#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:43:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181282 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/60/2236021.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236021_Fobs loop_ _publ_author_name 'Liu, Wei' 'Yan, Jun' 'Song, Qin' 'Gou, Xiao-Jun' 'Chen, Feng-Zheng' _publ_section_title ; Trehalose dihydrate from Tremella fuciformis ; _journal_coeditor_code XU5574 _journal_issue 8 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2511 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.6012 _cell_length_b 12.2380 _cell_length_c 17.8839 _exptl_crystal_F_000 808.00 _reflns_d_resolution_high 0.8410 _cod_data_source_file xu5574Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 120409_s6_cfz in P212121 19' _shelx_refln_list_code 4 _shelx_f_calc_maximum 148.04 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5137.95 4985.05 44.84 o 4 0 0 657.71 624.70 30.35 o 6 0 0 316.04 280.15 25.46 o 8 0 0 156.60 165.66 24.09 o 1 1 0 6777.85 6190.66 33.01 o 2 1 0 501.48 530.87 9.92 o 3 1 0 1896.03 1973.25 34.68 o 4 1 0 132.99 134.87 10.25 o 5 1 0 171.59 160.47 12.43 o 6 1 0 8.63 3.72 4.24 o 7 1 0 244.90 196.84 22.78 o 8 1 0 88.01 77.54 11.60 o 9 1 0 5.48 -6.41 9.94 o 0 2 0 2827.70 2684.89 33.41 o 1 2 0 4970.39 4639.16 37.53 o 2 2 0 1061.27 1120.49 17.60 o 3 2 0 7796.10 7695.46 100.77 o 4 2 0 0.61 0.53 3.55 o 5 2 0 29.62 41.35 10.31 o 6 2 0 5.10 2.75 6.51 o 7 2 0 58.89 63.87 15.22 o 8 2 0 353.31 408.20 37.27 o 1 3 0 5135.31 5001.16 43.27 o 2 3 0 2954.15 2952.53 37.83 o 3 3 0 413.86 440.12 23.47 o 4 3 0 652.75 601.16 31.23 o 5 3 0 169.25 195.73 20.13 o 6 3 0 312.93 290.41 26.79 o 7 3 0 22.33 18.16 9.37 o 8 3 0 30.47 16.98 9.45 o 0 4 0 5981.72 5893.65 71.14 o 1 4 0 6827.19 6714.59 79.83 o 2 4 0 2698.20 2893.84 56.90 o 3 4 0 763.31 841.92 33.81 o 4 4 0 1182.53 1128.09 44.54 o 5 4 0 77.69 69.36 12.86 o 6 4 0 466.36 444.26 33.85 o 7 4 0 25.03 29.74 11.08 o 8 4 0 21.71 28.84 10.87 o 1 5 0 751.12 785.02 19.87 o 2 5 0 17889.52 17632.13 167.58 o 3 5 0 29.10 31.11 6.84 o 4 5 0 67.14 69.69 11.92 o 5 5 0 16.76 10.61 7.03 o 6 5 0 18.45 24.44 9.39 o 7 5 0 0.55 -2.95 4.85 o 8 5 0 325.59 366.93 37.05 o 0 6 0 15.77 17.13 5.23 o 1 6 0 5517.92 5609.11 85.74 o 2 6 0 59.27 96.69 12.17 o 3 6 0 136.77 141.77 8.97 o 4 6 0 688.49 661.01 36.13 o 5 6 0 19.56 24.17 9.51 o 6 6 0 57.85 56.25 12.89 o 7 6 0 0.23 -2.58 5.99 o 8 6 0 20.16 41.30 13.78 o 1 7 0 2206.46 2344.59 57.88 o 2 7 0 4.22 18.46 6.42 o 3 7 0 6.00 7.13 5.18 o 4 7 0 0.45 -7.35 6.66 o 5 7 0 389.75 433.84 33.24 o 6 7 0 725.52 666.93 44.24 o 7 7 0 130.41 127.18 21.25 o 0 8 0 402.92 439.76 26.04 o 1 8 0 52.74 46.34 8.89 o 2 8 0 0.20 2.30 3.85 o 3 8 0 319.69 322.65 25.65 o 4 8 0 117.60 101.63 15.70 o 5 8 0 76.79 77.85 14.26 o 6 8 0 132.27 109.20 18.37 o 7 8 0 107.48 103.79 20.49 o 1 9 0 466.45 454.36 25.29 o 2 9 0 411.50 455.58 30.27 o 3 9 0 127.86 107.26 16.28 o 4 9 0 1.29 -2.71 6.04 o 5 9 0 201.71 183.03 23.21 o 6 9 0 0.56 -3.12 6.44 o 7 9 0 68.09 100.13 20.07 o 0 10 0 2657.92 2749.72 74.98 o 1 10 0 4.43 -2.98 3.67 o 2 10 0 13.85 9.33 4.98 o 3 10 0 