#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:43:23 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181281 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/59/2235945.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235945_Fobs loop_ _publ_author_name 'Fejfarov\'a, Karla' 'Du\E)-4-[(4-Bromophenyl)iminomethyl]-2-methoxyphenol ; _journal_coeditor_code PK2433 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2466 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90 _cell_angle_beta 97.798(4) _cell_angle_gamma 90 _cell_length_a 6.5692(3) _cell_length_b 11.4323(4) _cell_length_c 17.5552(9) _exptl_crystal_F_000 616 _reflns_d_resolution_high 0.8376 _cod_data_source_file pk2433Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 200.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 304.15 320.39 14.13 o 2 0 0 10915.20 10867.40 104.48 o 3 0 0 3287.88 3261.47 122.67 o 4 0 0 8.64 2.06 5.97 < 5 0 0 793.46 802.10 20.12 o 6 0 0 2.63 10.20 5.38 < 7 0 0 9.09 4.34 6.41 < 1 1 0 1079.88 1063.80 18.09 o 2 1 0 6.54 16.64 6.11 < 3 1 0 47.74 58.29 8.08 o 4 1 0 492.30 497.51 12.22 o 5 1 0 148.09 141.72 7.09 o 6 1 0 266.56 287.98 9.59 o 7 1 0 55.70 58.28 5.49 o 0 2 0 411.47 438.09 14.98 o 1 2 0 1938.88 1777.89 26.08 o 2 2 0 14514.30 14423.20 119.10 o 3 2 0 2792.30 2550.79 43.56 o 4 2 0 199.75 272.75 10.21 o 5 2 0 2378.16 2552.74 31.00 o 6 2 0 1718.46 1783.47 30.29 o 7 2 0 417.95 391.52 12.43 o 1 3 0 4183.88 3881.55 44.43 o 2 3 0 3252.11 3245.58 51.84 o 3 3 0 1903.14 1924.72 31.79 o 4 3 0 470.71 452.48 13.26 o 5 3 0 904.82 940.04 21.60 o 6 3 0 47.16 44.21 6.55 o 7 3 0 239.13 240.76 10.95 o 0 4 0 1616.50 1505.81 43.53 o 1 4 0 1750.91 1627.87 33.08 o 2 4 0 182.44 244.34 17.31 o 3 4 0 4476.40 4578.24 40.49 o 4 4 0 331.42 334.61 11.93 o 5 4 0 900.19 940.84 23.25 o 6 4 0 105.68 99.30 7.78 o 7 4 0 91.17 98.01 7.88 o 1 5 0 5707.65 5312.45 66.02 o 2 5 0 504.17 429.46 16.28 o 3 5 0 13.87 5.35 3.41 < 4 5 0 1923.99 1831.43 31.38 o 5 5 0 273.40 255.04 11.39 o 6 5 0 537.29 544.55 16.83 o 7 5 0 477.89 454.07 18.49 o 0 6 0 472.20 486.63 22.45 o 1 6 0 281.14 255.69 16.42 o 2 6 0 19.94 14.92 4.40 o 3 6 0 597.49 611.15 14.54 o 4 6 0 6.34 7.21 4.06 < 5 6 0 27.35 29.57 7.60 o 6 6 0 2.82 5.11 6.43 < 1 7 0 6255.00 6356.21 38.97 o 2 7 0 599.83 578.01 15.38 o 3 7 0 242.15 215.79 9.39 o 4 7 0 1776.05 1792.38 23.31 o 5 7 0 69.02 76.31 9.61 o 6 7 0 286.68 313.48 18.88 o 0 8 0 1753.35 