 o 7 3 1 410.64 402.63 8.94 o 9 3 1 356.33 344.53 9.79 o 11 3 1 16.71 10.05 7.29 o 13 3 1 0.13 0.99 9.56 o -14 4 1 80.47 77.97 12.52 o -12 4 1 0.41 10.56 7.90 o -10 4 1 221.52 237.09 13.64 o -8 4 1 318.32 320.13 8.61 o -6 4 1 637.24 587.74 10.00 o -4 4 1 6373.40 6832.18 57.86 o -2 4 1 723.52 812.86 9.69 o 0 4 1 2767.71 2788.27 31.63 o 2 4 1 890.87 968.84 11.20 o 4 4 1 3853.57 3819.81 32.87 o 6 4 1 283.24 337.55 7.42 o 8 4 1 458.85 469.00 9.68 o 10 4 1 66.83 90.24 8.78 o 12 4 1 7.23 7.19 8.89 o 14 4 1 11.09 22.93 9.92 o -13 5 1 105.49 141.99 14.11 o -11 5 1 174.66 194.62 15.65 o -9 5 1 789.87 787.59 15.20 o -7 5 1 2130.40 2247.10 25.08 o -5 5 1 10555.51 11159.81 92.65 o -3 5 1 10396.41 11921.57 96.91 o -1 5 1 8893.02 9190.34 80.12 o 1 5 1 260.18 288.61 5.91 o 3 5 1 4459.45 4490.75 39.86 o 5 5 1 4995.18 5365.75 48.26 o 7 5 1 180.28 204.21 7.33 o 9 5 1 1505.08 1453.36 22.23 o 11 5 1 47.86 29.02 8.97 o 13 5 1 1.25 31.82 9.46 o -14 6 1 58.97 83.91 12.71 o -12 6 1 97.13 118.30 12.44 o -10 6 1 445.20 450.16 16.61 o -8 6 1 620.77 564.19 12.56 o -6 6 1 4671.26 4801.32 44.88 o -4 6 1 12604.32 13400.49 109.68 o -2 6 1 963.11 903.49 15.27 o 0 6 1 10094.45 10007.49 117.64 o 2 6 1 1824.12 1709.30 18.14 o 4 6 1 3484.70 3413.13 32.83 o 6 6 1 631.09 633.57 11.33 o 8 6 1 2344.88 2227.47 33.74 o 10 6 1 280.13 259.82 11.97 o 12 6 1 182.57 189.82 15.70 o -13 7 1 120.47 135.06 14.10 o -11 7 1 1017.56 917.53 23.16 o -9 7 1 814.56 842.97 16.39 o -7 7 1 31.50 33.74 4.52 o -1 7 1 7175.42 7286.23 89.52 o 1 7 1 2249.09 2338.59 30.37 o 3 7 1 3340.06 3112.85 30.42 o 5 7 1 72.85 43.51 5.43 o 7 7 1 291.13 292.12 10.24 o 9 7 1 103.94 113.05 7.89 o 11 7 1 267.45 281.28 17.49 o 13 7 1 193.88 210.84 19.57 o -12 8 1 250.78 249.67 21.76 o -10 8 1 1323.98 1253.64 35.59 o -8 8 1 12.55 9.63 4.25 o -6 8 1 835.70 825.51 13.77 o -4 8 1 1577.21 1346.10 17.12 o -2 8 1 1457.81 1335.95 17.15 o 0 8 1 14417.72 15329.56 206.40 o 2 8 1 9831.35 10145.86 85.07 o 4 8 1 1906.88 1727.63 20.60 o 6 8 1 511.41 490.24 10.83 o 8 8 1 1053.99 1056.56 18.70 o 10 8 1 2.98 2.38 5.66 o 12 8 1 435.17 423.57 21.93 o -13 9 1 89.84 73.19 14.07 o -11 9 1 89.98 110.83 10.85 o -9 9 1 478.93 468.03 13.19 o -7 9 1 513.51 537.64 16.79 o -5 9 1 1804.25 1769.49 21.77 o -3 9 1 1803.89 1836.39 21.16 o -1 9 1 5881.25 6236.77 81.04 o 1 9 1 1575.47 1493.88 27.63 o 3 9 1 5781.39 5744.89 52.32 o 5 9 1 810.59 805.41 16.44 o 7 9 1 684.18 615.82 18.22 o 9 9 1 319.46 321.29 12.06 o 11 9 1 148.99 155.56 13.99 o -12 10 1 41.01 47.36 10.53 o -10 10 1 237.11 265.02 16.52 o -8 10 1 201.49 204.57 9.79 