#------------------------------------------------------------------------------ #$Date: 2012-09-11 12:26:43 +0300 (Tue, 11 Sep 2012) $ #$Revision: 66590 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/59/2235984.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2235984_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Quah, Ching Kheng' 'Sarojini, B. K.' 'Mohan, B. J.' 'Narayana, B.' _publ_section_title ; 1-(5-Chloro-6-fluoro-1,3-benzothiazol-2-yl)hydrazine ; _journal_coeditor_code SJ5255 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2459 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.552 _cell_angle_gamma 90.000 _cell_length_a 11.1287 _cell_length_b 5.6641 _cell_length_c 13.3419 _exptl_crystal_F_000 440.00 _reflns_d_resolution_high 0.6586 _[local]_cod_data_source_file sj5255Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_bks100_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 168.46 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 18.89 19.89 0.83 o 2 0 0 51.57 82.04 1.36 o 3 0 0 25.11 27.42 0.92 o 4 0 0 628.95 649.40 7.81 o 5 0 0 5822.42 5604.48 51.22 o 6 0 0 72.68 72.85 1.86 o 7 0 0 1007.83 951.22 8.89 o 8 0 0 28.91 43.40 1.49 o 9 0 0 63.99 59.30 1.79 o 10 0 0 18.40 21.04 3.75 o 11 0 0 79.64 85.42 2.67 o 12 0 0 469.09 463.10 8.40 o 13 0 0 132.93 124.87 6.65 o 14 0 0 488.57 520.02 15.09 o 15 0 0 62.65 60.57 5.68 o 1 1 0 625.48 660.68 7.59 o 2 1 0 2075.77 2177.58 52.77 o 3 1 0 2.54 3.06 0.62 o 4 1 0 130.97 131.59 1.72 o 5 1 0 133.23 147.26 1.61 o 6 1 0 3.50 3.44 0.36 o 7 1 0 2113.88 2154.42 13.83 o 8 1 0 439.72 450.62 3.69 o 9 1 0 17.13 16.64 0.94 o 10 1 0 536.75 542.22 6.26 o 11 1 0 78.39 73.43 2.09 o 12 1 0 68.64 59.91 2.24 o 13 1 0 16.50 16.82 1.54 o 14 1 0 204.41 198.53 4.17 o 15 1 0 193.95 198.34 7.91 o 0 2 0 626.86 673.50 7.88 o 1 2 0 1058.54 1113.87 10.86 o 2 2 0 1311.08 1382.35 29.66 o 3 2 0 668.72 642.80 28.90 o 4 2 0 568.21 525.77 4.58 o 5 2 0 1419.03 1514.18 13.70 o 6 2 0 7.08 9.80 0.53 o 7 2 0 32.99 41.77 2.14 o 8 2 0 596.21 575.45 5.61 o 9 2 0 1009.75 1013.49 9.07 o 10 2 0 38.33 36.63 1.40 o 11 2 0 7.32 7.59 0.98 o 12 2 0 604.08 591.34 8.21 o 13 2 0 55.73 57.55 2.78 o 14 2 0 85.58 88.12 3.45 o 15 2 0 8.08 7.94 1.92 o 1 3 0 391.00 410.03 3.86 o 2 3 0 6774.87 6734.99 47.36 o 3 3 0 1759.71 1744.11 14.01 o 4 3 0 59.21 66.56 