#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/60/2236057.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236057_Fobs loop_ _publ_author_name 'Song, Yun-Sung' 'Lee, Soon W.' _publ_section_title ; Poly[[aquabis[\m~2~-6-(pyridine-3-carboxamido)naphthalene-2-carboxylato]copper(II)] dihydrate] ; _journal_coeditor_code AA2070 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1422 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.728 _cell_angle_gamma 90.000 _cell_length_a 29.6255 _cell_length_b 6.8582 _cell_length_c 14.8264 _exptl_crystal_F_000 1444.00 _reflns_d_resolution_high 0.7499 _[local]_cod_data_source_file aa2070Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2C in C2c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 586.82 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z+1/2' '-x, -y, -z' '-x, y, -z-1/2' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 19693.15 19692.82 232.34 o 4 0 0 17324.70 16785.38 161.72 o 6 0 0 12766.59 12720.01 127.38 o 8 0 0 18733.13 17748.27 169.57 o 10 0 0 1900.34 1663.25 46.34 o 12 0 0 4648.63 4255.67 75.84 o 14 0 0 131770.86 145674.70 1264.18 o 16 0 0 12791.01 12150.93 160.46 o 18 0 0 15593.87 15387.78 217.98 o 20 0 0 5311.47 5026.37 121.53 o 22 0 0 1898.37 1771.37 113.86 o 24 0 0 96.69 85.44 63.23 o 26 0 0 5689.00 5801.58 175.16 o 28 0 0 50.93 57.94 76.20 o 30 0 0 4968.88 4776.86 256.54 o 32 0 0 2250.58 2131.86 131.88 o 34 0 0 2422.41 2469.06 258.45 o 36 0 0 2022.77 2157.82 393.87 o 38 0 0 1172.91 834.83 248.05 o 1 1 0 24256.77 24716.37 208.93 o 3 1 0 9.63 6.60 10.27 o 5 1 0 179.65 164.67 17.57 o 7 1 0 2028.97 2232.15 39.34 o 9 1 0 447.86 386.37 23.77 o 11 1 0 4588.73 4101.81 55.71 o 13 1 0 126.71 112.82 22.07 o 15 1 0 3394.62 3313.11 56.98 o 17 1 0 2380.99 2210.76 51.86 o 19 1 0 2863.54 2853.49 63.64 o 21 1 0 293.97 280.47 41.08 o 23 1 0 10.28 -42.03 42.03 o 25 1 0 936.49 914.70 62.79 o 27 1 0 432.80 557.76 72.12 o 29 1 0 4.87 -60.73 60.73 o 31 1 0 1559.43 1423.24 101.78 o 33 1 0 843.12 940.40 103.22 o 35 1 0 132.29 -90.69 90.69 o 37 1 0 373.09 441.96 116.89 o 39 1 0 106.37 41.82 209.14 o 0 2 0 36075.52 36973.75 448.66 o 2 2 0 32650.44 34055.21 311.36 o 4 2 0 6081.79 6363.44 85.65 o 6 2 0 12836.94 12266.07 129.54 o 8 2 0 3510.28 4036.65 69.13 o 10 2 0 4083.82 4157.62 71.25 o 12 2 0 5602.37 6004.69 86.74 o 14 2 0 1803.70 2057.79 57.95 o 16 2 0 1959.92 2072.91 63.52 o 18 2 0 2650.08 