237.85 250.87 25.12 o 4 10 0 193.08 148.01 20.41 o 5 10 0 18.28 15.58 9.01 o 6 10 0 19.06 20.07 9.72 o 1 11 0 0.00 -1.72 5.21 o 2 11 0 26.55 35.25 7.37 o 3 11 0 40.20 29.44 10.06 o 4 11 0 13.47 10.02 7.36 o 5 11 0 0.03 -11.02 7.49 o 0 12 0 38.38 38.27 10.01 o 1 12 0 363.64 394.58 31.55 o 2 12 0 74.20 61.42 9.43 o 3 12 0 57.31 71.49 15.55 o 4 12 0 0.62 1.25 4.84 o 5 12 0 15.03 16.16 9.60 o 1 13 0 101.64 115.57 17.86 o 2 13 0 11.73 7.33 3.60 o 3 13 0 39.93 32.75 9.89 o 4 13 0 16.76 8.53 7.32 o 0 14 0 23.21 21.26 8.83 o 1 14 0 43.98 42.54 9.17 o 2 14 0 7.42 15.32 5.57 o 1 0 1 4055.23 3866.60 29.05 o 2 0 1 0.87 1.59 1.08 o 3 0 1 864.63 837.52 32.42 o 4 0 1 459.36 470.50 18.65 o 5 0 1 170.83 168.45 12.57 o 6 0 1 476.20 467.85 23.33 o 7 0 1 128.89 98.10 12.17 o 8 0 1 73.93 74.42 11.69 o 9 0 1 11.33 10.51 7.24 o 1 1 1 1949.10 1910.65 11.66 o 2 1 1 1725.33 1755.18 16.57 o 3 1 1 1011.06 1019.44 16.86 o 4 1 1 229.44 212.94 8.96 o 5 1 1 296.99 303.47 12.07 o 6 1 1 128.28 134.72 9.00 o 7 1 1 1129.76 1093.63 27.69 o 8 1 1 22.77 23.88 6.18 o 9 1 1 66.03 81.77 13.23 o 0 2 1 1820.54 1662.62 17.75 o 1 2 1 271.29 283.41 6.94 o 2 2 1 3215.96 3138.52 25.78 o 3 2 1 177.53 191.09 8.63 o 4 2 1 1092.89 1095.86 23.64 o 5 2 1 32.92 33.01 6.64 o 6 2 1 662.29 682.60 23.24 o 7 2 1 22.01 18.52 6.03 o 8 2 1 13.61 9.30 4.81 o 0 3 1 2615.31 2540.36 27.22 o 1 3 1 3628.47 3448.09 51.94 o 2 3 1 3476.43 3519.71 29.39 o 3 3 1 1748.03 1871.63 83.64 o 4 3 1 839.24 908.28 27.09 o 5 3 1 771.98 786.99 28.19 o 6 3 1 11.34 10.47 4.69 o 7 3 1 129.75 130.12 14.20 o 8 3 1 23.28 30.43 8.06 o 0 4 1 385.14 385.64 11.91 o 1 4 1 1998.18 2028.80 20.71 o 2 4 1 1169.82 1183.62 20.35 o 3 4 1 2940.62 3119.51 46.98 o 4 4 1 899.47 890.55 27.72 o 5 4 1 726.60 715.87 59.64 o 6 4 1 48.21 39.60 7.49 o 7 4 1 67.58 66.03 10.42 o 8 4 1 5.34 8.97 18.33 o 0 5 1 2086.81 2107.52 31.72 o 1 5 1 3306.53 3381.09 42.00 o 2 5 1 812.94 759.67 21.61 o 3 5 1 932.53 1052.08 50.01 o 4 5 1 121.27 125.00 11.01 o 5 5 1 1193.48 1264.31 42.62 o 6 5 1 541.97 534.16 26.72 o 7 5 1 85.75 88.29 12.28 o 8 5 1 17.25 26.56 8.66 o 0 6 1 22.00 19.52 6.77 o 1 6 1 716.18 697.97 29.66 o 2 6 1 2360.31 2373.79 41.18 o 3 6 1 91.98 104.67 5.17 o 4 6 1 132.98 127.28 11.32 o 5 6 1 1968.33 1873.07 47.28 o 6 6 1 596.70 594.94 28.81 o 7 6 1 166.45 183.28 17.44 o 8 6 1 134.95 135.81 16.56 o 0 7 1 443.90 416.81 16.63 o 1 7 1 139.40 129.37 10.99 o 2 7 1 605.48 620.83 22.12 o 3 7 1 37.91 36.93 3.83 o 4 7 1 148.02 130.39 18.19 o 5 7 1 82.63 73.87 15.34 o 6 7 1 59.00 67.65 10.31 o 7 7 1 102.29 140.95 29.68 o 0 8 1 773.03 773.66 24.46 o 1 8 1 22.04 19.98 3.62 o 2 8 1 742.78 768.58 26.21 o 3 8 1 178.36 195.66 14.35 o 4 8 1 357.91 353.44 20.38 o 5 8 1 245.76 237.70 17.90 o 6 8 1 40.25 52.59 9.33 o 7 8 1 10.71 2.35 4.03 o 0 9 1 102.61 104.47 9.91 o 1 9 1 0.98 -2.59 2.22 o 2 9 1 248.49 250.16 16.05 o 3 9 1 14.35 6.57 10.93 o 4 9 1 19.76 12.30 4.06 o 5 9 1 21.84 59.43 9.64 o 6 9 1 63.04 42.40 11.82 o 7 9 1 92.58 126.73 15.85 o 0 10 1 1006.99 942.46 75.80 o 1 10 1 815.04 845.69 27.19 o 2 10 1 54.87 56.11 8.44 o 3 10 1 641.00 637.71 28.02 o 4 10 1 177.44 141.33 