1827.71 30.96 o 1 8 0 15.76 17.59 4.11 o 2 8 0 37.37 39.66 6.16 o 3 8 0 506.95 543.65 13.91 o 4 8 0 93.28 77.37 6.50 o 5 8 0 61.45 48.91 7.34 o 6 8 0 1.58 3.52 5.17 < 1 9 0 1002.59 981.53 20.00 o 2 9 0 1368.87 1471.21 27.74 o 3 9 0 292.85 279.55 10.94 o 4 9 0 456.27 478.23 12.25 o 5 9 0 267.17 244.17 10.34 o 0 10 0 112.67 155.01 14.15 o 1 10 0 385.62 428.72 13.45 o 2 10 0 1073.29 1098.23 21.84 o 3 10 0 237.88 254.37 10.25 o 4 10 0 105.14 91.40 6.16 o 5 10 0 408.60 339.23 15.73 o 1 11 0 148.08 140.04 10.89 o 2 11 0 208.99 229.32 10.70 o 3 11 0 139.23 142.71 7.32 o 4 11 0 343.43 352.65 15.42 o 0 12 0 4116.11 4018.67 101.14 o 1 12 0 2.38 6.36 5.05 < 2 12 0 139.85 119.04 8.50 o 3 12 0 458.93 466.02 15.80 o 1 13 0 5.46 4.85 8.59 < 2 13 0 96.85 85.43 14.97 o -7 1 1 11.74 10.23 4.49 < -6 1 1 1635.56 1758.31 23.37 o -5 1 1 1420.15 1508.79 19.13 o -4 1 1 3122.89 3189.80 30.16 o -3 1 1 7592.08 7606.63 88.02 o -2 1 1 262.39 248.71 16.10 o -1 1 1 15699.80 15399.80 118.99 o 0 1 1 1670.79 1686.24 20.96 o 1 1 1 1339.74 1307.40 17.25 o 2 1 1 7444.04 7135.38 94.18 o 3 1 1 2974.64 3054.35 50.60 o 4 1 1 3186.05 3352.31 31.07 o 5 1 1 1974.45 1975.54 23.70 o 6 1 1 124.00 130.43 6.95 o 7 1 1 138.47 177.06 9.72 o -7 2 1 86.54 86.08 6.58 o -6 2 1 87.07 86.51 7.68 o -5 2 1 95.21 102.75 6.40 o -4 2 1 843.97 891.49 14.03 o -3 2 1 501.34 573.60 19.42 o -2 2 1 3683.53 3834.72 61.78 o -1 2 1 1131.15 1059.96 30.18 o 0 2 1 308.72 325.43 9.66 o 1 2 1 10085.80 9717.72 52.57 o 2 2 1 248.15 258.43 18.24 o 3 2 1 537.79 506.93 16.99 o 4 2 1 1025.76 1050.96 21.07 o 5 2 1 0.31 -3.28 4.89 < 6 2 1 1532.35 1652.42 27.48 o 7 2 1 12.09 12.87 3.87 o -7 3 1 293.26 262.84 12.53 o -6 3 1 870.86 923.75 20.75 o -5 3 1 215.05 211.09 13.19 o -4 3 1 517.84 489.20 9.70 o -3 3 1 3637.29 3509.77 41.74 o -2 3 1 96.82 93.95 11.62 o -1 3 1 9914.25 9174.75 83.96 o 0 3 1 3821.79 3665.38 37.08 o 1 3 1 2285.15 2125.34 27.03 o 2 3 1 2960.44 2853.20 41.19 o 3 3 1 40.58 25.40 5.83 o 4 3 1 167.31 162.40 9.14 o 5 3 1 489.56 512.53 14.53 o 6 3 1 90.91 76.33 7.45 o 7 3 1 179.12 190.71 8.40 o -7 4 1 474.51 457.11 15.88 o -6 4 1 16.82 15.72 5.14 o -5 4 1 1447.04 1442.91 25.07 o -4 4 1 553.33 501.94 10.76 o -3 4 1 14.94 12.15 3.92 o -2 4 1 3333.01 3231.30 65.18 o -1 4 1 2801.49 2645.04 50.65 o 0 4 1 2067.84 2006.55 30.79 o 1 4 1 1996.58 1833.28 28.78 o 2 4 1 2188.76 2498.91 42.22 o 3 4 1 2743.94 2637.93 27.26 o 4 4 1 2054.29 1994.36 27.55 o 5 4 