2663.17 67.51 o 20 2 0 3932.94 3848.10 87.57 o 22 2 0 5919.08 5853.14 112.71 o 24 2 0 1864.65 1852.50 89.59 o 26 2 0 21.71 -46.31 61.11 o 28 2 0 2.53 -74.31 76.71 o 30 2 0 574.32 606.87 108.10 o 32 2 0 741.28 719.80 125.05 o 34 2 0 356.92 283.78 115.33 o 36 2 0 115.75 128.33 110.19 o 38 2 0 395.56 474.34 165.38 o 1 3 0 25079.84 25001.27 248.77 o 3 3 0 3964.09 3916.45 76.19 o 5 3 0 15239.44 15585.85 166.01 o 7 3 0 18804.20 18440.49 197.21 o 9 3 0 4629.58 4396.24 81.75 o 11 3 0 3516.47 3432.84 75.21 o 13 3 0 6992.64 6979.37 105.40 o 15 3 0 5949.47 5776.40 100.42 o 17 3 0 4237.81 4172.66 97.39 o 19 3 0 10017.84 9966.97 142.55 o 21 3 0 1479.50 1461.04 73.52 o 23 3 0 398.86 243.01 89.79 o 25 3 0 397.06 510.74 101.81 o 27 3 0 2932.11 3032.39 178.83 o 29 3 0 2669.55 2769.93 207.92 o 31 3 0 1992.21 1979.31 164.28 o 33 3 0 2397.71 2590.93 345.36 o 35 3 0 1024.84 947.24 150.15 o 37 3 0 35.51 -81.40 115.59 o 0 4 0 142.33 191.34 70.03 o 2 4 0 81.42 68.84 31.75 o 4 4 0 224.85 233.07 42.94 o 6 4 0 3814.18 4036.43 94.99 o 8 4 0 1292.93 1534.99 58.48 o 10 4 0 7.63 16.58 39.86 o 12 4 0 276.07 293.54 50.92 o 14 4 0 282.06 302.61 52.34 o 16 4 0 2435.16 2615.66 117.00 o 18 4 0 3450.14 3294.42 118.52 o 20 4 0 177.06 121.29 76.16 o 22 4 0 2973.29 2659.53 175.41 o 24 4 0 216.96 291.46 98.39 o 26 4 0 604.50 585.07 112.44 o 28 4 0 3.97 -89.71 89.71 o 30 4 0 316.26 490.80 132.98 o 32 4 0 649.12 637.52 131.25 o 34 4 0 116.02 33.84 120.05 o 1 5 0 89.94 69.54 62.90 o 3 5 0 1241.27 1337.51 86.21 o 5 5 0 1279.31 1356.36 93.72 o 7 5 0 906.73 1013.87 70.34 o 9 5 0 361.59 523.73 73.19 o 11 5 0 306.63 300.56 71.07 o 13 5 0 203.85 172.46 68.41 o 15 5 0 320.82 183.57 78.41 o 17 5 0 200.13 30.06 87.08 o 19 5 0 56.87 79.38 80.10 o 21 5 0 220.77 272.64 90.25 o 23 5 0 1.87 -90.40 90.40 o 25 5 0 197.33 245.43 134.79 o 27 5 0 66.68 4.11 100.16 o 29 5 0 216.60 -36.22 146.89 o 31 5 0 334.11 416.47 136.01 o 0 6 0 781.54 784.42 145.23 o 2 6 0 9058.75 8524.87 218.34 o 4 6 0 38.63 9.93 88.08 o 6 6 0 550.42 600.45 145.14 o 8 6 0 854.36 629.33 97.49 o 10 6 0 280.84 351.36 101.32 o 12 6 0 1236.50 1053.15 90.69 o 14 6 0 54.19 35.63 69.31 o 16 6 0 2339.12 2547.56 164.67 o 18 6 0 22.42 95.43 84.71 o 20 6 0 609.81 774.19 120.54 o 22 6 0 966.04 994.36 129.32 o 24 6 0 1220.32 1275.63 143.00 o 26 6 0 25.55 -1.33 107.96 o 28 6 0 1658.37 1993.32 177.61 o 1 7 0 64.03 -140.20 156.35 o 3 7 0 1334.84 1283.92 161.18 o 5 