#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:43:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181282 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/60/2236070.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236070_Fobs loop_ _publ_author_name 'Padayachy, Kamentheren' 'Fernandes, Manuel A.' 'Marques, Helder M.' 'Lemmerer, Andreas' 'de Sousa, Alvaro S.' _publ_section_title ; Bis(2-hydroxyethyl)ammonium 2-bromophenolate ; _journal_coeditor_code BH2446 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2610 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 107.250 _cell_angle_gamma 90.000 _cell_length_a 8.0592 _cell_length_b 7.6653 _cell_length_c 9.7659 _exptl_crystal_F_000 284.00 _reflns_d_resolution_high 0.7571 _cod_data_source_file bh2446Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 8m_alv20_0a in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 112.60 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 -10 0 389.55 408.84 17.35 o 1 -10 0 68.98 66.37 5.77 o 1 -9 0 267.69 282.73 7.13 o 2 -9 0 145.20 146.59 6.08 o 3 -9 0 40.39 39.71 4.22 o 4 -9 0 159.36 163.06 6.78 o 0 -8 0 568.83 572.23 20.89 o 1 -8 0 81.76 80.76 3.49 o 2 -8 0 330.98 339.77 6.55 o 3 -8 0 180.60 182.94 6.06 o 4 -8 0 24.27 26.54 3.83 o 5 -8 0 223.79 229.21 8.42 o 6 -8 0 140.15 139.21 7.85 o 1 -7 0 439.08 439.52 5.65 o 2 -7 0 385.77 382.78 5.39 o 3 -7 0 322.63 326.58 8.19 o 4 -7 0 271.84 270.98 6.72 o 5 -7 0 127.40 128.52 6.43 o 6 -7 0 276.89 272.29 8.84 o 7 -7 0 198.05 200.33 8.66 o 0 -6 0 301.70 280.16 7.65 o 1 -6 0 100.57 85.34 9.65 o 2 -6 0 428.44 444.11 6.32 o 3 -6 0 495.56 500.76 9.38 o 4 -6 0 4.75 4.58 2.04 o 5 -6 0 867.16 879.39 20.34 o 6 -6 0 90.86 86.99 5.59 o 7 -6 0 34.11 37.21 4.66 o 8 -6 0 266.91 275.64 12.64 o 1 -5 0 1330.36 1348.54 12.52 o 2 -5 0 412.69 409.73 5.54 o 3 -5 0 168.16 173.75 3.35 o 4 -5 0 1385.19 1403.91 18.55 o 5 -5 0 51.90 47.34 3.30 o 6 -5 0 216.95 214.94 5.96 o 7 -5 0 699.29 705.42 15.66 o 8 -5 0 5.12 7.30 4.14 o 0 -4 0 386.23 342.13 7.35 o 1 -4 0 193.34 186.41 2.04 o 2 -4 0 508.02 494.74 5.41 o 3 -4 0 1204.98 1210.93 9.47 o 4 -4 0 48.50 52.27 2.01 o 5 -4 0 1323.29 1358.19 13.10 o 6 -4 0 143.84 146.44 4.88 o 7 -4 0 94.04 97.14 4.97 o 8 -4 0 440.38 453.75 8.74 o 9 -4 0 10.58 10.26 5.76 o 1 -3 0 1985.53 1962.79 21.36 o 2 -3 0 649.88 626.65 3.83 