1.64 o 6 3 0 192.28 172.79 3.55 o 7 3 0 525.93 517.98 6.67 o 8 3 0 0.13 0.68 0.65 o 9 3 0 124.36 115.22 2.83 o 10 3 0 817.77 837.48 10.39 o 11 3 0 23.97 22.99 1.66 o 12 3 0 539.48 511.76 8.84 o 13 3 0 0.00 -0.37 1.01 o 14 3 0 137.02 150.70 5.27 o 15 3 0 345.44 358.99 11.68 o 0 4 0 54.01 55.23 3.24 o 1 4 0 220.11 237.78 5.33 o 2 4 0 298.05 265.15 3.39 o 3 4 0 28.05 23.00 0.97 o 4 4 0 1.23 1.12 0.55 o 5 4 0 512.89 490.44 8.04 o 6 4 0 237.04 229.28 4.56 o 7 4 0 34.45 42.76 2.01 o 8 4 0 13.33 14.81 1.47 o 9 4 0 23.40 23.92 1.58 o 10 4 0 48.54 48.83 2.28 o 11 4 0 87.17 92.89 2.92 o 12 4 0 24.22 21.31 1.96 o 13 4 0 78.87 78.64 4.18 o 14 4 0 8.24 4.74 1.92 o 1 5 0 328.83 317.05 4.86 o 2 5 0 2033.60 1948.60 19.88 o 3 5 0 1454.32 1444.17 24.68 o 4 5 0 83.01 84.96 3.71 o 5 5 0 75.55 78.56 3.69 o 6 5 0 89.79 95.20 4.18 o 7 5 0 617.10 631.69 9.58 o 8 5 0 21.33 19.22 1.63 o 9 5 0 0.55 0.67 0.89 o 10 5 0 73.14 68.20 2.93 o 11 5 0 98.83 104.61 3.14 o 12 5 0 26.49 28.98 3.65 o 13 5 0 62.28 70.44 3.68 o 0 6 0 22.46 31.79 2.62 o 1 6 0 96.07 89.89 4.24 o 2 6 0 103.19 107.96 3.41 o 3 6 0 100.03 108.76 5.88 o 4 6 0 440.30 445.99 10.16 o 5 6 0 141.17 136.67 11.09 o 6 6 0 48.09 49.54 3.82 o 7 6 0 60.69 59.51 6.55 o 8 6 0 194.37 181.66 6.69 o 9 6 0 315.24 308.40 9.20 o 10 6 0 188.73 198.40 7.38 o 11 6 0 17.72 17.70 7.07 o 1 7 0 37.16 34.32 3.07 o 2 7 0 27.81 26.99 2.87 o 3 7 0 37.97 43.41 3.63 o 4 7 0 304.22 301.45 9.49 o 5 7 0 13.52 12.21 2.28 o 6 7 0 1.09 2.07 1.68 o 7 7 0 0.12 -1.00 1.62 o 8 7 0 36.85 35.84 3.80 o 9 7 0 46.38 44.72 6.00 o 1 8 0 23.51 25.89 4.36 o 2 8 0 13.47 9.71 3.20 o 3 8 0 65.89 67.97 9.58 o 4 8 0 8.74 8.97 2.22 o 5 8 0 319.00 338.10 9.90 o -16 1 1 9.84 9.42 2.46 o -15 1 1 454.62 447.43 9.64 o -14 1 1 10.79 11.87 1.47 o -13 1 1 104.72 104.49 2.95 o -12 1 1 1005.08 997.10 10.40 o -11 1 1 25.85 26.71 1.43 o -10 1 1 560.21 543.88 6.22 o -9 1 1 89.00 85.44 1.70 o -8 1 1 387.72 333.17 3.28 o -7 1 1 772.44 725.64 6.14 o -6 1 1 95.38 105.10 1.41 o -5 1 1 98.34 139.29 1.56 o -4 1 1 544.04 502.63 6.44 o -3 1 1 3908.54 3788.81 31.24 o -2 1 1 246.30 245.50 3.13 o -1 1 1 46.99 51.21 1.44 o 0 1 1 5589.64 5891.05 107.80 o 2 1 1 20049.73 20917.38 228.90 o 3 1 1 1886.25 1981.43 14.04 o 4 1 1 95.04 125.98 1.21 o 5 1 1 1213.51 1191.53 8.45 o 6 1 1 649.90 631.32 4.59 o 7 1 1 2288.81 2350.26 16.67 