7 0 54.49 79.38 126.21 o 7 7 0 135.03 246.98 114.08 o 9 7 0 198.28 331.31 139.71 o 11 7 0 741.03 718.93 145.75 o 13 7 0 39.44 59.98 105.82 o 15 7 0 13.11 32.42 141.99 o 17 7 0 1029.16 919.47 146.84 o 19 7 0 171.81 118.17 137.04 o 21 7 0 86.50 29.06 140.77 o 23 7 0 64.18 64.84 143.90 o 25 7 0 148.78 -90.63 144.93 o 0 8 0 30.42 86.69 199.76 o 2 8 0 152.04 362.03 307.18 o 4 8 0 234.14 93.54 145.23 o 6 8 0 346.04 563.81 170.20 o 8 8 0 0.19 110.99 146.70 o 10 8 0 0.19 -67.34 137.63 o 12 8 0 103.56 57.85 136.72 o 14 8 0 12.64 -242.72 309.70 o 16 8 0 4.29 -58.01 135.59 o 18 8 0 8.82 72.09 262.85 o 1 9 0 1.54 88.90 160.83 o 3 9 0 178.99 465.37 226.15 o 5 9 0 1.41 145.87 209.19 o -39 1 1 185.32 268.87 157.46 o -37 1 1 2210.73 2298.81 235.05 o -35 1 1 1634.64 1695.36 177.06 o -33 1 1 1781.85 2029.09 127.04 o -31 1 1 1119.82 1114.81 94.15 o -29 1 1 4564.95 4204.64 198.78 o -27 1 1 91.04 39.13 64.35 o -25 1 1 209.22 204.21 58.13 o -23 1 1 2384.18 2517.02 87.63 o -21 1 1 2509.72 2370.61 79.36 o -19 1 1 762.79 757.10 47.54 o -17 1 1 2185.67 2173.87 58.06 o -13 1 1 11212.85 11442.78 107.46 o -11 1 1 15803.54 15661.06 133.59 o -9 1 1 3398.74 3539.99 53.13 o -7 1 1 725.40 690.91 25.83 o -5 1 1 1814.33 1605.61 34.85 o -3 1 1 13909.88 14604.78 123.50 o -1 1 1 3283.86 3520.49 44.16 o 1 1 1 66369.02 65754.75 513.87 o 3 1 1 19840.58 20035.09 164.72 o 5 1 1 46488.73 47122.71 309.17 o 7 1 1 20851.39 20726.47 150.83 o 9 1 1 4459.29 4225.78 50.94 o 11 1 1 1721.83 1658.83 44.85 o 13 1 1 3681.80 3756.83 55.05 o 15 1 1 15045.21 15371.99 134.26 o 17 1 1 2084.27 2154.21 53.18 o 19 1 1 4113.37 4004.63 75.06 o 21 1 1 1211.33 1201.99 55.25 o 23 1 1 741.80 851.22 55.21 o 25 1 1 2465.71 2718.66 97.33 o 27 1 1 1734.86 1557.91 94.05 o 29 1 1 111.24 170.69 62.50 o 31 1 1 820.36 1022.81 134.75 o 33 1 1 698.71 517.83 108.50 o 35 1 1 226.43 175.02 99.87 o 37 1 1 76.41 78.76 157.22 o -38 2 1 347.60 391.00 118.28 o -36 2 1 1609.44 1803.83 163.10 o -34 2 1 1356.06 1137.88 184.85 o -32 2 1 1256.04 1478.60 143.12 o -30 2 1 1170.24 1207.65 114.08 o -28 2 1 978.64 817.57 84.76 o -26 2 1 4536.33 4448.29 148.98 o -24 2 1 55.41 16.34 54.36 o -22 2 1 6040.76 5928.45 122.66 o -20 2 1 6441.30 6323.31 116.54 o -18 2 1 8481.51 8755.78 128.08 o -16 2 1 1482.14 1562.52 60.35 o -14 2 1 724.62 621.45 41.62 o -12 2 1 5004.74 4798.67 81.23 o -10 2 1 2410.87 1976.41 50.42 o -8 2 1 1247.23 1190.65 40.39 o -6 2 1 17914.87 