#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/61/2236139.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236139_Fobs loop_ _publ_author_name 'Madeley, Lee G.' 'Lemmerer, Andreas' 'Michael, Joseph P.' _publ_section_title ; (+-)-(rel-3R,3'R)-1,1'-Dimethyl-3,3'-bipyrrolidine-2,2'-dithione ; _journal_coeditor_code BT6851 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3211 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 122.009 _cell_angle_gamma 90.000 _cell_length_a 20.5199 _cell_length_b 5.7237 _cell_length_c 11.2201 _exptl_crystal_F_000 488.00 _reflns_d_resolution_high 0.8256 _[local]_cod_data_source_file bt6851Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 11a_jm1_p in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 209.68 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1244.43 1141.29 172.47 o 4 0 0 19322.01 16410.10 338.33 o 6 0 0 2270.15 2360.19 48.92 o 8 0 0 5829.18 5825.89 119.76 o 10 0 0 0.60 5.04 1.16 o 12 0 0 4883.32 4842.81 141.47 o 14 0 0 941.89 936.78 29.46 o 16 0 0 8.99 20.93 2.71 o 18 0 0 1628.48 1660.78 51.16 o 1 1 0 183.30 149.42 2.52 o 3 1 0 297.13 285.43 4.64 o 5 1 0 8658.13 8360.82 121.98 o 7 1 0 185.91 179.94 3.54 o 9 1 0 4144.67 4047.58 68.25 o 11 1 0 1722.67 1863.63 32.07 o 13 1 0 3666.27 3599.56 75.09 o 15 1 0 430.13 423.13 11.82 o 17 1 0 717.54 797.64 27.13 o 19 1 0 36.36 40.71 3.01 o 0 2 0 13543.45 13087.18 389.84 o 2 2 0 1076.30 1122.53 19.47 o 4 2 0 3666.15 3748.79 63.18 o 6 2 0 148.44 132.66 2.91 o 8 2 0 2073.47 2115.36 44.52 o 10 2 0 72.46 72.48 4.65 o 12 2 0 837.82 887.17 29.46 o 14 2 0 47.59 41.47 4.26 o 16 2 0 346.12 340.30 14.34 o 18 2 0 600.34 634.47 23.25 o 20 2 0 111.80 129.06 8.14 o 1 3 0 76.78 55.74 2.01 o 3 3 0 481.25 460.46 10.95 o 5 3 0 1577.83 1540.72 26.76 o 7 3 0 369.05 391.09 7.54 o 9 3 0 762.78 686.87 15.61 o 11 3 0 230.95 225.18 10.46 o 13 3 0 390.48 384.87 15.89 o 15 3 0 27.78 20.54 3.88 o 17 3 0 211.48 231.45 9.30 o 19 3 0 32.62 36.82 5.04 o 0 4 0 2780.90 2948.32 87.98 o 2 4 0 210.35 243.05 8.14 o 4 4 0 391.98 403.28 8.62 o 6 4 0 659.63 664.01 13.36 o 8 4 0 415.47 413.03 8.90 o 10 4 0 482.55 441.13 19.77 o 12 4 0 708.29 697.26 18.36 o 14 4 0 687.75 636.86 32.75 o 16 4 0 0.71 -1.36 1.64 o 1 5 0 658.42 620.27 16.28 o 3 5 0 120.59 126.83 6.40 o 5 5 0 296.53 296.33 11.63 o 7 5 0 93.24 90.69 4.08 o 9 5 0 4.01 1.94 1.94 o 11 5 0 1.18 1.16 2.33 o 13 5 0 46.38 52.71 5.81 o 0 6 0 365.26 380.22 15.89 o 2 6 0 57.21 