o -6 10 1 465.49 470.57 11.28 o -4 10 1 2029.64 2000.14 23.65 o -2 10 1 262.61 277.10 10.02 o 0 10 1 5410.20 5614.30 75.70 o 2 10 1 6241.21 6385.43 61.58 o 4 10 1 1372.86 1324.56 18.27 o 6 10 1 273.10 258.72 9.24 o 8 10 1 489.12 509.01 14.13 o 10 10 1 25.46 40.90 7.52 o 12 10 1 123.37 113.55 15.61 o -11 11 1 29.36 28.02 9.46 o -9 11 1 235.44 237.60 13.66 o -7 11 1 58.96 61.23 7.82 o -5 11 1 849.17 839.93 16.15 o -3 11 1 886.21 873.54 22.46 o -1 11 1 2772.90 2336.79 68.20 o 1 11 1 3409.09 3156.52 49.71 o 3 11 1 1207.22 1198.98 17.33 o 5 11 1 111.39 118.76 7.04 o 7 11 1 69.12 74.00 6.52 o 9 11 1 47.53 59.03 7.77 o 11 11 1 77.97 86.00 17.38 o -12 12 1 34.87 47.37 13.76 o -10 12 1 148.75 131.91 19.63 o -8 12 1 55.96 54.78 6.95 o -6 12 1 204.61 230.00 10.24 o -4 12 1 975.04 937.65 17.27 o -2 12 1 3.88 -2.22 6.84 o 0 12 1 223.95 231.15 13.80 o 2 12 1 410.34 416.05 15.81 o 4 12 1 312.57 327.29 10.81 o 6 12 1 3.25 5.30 6.23 o 8 12 1 212.00 239.30 14.01 o 10 12 1 8.12 16.46 9.17 o -11 13 1 0.55 30.59 11.88 o -9 13 1 116.42 111.39 11.22 o -7 13 1 458.03 448.36 14.18 o -5 13 1 229.89 230.37 10.28 o -3 13 1 560.58 532.45 17.06 o -1 13 1 96.47 85.75 10.72 o 1 13 1 860.47 882.78 24.18 o 3 13 1 1103.52 1140.88 28.07 o 5 13 1 283.55 303.39 14.20 o 7 13 1 321.38 318.13 15.32 o 9 13 1 219.83 245.31 23.75 o 11 13 1 4.61 24.48 24.29 o -10 14 1 1.71 31.79 11.99 o -8 14 1 19.09 10.46 6.80 o -6 14 1 170.44 163.72 9.78 o -4 14 1 5.27 6.92 6.19 o -2 14 1 283.28 289.59 16.80 o 0 14 1 0.16 -6.82 6.82 o 2 14 1 859.85 816.27 24.52 o 4 14 1 1043.78 1010.09 27.35 o 6 14 1 16.51 12.16 7.09 o 8 14 1 183.61 192.44 15.48 o 10 14 1 4.09 12.56 11.34 o -9 15 1 1.24 35.85 15.80 o -7 15 1 1.00 14.32 9.42 o -5 15 1 14.05 22.33 8.96 o -3 15 1 33.55 35.51 9.31 o -1 15 1 29.95 25.02 8.68 o 1 15 1 53.29 54.97 9.85 o 3 15 1 57.81 52.39 10.31 o 5 15 1 10.94 10.65 11.86 o 7 15 1 0.84 6.79 8.09 o 9 15 1 0.40 23.06 11.51 o -8 16 1 71.89 58.18 16.90 o -6 16 1 17.54 18.51 14.43 o -4 16 1 1.60 16.85 10.92 o -2 16 1 72.10 89.32 11.69 o 0 16 1 11.63 26.82 8.83 o 2 16 1 118.11 107.85 12.39 o 4 16 1 0.21 8.11 8.51 o 6 16 1 0.78 18.62 9.22 o 8 16 1 2.56 18.67 9.95 o -7 17 1 101.79 128.69 14.14 o -5 17 1 16.38 30.60 9.87 o -3 17 1 112.88 102.14 15.91 o -1 17 1 69.75 68.62 11.64 o 1 17 1 353.21 356.38 20.62 o 3 17 1 60.72 52.03 13.00 o 5 17 1 7.79 13.53 9.21 o 7 17 1 136.51 204.83 22.43 o -6 18 1 1.43 30.67 10.82 o -4 18 1 7.27 2.41 9.25 o -2 18 1 42.04 40.25 10.83 o 0 18 1 24.60 26.16 9.55 o 2 18 1 180.32 201.78 17.29 o 4 18 1 17.48 22.45 10.28 o 6 18 1 102.15 104.46 