18114.46 186.21 o -4 2 1 52798.86 54165.07 507.66 o -2 2 1 42419.07 42452.94 404.58 o 0 2 1 13742.85 13342.12 142.20 o 2 2 1 1867.82 2054.49 55.29 o 4 2 1 13944.89 13756.14 121.29 o 6 2 1 18980.87 18440.16 168.68 o 8 2 1 8265.80 7973.63 84.98 o 10 2 1 2358.26 2489.67 54.84 o 12 2 1 7165.04 7762.77 88.06 o 14 2 1 13968.21 13798.88 125.75 o 16 2 1 3504.97 3685.47 63.78 o 18 2 1 2710.59 2641.67 61.78 o 20 2 1 5702.65 5627.79 94.02 o 22 2 1 692.33 693.65 50.75 o 24 2 1 319.78 448.25 64.48 o 26 2 1 440.82 511.18 79.59 o 28 2 1 332.94 395.83 102.80 o 30 2 1 1167.30 884.48 112.10 o 32 2 1 832.55 836.40 121.03 o 34 2 1 1469.21 1696.09 162.86 o 36 2 1 510.45 273.95 163.21 o 38 2 1 130.59 -65.95 142.89 o -37 3 1 182.68 262.43 146.89 o -35 3 1 436.52 700.30 139.23 o -33 3 1 0.21 176.72 109.89 o -31 3 1 1.18 65.97 100.15 o -29 3 1 0.93 36.15 92.42 o -27 3 1 11.01 -77.43 77.43 o -25 3 1 38.20 -45.86 90.89 o -23 3 1 5343.61 5247.55 200.69 o -21 3 1 16603.01 16387.85 299.54 o -19 3 1 6.72 53.43 47.64 o -17 3 1 697.14 769.92 61.08 o -15 3 1 1122.62 1164.23 54.55 o -13 3 1 27.30 -6.81 32.15 o -11 3 1 148.64 183.89 32.15 o -9 3 1 7087.43 7784.50 109.77 o -7 3 1 7465.04 8134.70 111.06 o -5 3 1 224.43 254.55 34.60 o -3 3 1 3802.91 3997.73 82.58 o -1 3 1 796.23 954.75 54.06 o 1 3 1 3808.18 4117.00 78.15 o 3 3 1 9365.61 9575.39 122.34 o 5 3 1 5727.41 6000.03 77.38 o 7 3 1 7913.83 8900.69 109.58 o 9 3 1 87.76 70.68 22.28 o 11 3 1 0.71 21.59 28.46 o 13 3 1 1.38 28.14 32.78 o 15 3 1 10.18 22.61 33.87 o 17 3 1 30.60 41.69 34.40 o 19 3 1 4344.01 4266.78 98.23 o 21 3 1 1942.46 1810.46 107.91 o 23 3 1 1.13 -14.61 67.36 o 25 3 1 136.09 117.07 86.86 o 27 3 1 80.93 -71.05 80.23 o 29 3 1 0.80 -87.23 87.23 o 31 3 1 326.56 198.14 109.80 o 33 3 1 436.45 685.96 175.18 o 35 3 1 40.48 -109.86 146.34 o -34 4 1 23.59 271.59 119.66 o -32 4 1 170.72 302.93 122.41 o -30 4 1 722.70 826.83 129.76 o -28 4 1 1256.80 1066.94 134.91 o -26 4 1 430.65 401.06 108.56 o -24 4 1 7289.74 7439.49 267.86 o -22 4 1 835.30 939.33 132.83 o -20 4 1 11.20 -34.41 65.64 o -18 4 1 616.39 573.32 115.74 o -16 4 1 1222.62 1308.75 83.19 o -14 4 1 59.04 71.02 63.25 o -12 4 1 71.88 4.56 45.39 o -10 4 1 4003.73 4208.93 111.77 o -8 4 1 3894.23 3727.23 94.95 o -6 4 1 2013.27 1718.48 92.83 o -4 4 1 7737.57 7816.01 113.73 o -2 4 1 8298.04 8431.34 137.66 o 0 4 1 799.60 772.01 51.10 o 2 4 1 353.20 242.92 47.23 o 4 4 1 21.86 -27.12 