58.10 5.62 o 4 6 0 52.61 40.72 3.68 o 6 6 0 12.38 14.34 3.88 o 8 6 0 0.01 3.10 2.71 o 10 6 0 107.36 93.41 8.14 o -19 1 1 67.82 67.44 5.04 o -17 1 1 101.53 92.63 5.81 o -15 1 1 346.38 353.21 7.40 o -13 1 1 534.03 564.33 10.40 o -11 1 1 683.69 726.10 12.95 o -9 1 1 262.41 258.12 4.95 o -7 1 1 656.28 647.26 20.54 o -5 1 1 9.39 11.02 0.67 o -3 1 1 0.52 3.40 0.42 o -1 1 1 13267.21 11887.06 183.55 o 1 1 1 6113.47 5716.89 234.65 o 3 1 1 677.31 723.85 12.82 o 5 1 1 2780.28 2895.40 48.93 o 7 1 1 412.39 430.49 8.04 o 9 1 1 30.65 26.09 1.31 o 11 1 1 0.69 0.39 0.97 o 13 1 1 281.23 284.85 7.78 o 15 1 1 497.79 498.31 12.30 o 17 1 1 93.13 82.94 5.81 o 19 1 1 341.65 368.98 15.12 o -20 2 1 261.65 244.18 11.63 o -18 2 1 177.32 182.16 9.30 o -16 2 1 384.17 370.25 12.79 o -14 2 1 874.61 870.90 20.55 o -12 2 1 88.38 85.66 5.43 o -10 2 1 1288.22 1356.53 42.25 o -8 2 1 602.68 591.45 19.77 o -6 2 1 709.13 712.89 11.03 o -4 2 1 953.81 899.35 13.51 o -2 2 1 0.03 0.78 0.55 o 0 2 1 273.54 284.72 5.67 o 2 2 1 2484.78 2598.31 44.08 o 4 2 1 448.89 485.12 8.93 o 6 2 1 285.42 312.34 6.08 o 8 2 1 553.67 609.95 11.22 o 10 2 1 613.64 625.39 14.46 o 12 2 1 674.12 654.52 15.23 o 14 2 1 450.70 446.49 17.44 o 16 2 1 35.55 30.23 3.88 o 18 2 1 1.89 1.94 2.33 o -19 3 1 26.71 26.36 4.26 o -17 3 1 79.86 66.66 5.81 o -15 3 1 536.08 561.60 21.32 o -13 3 1 23.78 22.17 4.65 o -11 3 1 1696.29 1683.09 37.41 o -9 3 1 77.56 65.45 4.65 o -7 3 1 1514.59 1643.51 28.40 o -5 3 1 0.30 0.48 0.50 o -3 3 1 3332.82 3521.14 59.82 o -1 3 1 258.26 224.45 6.16 o 1 3 1 240.39 181.66 8.91 o 3 3 1 454.80 497.34 11.90 o 5 3 1 802.16 689.81 15.87 o 7 3 1 92.34 98.16 2.68 o 9 3 1 237.48 240.37 6.59 o 11 3 1 266.59 257.35 11.63 o 13 3 1 120.42 114.34 7.36 o 15 3 1 50.29 50.00 5.04 o 17 3 1 183.20 200.38 11.24 o -18 4 1 221.22 210.84 12.01 o -16 4 1 999.67 995.31 35.27 o -14 4 1 261.81 276.73 13.18 o -12 4 1 134.50 132.94 8.14 o -10 4 1 426.64 406.57 16.67 o -8 4 1 1245.33 1203.72 26.64 o -6 4 1 241.29 229.85 6.61 o -4 4 1 1796.79 1668.13 36.31 o -2 4 1 301.37 317.30 8.63 o 0 4 1 67.13 50.57 2.16 o 2 4 1 596.08 654.95 15.61 o 4 4 1 417.42 432.20 11.08 o 6 4 1 19.39 22.60 1.93 o 8 4 1 550.61 556.03 13.57 o 10 4 1 607.83 586.41 22.48 o 12 4 1 172.04 165.88 9.69 o 14 4 1 224.13 232.16 12.40 o 16 4 1 38.22 33.33 5.04 o -15 5 1 67.87 60.85 6.59 o -13 5 1 725.94 721.67 27.91 o -11 5 1 370.56 383.70 17.05 o -9 5 1 415.92 436.42 18.22 o -7 5 1 279.24 300.88 10.27 o -5 5 1 14.61 