1 542.36 573.31 17.33 o 6 4 1 175.61 184.77 9.72 o 7 4 1 23.40 11.51 3.98 < -7 5 1 152.15 161.61 11.82 o -6 5 1 9.17 16.75 6.49 < -5 5 1 315.68 314.39 13.81 o -4 5 1 65.84 57.84 5.35 o -3 5 1 251.52 230.77 8.55 o -2 5 1 89.84 103.28 10.52 o -1 5 1 188.99 137.40 14.73 o 0 5 1 1660.56 1585.34 30.76 o 1 5 1 542.54 497.08 17.52 o 2 5 1 1527.29 1594.30 31.36 o 3 5 1 38.66 32.75 4.14 o 4 5 1 7.01 6.27 5.00 < 5 5 1 416.46 415.79 13.90 o 6 5 1 28.47 32.07 5.22 o 7 5 1 96.37 96.14 8.94 o -7 6 1 155.01 145.38 7.95 o -6 6 1 87.57 89.96 10.52 o -5 6 1 469.41 496.40 23.01 o -4 6 1 2191.17 2116.78 23.72 o -3 6 1 546.50 554.30 12.96 o -2 6 1 8705.60 9286.40 66.78 o -1 6 1 478.27 456.70 18.75 o 0 6 1 2078.88 2145.97 35.30 o 1 6 1 6184.06 5992.56 54.53 o 2 6 1 50.10 60.91 4.94 o 3 6 1 2005.97 1946.90 22.91 o 4 6 1 1143.68 1141.65 25.02 o 5 6 1 103.75 112.94 7.83 o 6 6 1 1022.02 1054.14 29.12 o -6 7 1 17.25 21.02 6.00 o -5 7 1 51.78 44.98 9.41 o -4 7 1 48.18 44.51 5.65 o -3 7 1 43.38 48.94 5.67 o -2 7 1 1.16 1.68 5.97 < -1 7 1 18.60 24.34 3.47 o 0 7 1 200.97 193.36 6.46 o 1 7 1 21.67 24.60 4.45 o 2 7 1 61.04 61.96 6.18 o 3 7 1 1.39 7.78 4.11 < 4 7 1 17.84 9.24 4.81 < 5 7 1 44.66 41.47 8.17 o 6 7 1 93.38 72.54 7.87 o -6 8 1 229.74 196.80 13.00 o -5 8 1 1045.69 1054.15 18.91 o -4 8 1 1429.21 1556.20 20.83 o -3 8 1 16.83 14.37 5.25 < -2 8 1 2603.05 2659.62 34.38 o -1 8 1 832.07 793.47 16.60 o 0 8 1 2499.97 2480.26 23.99 o 1 8 1 1239.24 1224.67 19.23 o 2 8 1 399.30 411.02 14.60 o 3 8 1 1839.29 1796.19 26.97 o 4 8 1 1623.80 1694.93 24.19 o 5 8 1 135.13 115.82 11.63 o 6 8 1 227.70 231.13 13.94 o -5 9 1 26.72 14.43 3.90 o -4 9 1 178.20 146.82 7.53 o -3 9 1 1462.76 1506.18 25.44 o -2 9 1 436.86 399.29 15.27 o -1 9 1 1471.18 1468.31 24.21 o 0 9 1 301.44 284.66 10.63 o 1 9 1 686.97 687.84 15.87 o 2 9 1 525.20 540.07 16.77 o 3 9 1 53.39 54.86 6.10 o 4 9 1 64.71 64.62 5.49 o 5 9 1 525.41 465.86 15.54 o -5 10 1 33.10 37.44 6.48 o -4 10 1 36.71 35.32 5.38 o -3 10 1 109.06 109.80 8.18 o -2 10 1 597.31 666.84 20.36 o -1 10 1 564.73 594.42 14.15 o 0 10 1 33.37 22.32 6.68 o 1 10 1 1994.38 2121.47 30.45 o 2 10 1 24.09 27.01 6.37 o 3 10 1 93.26 100.53 7.33 o 4 10 1 89.26 108.99 7.20 o 5 10 1 43.63 30.11 5.82 o -4 11 1 232.23 222.31 8.71 o -3 11 1 953.12 952.56 16.43 o -2 11 1 32.11 37.38 6.80 o -1 11 1 1126.03 1215.67 29.86 o 0 11 1 535.66 552.70 17.97 o 1 11 1 20.01 25.36 7.16 o 2 11 1 456.06 482.65 14.66 