o 8 1 1 155.12 162.14 2.00 o 9 1 1 269.69 254.21 3.32 o 10 1 1 645.47 640.18 7.12 o 11 1 1 421.61 419.89 6.05 o 12 1 1 7.31 7.46 1.39 o 13 1 1 11.84 9.70 1.35 o 14 1 1 460.08 462.73 7.58 o 15 1 1 175.02 169.70 6.98 o -15 2 1 147.11 143.62 5.12 o -14 2 1 181.15 175.96 4.71 o -13 2 1 425.49 428.31 8.98 o -12 2 1 95.76 92.55 2.36 o -11 2 1 13.11 14.02 1.14 o -10 2 1 217.70 224.07 3.18 o -9 2 1 571.14 551.07 5.59 o -8 2 1 2116.64 2129.86 17.03 o -7 2 1 31.02 31.08 0.99 o -6 2 1 945.33 971.84 7.63 o -5 2 1 4488.03 4563.73 40.04 o -4 2 1 498.64 519.71 7.19 o -3 2 1 401.86 456.11 5.25 o -2 2 1 720.87 788.72 10.57 o -1 2 1 3499.94 3625.17 39.21 o 0 2 1 5829.91 6050.17 78.08 o 1 2 1 423.89 399.43 17.03 o 2 2 1 836.53 814.39 10.93 o 3 2 1 363.39 344.43 4.35 o 4 2 1 138.52 120.80 1.84 o 5 2 1 14.30 6.88 0.50 o 6 2 1 5.06 5.70 0.62 o 7 2 1 585.84 571.95 5.41 o 8 2 1 15.52 12.89 0.83 o 9 2 1 180.85 179.71 2.76 o 10 2 1 21.97 23.44 1.18 o 11 2 1 97.65 98.65 2.80 o 12 2 1 254.36 258.43 4.89 o 13 2 1 1.19 1.11 1.19 o 14 2 1 82.32 87.91 3.48 o 15 2 1 13.14 12.07 2.13 o -15 3 1 1.03 -1.59 1.59 o -14 3 1 0.57 0.54 1.32 o -13 3 1 14.95 16.09 1.62 o -12 3 1 80.04 75.57 2.66 o -11 3 1 100.46 99.73 2.89 o -10 3 1 462.28 447.12 6.59 o -9 3 1 5.48 5.29 0.92 o -8 3 1 76.68 68.26 2.09 o -7 3 1 516.54 493.54 6.39 o -6 3 1 1141.47 1108.18 16.35 o -5 3 1 0.55 2.07 0.57 o -4 3 1 34.70 38.93 1.20 o -3 3 1 1323.69 1428.48 52.58 o -2 3 1 1336.54 1363.99 31.75 o -1 3 1 165.91 190.12 2.50 o 0 3 1 427.01 386.64 4.16 o 1 3 1 110.82 119.25 2.88 o 2 3 1 17.12 10.39 0.71 o 3 3 1 194.66 203.56 2.85 o 4 3 1 11.15 13.56 0.67 o 5 3 1 0.63 0.13 0.35 o 6 3 1 14.41 18.07 1.26 o 7 3 1 65.96 70.29 2.49 o 8 3 1 883.29 860.13 10.20 o 9 3 1 52.24 46.15 1.88 o 10 3 1 157.31 162.56 3.62 o 11 3 1 0.83 0.67 0.80 o 12 3 1 15.23 17.84 1.64 o 13 3 1 99.13 100.09 3.19 o 14 3 1 89.54 95.28 4.38 o -14 4 1 106.40 111.17 6.83 o -13 4 1 175.62 185.94 5.35 o -12 4 1 125.45 129.08 3.54 o -11 4 1 29.75 34.77 2.05 o -10 4 1 1724.16 1721.85 29.56 o -9 4 1 18.88 17.77 1.38 o -8 4 1 0.14 1.30 0.78 o -7 4 1 9.23 7.81 1.38 o -6 4 1 161.67 156.05 3.47 o -5 4 1 486.05 475.72 11.55 o -4 4 1 0.08 0.22 0.50 o -3 4 1 368.37 379.60 5.28 o -2 4 1 561.23 579.78 5.60 o -1 4 1 630.84 639.56 8.15 o 0 4 1 2412.94 2333.38 20.44 o 1 4 1 242.65 230.11 3.27 o 2 4 1 