14.00 o 5 10 1 49.65 46.64 11.83 o 6 10 1 52.98 61.18 14.73 o 0 11 1 620.40 654.55 48.90 o 1 11 1 26.40 25.05 4.88 o 2 11 1 108.63 110.21 8.40 o 3 11 1 66.31 61.33 9.61 o 4 11 1 39.31 40.98 8.17 o 5 11 1 30.90 19.54 12.95 o 0 12 1 336.17 329.06 20.32 o 1 12 1 333.32 333.70 20.55 o 2 12 1 117.69 123.60 9.25 o 3 12 1 58.54 70.02 10.64 o 4 12 1 53.62 43.18 8.72 o 5 12 1 13.59 26.58 7.54 o 0 13 1 268.46 266.26 19.25 o 1 13 1 98.03 89.33 16.79 o 2 13 1 4.85 7.19 3.12 o 3 13 1 71.28 71.80 7.65 o 4 13 1 85.02 61.41 10.95 o 0 14 1 205.51 255.12 19.77 o 1 14 1 21.36 33.61 6.22 o 2 14 1 16.41 13.93 5.29 o 1 0 2 3824.13 3726.11 23.62 o 2 0 2 1868.55 1793.42 18.30 o 3 0 2 225.74 261.13 12.00 o 4 0 2 868.75 856.76 25.20 o 5 0 2 46.13 39.72 6.77 o 6 0 2 25.26 20.02 5.77 o 7 0 2 319.85 297.34 26.96 o 8 0 2 431.47 396.81 25.66 o 1 1 2 4147.04 3927.87 14.72 o 2 1 2 4605.43 4543.31 20.62 o 3 1 2 698.54 715.44 16.28 o 4 1 2 121.93 125.44 6.94 o 5 1 2 125.44 128.43 7.94 o 6 1 2 336.08 333.29 14.06 o 7 1 2 159.94 153.53 14.89 o 8 1 2 218.55 207.08 20.70 o 0 2 2 4549.20 4220.43 29.28 o 1 2 2 3694.92 3540.39 19.58 o 2 2 2 1089.60 1116.04 12.19 o 3 2 2 601.32 647.53 10.72 o 4 2 2 1236.46 1261.23 31.30 o 5 2 2 423.45 422.84 18.02 o 6 2 2 38.49 33.66 5.69 o 7 2 2 83.23 79.25 8.98 o 8 2 2 66.23 68.77 10.84 o 0 3 2 61.73 60.27 4.07 o 1 3 2 1969.44 1887.58 20.14 o 2 3 2 500.79 506.49 7.34 o 3 3 2 932.94 926.15 13.99 o 4 3 2 112.80 121.66 5.46 o 5 3 2 259.83 259.72 8.72 o 6 3 2 1133.42 1196.39 38.48 o 7 3 2 162.47 159.23 15.45 o 8 3 2 98.90 117.27 14.83 o 0 4 2 1090.71 1017.22 19.22 o 1 4 2 480.99 500.62 10.07 o 2 4 2 1431.19 1454.67 16.86 o 3 4 2 273.04 306.07 14.54 o 4 4 2 235.12 254.02 14.86 o 5 4 2 663.43 709.13 27.41 o 6 4 2 575.24 529.11 26.09 o 7 4 2 73.79 60.76 11.13 o 8 4 2 98.35 107.61 14.08 o 0 5 2 1214.58 1209.90 23.71 o 1 5 2 2371.41 2329.96 28.60 o 2 5 2 329.03 342.38 14.57 o 3 5 2 754.77 739.61 32.08 o 4 5 2 73.49 83.38 9.12 o 5 5 2 113.01 112.52 19.40 o 6 5 2 1159.72 1201.65 39.87 o 7 5 2 34.75 45.84 9.21 o 8 5 2 44.92 56.36 10.67 o 0 6 2 208.17 216.23 11.87 o 1 6 2 18.96 19.66 6.40 o 2 6 2 2633.08 2748.29 44.32 o 3 6 2 588.53 617.27 13.52 o 4 6 2 705.83 734.63 26.94 o 5 6 2 384.79 357.65 20.66 o 6 6 2 511.64 547.83 27.75 o 7 6 2 15.50 10.96 5.47 o 8 6 2 63.55 76.01 12.62 o 0 7 2 1271.14 1293.21 29.32 o 1 7 2 379.32 370.87 23.83 o 2 7 2 1339.91 1473.46 34.14 o 3 7 2 519.74 518.44 13.87 o 4 7 2 116.62 108.34 10.90 o 5 7 2 281.98 302.76 19.54 o 6 7 2 79.37 71.95 10.86 o 7 7 2 48.97 50.59 12.91 o 0 8 2 0.95 -0.42 2.55 o 1 8 2 569.66 560.71 20.96 o 2 8 2 340.96 371.95 18.24 o 3 8 2 8.34 9.46 2.72 o 4 8 2 263.86 247.55 24.79 o 5 8 2 377.26 371.79 22.41 o 6 8 2 90.75 112.75 13.54 o 7 8 2 5.79 21.39 7.19 o 0 9 2 78.22 75.27 8.41 o 1 9 2 129.47 138.75 9.33 o 2 9 2 157.62 154.45 29.08 o 3 9 2 286.94 318.28 19.01 o 4 9 2 97.19 97.68 11.30 o 5 9 2 56.73 58.08 9.77 o 6 9 2 4.87 4.04 4.58 o 7 9 2 42.59 28.61 10.91 o 0 10 2 1718.56 1708.78 65.92 o 1 10 2 203.33 230.81 12.74 o 2 10 2 55.89 59.57 8.37 o 3 10 2 4.59 21.27 17.79 o 4 10 2 28.64 18.07 5.48 o 5 10 2 19.53 13.41 