44.47 o 6 4 1 4459.23 4279.71 85.23 o 8 4 1 9673.20 9933.20 128.57 o 10 4 1 2897.53 2771.07 74.97 o 12 4 1 3547.29 3436.49 117.90 o 14 4 1 1230.31 1152.12 72.61 o 16 4 1 33.52 146.75 57.31 o 18 4 1 9.00 31.85 69.35 o 20 4 1 77.01 8.51 88.77 o 22 4 1 3280.72 3063.78 149.32 o 24 4 1 200.44 83.03 88.78 o 26 4 1 13.85 36.22 95.36 o 28 4 1 11.96 -41.58 122.41 o 30 4 1 26.61 -94.61 133.29 o 32 4 1 66.68 96.53 138.30 o 34 4 1 7.71 65.84 116.64 o -33 5 1 394.08 245.44 153.80 o -31 5 1 606.77 891.54 139.58 o -29 5 1 10.19 185.75 111.17 o -27 5 1 1168.08 1114.31 142.69 o -25 5 1 599.33 361.49 109.10 o -23 5 1 864.74 1059.54 216.52 o -21 5 1 3402.17 3238.39 201.62 o -19 5 1 2129.22 2061.63 149.74 o -17 5 1 8.10 26.01 86.27 o -15 5 1 3449.38 3472.45 153.67 o -13 5 1 2828.54 3231.25 145.17 o -11 5 1 3035.42 3117.44 150.92 o -9 5 1 1847.83 1879.74 103.02 o -7 5 1 3417.69 3565.52 131.53 o -5 5 1 3693.46 3473.39 129.98 o -3 5 1 355.40 372.40 77.07 o -1 5 1 6810.37 6780.81 169.68 o 1 5 1 161.93 135.13 62.33 o 3 5 1 2266.10 2358.00 110.05 o 5 5 1 1173.84 1210.08 83.47 o 7 5 1 3173.76 3126.72 124.89 o 9 5 1 4765.06 5106.45 166.25 o 11 5 1 1337.24 1412.36 86.27 o 13 5 1 1588.30 1596.69 105.46 o 15 5 1 1046.27 936.96 95.82 o 17 5 1 1116.10 1192.40 104.95 o 19 5 1 58.02 54.32 77.42 o 21 5 1 203.96 346.18 102.46 o 23 5 1 4521.20 4277.68 205.51 o 25 5 1 2502.20 2505.49 175.83 o 27 5 1 334.24 327.84 116.52 o 29 5 1 636.98 636.23 132.87 o 31 5 1 355.84 313.35 127.69 o -28 6 1 255.82 360.07 139.85 o -26 6 1 24.31 116.20 109.99 o -24 6 1 89.27 -66.51 98.55 o -22 6 1 9.99 25.82 95.12 o -20 6 1 1.69 21.88 90.00 o -18 6 1 6.75 -81.32 81.32 o -16 6 1 47.96 85.29 82.17 o -14 6 1 638.51 564.08 89.57 o -12 6 1 4.95 -78.94 78.94 o -10 6 1 152.22 226.67 79.98 o -8 6 1 13.66 -59.90 59.90 o -6 6 1 1672.19 1636.58 122.41 o -4 6 1 785.31 774.88 92.79 o -2 6 1 788.28 783.02 92.92 o 0 6 1 1217.90 1243.53 104.11 o 2 6 1 2367.91 2437.25 158.23 o 4 6 1 165.23 156.61 92.20 o 6 6 1 37.05 82.16 87.53 o 8 6 1 1406.03 1387.68 148.92 o 10 6 1 1162.67 950.40 120.03 o 12 6 1 265.54 312.54 102.58 o 14 6 1 1444.55 1329.94 135.38 o 16 6 1 4.21 -38.36 80.73 o 18 6 1 45.74 -53.77 98.85 o 20 6 1 41.41 53.69 84.26 o 22 6 1 23.85 -9.47 96.60 o 24 6 1 143.87 313.16 113.09 o 26 6 1 483.38 74.96 145.80 o 28 6 1 186.48 -17.63 110.56 o -25 7 1 73.47 -89.50 229.03 o -23 7 1 331.89 200.81 110.02 o -21 7 1 222.35 431.95 