o 3 -3 0 24.91 23.26 1.05 o 4 -3 0 1594.93 1622.65 12.00 o 5 -3 0 355.09 293.47 53.26 o 6 -3 0 293.79 284.78 6.62 o 7 -3 0 524.43 530.92 9.35 o 8 -3 0 88.61 99.02 6.52 o 9 -3 0 152.57 157.48 7.97 o 0 -2 0 12050.98 10462.29 215.94 o 1 -2 0 1449.53 1551.49 9.11 o 2 -2 0 1884.35 1978.71 12.06 o 3 -2 0 3622.51 3760.12 37.48 o 4 -2 0 72.55 76.92 2.14 o 5 -2 0 1029.92 1043.45 9.55 o 6 -2 0 599.60 604.35 6.01 o 7 -2 0 60.55 62.07 3.64 o 8 -2 0 465.34 470.78 9.97 o 9 -2 0 39.98 46.15 5.21 o 1 -1 0 1236.69 1259.90 8.74 o 2 -1 0 1790.70 1762.58 34.20 o 3 -1 0 291.95 323.03 2.99 o 4 -1 0 2101.29 2105.76 23.60 o 5 -1 0 201.08 204.91 3.28 o 6 -1 0 125.08 126.98 3.13 o 7 -1 0 640.76 641.70 10.15 o 8 -1 0 35.76 28.57 3.91 o 9 -1 0 163.89 155.14 7.42 o 10 -1 0 65.43 67.47 5.96 o 1 0 0 524.74 556.54 4.48 o 2 0 0 1919.08 1957.24 20.01 o 3 0 0 7431.50 7376.55 90.98 o 4 0 0 0.90 1.86 0.71 o 5 0 0 614.84 606.22 8.48 o 6 0 0 1015.39 1038.97 17.39 o 7 0 0 1.24 2.02 2.73 o 8 0 0 650.79 657.63 13.75 o 9 0 0 30.39 37.74 4.56 o 10 0 0 54.92 66.24 7.69 o 1 1 0 1360.17 1375.39 21.28 o 2 1 0 1790.25 1776.66 15.42 o 3 1 0 281.35 292.27 12.05 o 4 1 0 2242.66 2227.35 25.57 o 5 1 0 179.94 184.38 3.78 o 6 1 0 45.52 47.10 2.62 o 7 1 0 768.75 773.15 12.63 o 8 1 0 37.69 38.33 4.30 o 9 1 0 167.56 159.00 7.21 o 10 1 0 64.91 64.16 7.72 o 0 2 0 12678.15 9579.89 533.40 o 1 2 0 1224.94 1304.28 21.95 o 2 2 0 1856.60 1978.18 31.25 o 3 2 0 3493.67 3529.37 39.80 o 4 2 0 62.28 63.80 2.32 o 5 2 0 1016.78 991.39 8.76 o 6 2 0 544.10 536.80 6.58 o 7 2 0 54.77 54.47 3.08 o 8 2 0 482.77 497.80 14.60 o 9 2 0 27.80 23.28 6.21 o 1 3 0 1995.42 1948.01 38.98 o 2 3 0 633.61 603.43 8.05 o 3 3 0 36.12 32.98 1.51 o 4 3 0 1606.26 1652.32 32.80 o 5 3 0 399.82 394.76 8.65 o 6 3 0 265.13 260.47 5.87 o 7 3 0 613.69 606.88 12.15 o 8 3 0 97.00 99.68 6.04 o 9 3 0 166.44 149.94 9.95 o 0 4 0 295.18 244.33 4.14 o 1 4 0 205.21 194.21 4.92 o 2 4 0 588.79 568.46 6.64 o 3 4 0 1200.63 1195.21 17.11 o 4 4 0 45.77 47.14 1.98 o 5 4 0 1410.30 1397.96 14.00 o 6 4 0 95.17 88.06 4.33 o 7 4 0 99.12 98.54 4.96 o 8 4 0 448.75 427.73 13.08 o 9 4 0 0.62 -1.90 5.66 o 1 5 0 1306.85 1282.30 26.96 o 2 5 0 245.17 229.98 3.92 o 3 5 0 117.61 120.81 3.15 o 4 5 0 1386.97 1395.16 10.74 o 5 5 0 38.48 37.28 2.55 o 6 5 0 166.94 156.85 5.43 o 7 5 0 729.85 708.45 11.85 o 8 5 0 5.77 8.68 