5.79 o 6 10 2 23.52 40.54 9.03 o 0 11 2 166.75 167.50 13.74 o 1 11 2 946.75 918.63 26.67 o 2 11 2 471.97 467.15 16.75 o 3 11 2 19.72 21.00 5.72 o 4 11 2 108.58 108.78 13.24 o 5 11 2 151.33 170.98 17.06 o 0 12 2 86.27 87.61 18.82 o 1 12 2 7.71 11.76 4.10 o 2 12 2 156.58 168.06 10.71 o 3 12 2 161.33 175.83 17.75 o 4 12 2 210.73 217.79 18.89 o 5 12 2 63.25 62.97 10.78 o 0 13 2 0.24 -0.11 3.95 o 1 13 2 30.22 34.00 6.02 o 2 13 2 6.41 9.48 3.23 o 3 13 2 9.77 7.84 5.47 o 0 14 2 11.33 5.82 4.27 o 1 14 2 23.55 26.07 5.37 o 2 14 2 14.86 12.89 4.06 o 1 0 3 4316.14 3931.73 23.68 o 2 0 3 3928.82 3758.15 27.56 o 3 0 3 1389.08 1461.62 29.68 o 4 0 3 1677.89 1779.78 71.31 o 5 0 3 52.02 50.12 8.84 o 6 0 3 329.85 343.35 20.32 o 7 0 3 15.01 17.78 5.83 o 8 0 3 2.03 2.72 9.31 o 0 1 3 7402.58 6286.46 34.93 o 1 1 3 1662.10 1609.21 9.35 o 2 1 3 1032.90 1027.92 9.61 o 3 1 3 4.97 5.01 2.47 o 4 1 3 804.77 767.05 19.55 o 5 1 3 285.35 303.72 13.93 o 6 1 3 306.80 305.31 20.50 o 7 1 3 227.23 202.78 14.12 o 8 1 3 82.30 82.44 10.23 o 0 2 3 1760.96 1680.97 31.42 o 1 2 3 21916.19 18518.72 109.78 o 2 2 3 324.66 325.43 5.19 o 3 2 3 4156.38 4055.55 30.43 o 4 2 3 150.04 153.59 6.52 o 5 2 3 578.29 574.83 13.86 o 6 2 3 29.89 28.56 5.42 o 7 2 3 352.31 335.49 17.95 o 8 2 3 310.28 310.70 23.13 o 0 3 3 137.31 130.41 7.19 o 1 3 3 980.05 981.05 12.89 o 2 3 3 1202.05 1224.37 16.57 o 3 3 3 1805.74 1925.74 23.25 o 4 3 3 524.79 518.10 12.67 o 5 3 3 971.44 979.33 31.58 o 6 3 3 640.48 638.21 28.21 o 7 3 3 38.97 29.31 10.33 o 8 3 3 10.09 10.16 6.12 o 0 4 3 836.64 800.86 27.22 o 1 4 3 809.67 795.05 12.56 o 2 4 3 596.94 642.74 12.41 o 3 4 3 115.51 104.09 8.73 o 4 4 3 263.00 242.05 14.54 o 5 4 3 163.38 158.96 15.72 o 6 4 3 794.59 783.97 37.51 o 7 4 3 93.53 74.44 11.47 o 8 4 3 0.37 -5.19 5.53 o 0 5 3 964.53 917.79 20.23 o 1 5 3 886.35 892.22 16.54 o 2 5 3 357.63 386.78 12.14 o 3 5 3 1387.29 1475.65 19.38 o 4 5 3 250.57 238.13 14.90 o 5 5 3 112.68 112.93 23.17 o 6 5 3 895.94 857.63 33.71 o 7 5 3 39.99 46.85 8.86 o 8 5 3 116.87 135.00 16.14 o 0 6 3 38.89 33.62 4.49 o 1 6 3 1300.58 1266.65 32.09 o 2 6 3 3214.31 3355.77 49.24 o 3 6 3 88.66 95.22 5.76 o 4 6 3 326.60 319.08 17.97 o 5 6 3 540.74 489.53 24.17 o 6 6 3 677.38 649.04 30.10 o 7 6 3 7.70 10.50 5.93 o 8 6 3 123.18 160.17 37.23 o 0 7 3 549.80 540.07 18.77 o 1 7 3 1361.95 1505.88 49.29 o 2 7 3 141.55 178.48 11.87 o 3 7 3 834.83 893.63 19.03 o 4 7 3 83.20 75.47 9.40 o 5 7 3 364.09 360.67 21.38 o 6 7 3 19.71 16.68 5.93 o 7 7 3 60.21 77.00 12.82 o 0 8 3 327.84 317.60 15.49 o 1 8 3 97.80 95.97 7.28 o 2 8 3 193.66 193.36 13.14 o 3 8 3 58.18 63.46 6.11 o 4 8 3 428.98 438.73 36.44 o 5 8 3 51.26 50.07 10.92 o 6 8 3 153.20 136.91 14.82 o 7 8 3 305.15 344.50 24.59 o 0 9 3 3.02 9.64 3.84 o 1 9 3 485.23 545.30 18.43 o 2 9 3 183.22 189.62 13.81 o 3 9 3 46.87 44.18 9.08 o 4 9 3 104.34 80.12 10.90 o 5 9 3 40.26 38.92 8.04 o 6 9 3 8.82 7.54 5.51 o 0 10 3 728.06 741.31 27.06 o 1 10 3 1507.85 1499.63 36.43 o 2 10 3 22.78 24.05 6.06 o 3 10 3 157.74 153.28 13.84 o 4 10 3 96.18 92.79 11.47 o 5 10 3 6.14 11.08 6.17 o 6 10 3 0.51 0.08 4.96 o 0 11 3 26.80 30.45 6.51 o 1 11 3 