#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/61/2236147.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236147_Fobs loop_ _publ_author_name 'Rivera, Augusto' 'Camacho, Jairo' 'R\'ios-Motta, Jaime' 'Ku\H-1,3-benzoxazine) monohydrate ; _journal_coeditor_code BX2424 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2734 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90 _cell_angle_beta 91.153(2) _cell_angle_gamma 90 _cell_length_a 30.2999(9) _cell_length_b 5.2132(2) _cell_length_c 11.6058(4) _exptl_crystal_F_000 800 _reflns_d_resolution_high 0.8365 _[local]_cod_data_source_file bx2424Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 230.10 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1124.42 1135.56 11.60 o 4 0 0 9884.60 10101.80 45.22 o 6 0 0 1325.89 1459.04 22.09 o 8 0 0 505.15 435.56 11.81 o 10 0 0 2948.00 2712.10 32.32 o 12 0 0 618.80 520.84 14.49 o 14 0 0 56.01 90.34 6.56 o 16 0 0 1176.03 1177.69 21.54 o 18 0 0 52.50 69.26 4.26 o 20 0 0 8.80 17.68 3.27 o 22 0 0 281.71 280.50 8.69 o 24 0 0 73.91 72.32 5.15 o 26 0 0 647.44 640.72 12.42 o 28 0 0 9.20 11.05 4.04 < 30 0 0 77.58 79.92 6.05 o 32 0 0 530.79 509.61 12.42 o 34 0 0 234.60 241.12 7.81 o 36 0 0 143.12 134.52 8.10 o 1 1 0 11760.90 11542.60 48.40 o 3 1 0 3908.34 3663.13 18.70 o 5 1 0 38245.10 38331.10 77.91 o 7 1 0 368.90 333.14 7.33 o 9 1 0 4514.27 4407.34 26.96 o 11 1 0 5254.97 5238.67 28.50 o 13 1 0 45.53 29.23 4.85 o 15 1 0 2277.80 2165.98 21.97 o 17 1 0 304.94 271.98 5.21 o 19 1 0 108.01 108.91 3.50 o 21 1 0 1446.09 1432.68 11.36 o 23 1 0 124.04 123.31 4.27 o 25 1 0 31.45 28.92 3.29 o 27 1 0 128.28 120.54 4.83 o 29 1 0 1058.82 1118.52 11.36 o 31 1 0 269.95 284.39 6.96 o 33 1 0 16.92 22.79 2.77 o 35 1 0 636.37 643.60 7.99 o 0 2 0 306.36 288.65 7.93 o 2 2 0 2034.60 1896.44 14.11 o 4 2 0 293.68 274.41 7.12 o 6 2 0 1054.04 1026.69 11.72 o 8 2 0 237.25 243.43 6.94 o 10 2 0 12465.60 12608.60 63.37 o 12 2 0 5.54 9.27 4.92 < 14 2 0 1138.05 942.98 9.43 o 16 2 0 2413.67 2435.41 15.91 o 18 2 0 39.34 37.85 3.92 o 20 2 0 73.88 71.22 4.41 o 22 2 0 440.25 420.69 7.59 o 24 2 0 709.51 741.27 9.90 o 26 2 0 25.86 22.82 3.31 o 28 2 0 342.89 330.61 7.19 o 30 2 0 55.17 42.13 3.18 o 32 2 0 4.99 4.56 1.92 < 34 2 0 143.90 