25.98 o -3 19 1 637.75 635.04 28.04 o -1 19 1 123.25 151.12 16.24 o 1 19 1 225.82 203.08 17.48 o 3 19 1 321.46 365.56 22.74 o -14 0 2 13.41 8.59 33.03 o -12 0 2 9.36 16.79 21.86 o -10 0 2 1011.46 1018.68 45.29 o -8 0 2 9.57 4.42 3.71 o -4 0 2 4375.21 4466.24 63.93 o -2 0 2 3747.68 4316.11 50.63 o 0 0 2 42266.86 44764.34 695.66 o 2 0 2 187040.77 192066.00 2489.93 o 4 0 2 59085.13 63720.64 700.26 o 6 0 2 9237.91 9376.91 111.71 o 8 0 2 955.05 925.96 24.63 o 10 0 2 19.74 14.36 9.93 o 12 0 2 238.91 261.83 24.61 o 14 0 2 55.80 71.44 16.38 o -15 1 2 7.46 26.49 10.10 o -13 1 2 26.70 39.63 9.70 o -11 1 2 1001.79 900.86 19.25 o -9 1 2 1002.58 968.21 18.24 o -7 1 2 190.30 149.15 4.49 o -5 1 2 4776.19 4557.74 43.11 o -3 1 2 683.68 603.64 8.39 o -1 1 2 26583.50 30233.14 333.12 o 1 1 2 1272.70 1248.18 15.74 o 3 1 2 4394.03 4621.99 42.62 o 5 1 2 4262.00 4322.16 38.90 o 7 1 2 814.77 756.12 11.85 o 9 1 2 1.50 7.25 4.89 o 11 1 2 318.84 321.12 17.95 o 13 1 2 86.25 90.53 12.02 o -14 2 2 138.28 150.90 16.41 o -12 2 2 336.25 310.91 16.47 o -10 2 2 2479.33 2379.78 33.62 o -8 2 2 889.36 873.31 12.85 o -6 2 2 2088.32 2117.30 21.80 o -4 2 2 2027.73 2020.97 19.57 o -2 2 2 38804.34 42543.73 330.71 o 2 2 2 5076.18 5738.52 47.65 o 4 2 2 173.26 132.86 4.19 o 6 2 2 469.12 493.49 8.83 o 8 2 2 1911.13 1856.27 24.39 o 10 2 2 147.32 157.57 9.42 o 12 2 2 138.59 162.25 14.91 o 14 2 2 39.08 58.69 11.16 o -15 3 2 74.33 89.35 20.05 o -13 3 2 33.66 39.69 9.60 o -11 3 2 765.76 687.13 22.46 o -9 3 2 594.58 562.19 18.55 o -7 3 2 784.14 753.23 11.48 o -5 3 2 6885.72 6929.73 58.94 o -3 3 2 23.02 28.66 2.50 o -1 3 2 44261.82 49263.21 484.57 o 1 3 2 3547.89 4057.02 34.52 o 3 3 2 3926.99 4002.05 37.77 o 5 3 2 1786.62 1838.52 21.30 o 7 3 2 763.93 769.22 12.28 o 9 3 2 94.45 91.67 8.64 o 11 3 2 208.46 205.97 15.14 o 13 3 2 81.68 106.39 12.82 o -14 4 2 87.56 106.15 13.21 o -12 4 2 11.65 11.27 6.85 o -10 4 2 1099.16 1082.60 27.62 o -8 4 2 473.60 430.32 9.43 o -6 4 2 1469.50 1537.27 17.98 o -4 4 2 6773.42 7467.78 62.81 o -2 4 2 8533.65 9087.08 78.98 o 0 4 2 3152.72 3568.50 39.39 o 2 4 2 181.02 192.42 4.75 o 4 4 2 482.87 449.99 7.55 o 6 4 2 7.71 2.88 2.73 o 8 4 2 609.15 572.56 11.82 o 10 4 2 27.78 18.22 6.65 o 12 4 2 343.35 333.33 20.39 o -13 5 2 27.66 47.48 12.84 o -11 5 2 1.40 1.02 6.15 o -9 5 2 76.06 66.52 6.14 o -7 5 2 355.70 370.12 8.81 o -5 5 2 3061.32 3103.83 30.29 o -3 5 2 9676.83 10684.55 87.45 o -1 5 2 10122.30 11054.38 113.61 o 1 5 2 664.21 730.72 9.99 o 3 5 2 592.68 544.56 9.31 o 5 5 2 2929.82 3064.48 29.90 o 7 5 2 1012.44 1009.17 14.28 o 9 5 2 39.39 