39.79 43.99 6.55 o 2 11 3 21.82 13.02 5.60 o 3 11 3 131.81 118.51 20.42 o 4 11 3 125.96 142.04 16.56 o 5 11 3 25.01 30.57 8.11 o 0 12 3 42.80 43.86 13.71 o 1 12 3 39.32 38.52 5.33 o 2 12 3 18.66 12.98 3.79 o 3 12 3 26.38 28.00 11.82 o 4 12 3 16.13 11.13 5.27 o 0 13 3 75.37 83.55 12.19 o 1 13 3 79.39 90.27 9.25 o 2 13 3 97.12 106.98 9.07 o 3 13 3 12.62 4.24 3.54 o 0 14 3 18.86 14.65 9.19 o 1 14 3 59.40 72.58 8.92 o 2 14 3 6.55 8.68 3.82 o 0 0 4 4697.36 4304.15 31.59 o 1 0 4 2594.88 2463.37 18.65 o 2 0 4 126.29 122.59 5.33 o 3 0 4 12905.25 12514.18 93.02 o 4 0 4 2847.27 2989.74 48.14 o 5 0 4 0.10 0.21 3.03 o 6 0 4 700.76 739.83 29.60 o 7 0 4 420.23 409.32 34.27 o 8 0 4 495.56 425.52 37.88 o 0 1 4 2592.91 2446.70 28.14 o 1 1 4 1670.88 1654.59 9.99 o 2 1 4 380.72 386.12 5.98 o 3 1 4 1882.13 1956.60 23.88 o 4 1 4 212.36 236.77 8.67 o 5 1 4 261.37 250.10 12.69 o 6 1 4 316.50 299.61 15.80 o 7 1 4 251.04 252.75 15.64 o 8 1 4 137.74 143.95 12.88 o 0 2 4 6097.00 5569.12 51.38 o 1 2 4 876.07 864.89 8.34 o 2 2 4 234.81 230.95 4.61 o 3 2 4 227.80 220.82 7.10 o 4 2 4 1463.25 1562.70 21.59 o 5 2 4 224.03 229.30 9.06 o 6 2 4 217.10 208.05 12.96 o 7 2 4 125.46 125.72 11.30 o 8 2 4 78.34 80.68 9.65 o 0 3 4 6132.83 5771.51 43.92 o 1 3 4 2476.10 2452.46 19.41 o 2 3 4 1238.20 1258.45 12.64 o 3 3 4 98.60 98.26 5.76 o 4 3 4 209.93 215.99 8.91 o 5 3 4 262.96 280.42 10.87 o 6 3 4 400.54 395.00 22.23 o 7 3 4 284.52 270.26 20.01 o 8 3 4 34.35 29.20 8.30 o 0 4 4 624.27 619.51 14.02 o 1 4 4 366.97 395.17 8.51 o 2 4 4 818.49 872.34 12.45 o 3 4 4 2776.66 2857.76 29.77 o 4 4 4 91.46 107.79 9.93 o 5 4 4 1799.56 1914.33 47.60 o 6 4 4 270.67 277.88 19.02 o 7 4 4 145.00 115.00 13.76 o 8 4 4 68.05 65.80 11.10 o 0 5 4 2.74 7.05 2.37 o 1 5 4 310.21 335.04 9.85 o 2 5 4 15.28 14.55 2.18 o 3 5 4 405.51 402.78 11.09 o 4 5 4 173.39 170.77 12.68 o 5 5 4 2568.27 2415.94 52.31 o 6 5 4 112.54 127.40 17.58 o 7 5 4 157.23 144.72 15.15 o 8 5 4 75.49 87.79 13.73 o 0 6 4 2361.89 2291.83 35.36 o 1 6 4 718.22 669.66 18.47 o 2 6 4 414.71 445.99 13.32 o 3 6 4 273.36 280.97 10.92 o 4 6 4 374.16 385.61 19.60 o 5 6 4 297.01 318.66 22.86 o 6 6 4 95.03 88.72 11.59 o 7 6 4 150.61 155.89 26.84 o 8 6 4 39.82 33.00 31.12 o 0 7 4 47.99 53.19 6.03 o 1 7 4 1064.47 1058.32 26.79 o 2 7 4 48.45 37.22 5.88 o 3 7 4 638.70 650.99 16.79 o 4 7 4 271.19 286.77 17.69 o 5 7 4 79.81 73.09 9.92 o 6 7 4 687.81 683.21 34.25 o 7 7 4 29.91 27.90 8.03 o 0 8 4 0.59 2.10 2.27 o 1 8 4 12.88 12.32 2.60 o 2 8 4 433.14 426.67 19.34 o 3 8 4 23.28 29.63 4.12 o 4 8 4 141.52 152.68 13.50 o 5 8 4 384.27 362.69 22.02 o 6 8 4 50.42 51.28 9.73 o 7 8 4 1.90 0.84 3.87 o 0 9 4 206.14 202.94 13.33 o 1 9 4 409.00 412.04 14.71 o 2 9 4 283.98 283.95 16.80 o 3 9 4 103.54 86.40 9.99 o 4 9 4 3.72 3.94 6.82 o 5 9 4 6.27 2.90 5.40 o 6 9 4 64.51 68.87 11.12 o 0 10 4 103.63 102.67 10.36 o 1 10 4 962.20 945.31 21.71 o 2 10 4 483.89 463.66 22.44 o 3 10 4 381.80 344.83 25.13 o 4 10 4 187.29 195.33 18.23 o 5 10 4 159.49 165.34 16.16 o 6 10 4 60.19 55.44 10.62 o 0 11 4 1191.04 1142.98 35.46 o 1 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6 6.85 0.28 3.92 