270.62 254.78 2.97 o 3 4 1 766.08 793.92 7.21 o 4 4 1 3754.17 3772.57 36.68 o 5 4 1 3265.07 3245.42 37.07 o 6 4 1 28.98 26.24 1.62 o 7 4 1 205.23 196.89 4.48 o 8 4 1 60.98 66.46 4.68 o 9 4 1 668.66 681.34 11.04 o 10 4 1 0.01 0.76 0.80 o 11 4 1 24.78 25.83 1.86 o 12 4 1 912.09 922.98 12.02 o 13 4 1 33.17 35.14 3.79 o -13 5 1 1.34 2.08 1.51 o -12 5 1 92.32 91.23 3.74 o -11 5 1 26.50 31.58 2.55 o -10 5 1 123.02 112.73 5.15 o -9 5 1 71.44 73.16 4.09 o -8 5 1 78.20 86.43 4.31 o -7 5 1 797.17 803.69 15.24 o -6 5 1 137.07 138.92 5.06 o -5 5 1 4.41 5.00 1.38 o -4 5 1 232.79 234.36 6.35 o -3 5 1 1692.49 1663.06 17.34 o -2 5 1 841.37 864.12 8.79 o -1 5 1 17.63 24.21 1.30 o 0 5 1 1.91 1.26 0.67 o 1 5 1 30.98 28.18 1.42 o 2 5 1 61.20 61.95 2.66 o 3 5 1 4.86 3.79 1.28 o 4 5 1 211.70 207.66 6.00 o 5 5 1 114.06 114.18 4.77 o 6 5 1 1.80 3.25 0.80 o 7 5 1 47.34 44.23 2.57 o 8 5 1 21.08 22.89 1.82 o 9 5 1 458.55 464.15 8.92 o 10 5 1 6.72 5.40 1.31 o 11 5 1 10.49 10.88 1.79 o 12 5 1 201.08 206.37 5.62 o -11 6 1 174.38 184.04 7.33 o -10 6 1 15.93 19.66 3.32 o -9 6 1 155.50 164.04 6.46 o -8 6 1 218.74 223.94 7.44 o -7 6 1 178.60 181.00 6.45 o -6 6 1 0.78 2.73 1.62 o -5 6 1 252.92 254.22 10.58 o -4 6 1 81.77 75.50 3.87 o -3 6 1 2.72 3.88 1.51 o -2 6 1 463.18 466.89 7.99 o -1 6 1 314.19 310.90 5.21 o 0 6 1 348.82 361.45 5.73 o 1 6 1 167.40 164.22 5.67 o 2 6 1 15.67 17.36 2.16 o 3 6 1 141.52 137.23 12.38 o 4 6 1 188.91 180.81 6.36 o 5 6 1 0.01 1.87 1.35 o 6 6 1 214.80 201.78 6.76 o 7 6 1 128.07 121.00 5.32 o 8 6 1 0.42 1.23 1.60 o 9 6 1 93.38 102.61 5.26 o 10 6 1 13.11 14.72 2.67 o 11 6 1 0.12 -0.23 2.77 o -9 7 1 0.98 1.23 1.88 o -8 7 1 277.92 269.50 8.78 o -7 7 1 364.49 368.75 10.24 o -6 7 1 30.88 26.58 4.05 o -5 7 1 179.00 167.58 6.33 o -4 7 1 7.42 9.61 2.14 o -3 7 1 267.50 282.02 11.21 o -2 7 1 245.41 254.39 7.35 o -1 7 1 14.11 12.97 2.22 o 0 7 1 403.40 408.38 7.72 o 1 7 1 0.48 0.60 1.36 o 2 7 1 934.86 924.10 17.10 o 3 7 1 58.34 67.73 4.87 o 4 7 1 7.99 12.09 2.26 o 5 7 1 124.71 134.35 5.70 o 6 7 1 20.33 20.65 2.92 o 7 7 1 113.69 116.50 5.67 o 8 7 1 1.53 5.44 2.16 o -6 8 1 86.41 99.29 13.20 o -5 8 1 104.80 102.74 6.60 o -4 8 1 3.67 3.47 1.86 o -3 8 1 28.76 28.56 4.62 o -2 8 1 65.11 61.55 6.38 o -1 8 1 56.17 51.50 5.75 o 0 8 1 5.91 2.07 2.71 o 1 8 1 60.38 46.72 5.58 o 2 8 1 12.00 10.21 2.25 o 3 8 1 