#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:43:47 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181282 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/60/2236073.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236073_Fobs loop_ _publ_author_name 'Ye, Bao-fen' _publ_section_title ; 4,6-Dibromoisophthalic acid monohydrate ; _journal_coeditor_code BH2450 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2642 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.910 _cell_angle_gamma 90.000 _cell_length_a 3.8740 _cell_length_b 17.3660 _cell_length_c 15.7100 _exptl_crystal_F_000 656.00 _reflns_d_resolution_high 0.8355 _cod_data_source_file bh2450Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' S in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 240.88 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 271.72 235.43 44.44 o 2 0 0 16.28 3.95 68.67 o 3 0 0 155.00 166.91 98.71 o 4 0 0 850.28 772.23 151.48 o 1 1 0 7681.72 7501.88 110.67 o 2 1 0 1494.11 1573.30 100.44 o 3 1 0 619.71 695.52 123.87 o 4 1 0 10.33 166.58 140.87 o 0 2 0 4903.78 5069.33 54.89 o 1 2 0 11445.84 11876.03 134.45 o 2 2 0 157.89 197.49 63.06 o 3 2 0 704.92 802.81 131.35 o 4 2 0 360.98 592.31 147.59 o 1 3 0 10812.25 10147.96 128.67 o 2 3 0 6.78 17.32 61.27 o 3 3 0 1627.23 1512.52 127.51 o 4 3 0 7.85 110.26 143.98 o 0 4 0 1175.72 1273.82 45.09 o 1 4 0 4816.20 4817.53 96.18 o 2 4 0 1341.38 1466.79 92.11 o 3 4 0 3693.09 3641.66 167.89 o 4 4 0 2.20 96.39 120.51 o 1 5 0 239.69 298.55 45.04 o 2 5 0 10072.86 9914.30 187.43 o 3 5 0 16.37 98.77 98.77 o 4 5 0 61.30 164.55 118.64 o 0 6 0 12.08 4.84 33.89 o 1 6 0 576.11 583.59 55.87 o 2 6 0 742.61 797.10 80.59 o 3 6 0 503.20 436.08 109.80 o 4 6 0 6.09 16.21 112.08 o 1 7 0 268.01 349.53 55.76 o 2 7 0 9516.78 9061.39 189.37 o 3 7 0 71.82 125.16 94.46 o 4 7 0 12.53 151.16 113.34 o 0 8 0 4076.13 4037.20 106.42 o 1 8 0 2404.51 2362.59 96.04 o 2 8 0 26.76 72.59 72.59 o 3 8 0 126.72 196.12 89.67 o 4 8 0 130.41 10.15 116.03 o 1 9 0 5384.59 5605.70 142.37 o 2 9 0 1145.60 997.71 99.93 o 3 9 0 316.09 332.70 100.45 o 4 9 0 66.00 148.24 109.64 o 0 10 0 207.25 305.40 65.48 o 1 10 0 577.90 567.13 79.48 o 2 10 0 149.22 185.48 84.56 o 3 10 0 2.78 36.31 102.88 o 4 10 0 0.30 198.63 108.65 o 1 11 0 7399.65 7314.40 185.99 o 2 11 0 8.60 85.22 86.94 o 3 11 0 238.27 232.83 107.80 o 0 12 0 7968.23 8306.74 197.06 o 1 12 0 96.75 47.42 94.84 o 2 12 0 97.77 47.83 