21.04 2.14 o -3 5 1 553.90 566.37 14.37 o -1 5 1 1254.23 1280.95 29.05 o 1 5 1 1872.82 1862.96 40.97 o 3 5 1 29.42 35.12 3.23 o 5 5 1 2006.12 1896.46 34.22 o 7 5 1 331.63 325.18 10.41 o 9 5 1 698.73 719.42 19.18 o 11 5 1 9.65 17.02 2.87 o 13 5 1 371.28 359.93 12.06 o -10 6 1 82.90 94.96 7.75 o -8 6 1 920.89 920.50 33.33 o -6 6 1 96.65 117.05 8.14 o -4 6 1 1088.95 1119.05 26.42 o -2 6 1 44.38 43.75 3.42 o 0 6 1 813.67 859.46 21.10 o 2 6 1 140.47 169.03 6.56 o 4 6 1 586.09 615.11 16.14 o 6 6 1 8.89 7.75 3.10 o 8 6 1 98.86 98.45 8.14 o -18 0 2 5.04 6.98 1.94 o -16 0 2 22.26 27.13 2.71 o -14 0 2 1157.67 1139.10 34.88 o -12 0 2 9210.40 9637.17 279.06 o -10 0 2 4619.21 5187.50 106.61 o -8 0 2 12547.43 12308.73 252.14 o -6 0 2 2759.36 2789.01 57.55 o -4 0 2 4403.45 4836.64 99.35 o -2 0 2 9236.28 9204.23 190.20 o 0 0 2 9323.88 9790.02 200.88 o 2 0 2 2184.04 2322.44 48.23 o 4 0 2 1803.71 2058.44 60.85 o 6 0 2 8022.24 8171.35 237.20 o 8 0 2 4.55 13.18 1.94 o 10 0 2 1027.90 998.02 31.39 o 12 0 2 642.07 610.83 20.54 o 14 0 2 1902.53 1930.92 59.30 o 16 0 2 356.72 359.29 13.95 o -21 1 2 597.31 587.18 21.32 o -19 1 2 176.15 153.48 7.75 o -17 1 2 2530.20 2489.04 75.58 o -15 1 2 164.06 152.28 4.37 o -13 1 2 435.30 413.97 7.71 o -11 1 2 1602.94 1471.29 25.35 o -9 1 2 8.56 4.15 1.43 o -7 1 2 6208.27 6075.51 323.89 o -5 1 2 3488.50 3647.87 53.24 o -3 1 2 11248.56 11012.10 160.07 o -1 1 2 1957.14 2050.09 34.91 o 1 1 2 43964.17 37870.97 634.39 o 3 1 2 414.29 493.16 9.09 o 5 1 2 7590.07 7656.30 128.22 o 7 1 2 330.90 278.17 7.11 o 9 1 2 2707.91 2721.28 57.28 o 11 1 2 186.88 194.75 5.85 o 13 1 2 2418.63 2437.29 51.93 o 15 1 2 59.29 72.87 5.43 o 17 1 2 42.58 62.01 5.43 o -20 2 2 246.56 274.41 12.79 o -18 2 2 281.14 297.66 13.18 o -16 2 2 1623.81 1620.08 51.16 o -14 2 2 20.61 30.62 3.49 o -12 2 2 3887.98 3795.96 112.79 o -10 2 2 139.49 155.42 7.36 o -8 2 2 2398.30 2257.27 67.83 o -6 2 2 1842.21 1866.86 31.84 o -4 2 2 4595.50 4741.77 79.81 o -2 2 2 2141.93 2286.47 39.01 o 0 2 2 98.39 118.22 3.56 o 4 2 2 50.88 65.49 2.04 o 6 2 2 1650.96 1516.96 34.80 o 8 2 2 53.41 46.41 2.22 o 10 2 2 1073.99 1024.79 22.98 o 12 2 2 1206.90 1181.14 26.39 o 14 2 2 143.48 136.82 8.14 o 16 2 2 177.17 174.02 9.69 o 18 2 2 69.98 83.33 6.59 o -19 3 2 76.79 77.90 6.59 o -17 3 2 978.56 963.52 33.33 o -15 3 2 383.70 377.50 15.89 o -13 3 2 151.23 163.17 8.53 o -11 3 2 1255.54 1265.84 40.70 o -9 3 2 297.89 295.34 12.01 o -7 3 2 1797.00 1830.14 31.53 