o 0 12 6 60.64 56.73 13.58 o 1 12 6 89.90 83.69 7.32 o 2 12 6 130.11 140.74 9.61 o 3 12 6 23.60 23.12 4.77 o 4 12 6 117.87 164.84 16.54 o 0 13 6 0.20 -1.96 5.63 o 1 13 6 34.42 29.16 7.62 o 2 13 6 71.04 65.89 14.90 o 3 13 6 327.65 369.28 26.21 o 1 0 7 1231.40 1224.95 16.99 o 2 0 7 1669.69 1662.57 22.19 o 3 0 7 329.09 379.27 21.38 o 4 0 7 120.50 123.47 14.20 o 5 0 7 219.62 235.74 21.79 o 6 0 7 226.57 208.46 22.80 o 7 0 7 122.05 100.73 17.64 o 8 0 7 181.80 168.23 24.66 o 0 1 7 522.42 521.82 16.70 o 1 1 7 3372.56 3415.36 18.29 o 2 1 7 894.29 932.92 11.78 o 3 1 7 169.59 194.97 10.89 o 4 1 7 18.86 20.12 4.51 o 5 1 7 223.08 220.40 15.02 o 6 1 7 176.68 188.79 22.34 o 7 1 7 57.63 55.03 9.25 o 8 1 7 141.01 153.76 16.68 o 0 2 7 2557.08 2671.57 37.02 o 1 2 7 752.16 757.21 7.95 o 2 2 7 203.90 227.37 5.74 o 3 2 7 264.82 270.65 11.39 o 4 2 7 447.62 454.30 15.45 o 5 2 7 60.05 63.89 6.54 o 6 2 7 121.20 144.50 10.95 o 7 2 7 194.69 191.83 13.79 o 8 2 7 142.96 146.13 16.22 o 0 3 7 111.03 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275.79 22.61 o 0 0 8 102.16 95.35 6.07 o 1 0 8 625.41 613.50 12.52 o 2 0 8 662.07 696.19 17.92 o 3 0 8 998.37 1056.71 36.72 o 4 0 8 6.91 9.89 5.18 o 5 0 8 4.23 5.51 5.48 o 6 0 8 0.18 -3.38 4.64 o 7 0 8 77.78 104.20 18.01 o 8 0 8 5.62 12.67 9.34 o 0 1 8 493.61 443.28 11.64 o 1 1 8 6283.05 6164.30 25.76 o 2 1 8 236.63 244.66 6.24 o 3 1 8 145.92 145.41 9.65 o 4 1 8 5.74 4.33 3.35 o 5 1 8 403.83 381.21 19.76 o 6 1 8 184.70 163.40 14.34 o 7 1 8 4.99 9.17 8.42 o 8 1 8 65.85 64.01 10.90 o 0 2 8 614.03 660.22 18.99 o 1 2 8 250.69 265.15 4.76 o 2 2 8 1015.65 1002.88 12.36 o 3 2 8 486.41 452.45 13.78 o 4 2 8 1091.37 1090.51 23.68 o 5 2 8 336.15 324.43 18.32 o 6 2 8 176.06 155.55 14.03 o 7 2 8 242.39 275.75 20.39 o 8 2 8 401.67 423.61 57.37 o 0 3 8 3.23 -0.71 2.97 o 1 3 8 1317.80 1230.40 19.06 o 2 3 8 102.32 99.40 3.87 o 3 3 8 9.02 7.67 1.61 o 4 3 8 364.73 392.99 12.28 o 5 3 8 94.03 85.56 6.40 o 6 3 8 156.16 153.12 9.05 o 7 3 8 23.86 15.95 4.70 o 8 3 8 176.51 189.29 26.85 o 0 4 8 1565.87 1578.74 46.00 o 1 4 8 236.05 220.57 4.46 o 2 4 8 311.29 329.60 7.60 o 3 4 8 818.68 822.16 16.48 o 4 4 8 136.63 143.33 8.91 o 5 4 8 54.98 58.43 6.19 o 6 4 8 357.23 358.00 21.84 o 7 4 8 60.97 58.05 15.22 o 0 5 8 215.37 220.53 6.47 o 1 5 8 47.07 44.71 2.46 o 2 5 8 508.04 532.30 12.95 o 3 5 8 1224.11 1227.49 23.72 o 4 5 8 132.27 124.18 10.86 o 5 5 8 845.56 867.59 31.44 o 6 5 8 19.94 32.52 7.00 o 7 5 8 108.46 107.98 29.96 o 0 6 8 101.91 97.87 6.01 o 1 6 8 431.87 432.95 8.68 o 2 6 8 67.04 68.46 4.23 o 3 6 8 3202.97 3262.80 40.22 o 4 6 8 150.13 147.95 16.62 o 5 6 8 188.46 198.50 15.44 o 6 6 8 22.24 18.67 6.17 o 7 6 8 13.62 7.38 4.33 o 0 7 8 303.68 315.38 13.69 o 1 7 8 204.40 202.83 10.62 o 2 7 8 690.12 698.50 14.18 o 3 7 8 571.87 613.96 17.74 o 4 7 8 257.70 270.17 12.11 o 5 7 8 241.91 215.96 16.47 o 6 7 8 206.65 229.17 18.49 o 7 7 8 5.27 1.16 4.03 o 0 8 8 14.61 13.22 3.58 o 1 8 8 428.69 403.75 11.61 o 2 8 8 711.21 720.89 24.02 o 3 8 8 603.76 562.25 35.35 o 4 8 8 123.23 103.50 11.12 o 5 8 8 4.79 17.59 8.26 o 6 8 8 80.06 75.86 11.46 o 0 9 8 51.83 41.59 5.73 o 1 