149.96 6.11 o 1 3 0 397.72 359.82 8.24 o 3 3 0 304.19 315.16 6.93 o 5 3 0 116.42 106.75 4.24 o 7 3 0 66.85 57.57 3.07 o 9 3 0 56.83 58.09 2.91 o 11 3 0 41.61 49.75 2.99 o 13 3 0 20.80 20.11 2.22 o 15 3 0 436.58 455.75 7.89 o 17 3 0 156.62 160.40 5.70 o 19 3 0 4085.07 4142.77 25.66 o 21 3 0 1545.62 1528.00 14.51 o 23 3 0 47.40 42.78 4.70 o 25 3 0 361.32 356.46 7.76 o 27 3 0 3.80 3.22 2.94 < 29 3 0 1.42 -1.94 2.46 < 31 3 0 124.28 91.75 3.89 o 0 4 0 342.74 313.88 11.47 o 2 4 0 30.48 36.07 4.02 o 4 4 0 479.19 482.95 10.02 o 6 4 0 16.11 8.00 3.51 < 8 4 0 1354.34 1429.50 16.64 o 10 4 0 507.38 550.60 9.78 o 12 4 0 4.75 5.77 3.17 < 14 4 0 4860.71 4944.54 29.51 o 16 4 0 4.56 4.06 3.83 < 18 4 0 97.70 99.86 6.56 o 20 4 0 177.20 178.40 10.34 o 22 4 0 52.90 49.83 6.66 o 24 4 0 23.31 17.09 4.65 o 26 4 0 197.80 205.44 7.26 o 1 5 0 319.43 305.03 14.26 o 3 5 0 706.15 701.36 19.93 o 5 5 0 1978.86 2004.82 23.04 o 7 5 0 25.11 28.69 4.58 o 9 5 0 1804.10 1896.07 21.41 o 11 5 0 20.72 14.26 3.94 o 13 5 0 234.25 232.62 7.80 o 15 5 0 133.45 129.30 7.07 o 17 5 0 2.66 2.10 4.92 < 19 5 0 1.70 0.49 5.91 < 21 5 0 13.27 10.06 3.89 < 0 6 0 1337.95 1358.66 19.13 o 2 6 0 412.89 402.86 8.63 o 4 6 0 518.55 496.64 10.37 o 6 6 0 17.48 11.46 2.90 o 8 6 0 2.39 7.12 3.18 < -35 1 1 95.71 93.86 3.99 o -33 1 1 524.17 562.96 8.93 o -31 1 1 158.10 157.35 5.17 o -29 1 1 560.92 570.55 8.54 o -27 1 1 3.63 5.52 2.56 < -25 1 1 1053.05 1058.05 11.31 o -23 1 1 256.80 264.86 5.84 o -21 1 1 31.00 25.02 2.73 o -19 1 1 371.75 383.22 5.66 o -17 1 1 309.67 296.19 5.31 o -15 1 1 114.08 121.59 7.14 o -13 1 1 1487.27 1576.17 17.76 o -11 1 1 12.31 5.09 3.56 < -9 1 1 3735.93 3231.63 26.47 o -7 1 1 814.52 790.59 10.39 o -5 1 1 10978.10 10757.40 31.71 o -3 1 1 358.03 340.07 6.59 o -1 1 1 66.16 73.31 3.59 o 1 1 1 174.20 238.26 7.24 o 3 1 1 4130.99 4060.38 18.30 o 5 1 1 51886.30 52945.90 107.21 o 7 1 1 20879.00 20332.10 84.88 o 9 1 1 4221.12 4195.41 25.52 o 11 1 1 124.25 117.03 4.85 o 13 1 1 221.87 231.91 6.99 o 15 1 1 71.91 92.34 6.00 o 17 1 1 335.74 387.88 6.12 o 19 1 1 260.40 275.14 5.09 o 21 1 1 24.14 23.53 2.89 o 23 1 1 58.16 70.94 3.82 o 25 1 1 548.52 584.70 8.84 o 27 1 1 41.66 43.11 3.29 o 29 1 1 1043.26 1127.96 13.15 o 31 1 1 1636.10 1731.71 14.52 o 33 1 1 