98.12 o 3 12 0 12.53 43.07 106.48 o 1 13 0 605.53 704.20 102.11 o 2 13 0 788.50 535.26 130.10 o 3 13 0 2.25 44.26 108.73 o 0 14 0 1156.72 1142.73 121.28 o 1 14 0 227.70 308.07 98.44 o 2 14 0 0.45 54.65 105.50 o 3 14 0 91.95 118.32 118.32 o 1 15 0 26.47 57.90 113.75 o 2 15 0 1134.96 923.82 143.52 o 3 15 0 189.17 164.74 117.85 o 0 16 0 30.89 80.62 115.13 o 1 16 0 815.34 925.87 151.46 o 2 16 0 7.94 126.09 126.09 o 1 17 0 466.17 510.79 144.43 o 2 17 0 40.02 58.56 133.47 o 0 18 0 205.93 104.81 149.37 o 1 18 0 1468.26 1326.12 187.29 o 2 18 0 128.02 115.66 136.82 o 1 19 0 143.21 103.93 154.11 o 0 20 0 1133.13 1123.53 181.38 o 1 20 0 0.32 122.79 156.02 o -4 1 1 811.99 638.30 113.52 o -3 1 1 834.81 607.77 91.28 o -2 1 1 1891.96 1596.54 80.21 o -1 1 1 498.67 578.66 37.31 o 0 1 1 3256.51 3463.52 1266.84 o 1 1 1 15367.92 14048.37 175.16 o 2 1 1 2424.47 2218.76 118.71 o 3 1 1 29.38 111.26 103.57 o 4 1 1 3.68 151.60 135.26 o -4 2 1 153.93 242.45 116.09 o -3 2 1 1444.50 1469.75 146.61 o -2 2 1 2533.40 2340.66 97.69 o -1 2 1 39772.25 37919.86 221.38 o 0 2 1 595.30 687.03 141.67 o 1 2 1 2284.56 2584.05 80.01 o 2 2 1 4547.56 4406.46 150.19 o 3 2 1 180.52 170.01 112.87 o 4 2 1 176.37 161.75 141.40 o -4 3 1 0.71 100.22 162.27 o -3 3 1 372.75 486.20 112.00 o -2 3 1 8245.31 7645.85 162.32 o -1 3 1 13186.77 13547.08 140.80 o 0 3 1 2166.68 2282.03 384.92 o 1 3 1 331.19 367.70 42.30 o 2 3 1 2419.21 2658.66 121.78 o 3 3 1 402.09 383.21 113.37 o 4 3 1 233.30 431.95 147.34 o -4 4 1 57.14 221.22 158.52 o -3 4 1 1250.37 1310.61 131.65 o -2 4 1 856.03 831.24 77.72 o -1 4 1 554.22 529.39 45.82 o 0 4 1 6391.25 6142.01 600.51 o 1 4 1 2646.85 2839.08 84.11 o 2 4 1 2491.00 2809.32 125.25 o 3 4 1 121.14 78.68 115.30 o 4 4 1 177.56 127.30 145.08 o -4 5 1 38.70 119.39 147.19 o -3 5 1 3.25 105.43 105.43 o -2 5 1 2536.08 2524.80 111.12 o -1 5 1 16956.58 17080.73 176.41 o 0 5 1 13277.17 12564.56 1165.87 o 1 5 1 1559.17 1604.50 71.01 o 2 5 1 4343.87 4398.19 143.33 o 3 5 1 226.07 486.94 102.98 o 4 5 1 388.45 373.67 139.48 o -4 6 1 144.19 217.71 140.83 o -3 6 1 4.31 216.31 99.47 o -2 6 1 2710.60 2831.24 118.65 o -1 6 1 5761.00 5625.06 116.66 o 0 6 1 3347.22 3328.08 403.79 o 1 6 1 1093.07 1084.78 68.22 o 2 6 1 3733.23 3727.39 134.12 o 3 6 1 2374.77 2439.07 153.67 o 4 6 1 15.54 12.05 120.37 o -4 7 1 96.83 31.96 150.16 o -3 7 1 94.88 62.08 108.57 o -2 7 1 85.08 6.53 74.57 o -1 7 1 8.90 0.00 51.59 o 0 7 1 5936.80 6257.55 