o 3 11 1 74.78 62.16 6.28 o 4 11 1 104.81 90.55 8.42 o -3 12 1 13.20 6.73 5.40 < -2 12 1 43.63 44.96 6.76 o -1 12 1 70.51 68.37 9.73 o 0 12 1 62.22 40.94 10.00 o 1 12 1 569.15 601.82 19.94 o 2 12 1 3.51 -5.09 5.80 < 3 12 1 206.13 193.25 12.36 o -2 13 1 1.63 -10.99 8.98 < -1 13 1 178.29 192.20 22.19 o 0 13 1 195.49 153.99 13.28 o 1 13 1 75.39 54.39 10.47 o 2 13 1 633.92 477.04 31.02 o -7 0 2 202.48 210.81 15.59 o -6 0 2 909.26 1000.70 24.41 o -5 0 2 165.29 155.20 9.65 o -4 0 2 2798.87 2656.57 39.75 o -3 0 2 4749.18 4626.92 68.12 o -2 0 2 7132.71 7264.04 63.20 o -1 0 2 6309.81 6427.75 70.10 o 0 0 2 360.99 365.87 18.18 o 1 0 2 43.00 46.89 11.24 o 2 0 2 2586.26 2552.69 90.39 o 3 0 2 397.14 422.33 28.36 o 4 0 2 5205.64 5306.83 65.83 o 5 0 2 532.27 536.52 19.50 o 6 0 2 255.92 272.29 13.95 o 7 0 2 2185.32 2341.98 45.84 o -7 1 2 113.92 128.37 9.03 o -6 1 2 299.23 302.53 10.30 o -5 1 2 12.93 11.85 4.08 < -4 1 2 2.55 5.19 3.43 < -3 1 2 5971.66 6192.31 72.15 o -2 1 2 386.59 364.33 15.72 o -1 1 2 3952.28 4250.87 44.68 o 0 1 2 5.35 10.35 4.35 < 1 1 2 21311.70 20699.90 86.55 o 2 1 2 41.26 40.26 9.71 o 3 1 2 456.78 450.50 17.92 o 4 1 2 145.43 138.94 7.24 o 5 1 2 1363.26 1417.15 21.75 o 6 1 2 387.47 427.72 12.19 o 7 1 2 26.10 24.30 4.78 o -7 2 2 526.61 493.90 14.81 o -6 2 2 608.18 681.87 16.14 o -5 2 2 107.92 102.29 7.05 o -4 2 2 5268.89 5251.90 33.67 o -3 2 2 146.05 121.30 8.66 o -2 2 2 2516.77 2711.47 62.89 o -1 2 2 5117.29 5031.65 54.33 o 0 2 2 126.33 128.81 8.01 o 1 2 2 3817.96 3476.55 37.27 o 2 2 2 9909.37 9592.14 65.78 o 3 2 2 49.18 49.43 8.54 o 4 2 2 1169.19 1188.21 21.26 o 5 2 2 603.59 609.47 17.32 o 6 2 2 35.52 43.99 6.36 o 7 2 2 24.86 28.86 4.45 o -7 3 2 75.06 78.49 7.46 o -6 3 2 182.28 190.36 10.29 o -5 3 2 3451.51 3530.66 34.53 o -4 3 2 399.50 369.34 8.75 o -3 3 2 2665.77 2502.20 34.30 o -2 3 2 26.06 7.16 8.07 < -1 3 2 1033.04 1026.65 21.03 o 0 3 2 2294.33 2231.60 32.25 o 1 3 2 555.91 528.26 14.59 o 2 3 2 2902.51 2920.68 43.40 o 3 3 2 7164.27 6874.84 64.78 o 4 3 2 0.70 2.54 4.96 < 5 3 2 1023.76 1118.18 21.18 o 6 3 2 190.44 190.04 10.08 o 7 3 2 85.15 96.77 6.50 o -7 4 2 79.20 78.98 7.65 o -6 4 2 54.06 51.34 8.39 o -5 4 2 0.81 3.52 5.03 < -4 4 2 780.26 744.75 12.35 o -3 4 2 485.22 497.70 12.72 o -2 4 2 847.11 822.78 29.60 o -1 4 2 1734.56 1716.75 35.70 o 0 4 2 1057.88 997.65 24.75 o 1 4 2 1998.36 1941.65 30.72 o 2 4 2 946.78 892.98 19.94 o 3 4 2 273.08 266.98 8.75 o 4 4 2 