9 8 481.70 493.31 19.32 o 2 9 8 513.53 368.50 45.41 o 3 9 8 61.84 61.68 8.29 o 4 9 8 50.65 58.98 8.86 o 5 9 8 81.96 72.78 10.59 o 6 9 8 8.22 18.18 6.27 o 0 10 8 453.94 346.79 79.79 o 1 10 8 123.16 111.82 11.18 o 2 10 8 485.12 484.55 15.40 o 3 10 8 20.08 15.83 4.95 o 4 10 8 41.66 47.18 8.27 o 5 10 8 72.04 122.33 21.96 o 0 11 8 355.32 345.61 32.50 o 1 11 8 556.06 544.82 37.45 o 2 11 8 242.79 240.29 19.49 o 3 11 8 71.76 59.72 14.91 o 4 11 8 51.89 47.25 15.26 o 0 12 8 13.25 14.88 9.89 o 1 12 8 310.27 297.97 22.30 o 2 12 8 15.02 20.81 7.45 o 3 12 8 113.64 133.54 15.60 o 0 13 8 28.24 36.23 12.40 o 1 13 8 11.44 6.17 7.10 o 2 13 8 92.44 82.61 12.82 o 1 0 9 3193.34 3256.86 28.43 o 2 0 9 6501.25 6496.94 48.09 o 3 0 9 60.12 49.13 8.31 o 4 0 9 329.40 366.61 24.53 o 5 0 9 613.55 655.62 36.64 o 6 0 9 150.79 123.09 18.07 o 7 0 9 15.71 17.46 8.21 o 8 0 9 30.23 18.46 9.66 o 0 1 9 2580.74 2483.40 31.03 o 1 1 9 829.80 877.81 9.32 o 2 1 9 1498.35 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9 63.77 53.52 11.07 o 6 5 9 67.91 69.73 18.91 o 7 5 9 106.28 129.59 15.96 o 0 6 9 89.05 90.57 4.54 o 1 6 9 51.49 44.62 2.71 o 2 6 9 248.71 245.79 9.90 o 3 6 9 497.26 515.67 16.05 o 4 6 9 452.45 352.94 50.53 o 5 6 9 247.91 238.32 16.88 o 6 6 9 19.63 11.41 5.03 o 7 6 9 20.14 13.23 15.88 o 0 7 9 329.66 327.88 11.69 o 1 7 9 169.95 173.89 5.49 o 2 7 9 9.98 9.81 2.42 o 3 7 9 772.48 785.80 33.82 o 4 7 9 869.56 776.06 78.24 o 5 7 9 22.39 28.84 6.95 o 6 7 9 95.32 92.30 11.78 o 0 8 9 87.23 74.22 6.45 o 1 8 9 79.95 85.14 5.06 o 2 8 9 228.93 224.77 13.25 o 3 8 9 226.44 220.91 17.39 o 4 8 9 207.87 193.85 14.99 o 5 8 9 114.77 109.59 13.12 o 6 8 9 7.41 11.76 5.94 o 0 9 9 230.42 224.35 12.48 o 1 9 9 78.33 74.17 6.23 o 2 9 9 85.63 70.92 11.23 o 3 9 9 815.71 811.55 43.50 o 4 9 9 40.19 43.80 11.36 o 5 9 9 19.46 30.80 12.03 o 0 10 9 7.25 12.74 7.69 o 1 10 9 35.97 32.53 8.42 o 2 10 9 90.08 78.60 21.61 o 3 10 9 84.36 118.38 20.16 o 4 10 9 97.18 102.98 20.12 o 5 10 9 3.89 -1.35 6.04 o 0 11 9 339.70 371.01 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9.44 o 7 2 13 19.65 24.54 6.68 o 0 3 13 245.59 248.64 14.87 o 1 3 13 798.37 756.52 22.06 o 2 3 13 409.56 421.49 16.81 o 3 3 13 1038.87 1083.11 21.12 o 4 3 13 778.54 745.43 22.45 o 5 3 13 105.93 100.71 8.84 o 6 3 13 46.90 51.21 6.89 o 0 4 13 19.76 25.38 7.52 o 1 4 13 119.93 128.69 11.25 o 2 4 13 22.40 13.98 4.71 o 3 4 13 1308.13 1361.31 33.57 o 4 4 13 1105.49 1075.48 35.44 o 5 4 13 159.81 176.60 15.19 o 6 4 13 98.40 109.78 19.58 o 0 5 13 0.06 1.20 4.35 o 1 5 13 65.41 76.51 9.23 o 2 5 13 326.66 340.04 19.12 o 3 5 13 23.23 23.89 5.77 o 4 5 13 10.27 11.93 7.38 o 5 5 13 14.32 11.20 8.54 o 6 5 13 100.40 109.89 20.14 o 0 6 13 33.21 49.71 11.29 o 1 6 13 239.54 224.08 15.89 o 2 6 13 38.61 36.13 6.84 o 3 6 13 4.53 7.35 4.30 o 4 6 13 421.26 428.33 31.17 o 5 6 13 224.13 248.61 28.03 o 6 6 13 101.17 96.49 19.00 o 0 7 13 9.23 8.63 7.97 o 1 7 13 120.42 110.19 15.51 o 2 7 13 10.79 6.87 4.49 o 3 7 13 137.23 113.52 12.04 o 4 7 13 24.02 50.36 13.67 o 5 7 13 70.15 60.58 14.95 o 0 8 13 21.01 28.06 9.87 o 1 8 13 71.62 62.43 21.48 o 2 8 13 272.86 257.71 34.13 o 