505.54 o 1 7 1 7269.16 7423.74 146.79 o 2 7 1 235.37 96.97 82.10 o 3 7 1 38.83 24.05 103.44 o 4 7 1 3.85 40.30 123.62 o -4 8 1 245.71 355.89 147.12 o -3 8 1 514.16 531.45 122.17 o -2 8 1 1484.13 1600.71 115.41 o -1 8 1 5973.49 6136.05 139.26 o 0 8 1 10884.19 10977.67 457.45 o 1 8 1 644.17 642.63 69.70 o 2 8 1 20.21 10.83 78.83 o 3 8 1 1563.23 1293.30 134.82 o 4 8 1 135.60 38.81 128.01 o -4 9 1 197.52 19.70 162.13 o -3 9 1 434.39 481.20 130.78 o -2 9 1 43.91 88.19 88.19 o -1 9 1 1156.96 1212.19 83.04 o 0 9 1 3400.35 3391.44 138.28 o 1 9 1 4982.70 5145.47 141.71 o 2 9 1 32.14 34.15 78.11 o 3 9 1 257.21 255.25 113.02 o 4 9 1 14.52 69.76 117.00 o -4 10 1 189.78 213.55 157.90 o -3 10 1 1509.33 1617.64 153.46 o -2 10 1 1202.43 1200.37 108.53 o -1 10 1 145.36 204.22 66.09 o 0 10 1 6354.45 6699.12 107.64 o 1 10 1 5702.36 5774.77 156.80 o 2 10 1 3120.33 2945.07 140.95 o 3 10 1 62.57 77.97 107.85 o 4 10 1 216.64 41.72 123.43 o -3 11 1 179.71 263.86 126.67 o -2 11 1 35.27 17.21 101.54 o -1 11 1 138.36 192.03 79.42 o 0 11 1 73.40 100.50 92.88 o 1 11 1 50.18 62.31 70.58 o 2 11 1 188.19 238.96 94.29 o 3 11 1 6.65 69.32 111.64 o -3 12 1 550.32 548.35 147.58 o -2 12 1 371.04 294.90 110.39 o -1 12 1 1190.92 1123.12 111.38 o 0 12 1 3940.86 3959.69 107.00 o 1 12 1 1763.71 1755.07 124.85 o 2 12 1 317.47 531.02 96.60 o 3 12 1 102.19 10.07 113.72 o -3 13 1 606.80 882.10 144.53 o -2 13 1 452.60 624.31 112.40 o -1 13 1 367.37 174.16 101.55 o 0 13 1 4091.80 4158.22 114.03 o 1 13 1 3144.87 3131.02 155.45 o 2 13 1 162.85 96.50 108.56 o 3 13 1 8.11 77.15 113.76 o -3 14 1 119.95 218.06 144.64 o -2 14 1 1421.40 1509.38 144.27 o -1 14 1 3487.82 3431.46 161.05 o 0 14 1 2384.91 2460.23 105.29 o 1 14 1 213.64 230.23 104.51 o 2 14 1 80.76 128.01 110.18 o 3 14 1 710.78 523.60 133.06 o -3 15 1 41.94 83.06 141.00 o -2 15 1 709.21 805.80 134.09 o -1 15 1 1896.21 1811.07 143.71 o 0 15 1 595.94 546.90 81.51 o 1 15 1 567.40 475.39 137.13 o 2 15 1 673.71 730.89 130.30 o 3 15 1 211.75 233.82 122.35 o -2 16 1 698.87 573.66 147.85 o -1 16 1 114.02 226.20 118.22 o 0 16 1 201.46 215.69 85.11 o 1 16 1 0.16 123.01 123.01 o 2 16 1 13.57 131.70 131.70 o -2 17 1 655.11 549.28 146.51 o -1 17 1 633.27 689.37 134.16 o 0 17 1 533.80 435.65 96.40 o 1 17 1 188.70 422.65 132.15 o 2 17 1 1124.11 1041.64 158.47 o -2 18 1 5.29 149.57 139.06 o -1 18 1 497.21 615.19 146.59 o 0 18 1 77.33 141.15 90.10 o 1 18 1 18.92 46.30 144.22 o 2 18 1 