32.47 32.48 2.88 o 35 1 1 574.42 571.94 9.22 o -34 2 1 8.49 1.65 2.21 < -32 2 1 199.81 213.48 5.20 o -30 2 1 1451.22 1467.85 14.04 o -28 2 1 757.90 734.70 9.80 o -26 2 1 35.98 38.30 3.52 o -24 2 1 660.30 713.09 10.52 o -22 2 1 191.47 191.20 5.59 o -20 2 1 74.18 60.94 4.54 o -18 2 1 1432.49 1444.10 15.37 o -16 2 1 1119.80 1106.40 12.06 o -14 2 1 16.20 17.70 3.31 o -12 2 1 1.05 1.71 4.58 < -10 2 1 180.96 173.07 7.39 o -8 2 1 93.58 108.35 5.23 o -6 2 1 657.10 701.05 13.89 o -4 2 1 29.88 24.70 3.25 o -2 2 1 23.81 21.45 3.74 o 0 2 1 105.40 98.34 5.78 o 2 2 1 1178.85 1200.76 17.68 o 4 2 1 29.84 19.34 4.29 o 6 2 1 1066.74 1253.79 12.81 o 8 2 1 2067.30 2071.82 18.78 o 10 2 1 15086.10 15415.90 55.72 o 12 2 1 2914.03 2717.23 25.13 o 14 2 1 487.66 553.76 6.87 o 16 2 1 4582.10 4692.05 21.96 o 18 2 1 374.50 346.15 6.67 o 20 2 1 2915.03 3059.47 17.94 o 22 2 1 485.78 472.62 7.79 o 24 2 1 5304.36 5491.82 24.45 o 26 2 1 664.52 656.89 9.87 o 28 2 1 0.72 0.82 2.75 < 30 2 1 283.57 280.46 5.72 o 32 2 1 143.24 132.29 4.46 o 34 2 1 0.32 1.13 2.35 < -31 3 1 94.47 110.24 4.63 o -29 3 1 157.26 171.30 5.85 o -27 3 1 8.26 16.24 2.98 o -25 3 1 210.26 221.87 5.89 o -23 3 1 511.11 491.36 8.78 o -21 3 1 0.37 1.00 3.89 < -19 3 1 2323.79 2397.44 20.84 o -17 3 1 152.52 148.15 5.23 o -15 3 1 1082.66 1064.48 12.12 o -13 3 1 0.11 -5.85 2.68 < -11 3 1 283.47 279.33 5.94 o -9 3 1 0.74 1.16 2.22 < -7 3 1 48.82 36.07 2.86 o -5 3 1 166.68 158.35 4.96 o -3 3 1 162.68 161.12 5.42 o -1 3 1 510.50 520.59 9.01 o 1 3 1 235.54 274.04 6.71 o 3 3 1 3.73 2.43 2.81 < 5 3 1 181.49 202.77 5.29 o 7 3 1 610.72 667.21 8.04 o 9 3 1 1240.68 1363.87 10.27 o 11 3 1 136.92 134.26 4.01 o 13 3 1 25.93 25.82 2.68 o 15 3 1 6381.95 6581.76 28.32 o 17 3 1 4265.11 4326.26 23.44 o 19 3 1 7533.23 7821.88 36.45 o 21 3 1 2540.20 2506.21 19.78 o 23 3 1 26.11 20.04 4.89 o 25 3 1 237.06 240.52 7.27 o 27 3 1 7.52 4.90 2.97 < 29 3 1 24.93 24.11 2.71 o 31 3 1 65.61 63.79 4.63 o -26 4 1 111.34 125.62 6.53 o -24 4 1 351.70 372.55 9.36 o -22 4 1 169.13 175.88 6.80 o -20 4 1 685.18 721.18 12.89 o -18 4 1 168.05 158.48 6.64 o -16 4 1 91.18 98.22 6.23 o -14 4 1 848.30 854.17 14.06 o -12 4 1 2967.09 3117.72 23.52 o -10 4 1 1829.58 1877.51 18.12 o -8 4 1 15.05 15.03 3.70 o -6 4 1 