3 8 13 220.37 265.52 18.57 o 4 8 13 102.66 94.14 18.87 o 5 8 13 25.23 28.28 11.61 o 0 9 13 44.09 33.18 10.45 o 1 9 13 135.80 139.33 14.80 o 2 9 13 256.33 261.44 20.43 o 3 9 13 56.42 73.64 16.78 o 4 9 13 24.36 17.24 9.06 o 0 10 13 179.67 139.81 22.37 o 1 10 13 66.84 49.25 9.82 o 2 10 13 140.41 143.00 15.91 o 3 10 13 181.07 179.18 18.07 o 0 11 13 4.05 3.07 8.68 o 1 11 13 15.60 11.33 6.66 o 2 11 13 131.35 132.78 25.89 o 0 0 14 3861.88 3682.40 93.08 o 1 0 14 451.02 451.81 12.51 o 2 0 14 216.80 249.78 14.19 o 3 0 14 53.19 53.50 7.40 o 4 0 14 1.92 -0.58 3.44 o 5 0 14 8.92 1.49 4.51 o 6 0 14 55.14 59.04 13.35 o 0 1 14 51.05 48.15 3.90 o 1 1 14 167.03 158.86 5.09 o 2 1 14 16.57 15.62 3.05 o 3 1 14 21.68 18.81 3.60 o 4 1 14 278.40 256.29 13.05 o 5 1 14 58.93 54.93 6.81 o 6 1 14 72.45 60.43 7.65 o 0 2 14 128.82 145.30 9.81 o 1 2 14 104.82 100.92 3.55 o 2 2 14 1025.43 1039.08 19.19 o 3 2 14 776.39 790.98 20.75 o 4 2 14 167.09 172.97 10.79 o 5 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16.96 o 2 8 14 36.39 35.15 5.96 o 3 8 14 6.56 10.03 5.52 o 4 8 14 14.75 15.83 9.43 o 0 9 14 162.16 143.80 21.46 o 1 9 14 44.79 32.93 10.60 o 2 9 14 145.58 144.14 15.59 o 3 9 14 105.02 73.27 11.99 o 0 10 14 258.86 220.63 27.73 o 1 10 14 59.00 82.76 17.36 o 2 10 14 134.67 162.32 17.14 o 1 0 15 157.37 148.55 7.94 o 2 0 15 217.49 209.23 13.29 o 3 0 15 139.52 163.85 12.63 o 4 0 15 80.42 82.84 10.03 o 5 0 15 30.66 32.03 7.04 o 6 0 15 19.85 11.75 4.94 o 0 1 15 72.31 74.27 5.77 o 1 1 15 125.42 130.06 4.75 o 2 1 15 58.05 68.50 5.42 o 3 1 15 24.98 25.63 4.50 o 4 1 15 19.25 17.78 3.91 o 5 1 15 45.75 40.21 11.49 o 6 1 15 4.74 0.13 5.12 o 0 2 15 0.02 1.73 2.75 o 1 2 15 135.15 120.67 7.64 o 2 2 15 168.00 194.33 12.52 o 3 2 15 128.60 156.83 13.32 o 4 2 15 98.93 98.51 11.11 o 5 2 15 43.28 41.68 8.07 o 6 2 15 14.94 12.80 8.38 o 0 3 15 207.60 196.65 14.08 o 1 3 15 203.08 212.07 12.19 o 2 3 15 183.05 160.79 15.80 o 3 3 15 424.01 454.02 22.69 o 4 3 15 50.99 47.21 8.47 o 5 3 15 28.47 17.36 8.74 o 6 3 15 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16 613.23 581.55 17.14 o 3 0 16 0.06 -3.03 4.34 o 4 0 16 136.46 125.73 19.56 o 5 0 16 18.46 19.81 10.12 o 0 1 16 152.75 180.69 16.23 o 1 1 16 199.41 208.94 9.03 o 2 1 16 485.55 526.67 14.73 o 3 1 16 319.74 322.85 16.97 o 4 1 16 72.79 63.60 7.65 o 5 1 16 64.38 68.97 12.14 o 0 2 16 249.73 232.19 13.24 o 1 2 16 399.28 385.30 12.74 o 2 2 16 222.83 220.82 10.01 o 3 2 16 35.17 33.13 6.89 o 4 2 16 45.35 49.32 13.98 o 5 2 16 74.71 65.79 9.98 o 0 3 16 41.01 43.28 9.82 o 1 3 16 269.89 269.48 11.16 o 2 3 16 0.31 2.63 2.82 o 3 3 16 46.94 66.70 8.18 o 4 3 16 94.94 101.80 12.84 o 5 3 16 178.53 178.59 16.11 o 0 4 16 138.42 156.16 13.42 o 1 4 16 161.77 190.89 11.81 o 2 4 16 160.56 157.16 11.17 o 3 4 16 187.20 216.15 13.98 o 4 4 16 132.70 127.22 13.88 o 5 4 16 121.11 147.49 15.29 o 0 5 16 4.15 0.65 4.10 o 1 5 16 1.16 0.80 3.07 o 2 5 16 188.62 197.15 12.83 o 3 5 16 18.07 4.78 7.72 o 4 5 16 458.40 473.91 37.03 o 5 5 16 29.27 35.33 12.25 o 0 6 16 54.12 38.64 10.72 o 1 6 16 181.68 148.30 14.25 o 2 6 16 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