317.29 475.01 136.68 o -1 19 1 333.09 407.74 147.48 o 0 19 1 2.12 111.13 160.81 o 1 19 1 219.68 202.13 151.57 o -1 20 1 151.23 12.76 144.23 o 0 20 1 0.75 89.11 100.77 o 1 20 1 0.30 158.24 158.24 o -4 0 2 3.12 162.75 141.85 o -3 0 2 4416.70 5086.89 176.05 o -2 0 2 1037.78 1216.77 94.10 o -1 0 2 58021.66 56209.44 1189.06 o 0 0 2 18.79 17.92 9.43 o 1 0 2 26723.66 27375.92 198.73 o 2 0 2 3887.30 3755.00 116.59 o 3 0 2 2430.44 2540.92 135.41 o 4 0 2 1.30 139.24 108.44 o -4 1 2 30.76 6.32 139.24 o -3 1 2 17.79 91.03 96.50 o -2 1 2 4015.30 4194.84 118.97 o -1 1 2 1688.01 1712.90 57.48 o 0 1 2 344.82 436.23 116.19 o 1 1 2 1983.62 2198.58 75.90 o 2 1 2 2150.70 2288.75 112.02 o 3 1 2 386.62 584.74 109.84 o 4 1 2 97.45 32.13 130.85 o -4 2 2 109.13 24.40 114.65 o -3 2 2 929.97 1021.78 113.88 o -2 2 2 94.33 133.90 58.23 o -1 2 2 34.32 124.56 32.02 o 0 2 2 11231.57 11301.00 4053.06 o 1 2 2 8484.64 8171.52 144.34 o 2 2 2 281.51 355.98 76.88 o 3 2 2 1188.93 1307.99 140.79 o 4 2 2 239.10 224.10 139.74 o -4 3 2 0.87 155.96 155.96 o -3 3 2 19.79 88.32 103.53 o -2 3 2 11736.04 11414.39 180.39 o -1 3 2 2817.64 3114.19 75.99 o 0 3 2 1744.56 1807.96 556.84 o 1 3 2 594.90 587.63 58.06 o 2 3 2 3640.66 3713.03 144.29 o 3 3 2 373.38 468.42 126.99 o 4 3 2 42.80 85.47 130.61 o -4 4 2 902.91 961.90 155.27 o -3 4 2 0.36 26.87 101.63 o -2 4 2 2694.96 2576.14 109.97 o -1 4 2 63.66 95.57 38.00 o 0 4 2 24025.05 22083.57 4586.37 o 1 4 2 1320.43 1344.48 73.44 o 2 4 2 37.91 81.68 79.39 o 3 4 2 828.06 1092.57 139.30 o 4 4 2 369.70 412.02 137.71 o -4 5 2 0.78 296.25 129.25 o -3 5 2 211.38 283.27 105.16 o -2 5 2 8.09 23.35 69.86 o -1 5 2 12052.61 12421.96 153.86 o 0 5 2 2660.75 2507.87 478.58 o 1 5 2 11612.02 12000.69 180.13 o 2 5 2 216.43 355.47 78.60 o 3 5 2 721.81 715.02 128.41 o 4 5 2 112.54 94.26 145.03 o -4 6 2 89.38 104.93 137.65 o -3 6 2 428.82 459.88 122.88 o -2 6 2 688.75 572.93 93.47 o -1 6 2 364.57 314.77 53.68 o 0 6 2 12156.51 11638.33 1717.60 o 1 6 2 441.98 544.99 63.11 o 2 6 2 41.59 77.77 77.77 o 3 6 2 259.26 269.65 119.16 o 4 6 2 116.55 167.87 142.61 o -4 7 2 31.96 153.20 153.20 o -3 7 2 359.16 387.24 124.00 o -2 7 2 0.41 42.85 79.06 o -1 7 2 15987.32 15698.34 195.50 o 0 7 2 4789.71 4797.17 523.64 o 1 7 2 7768.06 7666.39 155.86 o 2 7 2 281.63 321.32 83.11 o 3 7 2 1752.96 1719.47 158.31 o 4 7 2 379.90 222.98 135.68 o -4 8 2 56.92 63.97 150.78 o -3 8 2 1126.23 1166.61 138.64 o -2 8 2 8.83 17.61 80.49 o -1 