270.25 313.30 9.20 o -4 4 1 122.81 103.55 5.29 o -2 4 1 27.45 22.41 3.97 o 0 4 1 877.00 902.43 14.37 o 2 4 1 11.42 6.65 3.13 < 4 4 1 34.00 30.32 3.77 o 6 4 1 180.40 158.40 7.17 o 8 4 1 104.83 107.79 5.24 o 10 4 1 3737.95 3857.76 27.26 o 12 4 1 6.00 0.21 3.32 < 14 4 1 1510.86 1548.27 19.76 o 16 4 1 8.77 21.03 4.62 o 18 4 1 25.74 32.12 6.06 o 20 4 1 873.15 899.51 16.61 o 22 4 1 14.01 8.90 5.04 < 24 4 1 0.01 9.24 4.17 < 26 4 1 591.90 601.64 10.44 o -21 5 1 53.89 61.66 4.49 o -19 5 1 20.45 16.97 5.16 o -17 5 1 40.19 30.33 5.49 o -15 5 1 91.88 85.04 5.84 o -13 5 1 41.23 38.87 5.09 o -11 5 1 1645.39 1691.18 19.51 o -9 5 1 1783.13 1863.64 19.42 o -7 5 1 856.09 852.21 13.52 o -5 5 1 17.05 13.31 3.96 o -3 5 1 494.73 524.66 15.59 o -1 5 1 0.97 -16.88 5.88 < 1 5 1 63.64 56.59 6.52 o 3 5 1 865.21 823.42 16.95 o 5 5 1 90.70 101.99 7.89 o 7 5 1 451.90 469.76 11.04 o 9 5 1 415.52 407.02 11.80 o 11 5 1 70.53 74.92 5.99 o 13 5 1 84.55 80.88 6.22 o 15 5 1 142.02 145.36 9.16 o 17 5 1 6.44 5.40 4.48 < 19 5 1 34.39 47.98 6.18 o 21 5 1 204.40 202.35 8.20 o -8 6 1 48.11 49.09 5.71 o -6 6 1 15.15 14.20 4.79 < -4 6 1 138.00 136.09 6.14 o -2 6 1 1397.97 1374.61 17.53 o 0 6 1 13.72 11.30 2.81 o 2 6 1 928.55 943.49 14.56 o 4 6 1 256.05 259.79 6.63 o 6 6 1 66.67 71.34 5.30 o 8 6 1 3.97 9.78 3.97 < -34 0 2 3450.43 3646.42 30.27 o -32 0 2 10.05 11.43 3.53 o -30 0 2 2.62 3.87 3.84 < -28 0 2 678.88 676.44 12.79 o -26 0 2 150.64 174.07 7.11 o -24 0 2 6.91 -0.07 3.36 < -22 0 2 1897.57 2064.90 21.10 o -20 0 2 2710.68 2788.66 23.51 o -18 0 2 7618.95 7842.96 39.11 o -16 0 2 687.41 685.31 17.10 o -14 0 2 10566.10 10945.00 50.76 o -12 0 2 233.59 187.31 8.36 o -10 0 2 28.99 35.29 5.41 o -8 0 2 132.31 101.25 6.86 o -6 0 2 6698.99 6047.64 58.75 o -4 0 2 10185.20 9977.92 73.22 o -2 0 2 40420.00 41083.80 130.09 o 0 0 2 15790.40 15080.80 68.27 o 2 0 2 4596.46 4758.51 40.88 o 4 0 2 2242.51 2153.31 24.26 o 6 0 2 13744.30 12838.10 48.97 o 8 0 2 558.96 557.28 9.16 o 10 0 2 3892.53 3771.85 25.93 o 12 0 2 4.44 2.64 2.83 < 14 0 2 1166.85 1175.06 15.73 o 16 0 2 493.88 418.23 12.34 o 18 0 2 564.92 528.19 9.39 o 20 0 2 189.26 190.41 5.74 o 22 0 2 0.00 -1.59 3.69 < 24 0 2 128.81 145.29 6.95 o 26 0 2 1087.57 1045.62 16.12 o 28 0 2 1329.74 1399.71 20.33 