o -5 3 2 1418.09 1378.91 29.86 o -3 3 2 3214.77 3175.48 66.32 o -1 3 2 116.78 110.28 3.84 o 1 3 2 3573.44 3640.11 75.91 o 3 3 2 19.13 32.61 2.04 o 5 3 2 415.50 419.63 10.48 o 7 3 2 56.46 55.41 2.91 o 9 3 2 547.01 538.41 13.02 o 11 3 2 335.27 318.98 13.95 o 13 3 2 368.40 381.77 16.28 o 15 3 2 74.92 67.83 6.20 o -18 4 2 103.90 98.83 7.75 o -16 4 2 10.23 8.53 3.10 o -14 4 2 615.16 570.52 22.09 o -12 4 2 286.92 269.37 12.79 o -10 4 2 461.14 458.89 18.22 o -8 4 2 136.12 127.75 5.04 o -6 4 2 102.32 93.41 3.63 o -4 4 2 118.28 115.11 4.36 o -2 4 2 13.45 12.62 1.64 o 0 4 2 968.84 954.77 21.79 o 2 4 2 587.32 522.68 13.00 o 4 4 2 588.36 564.93 13.94 o 6 4 2 1469.37 1473.26 32.56 o 8 4 2 121.55 110.98 4.26 o 10 4 2 112.27 115.50 7.75 o 12 4 2 65.79 49.61 5.81 o 14 4 2 261.60 264.72 13.57 o -15 5 2 5.40 4.65 2.71 o -13 5 2 114.13 105.42 8.14 o -11 5 2 133.70 146.89 9.30 o -9 5 2 352.67 329.06 14.73 o -7 5 2 301.35 291.65 8.55 o -5 5 2 330.47 334.66 9.55 o -3 5 2 6.39 8.30 1.77 o -1 5 2 304.20 322.72 7.61 o 1 5 2 128.96 151.44 5.61 o 3 5 2 137.42 130.79 5.19 o 5 5 2 37.17 43.36 3.68 o 7 5 2 35.32 29.46 4.65 o 9 5 2 1.41 1.94 2.33 o 11 5 2 97.86 99.22 8.14 o -12 6 2 6.59 5.04 3.10 o -10 6 2 0.59 3.88 2.71 o -8 6 2 75.36 64.34 6.59 o -6 6 2 3.13 2.71 2.71 o -4 6 2 29.51 33.01 3.10 o -2 6 2 290.28 282.97 9.18 o 0 6 2 9.79 11.18 2.13 o 2 6 2 159.81 159.68 6.40 o 4 6 2 17.39 17.05 2.74 o 6 6 2 18.04 21.17 3.01 o 8 6 2 49.53 52.58 4.38 o -21 1 3 20.09 24.42 3.49 o -19 1 3 334.41 359.29 13.95 o -17 1 3 172.54 160.38 4.65 o -13 1 3 427.92 444.41 10.37 o -11 1 3 5.44 4.79 0.52 o -9 1 3 3444.86 3830.32 64.52 o -7 1 3 1195.28 1274.44 22.00 o -5 1 3 419.84 398.23 7.46 o -3 1 3 213.43 248.03 4.99 o -1 1 3 2749.39 2961.19 61.53 o 1 1 3 32.80 38.77 1.92 o 3 1 3 571.93 638.66 14.52 o 5 1 3 886.00 939.85 20.82 o 7 1 3 125.72 156.18 5.04 o 9 1 3 44.00 50.43 2.71 o 11 1 3 38.48 41.88 2.71 o 13 1 3 182.29 170.95 5.85 o 15 1 3 98.63 100.00 6.59 o 17 1 3 155.91 155.42 8.91 o -22 2 3 51.99 62.79 5.81 o -20 2 3 26.29 19.77 3.49 o -18 2 3 148.00 140.69 8.14 o -16 2 3 3.29 9.69 2.71 o -14 2 3 0.31 -0.78 1.16 o -12 2 3 18.06 27.13 3.10 o -10 2 3 1097.80 1125.92 35.66 o -8 2 3 27.68 53.76 1.51 o -6 2 3 1720.83 1773.66 30.43 o -4 2 3 291.14 353.19 8.63 o -2 2 3 2602.02 2624.15 54.95 o 0 2 3 1050.46 1126.15 26.55 o 2 2 3 2347.65 2436.57 51.38 o 4 2 3 564.55 590.22 13.82 o 6 2 3 1316.75 1220.42 26.84 o 8 2 3 41.48 33.04 2.14 o 10 2 3 135.50 