8 2 603.78 618.64 70.46 o 0 8 2 3535.81 3537.75 170.32 o 1 8 2 8410.45 8286.72 173.92 o 2 8 2 648.21 784.10 96.44 o 3 8 2 74.32 41.90 119.16 o 4 8 2 51.71 291.86 125.67 o -4 9 2 74.68 129.77 150.22 o -3 9 2 249.51 300.92 122.98 o -2 9 2 3880.88 3638.53 150.07 o -1 9 2 691.14 711.79 72.63 o 0 9 2 142.63 177.25 39.34 o 1 9 2 1788.17 1479.00 102.71 o 2 9 2 3653.26 3480.37 157.58 o 3 9 2 7.73 41.73 113.43 o 4 9 2 1.40 128.70 128.70 o -4 10 2 59.79 85.41 158.60 o -3 10 2 365.20 494.89 133.92 o -2 10 2 349.90 378.44 102.34 o -1 10 2 68.58 56.21 71.34 o 0 10 2 569.62 602.49 52.21 o 1 10 2 161.54 126.67 77.60 o 2 10 2 823.20 929.74 110.02 o 3 10 2 15.81 78.58 114.41 o 4 10 2 28.29 38.87 121.74 o -3 11 2 78.11 217.35 127.00 o -2 11 2 6384.98 6348.14 203.27 o -1 11 2 2.27 75.94 74.55 o 0 11 2 1882.80 2025.47 167.29 o 1 11 2 562.67 672.13 92.71 o 2 11 2 4410.11 4523.34 182.24 o 3 11 2 91.38 5.28 111.09 o -3 12 2 1032.09 1003.24 161.05 o -2 12 2 377.21 436.25 109.57 o -1 12 2 2528.22 2365.82 128.84 o 0 12 2 224.03 245.57 66.53 o 1 12 2 3504.29 3736.53 158.75 o 2 12 2 327.71 335.44 114.19 o 3 12 2 35.17 21.35 108.78 o -3 13 2 1.41 154.64 141.49 o -2 13 2 146.99 0.00 116.59 o -1 13 2 2025.15 1840.63 134.17 o 0 13 2 0.67 7.44 62.30 o 1 13 2 652.51 639.69 114.09 o 2 13 2 482.57 550.82 113.59 o 3 13 2 0.90 75.54 114.90 o -3 14 2 603.73 635.34 159.98 o -2 14 2 206.68 186.25 114.79 o -1 14 2 118.66 0.00 104.43 o 0 14 2 34.28 17.85 69.65 o 1 14 2 1435.40 1389.56 142.68 o 2 14 2 44.07 106.46 113.40 o 3 14 2 136.37 92.69 122.23 o -3 15 2 57.19 31.22 150.47 o -2 15 2 51.14 147.20 122.01 o -1 15 2 2665.91 2557.66 167.51 o 0 15 2 5.55 75.44 75.44 o 1 15 2 467.61 789.27 123.77 o 2 15 2 45.24 128.62 114.46 o 3 15 2 130.41 203.27 121.25 o -2 16 2 496.17 433.78 136.04 o -1 16 2 7.64 5.24 113.06 o 0 16 2 2244.63 2008.70 115.15 o 1 16 2 0.86 121.56 121.56 o 2 16 2 0.84 40.94 120.01 o -2 17 2 269.78 142.30 138.54 o -1 17 2 0.86 83.45 118.42 o 0 17 2 13.58 89.17 89.17 o 1 17 2 239.39 196.00 136.90 o 2 17 2 60.42 66.87 138.74 o -2 18 2 43.67 85.50 136.53 o -1 18 2 209.45 64.46 139.74 o 0 18 2 2713.02 2639.87 134.74 o 1 18 2 12.15 46.91 143.35 o 2 18 2 4.68 56.40 136.90 o -1 19 2 413.84 390.75 148.53 o 0 19 2 21.06 3.58 131.34 o 1 19 2 0.50 0.00 147.39 o -1 20 2 203.72 402.28 142.54 o 0 20 2 52.35 119.57 99.48 o 1 20 2 550.55 481.98 172.53 o -4 1 3 1.75 299.46 135.33 o -3 1 3 447.36 448.71 136.38 o -2 1 3 5917.29 