o 30 0 2 1968.27 2061.51 25.48 o 32 0 2 510.59 542.54 13.98 o 34 0 2 1129.62 1195.38 17.49 o -35 1 2 163.67 162.04 5.17 o -33 1 2 383.59 380.91 7.82 o -31 1 2 87.11 91.10 3.98 o -29 1 2 120.60 107.34 4.77 o -27 1 2 7.96 7.18 2.59 < -25 1 2 107.13 108.18 4.79 o -23 1 2 1267.03 1235.45 12.46 o -21 1 2 149.10 151.39 4.89 o -19 1 2 2494.60 2593.61 16.20 o -17 1 2 129.86 133.82 4.49 o -15 1 2 539.90 548.76 13.49 o -13 1 2 5469.24 5757.39 39.18 o -11 1 2 92.14 116.37 6.96 o -9 1 2 16116.90 15955.50 59.98 o -7 1 2 2577.52 2452.94 20.79 o -5 1 2 11890.70 11076.10 36.83 o -3 1 2 6107.17 5863.34 42.77 o -1 1 2 2946.25 2915.07 25.48 o 1 1 2 18144.20 18040.20 57.39 o 3 1 2 2669.37 2633.36 17.49 o 5 1 2 627.43 605.58 7.95 o 7 1 2 9901.76 9365.87 44.10 o 9 1 2 1665.83 1620.02 17.07 o 11 1 2 38.29 76.95 4.54 o 13 1 2 0.27 1.32 3.40 < 15 1 2 85.92 113.63 5.55 o 17 1 2 194.23 215.75 4.35 o 19 1 2 5.07 2.50 2.44 < 21 1 2 474.12 426.55 7.18 o 23 1 2 70.39 62.19 3.93 o 25 1 2 199.04 223.60 5.99 o 27 1 2 2174.44 2270.31 17.14 o 29 1 2 1779.94 1807.29 15.50 o 31 1 2 984.94 1019.44 11.00 o 33 1 2 60.48 71.25 3.91 o 35 1 2 28.67 31.27 3.24 o -32 2 2 223.27 216.89 4.84 o -30 2 2 155.72 161.55 5.04 o -28 2 2 137.49 142.02 4.94 o -26 2 2 514.64 510.87 9.60 o -24 2 2 1773.96 1760.83 17.19 o -22 2 2 4.31 1.62 3.72 < -20 2 2 0.33 -0.29 3.52 < -18 2 2 3.34 -1.20 4.69 < -16 2 2 0.00 -1.84 4.18 < -14 2 2 633.54 634.04 9.83 o -12 2 2 0.70 -2.55 3.21 < -10 2 2 2428.00 2380.15 27.86 o -8 2 2 6064.62 6150.87 36.94 o -6 2 2 20.52 35.88 3.50 o -4 2 2 981.19 1125.46 15.69 o -2 2 2 0.37 3.76 3.57 < 0 2 2 483.20 467.54 11.53 o 2 2 2 1848.77 1978.24 21.33 o 4 2 2 787.10 815.13 14.66 o 6 2 2 63.62 104.18 5.48 o 8 2 2 3205.24 3520.54 30.69 o 10 2 2 1193.10 1131.25 18.17 o 12 2 2 7120.51 6784.31 23.71 o 14 2 2 656.21 611.88 7.68 o 16 2 2 774.16 755.03 9.24 o 18 2 2 534.16 546.51 8.03 o 20 2 2 2188.87 2290.79 16.91 o 22 2 2 495.50 509.04 8.83 o 24 2 2 267.01 286.38 6.76 o 26 2 2 2255.50 2301.13 15.87 o 28 2 2 340.29 312.25 6.71 o 30 2 2 132.35 133.54 4.57 o 32 2 2 42.52 37.82 2.92 o -31 3 2 0.03 -1.56 2.52 < -29 3 2 7.84 13.70 2.50 o -27 3 2 43.87 37.70 3.13 o -25 3 2 197.70 175.52 5.33 o -23 3 2 30.13 21.97 4.00 o -21 3 2 101.84 103.12 5.58 