4.93 5.36 1.96 o 4 8 1 18.92 19.28 4.01 o 5 8 1 18.98 14.59 2.77 o -16 0 2 66.38 63.52 5.61 o -15 0 2 448.36 426.43 13.46 o -14 0 2 20.21 25.60 3.91 o -13 0 2 768.54 776.60 19.24 o -12 0 2 43.91 37.82 2.25 o -11 0 2 73.77 76.13 2.16 o -10 0 2 2172.96 2105.97 21.04 o -9 0 2 3.55 3.80 0.73 o -8 0 2 1231.07 1271.47 11.66 o -7 0 2 6.10 8.15 0.74 o -6 0 2 1666.61 1579.08 13.75 o -5 0 2 9942.44 9856.48 105.57 o -4 0 2 23.71 36.30 2.23 o -3 0 2 3199.99 3216.67 29.46 o -2 0 2 1564.45 1567.34 16.38 o -1 0 2 746.60 681.27 12.41 o 1 0 2 367.40 412.68 5.67 o 3 0 2 249.11 297.04 3.43 o 4 0 2 325.56 295.77 3.58 o 5 0 2 317.93 331.78 5.98 o 6 0 2 0.73 1.61 0.35 o 7 0 2 2321.18 2311.90 22.33 o 8 0 2 84.05 79.98 2.03 o 9 0 2 1368.99 1376.13 16.76 o 10 0 2 428.77 436.85 8.39 o 11 0 2 124.93 116.33 3.65 o 12 0 2 700.13 700.06 11.64 o 13 0 2 264.87 261.49 9.76 o 14 0 2 5.57 0.54 2.76 o 15 0 2 85.04 75.78 6.14 o -16 1 2 1.97 0.05 2.11 o -15 1 2 98.67 92.98 3.76 o -14 1 2 147.65 153.08 5.82 o -13 1 2 440.35 450.94 6.60 o -12 1 2 491.76 489.87 6.14 o -11 1 2 55.81 52.54 1.79 o -10 1 2 36.75 35.56 1.28 o -9 1 2 71.92 78.50 1.50 o -8 1 2 210.13 220.94 6.64 o -7 1 2 20.25 24.33 0.82 o -6 1 2 151.01 172.13 2.06 o -5 1 2 6.03 5.24 0.41 o -4 1 2 10.38 4.81 0.63 o -3 1 2 1954.77 1935.13 18.33 o -2 1 2 2.87 0.19 0.28 o -1 1 2 440.61 424.13 8.82 o 0 1 2 1027.30 1011.83 18.86 o 2 1 2 28377.76 29409.53 269.50 o 3 1 2 17.96 17.47 0.55 o 4 1 2 78.25 53.52 0.84 o 5 1 2 10.67 6.85 0.42 o 6 1 2 67.55 74.11 1.15 o 7 1 2 29.64 23.33 0.76 o 8 1 2 32.50 35.24 0.99 o 9 1 2 957.86 951.55 8.43 o 10 1 2 61.24 61.94 2.48 o 11 1 2 56.00 57.47 2.15 o 12 1 2 126.59 119.16 3.07 o 13 1 2 10.76 9.11 1.47 o 14 1 2 20.70 22.48 2.20 o 15 1 2 0.01 -1.34 3.15 o -16 2 2 109.11 109.22 4.53 o -15 2 2 339.59 340.05 8.07 o -14 2 2 49.58 47.80 2.41 o -13 2 2 85.67 90.30 2.44 o -12 2 2 35.98 34.93 1.62 o -11 2 2 124.34 120.80 2.36 o -10 2 2 1404.90 1368.72 11.88 o -9 2 2 24.85 25.88 1.16 o -8 2 2 313.69 309.10 4.09 o -7 2 2 258.03 264.40 2.87 o -6 2 2 24.83 49.23 1.87 o -5 2 2 10.20 19.25 0.78 o -4 2 2 18.78 18.50 0.68 o -3 2 2 325.19 398.51 6.85 o -2 2 2 301.76 296.83 4.34 o -1 2 2 4347.96 4494.95 47.73 o 0 2 2 2965.24 3298.87 42.95 o 1 2 2 0.21 3.50 0.67 o 2 2 2 133.91 135.92 2.60 o 3 2 2 1098.46 1172.58 17.08 o 4 2 2 6875.54 7005.61 52.73 