112.69 o -19 7 1 253.52 192.59 125.67 o -17 7 1 2.46 3.22 88.13 o -15 7 1 41.62 188.86 111.35 o -13 7 1 182.75 310.31 135.46 o -11 7 1 510.28 617.59 125.56 o -9 7 1 1929.59 2119.74 160.47 o -7 7 1 668.04 789.42 122.29 o -5 7 1 172.74 306.01 108.10 o -3 7 1 45.45 -94.95 94.95 o -1 7 1 21.70 82.75 145.75 o 1 7 1 759.82 700.02 146.89 o 3 7 1 1553.45 1485.38 159.84 o 5 7 1 813.41 805.05 141.14 o 7 7 1 676.52 798.37 138.36 o 9 7 1 316.76 476.53 238.47 o 11 7 1 431.97 318.81 133.66 o 13 7 1 81.54 -70.27 121.16 o 15 7 1 427.09 320.60 143.30 o 17 7 1 49.86 147.08 133.29 o 19 7 1 8.06 23.84 119.33 o 21 7 1 81.73 -8.15 129.82 o 23 7 1 180.50 369.21 183.94 o 25 7 1 290.38 630.13 261.80 o -18 8 1 79.05 69.00 139.81 o -16 8 1 11.05 202.15 149.27 o -14 8 1 149.36 425.94 137.69 o -12 8 1 307.46 398.93 156.16 o -10 8 1 283.16 159.16 152.60 o -8 8 1 291.04 484.60 235.57 o -6 8 1 429.66 541.07 169.01 o -4 8 1 271.87 160.52 144.79 o -2 8 1 151.02 177.15 152.81 o 0 8 1 5.47 79.22 141.18 o 2 8 1 252.04 291.37 161.09 o 4 8 1 87.28 71.89 142.57 o 6 8 1 350.16 391.00 222.38 o 8 8 1 129.52 53.95 457.95 o 10 8 1 303.97 645.35 168.99 o 12 8 1 124.30 377.44 148.48 o 14 8 1 126.87 431.82 159.49 o 16 8 1 566.09 596.19 237.04 o 18 8 1 346.87 351.84 204.87 o -5 9 1 112.18 273.45 179.77 o -3 9 1 5.08 118.98 258.18 o -1 9 1 13.37 215.38 167.84 o 1 9 1 35.93 23.10 155.49 o 3 9 1 2.60 -252.53 252.53 o 5 9 1 187.06 178.95 177.08 o -38 0 2 987.75 862.27 223.68 o -36 0 2 1204.26 1581.26 249.01 o -34 0 2 2593.74 2384.28 268.69 o -32 0 2 6427.99 6194.81 250.93 o -30 0 2 2213.87 2123.12 215.62 o -28 0 2 5477.57 4961.20 265.46 o -26 0 2 3556.86 3768.82 229.61 o -24 0 2 3047.00 3060.39 129.03 o -22 0 2 3293.07 3089.67 103.69 o -20 0 2 340.01 307.80 43.06 o -18 0 2 3359.72 2809.90 92.02 o -16 0 2 18231.40 17681.05 211.20 o -12 0 2 4250.88 4052.18 71.66 o -10 0 2 561.89 469.96 29.15 o -8 0 2 37.81 93.65 28.75 o -6 0 2 953.05 745.13 34.09 o -4 0 2 3767.75 3606.29 66.83 o -2 0 2 13730.61 14734.15 175.80 o 0 0 2 1016.49 1146.02 27.22 o 2 0 2 11871.09 12224.73 140.40 o 4 0 2 51690.18 51209.48 513.10 o 6 0 2 2378.34 2516.96 51.93 o 8 0 2 4399.39 4672.99 75.54 o 10 0 2 9304.14 9183.59 113.13 o 12 0 2 22534.13 21716.02 221.58 o 14 0 2 25563.14 27552.04 277.35 o 16 0 2 4298.37 4431.14 88.84 o 18 0 2 15874.10 15368.91 203.93 o 20 0 2 3050.91 3066.66 98.15 o 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