40.11 5.32 o 11 5 2 273.73 244.44 18.00 o 13 5 2 0.16 22.40 10.97 o -14 6 2 21.41 28.14 10.06 o -12 6 2 40.38 47.42 9.09 o -10 6 2 534.42 547.17 15.35 o -8 6 2 45.89 50.65 5.07 o -6 6 2 940.29 1026.29 14.62 o -4 6 2 73.12 99.41 4.64 o -2 6 2 7597.05 8407.45 81.47 o 0 6 2 3463.96 3745.91 42.97 o 2 6 2 1076.20 1116.00 13.49 o 4 6 2 3531.72 3682.21 35.18 o 6 6 2 2538.02 2493.58 27.28 o 8 6 2 60.39 57.57 6.08 o 10 6 2 33.72 39.67 7.89 o 12 6 2 200.20 184.49 15.30 o -13 7 2 0.13 5.33 13.18 o -11 7 2 33.25 25.44 7.75 o -9 7 2 29.14 34.87 5.68 o -7 7 2 0.05 -0.13 3.36 o -5 7 2 531.87 578.65 10.45 o -3 7 2 370.56 377.48 7.49 o -1 7 2 24.15 40.70 8.33 o 1 7 2 216.24 184.82 6.08 o 3 7 2 126.00 126.86 5.21 o 5 7 2 1753.13 1784.63 21.34 o 7 7 2 317.30 304.27 10.47 o 9 7 2 65.20 59.08 6.81 o 11 7 2 9.99 18.33 9.20 o 13 7 2 75.85 66.58 11.76 o -12 8 2 1.25 11.27 7.43 o -10 8 2 137.57 120.86 9.34 o -8 8 2 3.94 3.26 4.60 o -6 8 2 16.68 6.30 3.68 o -4 8 2 291.04 330.32 8.34 o -2 8 2 342.21 349.28 10.11 o 0 8 2 1602.09 1491.36 38.27 o 2 8 2 43.02 47.36 3.86 o 4 8 2 648.89 670.36 11.66 o 6 8 2 4.00 4.38 3.74 o 8 8 2 19.60 22.74 5.21 o 10 8 2 1.25 10.83 6.53 o 12 8 2 86.01 87.99 13.37 o -13 9 2 49.14 57.65 14.67 o -11 9 2 23.08 20.50 8.08 o -9 9 2 11.31 6.22 4.95 o -7 9 2 242.23 264.36 9.16 o -5 9 2 1.27 11.70 3.78 o -3 9 2 35.94 39.46 4.06 o -1 9 2 493.67 511.13 15.41 o 1 9 2 932.23 889.51 14.68 o 3 9 2 247.14 242.00 7.53 o 5 9 2 261.22 266.62 8.70 o 7 9 2 6.83 12.66 4.93 o 9 9 2 106.49 128.91 8.83 o 11 9 2 7.09 17.68 10.54 o -12 10 2 1.56 15.48 8.74 o -10 10 2 0.28 19.96 7.88 o -8 10 2 125.51 130.37 8.20 o -6 10 2 125.18 133.74 7.89 o -4 10 2 268.28 229.19 8.75 o -2 10 2 13.84 18.39 6.22 o 0 10 2 2028.96 1983.50 44.48 o 2 10 2 957.59 999.62 15.60 o 4 10 2 863.35 819.11 14.75 o 6 10 2 208.82 217.81 8.84 o 8 10 2 101.15 91.86 7.86 o 10 10 2 94.21 104.11 10.46 o 12 10 2 0.92 3.75 11.48 o -11 11 2 46.46 58.39 10.72 o -9 11 2 32.98 35.26 6.73 o -7 11 2 571.23 550.55 18.32 o -5 11 2 762.26 740.34 15.14 o -3 11 2 600.72 601.76 29.06 o -1 11 2 1593.62 1427.26 71.88 o 1 11 2 1341.20 1333.39 23.72 o 3 11 2 4078.54 3967.42 40.04 o 5 11 2 2640.80 2551.86 29.92 o 7 11 2 734.65 734.09 17.71 o 9 11 2 315.22 337.81 15.48 o 11 11 2 29.91 50.34 15.16 o -12 12 2 62.48 73.56 12.35 o -10 12 2 32.66 52.03 10.08 o -8 12 2 648.12 569.87 14.96 o -6 12 2 1801.28 1597.72 32.25 o -4 12 2 1138.99 1045.41 20.11 o -2 12 2 996.80 945.13 24.28 o 0 12 2 70.42 73.23 10.57 o 2 12 2 517.44 529.01 16.09 o 4 12 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