1234.88 1244.14 22.05 o 5 4 2 77.77 81.40 8.04 o 6 4 2 44.67 48.27 6.11 o 7 4 2 111.85 113.57 9.03 o -7 5 2 143.41 119.34 8.27 o -6 5 2 226.26 243.36 17.01 o -5 5 2 1209.83 1211.02 22.05 o -4 5 2 197.80 188.51 7.72 o -3 5 2 4610.17 4866.23 38.04 o -2 5 2 5296.85 5340.94 64.59 o -1 5 2 2504.41 2688.50 49.58 o 0 5 2 7331.25 7071.30 77.56 o 1 5 2 1046.80 1046.10 22.57 o 2 5 2 1311.42 1250.98 25.48 o 3 5 2 2181.57 1973.04 22.35 o 4 5 2 1.93 -3.23 5.08 < 5 5 2 444.46 463.16 14.58 o 6 5 2 364.78 383.63 12.53 o 7 5 2 1.74 -0.37 3.60 < -7 6 2 20.94 9.06 4.52 < -6 6 2 1.17 4.48 5.56 < -5 6 2 52.15 40.45 7.95 o -4 6 2 0.19 4.05 3.93 < -3 6 2 13.10 11.45 4.14 < -2 6 2 402.08 476.09 18.28 o -1 6 2 129.53 109.34 9.70 o 0 6 2 1129.09 1237.22 30.27 o 1 6 2 284.21 269.28 12.07 o 2 6 2 214.91 239.41 9.61 o 3 6 2 0.09 -1.96 3.85 < 4 6 2 79.44 62.16 6.04 o 5 6 2 37.33 36.72 5.47 o 6 6 2 25.76 24.00 5.64 o -6 7 2 691.62 708.65 19.02 o -5 7 2 785.99 824.24 18.64 o -4 7 2 130.86 119.11 8.21 o -3 7 2 1899.35 1945.55 27.90 o -2 7 2 5422.10 5543.52 46.19 o -1 7 2 53.33 55.64 4.39 o 0 7 2 5951.28 5977.72 35.81 o 1 7 2 2172.28 2233.11 23.85 o 2 7 2 1299.54 1286.89 22.84 o 3 7 2 2236.47 2342.93 25.87 o 4 7 2 0.33 -0.07 5.53 < 5 7 2 631.95 664.98 21.84 o 6 7 2 197.95 198.52 14.68 o -6 8 2 56.45 35.61 4.98 o -5 8 2 146.61 149.97 9.39 o -4 8 2 432.47 460.65 12.69 o -3 8 2 311.34 299.03 11.98 o -2 8 2 157.68 150.33 8.72 o -1 8 2 89.55 95.59 5.98 o 0 8 2 234.37 240.93 7.92 o 1 8 2 401.03 386.12 11.91 o 2 8 2 317.08 305.13 11.66 o 3 8 2 659.07 665.96 15.51 o 4 8 2 724.50 691.17 17.16 o 5 8 2 115.62 112.09 11.21 o 6 8 2 176.67 128.43 10.49 o -5 9 2 939.26 904.22 18.11 o -4 9 2 3.81 9.83 5.13 < -3 9 2 240.19 269.80 11.59 o -2 9 2 715.08 705.22 19.65 o -1 9 2 160.46 183.06 9.49 o 0 9 2 2577.45 2599.55 27.57 o 1 9 2 147.64 148.71 8.80 o 2 9 2 842.32 844.88 16.19 o 3 9 2 2306.09 2365.63 26.02 o 4 9 2 7.34 13.84 5.31 < 5 9 2 251.64 250.17 11.43 o -5 10 2 0.35 -9.10 5.72 < -4 10 2 716.17 726.21 15.79 o -3 10 2 18.08 20.22 5.70 o -2 10 2 87.48 95.79 8.75 o -1 10 2 757.18 764.23 17.22 o 0 10 2 775.70 798.46 20.72 o 1 10 2 1340.18 1474.47 31.95 o 2 10 2 2020.22 2083.71 28.97 o 3 10 2 140.91 120.57 7.38 o 4 10 2 513.21 557.73 14.44 o 5 10 2 7.37 14.01 5.08 < -4 11 2 2.29 -2.18 4.26 < -3 11 2 1062.70 1077.48 18.61 o -2 11 2 264.46 270.66 13.71 o -1 11 2 10.80 9.23 8.23 < 0 11 2 454.43 454.65 17.91 o 1 11 2 711.90 738.17 