3.55 o 0 6 0 370.54 324.97 5.65 o 1 6 0 109.74 107.91 4.05 o 2 6 0 400.51 394.77 9.67 o 3 6 0 680.76 668.56 8.84 o 4 6 0 2.95 1.98 1.50 o 5 6 0 968.56 941.20 23.78 o 6 6 0 63.07 63.30 4.21 o 7 6 0 37.63 38.60 5.14 o 8 6 0 303.00 300.09 10.00 o 1 7 0 395.08 388.41 10.20 o 2 7 0 296.51 285.95 5.24 o 3 7 0 287.35 283.92 5.95 o 4 7 0 264.64 268.94 4.28 o 5 7 0 95.00 95.50 5.96 o 6 7 0 231.09 225.46 8.42 o 7 7 0 204.08 197.82 8.80 o 0 8 0 655.80 643.21 7.06 o 1 8 0 86.06 84.17 3.65 o 2 8 0 349.48 357.13 6.28 o 3 8 0 212.23 224.07 6.93 o 4 8 0 23.38 25.42 4.35 o 5 8 0 257.34 250.90 7.58 o 6 8 0 136.25 131.07 8.72 o 1 9 0 228.49 236.56 7.75 o 2 9 0 160.96 160.52 6.12 o 3 9 0 38.92 36.40 3.98 o 4 9 0 135.40 143.68 6.52 o 0 10 0 479.55 482.77 14.31 o 1 10 0 49.21 41.44 4.53 o -1 -10 1 169.28 184.75 10.32 o 0 -10 1 18.93 19.46 4.16 o 1 -10 1 98.07 107.66 6.21 o -4 -9 1 6.03 2.11 4.73 o -3 -9 1 186.27 209.02 7.92 o -2 -9 1 51.19 35.18 11.93 o -1 -9 1 1.06 -0.20 2.38 o 0 -9 1 408.01 404.77 9.89 o 1 -9 1 0.14 -0.99 2.95 o 2 -9 1 36.32 38.93 4.15 o 3 -9 1 314.45 321.79 8.23 o 4 -9 1 37.61 39.69 4.65 o -6 -8 1 270.81 272.99 24.76 o -5 -8 1 114.03 110.33 8.68 o -4 -8 1 589.39 600.53 43.86 o -3 -8 1 1.12 2.24 2.48 o -2 -8 1 238.35 240.09 5.34 o -1 -8 1 377.49 389.19 6.45 o 0 -8 1 0.81 -0.36 2.24 o 1 -8 1 255.01 252.62 5.03 o 2 -8 1 313.60 300.89 7.22 o 3 -8 1 17.85 21.10 3.48 o 4 -8 1 285.04 289.93 7.63 o 5 -8 1 75.87 80.06 5.28 o -7 -7 1 15.01 19.70 5.72 o -6 -7 1 59.71 68.89 6.51 o -5 -7 1 259.51 262.86 7.31 o -4 -7 1 38.44 42.62 3.13 o -3 -7 1 346.84 325.33 22.03 o -2 -7 1 461.00 470.78 7.23 o -1 -7 1 268.03 261.23 4.57 o 0 -7 1 842.16 859.33 14.03 o 1 -7 1 95.59 95.91 3.37 o 2 -7 1 128.00 131.04 4.20 o 3 -7 1 1091.71 1079.30 16.70 o 4 -7 1 6.57 7.18 3.07 o 5 -7 1 196.12 201.74 6.75 o 6 -7 1 237.99 233.44 8.59 o 7 -7 1 9.79 9.70 4.56 o -8 -6 1 10.40 11.71 5.63 o -7 -6 1 219.60 218.65 9.94 o -6 -6 1 115.12 128.29 5.31 o -5 -6 1 194.77 193.30 7.07 o -4 -6 1 653.13 669.39 9.81 o -3 -6 1 49.57 31.81 7.32 o -2 -6 1 559.59 569.10 8.41 o -1 -6 1 805.47 807.37 9.21 o 0 -6 1 84.87 89.17 2.72 o 1 -6 1 1557.68 1572.66 17.15 o 2 -6 1 382.25 394.50 9.38 o 3 -6 1 90.34 88.15 3.42 o 4 -6 1 861.23 833.32 10.14 o 5 -6 1 53.29 52.81 4.06 o 6 -6 1 149.47 143.32 6.87 o 7 -6 1 261.67 270.93 9.07 o -9 -5 1 32.96 