o 5 2 2 90.20 100.64 1.68 o 6 2 2 81.71 73.85 1.54 o 7 2 2 364.38 355.03 3.85 o 8 2 2 103.81 98.69 1.81 o 9 2 2 8.68 10.40 1.03 o 10 2 2 385.29 379.13 5.18 o 11 2 2 364.98 373.69 8.07 o 12 2 2 22.32 28.96 2.63 o 13 2 2 13.95 15.78 2.40 o 14 2 2 12.65 14.79 1.93 o -15 3 2 153.04 154.72 4.69 o -14 3 2 16.26 13.66 1.61 o -13 3 2 357.10 359.54 7.12 o -12 3 2 415.94 427.97 6.78 o -11 3 2 82.66 78.08 2.55 o -10 3 2 7.25 4.78 0.95 o -9 3 2 0.01 1.18 0.68 o -8 3 2 1878.92 1966.98 20.15 o -7 3 2 1057.49 1054.55 11.58 o -6 3 2 409.27 415.82 6.06 o -5 3 2 118.28 112.66 5.97 o -4 3 2 38.68 38.99 4.58 o -3 3 2 3476.68 3536.44 39.25 o -2 3 2 64.97 54.83 1.44 o -1 3 2 166.50 175.87 2.71 o 0 3 2 2808.05 3061.05 33.37 o 1 3 2 1631.14 1731.13 16.95 o 2 3 2 684.03 631.71 7.94 o 3 3 2 40.69 48.06 1.21 o 5 3 2 1276.41 1244.18 14.92 o 6 3 2 635.57 624.08 6.87 o 7 3 2 875.51 856.71 9.01 o 8 3 2 204.09 201.97 4.66 o 9 3 2 306.11 301.80 5.07 o 10 3 2 119.32 125.68 2.83 o 11 3 2 240.95 254.00 4.35 o 12 3 2 38.20 39.01 2.26 o 13 3 2 34.47 37.68 2.61 o 14 3 2 449.31 454.62 10.08 o -14 4 2 0.70 0.13 1.50 o -13 4 2 28.41 28.01 2.42 o -12 4 2 88.55 94.51 3.57 o -11 4 2 3.44 5.81 1.08 o -10 4 2 36.86 33.38 1.94 o -9 4 2 46.67 45.28 2.42 o -8 4 2 5.91 7.97 1.49 o -7 4 2 27.45 21.84 2.27 o -6 4 2 129.33 124.85 10.18 o -5 4 2 21.13 23.45 2.17 o -4 4 2 557.24 525.08 7.75 o -3 4 2 256.85 231.91 3.70 o -2 4 2 27.59 32.71 1.59 o -1 4 2 1.09 0.71 0.90 o 0 4 2 201.80 218.79 4.34 o 1 4 2 153.04 140.12 5.00 o 2 4 2 0.02 0.00 0.36 o 3 4 2 4.26 5.74 0.78 o 4 4 2 2.54 1.36 0.82 o 5 4 2 12.68 14.11 1.67 o 6 4 2 6.51 7.89 0.98 o 7 4 2 124.91 117.77 3.44 o 8 4 2 6.63 8.09 1.32 o 9 4 2 9.61 10.49 1.24 o 10 4 2 11.14 11.42 1.32 o 11 4 2 78.74 77.52 2.78 o 12 4 2 98.37 100.58 4.72 o 13 4 2 50.99 52.50 3.93 o -13 5 2 162.96 165.97 5.17 o -12 5 2 266.46 266.59 6.42 o -11 5 2 482.86 492.37 9.03 o -10 5 2 349.59 358.31 9.62 o -9 5 2 113.25 128.52 8.07 o -8 5 2 478.22 476.45 13.13 o -7 5 2 208.56 193.74 6.24 o -6 5 2 199.19 191.22 5.99 o -5 5 2 274.86 276.88 15.83 o -4 5 2 2.59 1.98 1.40 o -3 5 2 144.37 154.45 4.05 o -2 5 2 17.90 20.47 1.20 o -1 5 2 352.78 348.10 4.05 o 0 5 2 2248.57 2178.75 19.74 o 1 5 2 317.82 280.09 4.07 o 2 5 2 185.59 207.58 3.94 o 3 5 2 155.16 165.50 3.03 o 4 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