128.00 4.56 o 12 2 3 14.90 13.56 1.86 o 14 2 3 6.83 11.24 3.10 o 16 2 3 31.83 21.70 3.88 o -21 3 3 250.74 263.17 12.79 o -19 3 3 597.32 587.18 22.48 o -17 3 3 420.89 430.21 17.44 o -15 3 3 2770.42 2631.28 81.00 o -13 3 3 754.23 794.93 27.52 o -11 3 3 1773.39 1778.22 55.42 o -9 3 3 798.49 806.64 14.57 o -7 3 3 2467.06 2456.55 51.92 o -5 3 3 775.63 827.11 18.76 o -3 3 3 3083.05 3234.31 67.83 o -1 3 3 542.35 552.05 25.97 o 1 3 3 50.61 74.58 3.25 o 3 3 3 1083.87 1088.35 24.37 o 5 3 3 25.63 24.28 1.86 o 7 3 3 57.82 52.96 2.79 o 9 3 3 151.22 169.23 5.58 o 11 3 3 988.66 921.67 32.17 o 13 3 3 19.99 17.05 3.88 o 15 3 3 286.31 282.55 13.95 o -18 4 3 310.55 310.45 14.73 o -16 4 3 422.48 422.85 18.22 o -14 4 3 82.49 91.86 6.98 o -12 4 3 217.21 220.53 10.85 o -10 4 3 1534.29 1505.08 32.80 o -8 4 3 39.13 46.26 1.95 o -6 4 3 638.03 634.84 15.32 o -4 4 3 20.11 13.13 1.64 o -2 4 3 2958.75 2946.60 62.49 o 0 4 3 338.05 312.87 8.76 o 2 4 3 2543.90 2451.92 52.61 o 4 4 3 1.90 1.42 1.21 o 6 4 3 847.63 834.54 19.80 o 8 4 3 127.70 141.08 8.91 o 10 4 3 372.08 399.21 17.44 o 12 4 3 8.00 7.75 3.10 o -15 5 3 229.07 232.55 12.79 o -13 5 3 567.45 572.07 22.87 o -11 5 3 161.28 163.17 9.69 o -9 5 3 682.04 644.16 24.42 o -7 5 3 1757.55 1735.83 38.47 o -5 5 3 29.58 30.55 1.99 o -3 5 3 750.65 688.37 18.60 o -1 5 3 89.01 90.74 4.11 o 1 5 3 191.62 195.19 6.68 o 3 5 3 0.14 2.13 1.37 o 5 5 3 901.17 887.93 21.45 o 7 5 3 44.75 44.96 5.43 o 9 5 3 158.73 157.75 10.08 o -12 6 3 162.27 181.77 11.63 o -10 6 3 125.89 125.96 8.91 o -8 6 3 287.79 304.25 14.73 o -6 6 3 59.05 69.11 5.23 o -4 6 3 1.84 2.13 1.64 o -2 6 3 203.90 211.93 6.18 o 0 6 3 199.08 194.67 5.89 o 2 6 3 491.17 491.58 13.67 o 4 6 3 9.49 11.24 3.49 o 6 6 3 552.70 629.82 25.19 o -20 0 4 1524.90 1648.38 50.39 o -18 0 4 2255.46 2200.68 66.28 o -16 0 4 2200.60 2221.22 66.66 o -14 0 4 991.62 951.51 29.84 o -12 0 4 319.49 282.16 10.08 o -8 0 4 1992.93 2194.87 65.11 o -6 0 4 6881.50 7376.03 213.94 o -4 0 4 3101.97 3204.12 94.18 o -2 0 4 2898.15 2938.63 86.82 o 0 0 4 2465.30 2567.72 75.97 o 2 0 4 4303.24 4214.16 123.64 o 4 0 4 30.03 13.95 1.94 o 6 0 4 5097.36 5022.26 147.67 o 8 0 4 122.21 88.37 5.43 o 10 0 4 1614.21 1663.11 51.94 o 12 0 4 184.50 193.01 9.30 o 14 0 4 1534.10 1508.07 48.06 o -21 1 4 519.24 494.55 18.22 o -19 1 4 157.92 192.63 8.91 o -17 1 4 548.94 604.20 14.06 o -15 1 4 300.90 275.47 5.62 o -13 1 4 13.59 11.55 1.53 o -11 1 4 7112.40 7280.36 121.95 o -9 1 4 183.11 216.10 