5907.21 143.00 o -1 1 3 15481.47 15220.05 152.75 o 0 1 3 3706.29 3843.75 543.81 o 1 1 3 848.75 985.11 56.30 o 2 1 3 10527.66 11002.00 208.72 o 3 1 3 9.58 94.17 93.94 o 4 1 3 320.34 306.51 119.60 o -4 2 3 0.12 286.50 163.16 o -3 2 3 10.66 190.80 84.80 o -2 2 3 8764.21 8743.00 166.84 o -1 2 3 15541.52 15453.82 163.69 o 0 2 3 1583.68 1775.87 493.71 o 1 2 3 2803.27 2707.73 92.70 o 2 2 3 2748.85 2684.76 126.50 o 3 2 3 2270.42 2221.27 153.51 o 4 2 3 131.01 12.81 132.66 o -4 3 3 450.52 566.08 146.54 o -3 3 3 1708.70 1706.25 127.76 o -2 3 3 3319.76 3374.12 114.92 o -1 3 3 8852.67 9188.70 132.68 o 0 3 3 9915.25 9283.85 3156.08 o 1 3 3 19120.41 17838.53 222.14 o 2 3 3 523.61 521.54 87.24 o 3 3 3 429.05 461.67 122.69 o 4 3 3 28.07 88.26 129.72 o -4 4 3 187.93 189.49 161.52 o -3 4 3 1526.34 1478.27 129.97 o -2 4 3 6.94 22.24 61.78 o -1 4 3 5746.02 6044.47 112.66 o 0 4 3 4838.19 4680.43 1540.29 o 1 4 3 448.20 401.38 59.40 o 2 4 3 137.14 113.37 73.87 o 3 4 3 640.57 558.34 133.32 o 4 4 3 100.75 124.16 134.17 o -4 5 3 126.98 131.11 163.23 o -3 5 3 1642.34 1605.57 144.50 o -2 5 3 18.68 41.35 66.45 o -1 5 3 253.79 286.05 46.79 o 0 5 3 5327.12 4998.65 1218.98 o 1 5 3 11919.09 11624.35 191.80 o 2 5 3 12.48 54.83 74.65 o 3 5 3 47.28 81.84 115.99 o 4 5 3 40.77 75.08 134.65 o -4 6 3 625.28 825.32 161.25 o -3 6 3 853.52 960.20 133.23 o -2 6 3 462.73 572.79 79.85 o -1 6 3 1137.84 1220.44 68.74 o 0 6 3 14022.76 13050.86 2676.65 o 1 6 3 7345.40 7431.84 160.28 o 2 6 3 968.30 1186.12 109.18 o 3 6 3 3.14 86.42 111.59 o 4 6 3 954.00 852.45 160.96 o -4 7 3 61.54 85.27 155.63 o -3 7 3 608.84 777.31 135.71 o -2 7 3 1134.25 1078.02 100.92 o -1 7 3 739.56 814.68 67.85 o 0 7 3 6162.35 6275.48 1073.50 o 1 7 3 164.26 177.47 60.73 o 2 7 3 1957.06 2146.71 133.37 o 3 7 3 1.10 28.38 110.33 o 4 7 3 256.36 187.10 142.99 o -4 8 3 152.05 295.99 161.53 o -3 8 3 1737.49 1659.20 156.76 o -2 8 3 9.63 17.93 81.85 o -1 8 3 316.48 398.37 68.66 o 0 8 3 6042.05 5644.30 1033.46 o 1 8 3 307.09 254.96 68.44 o 2 8 3 741.65 730.45 104.30 o 3 8 3 447.02 354.37 126.61 o 4 8 3 217.93 81.05 141.73 o -4 9 3 103.84 138.53 156.27 o -3 9 3 836.26 800.70 139.75 o -2 9 3 375.76 517.04 95.92 o -1 9 3 281.88 339.83 72.00 o 0 9 3 3118.78 3029.39 474.50 o 1 9 3 1123.77 1020.39 94.11 o 2 9 3 578.17 833.16 112.42 o 3 9 3 128.09 268.42 122.47 o 4 9 3 69.75 72.23 130.19 o -4 10 3 4.61 59.51 159.94 o 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