34.34 6.74 o -8 -5 1 308.51 219.92 100.97 o -7 -5 1 9.47 3.76 3.02 o -6 -5 1 187.60 146.21 41.45 o -5 -5 1 695.16 538.72 145.80 o -4 -5 1 40.55 24.99 7.65 o -3 -5 1 1418.59 1422.44 10.59 o -2 -5 1 719.27 737.69 8.19 o -1 -5 1 330.59 332.97 4.96 o 0 -5 1 3122.80 3148.70 20.86 o 1 -5 1 304.88 308.66 3.95 o 2 -5 1 438.55 439.84 8.87 o 3 -5 1 1450.70 1468.87 23.82 o 4 -5 1 362.98 367.18 5.52 o 5 -5 1 558.86 564.42 8.31 o 6 -5 1 411.87 390.66 9.69 o 7 -5 1 6.27 5.98 3.83 o 8 -5 1 269.77 292.40 9.77 o -9 -4 1 155.19 164.07 8.18 o -8 -4 1 12.19 12.53 4.02 o -7 -4 1 701.23 696.20 12.03 o -6 -4 1 20.06 19.93 2.81 o -5 -4 1 272.92 283.09 3.95 o -4 -4 1 806.27 842.34 6.94 o -3 -4 1 6.45 8.25 0.99 o -2 -4 1 1054.17 986.80 37.70 o -1 -4 1 1811.68 1860.97 10.85 o 0 -4 1 107.49 117.49 2.89 o 1 -4 1 3053.22 3159.03 28.41 o 2 -4 1 542.44 530.72 9.25 o 3 -4 1 177.16 185.22 2.68 o 4 -4 1 1473.24 1478.70 17.27 o 5 -4 1 6.91 8.79 1.68 o 6 -4 1 12.81 12.49 2.75 o 7 -4 1 564.03 578.51 10.80 o 8 -4 1 15.86 20.03 4.49 o 9 -4 1 164.43 165.44 10.98 o -9 -3 1 139.01 135.08 7.54 o -8 -3 1 415.21 428.85 9.92 o -7 -3 1 28.49 32.41 3.82 o -6 -3 1 343.37 349.38 5.27 o -5 -3 1 1708.83 1692.31 9.56 o -4 -3 1 160.55 165.85 2.61 o -3 -3 1 1220.18 1243.80 6.43 o -2 -3 1 2028.03 2087.04 13.41 o -1 -3 1 729.41 773.76 4.57 o 0 -3 1 3041.31 3060.00 23.61 o 1 -3 1 956.37 979.98 11.05 o 2 -3 1 1298.59 1335.63 11.38 o 3 -3 1 1083.19 1066.81 6.92 o 4 -3 1 182.88 189.07 3.34 o 5 -3 1 805.03 798.96 7.13 o 6 -3 1 560.22 561.15 7.81 o 7 -3 1 41.36 48.99 3.60 o 8 -3 1 329.01 336.24 11.97 o 9 -3 1 69.62 65.31 7.69 o -10 -2 1 142.89 154.30 9.98 o -9 -2 1 421.04 429.83 10.26 o -8 -2 1 67.70 64.68 5.11 o -7 -2 1 848.66 885.91 13.59 o -6 -2 1 731.33 717.55 7.25 o -5 -2 1 333.14 315.84 4.82 o -4 -2 1 1783.91 1800.56 15.00 o -3 -2 1 1113.48 1181.02 10.98 o -2 -2 1 1164.35 1130.46 7.31 o -1 -2 1 6132.13 5863.92 94.98 o 0 -2 1 398.68 435.40 2.53 o 1 -2 1 983.30 968.53 9.09 o 2 -2 1 1649.75 1755.95 12.11 o 3 -2 1 418.58 456.36 3.55 o 4 -2 1 1086.32 1076.01 9.93 o 5 -2 1 402.06 414.49 6.59 o 6 -2 1 572.82 546.19 15.36 o 7 -2 1 495.25 519.46 7.79 o 8 -2 1 40.26 39.64 4.61 o 9 -2 1 277.45 291.31 9.28 o -10 -1 1 77.31 81.16 8.09 o -9 -1 1 147.78 158.43 7.07 o -8 -1 1 534.90 533.54 9.89 o -7 -1 1 184.80 180.00 5.28 o -6 -1 1 1105.25 1102.62 12.65 o -5 -1 1 1180.28 1152.72 10.49 o -4 -1 1 393.75 414.05 6.23 o -3 -1 1 2737.33 2766.81 24.52 o -2 -1 1 631.17 639.37 6.14 o -1 -1 1 144.14 177.59 2.15 o 0 -1 1 1867.40 1952.24 20.90 o 1 -1 1 88.70 81.93 1.03 o 2 -1 1 1198.44 1236.31 15.53 o 3 -1 1 1512.20 1624.29 19.13 o 4 -1 1 299.61 344.03 6.97 o 5 -1 1 1406.12 1456.57 23.53 o 6 -1 1 145.32 152.14 3.51 o 7 -1 1 95.40 90.59 5.42 o 8 -1 1 657.68 632.54 12.83 o 9 -1 1 50.87 55.81 5.45 o -10 0 1 352.82 349.79 12.74 o -9 0 1 314.92 315.47 9.74 o -8 0 1 26.05 26.60 3.77 o -7 0 1 853.86 824.44 11.12 o -6 0 1 1447.41 1469.69 19.60 o -5 0 1 74.30 72.46 2.39 o -4 0 1 5576.27 5805.89 73.32 o -3 0 1 1226.99 1248.67 14.32 o -2 0 1 886.95 898.63 9.74 o -1 0 1 2196.34 2176.73 18.05 o 0 0 1 722.26 705.22 8.37 o 1 0 1 683.08 702.57 6.58 o 2 0 1 370.07 359.36 3.78 o 3 0 1 108.62 131.84 2.06 o 4 0 1 1954.16 1983.41 20.94 o 5 0 1 522.54 537.88 8.21 o 6 0 1 962.99 943.94 16.29 o 7 0 1 408.97 424.11 8.82 o 8 0 1 7.49 8.56 3.57 o 9 0 1 282.79 290.66 9.06 o -10 1 1 81.35 87.39 8.20 o -9 1 1 138.26 142.34 9.41 o -8 1 1 570.88 577.07 20.37 o -7 1 1 202.62 201.25 4.32 o -6 1 1 1168.76 1176.17 8.54 o -5 1 1 1064.88 1035.63 6.92 o -4 1 1 371.92 400.30 4.16 o -3 1 1 3049.36 2922.79 106.33 o -2 1 1 583.42 573.41 4.30 o -1 1 1 86.01 107.10 1.00 o 0 1 1 2095.72 2210.30 21.53 o 1 1 1 86.18 80.73 1.04 o 2 1 1 1055.07 994.68 35.28 o 3 1 1 1724.38 1776.39 18.95 o 4 1 1 306.86 339.31 8.55 o 5 1 1 1431.25 1459.55 20.84 o 6 1 1 81.45 82.98 3.60 o 7 1 1 72.52 76.56 4.25 o 8 1 1 671.44 643.36 12.34 o 9 1 1 42.39 51.82 5.26 o -10 2 1 131.48 133.27 10.34 o -9 2 1 386.20 377.45 12.45 o -8 2 1 63.05 59.15 4.77 o -7 2 1 677.80 686.37 7.35 o -6 2 1 799.15 781.44 13.07 o -5 2 1 366.58 354.12 5.25 o -4 2 1 1722.67 1711.05 17.04 o -3 2 1 1009.62 1044.81 14.39 o -2 2 1 1339.72 1317.46 22.27 o -1 2 1 5304.62 5187.96 40.49 o 0 2 1 399.15 422.20 4.01 o 1 2 1 1137.24 1098.22 9.11 o 2 2 1 1476.30 1552.23 27.09 o 3 2 1 362.61 382.45 6.52 o 4 2 1 1189.80 1202.35 18.94 o 5 2 1 389.36 354.24 27.37 o 6 2 1 644.90 611.48 8.31 o 7 2 1 435.60 433.79 7.92 o 8 2 1 32.49 30.20 4.36 o 9 2 1 290.69 294.65 11.83 o -9 3 1 141.95 139.47 9.24 o -8 3 1 453.93 462.12 24.33 o -7 3 1 39.49 26.75 6.47 o -6 3 1 357.52 352.32 4.88 o -5 3 1 1698.62 1645.22 12.44 o -4 3 1 152.17 154.29 2.02 o -3 3 1 1258.81 1252.79 