4.53 o -7 1 4 3915.80 3898.29 65.79 o -5 1 4 3562.62 3556.66 73.86 o -3 1 4 2880.21 3025.88 63.03 o -1 1 4 215.29 188.79 12.40 o 1 1 4 4124.49 4236.84 87.97 o 3 1 4 0.39 5.20 1.16 o 5 1 4 330.64 384.11 9.85 o 7 1 4 1646.09 1551.97 33.98 o 9 1 4 1.79 0.61 1.16 o 11 1 4 258.16 252.23 11.05 o 13 1 4 355.13 348.74 9.98 o 15 1 4 130.25 149.61 8.91 o -22 2 4 20.60 18.99 3.88 o -20 2 4 599.14 610.05 22.48 o -18 2 4 160.42 156.19 8.53 o -16 2 4 4121.71 4044.40 120.92 o -14 2 4 931.06 869.34 29.07 o -12 2 4 1825.24 1887.91 32.50 o -10 2 4 3058.12 3013.03 51.23 o -8 2 4 540.82 593.05 13.15 o -6 2 4 3684.39 3599.86 74.95 o -4 2 4 4608.75 4860.35 100.58 o -2 2 4 7776.81 8225.29 169.10 o 0 2 4 870.34 902.66 20.42 o 2 2 4 7318.20 7244.64 149.50 o 4 2 4 1405.77 1603.49 34.94 o 6 2 4 859.23 840.84 19.44 o 8 2 4 79.64 81.09 3.63 o 10 2 4 876.63 849.93 21.32 o 12 2 4 539.20 565.48 21.70 o 14 2 4 522.31 537.19 21.32 o -21 3 4 285.82 305.41 14.34 o -19 3 4 122.70 147.67 8.91 o -17 3 4 704.94 693.38 25.58 o -15 3 4 497.07 500.37 19.38 o -13 3 4 280.98 234.49 10.85 o -11 3 4 2754.01 2661.56 45.47 o -9 3 4 118.03 123.30 4.08 o -7 3 4 358.65 361.57 9.27 o -5 3 4 372.02 355.40 9.50 o -3 3 4 868.75 746.31 17.40 o -1 3 4 250.47 256.49 7.26 o 1 3 4 699.99 673.07 16.16 o 3 3 4 767.23 694.19 21.70 o 5 3 4 0.95 0.22 0.93 o 7 3 4 1075.11 1033.81 23.92 o 9 3 4 8.33 5.69 1.58 o 11 3 4 232.71 222.86 11.63 o 13 3 4 47.38 43.80 5.43 o -18 4 4 148.58 172.09 10.46 o -16 4 4 4.76 4.26 2.71 o -14 4 4 20.69 13.18 3.49 o -12 4 4 1.43 -1.55 1.94 o -10 4 4 97.72 113.65 10.85 o -8 4 4 441.44 411.30 10.87 o -6 4 4 1310.54 1269.24 28.49 o -4 4 4 255.65 220.82 6.84 o -2 4 4 229.99 214.13 12.01 o 0 4 4 91.28 89.38 3.97 o 2 4 4 206.44 227.12 7.23 o 4 4 4 548.24 510.95 15.50 o 6 4 4 315.74 322.52 9.49 o 8 4 4 8.34 7.75 3.10 o 10 4 4 22.57 22.09 4.26 o 12 4 4 13.77 20.15 4.26 o -17 5 4 40.65 41.47 5.81 o -15 5 4 24.98 26.74 4.65 o -13 5 4 88.58 77.90 6.98 o -11 5 4 17.25 15.89 3.88 o -9 5 4 378.71 395.88 10.98 o -7 5 4 0.36 1.59 1.36 o -5 5 4 2.35 2.24 1.21 o -3 5 4 2.40 3.64 2.13 o -1 5 4 1.98 1.46 2.52 o 1 5 4 3.82 2.96 1.55 o 3 5 4 31.94 37.89 3.29 o 5 5 4 23.27 19.83 2.42 o 7 5 4 285.97 310.45 15.12 o 9 5 4 27.45 25.58 5.04 o -12 6 4 64.50 51.55 6.59 o -10 6 4 157.91 157.36 10.08 o -8 6 4 4.07 8.91 3.49 o -6 6 4 73.42 68.21 4.08 o -4 6 4 114.10 122.10 5.61 o -2 6 4 62.14 68.09 4.11 o 0 6 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