22.91 o 2 11 2 41.71 37.80 5.50 o 3 11 2 2.79 1.61 4.98 < 4 11 2 101.33 117.75 9.19 o -3 12 2 342.58 295.00 12.92 o -2 12 2 410.41 451.33 15.52 o -1 12 2 836.67 867.14 23.37 o 0 12 2 216.44 199.28 13.93 o 1 12 2 336.99 303.42 14.73 o 2 12 2 13.59 9.03 5.24 < 3 12 2 45.81 32.67 6.64 o -2 13 2 27.39 23.56 10.73 < -1 13 2 4.54 2.21 11.32 < 0 13 2 73.52 67.25 14.53 o 1 13 2 107.13 86.83 10.32 o 2 13 2 8.48 7.04 8.94 < -7 1 3 525.64 548.96 14.56 o -6 1 3 74.65 87.15 6.27 o -5 1 3 1771.12 1730.84 20.66 o -4 1 3 1604.24 1474.94 20.46 o -3 1 3 0.42 0.51 7.08 < -2 1 3 5891.69 5907.28 92.12 o -1 1 3 17063.80 17370.90 108.56 o 0 1 3 219.39 183.39 10.10 o 1 1 3 26928.20 25559.50 136.58 o 2 1 3 1871.26 1887.37 57.13 o 3 1 3 6168.12 6059.07 69.38 o 4 1 3 1574.96 1620.90 24.49 o 5 1 3 0.32 7.19 5.76 < 6 1 3 812.16 906.66 17.05 o 7 1 3 324.08 359.40 13.09 o -7 2 3 2.30 5.64 4.40 < -6 2 3 98.77 92.56 7.60 o -5 2 3 642.63 658.21 13.09 o -4 2 3 5.14 2.82 3.24 < -3 2 3 1502.96 1537.06 28.45 o -2 2 3 1453.04 1490.27 51.21 o -1 2 3 6231.99 6171.99 60.34 o 0 2 3 15824.20 15327.10 100.35 o 1 2 3 15035.30 15159.90 100.07 o 2 2 3 138.24 125.51 11.05 o 3 2 3 1.80 -2.69 5.92 < 4 2 3 0.61 3.01 3.95 < 5 2 3 226.79 237.27 10.54 o 6 2 3 49.18 43.09 5.13 o 7 2 3 30.31 28.90 4.90 o -7 3 3 616.61 575.93 18.63 o -6 3 3 334.38 361.23 16.90 o -5 3 3 624.91 607.41 14.82 o -4 3 3 3422.29 3378.21 28.55 o -3 3 3 1.16 3.56 5.20 < -2 3 3 5422.73 5339.77 77.78 o -1 3 3 4.61 4.21 11.82 < 0 3 3 1904.57 1831.62 31.92 o 1 3 3 5092.61 4909.01 49.68 o 2 3 3 1.75 -0.05 8.59 < 3 3 3 517.82 419.94 13.40 o 4 3 3 1993.25 2011.99 28.48 o 5 3 3 2.62 -1.24 4.31 < 6 3 3 714.23 798.21 18.82 o 7 3 3 106.76 98.13 6.19 o -7 4 3 5.43 7.82 4.46 < -6 4 3 2816.20 2980.21 55.90 o -5 4 3 432.34 425.55 12.18 o -4 4 3 1079.28 1010.89 16.69 o -3 4 3 4043.67 4251.15 35.79 o -2 4 3 900.51 961.84 27.46 o -1 4 3 4792.41 4909.57 78.40 o 0 4 3 1985.66 1894.73 35.89 o 1 4 3 37.23 43.51 8.02 o 2 4 3 7152.54 7298.25 57.26 o 3 4 3 22.65 26.40 4.95 o 4 4 3 437.24 447.81 13.94 o 5 4 3 245.43 253.80 10.77 o 6 4 3 90.54 92.31 7.23 o 7 4 3 165.04 170.15 10.96 o -7 5 3 12.92 10.13 4.07 < -6 5 3 0.17 -4.64 6.45 < -5 5 3 249.84 251.77 13.78 o -4 5 3 254.73 234.92 8.38 o -3 5 3 98.73 90.51 6.01 o -2 5 3 720.47 676.27 25.24 o -1 5 3 8577.89 9295.93 123.08 o 0 5 3 1090.84 1071.69 26.67 o 1 5 3 243.86 233.45 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