14.01 o -2 3 1 2165.71 2132.24 27.96 o -1 3 1 819.40 841.63 6.84 o 0 3 1 3075.17 3012.13 36.03 o 1 3 1 1009.95 1007.84 8.11 o 2 3 1 1268.33 1268.70 19.21 o 3 3 1 1145.63 1117.08 18.94 o 4 3 1 189.22 193.96 2.57 o 5 3 1 768.59 741.30 17.20 o 6 3 1 555.18 524.73 10.97 o 7 3 1 33.18 31.97 5.37 o 8 3 1 293.54 294.43 9.07 o 9 3 1 74.99 69.43 7.58 o -9 4 1 167.28 181.79 10.68 o -8 4 1 14.61 14.50 3.22 o -7 4 1 595.29 585.11 7.61 o -6 4 1 71.56 63.22 3.17 o -5 4 1 325.03 334.78 6.51 o -4 4 1 607.51 611.46 4.73 o -3 4 1 7.64 10.15 1.37 o -2 4 1 1136.34 1077.31 23.93 o -1 4 1 1645.10 1571.63 24.91 o 0 4 1 107.00 119.25 1.98 o 1 4 1 3103.43 3084.61 27.18 o 2 4 1 628.10 595.82 7.86 o 3 4 1 199.55 201.15 3.22 o 4 4 1 1469.37 1471.91 33.11 o 5 4 1 13.37 9.11 2.01 o 6 4 1 24.17 21.75 3.15 o 7 4 1 535.43 520.59 10.17 o 8 4 1 16.08 16.16 4.30 o 9 4 1 187.35 182.60 11.12 o -9 5 1 47.61 43.74 7.48 o -8 5 1 288.59 288.69 7.70 o -7 5 1 4.44 4.73 3.10 o -6 5 1 166.10 170.60 4.73 o -5 5 1 703.66 699.30 8.77 o -4 5 1 42.59 37.83 2.00 o -3 5 1 1416.59 1397.61 18.71 o -2 5 1 721.04 693.07 15.28 o -1 5 1 380.01 365.92 12.41 o 0 5 1 3114.18 3074.06 27.23 o 1 5 1 292.80 283.60 3.80 o 2 5 1 483.97 466.32 8.50 o 3 5 1 1319.68 1308.00 20.26 o 4 5 1 364.97 365.51 5.83 o 5 5 1 598.22 582.80 10.49 o 6 5 1 404.66 379.27 7.72 o 7 5 1 5.49 3.71 3.27 o 8 5 1 274.02 257.00 11.83 o -8 6 1 7.27 2.75 4.36 o -7 6 1 298.33 288.55 8.82 o -6 6 1 74.75 78.12 4.53 o -5 6 1 187.90 186.30 4.86 o -4 6 1 611.97 618.33 8.51 o -3 6 1 77.59 72.08 1.78 o -2 6 1 555.76 536.60 11.22 o -1 6 1 858.06 825.05 9.50 o 0 6 1 85.06 84.02 2.28 o 1 6 1 1678.85 1670.82 15.11 o 2 6 1 362.52 350.03 4.06 o 3 6 1 66.21 67.70 2.68 o 4 6 1 927.60 940.73 14.36 o 5 6 1 28.18 25.89 3.31 o 6 6 1 81.96 78.63 4.58 o 7 6 1 294.53 288.83 11.88 o -7 7 1 6.50 5.57 4.64 o -6 7 1 54.84 54.48 5.46 o -5 7 1 261.06 270.31 6.70 o -4 7 1 38.83 36.85 1.75 o -3 7 1 349.25 341.91 5.76 o -2 7 1 444.21 432.74 7.20 o -1 7 1 276.67 257.22 8.10 o 0 7 1 820.29 825.53 6.15 o 1 7 1 78.31 76.91 2.90 o 2 7 1 161.46 163.50 3.74 o 3 7 1 1012.64 994.01 9.95 o 4 7 1 8.71 10.50 3.16 o 5 7 1 239.06 254.14 8.03 o 6 7 1 218.30 215.81 8.54 o 7 7 1 8.87 11.84 6.58 o -6 8 1 276.60 256.40 9.18 o -5 8 1 111.28 108.19 6.89 o -4 8 1 623.21 646.77 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