o -19 3 2 311.97 333.09 7.74 o -17 3 2 1029.39 1046.98 14.82 o -15 3 2 2785.51 2870.91 21.50 o -13 3 2 990.13 1069.13 12.82 o -11 3 2 407.22 402.92 7.68 o -9 3 2 225.87 217.03 5.36 o -7 3 2 57.01 63.97 3.70 o -5 3 2 9.19 8.50 2.69 o -3 3 2 244.90 259.19 6.01 o -1 3 2 966.18 1059.88 11.48 o 1 3 2 57.83 72.99 3.76 o 3 3 2 146.75 161.15 5.06 o 5 3 2 2688.30 3030.05 17.82 o 7 3 2 769.65 830.06 9.02 o 9 3 2 555.23 598.78 7.79 o 11 3 2 1160.23 1149.35 10.89 o 13 3 2 610.06 636.62 8.72 o 15 3 2 21.42 20.17 3.14 o 17 3 2 410.72 390.54 8.14 o 19 3 2 1057.12 1024.85 13.78 o 21 3 2 499.37 444.38 9.88 o 23 3 2 10.37 11.50 4.43 < 25 3 2 136.27 134.58 5.10 o 27 3 2 148.82 163.26 4.87 o 29 3 2 101.77 106.39 4.77 o 31 3 2 0.19 -1.03 4.16 < -26 4 2 73.76 66.36 4.11 o -24 4 2 217.85 236.51 6.68 o -22 4 2 377.95 371.89 9.12 o -20 4 2 586.53 603.92 12.82 o -18 4 2 407.25 404.35 12.30 o -16 4 2 199.65 181.84 7.32 o -14 4 2 1040.45 1123.77 15.60 o -12 4 2 355.03 373.23 9.67 o -10 4 2 111.30 122.92 6.61 o -8 4 2 1089.70 1099.71 14.98 o -6 4 2 567.63 536.61 10.38 o -4 4 2 85.38 101.66 5.62 o -2 4 2 22.65 26.79 4.33 o 0 4 2 879.90 897.52 16.13 o 2 4 2 25.69 25.61 3.52 o 4 4 2 2.32 0.49 3.22 < 6 4 2 28.32 29.98 3.17 o 8 4 2 160.19 146.55 7.32 o 10 4 2 786.33 835.88 15.47 o 12 4 2 55.40 36.99 4.17 o 14 4 2 110.43 98.08 6.90 o 16 4 2 106.32 87.03 7.16 o 18 4 2 8.72 5.02 5.51 < 20 4 2 44.27 57.08 6.78 o 22 4 2 2412.88 2333.48 23.82 o 24 4 2 17.81 15.90 4.29 o 26 4 2 819.21 776.81 12.47 o -21 5 2 6.13 1.99 3.92 < -19 5 2 0.04 7.94 4.11 < -17 5 2 12.21 8.98 3.72 < -15 5 2 238.74 244.61 9.12 o -13 5 2 732.44 756.09 14.74 o -11 5 2 0.67 5.47 3.61 < -9 5 2 745.78 745.30 11.74 o -7 5 2 1791.07 1878.76 20.57 o -5 5 2 424.76 418.18 11.11 o -3 5 2 17.62 19.42 3.95 o -1 5 2 23.29 11.04 4.89 < 1 5 2 22.41 4.14 5.21 < 3 5 2 11.74 4.53 4.34 < 5 5 2 208.41 201.73 9.54 o 7 5 2 95.04 77.63 6.66 o 9 5 2 175.36 170.43 8.06 o 11 5 2 72.95 67.32 5.70 o 13 5 2 11.26 7.92 5.05 < 15 5 2 22.14 30.05 5.58 o 17 5 2 84.23 90.85 7.48 o 19 5 2 135.97 138.29 7.95 o -8 6 2 109.85 109.21 10.82 o -6 6 2 32.85 28.17 5.43 o -4 6 2 304.67 292.39 9.93 o -2 6 2 1212.14 1228.75 19.22 o 0 6 2 48.76 55.24 5.31 o 2 6 2 128.90 117.29 5.36 o 4 6 2 538.26 552.53 14.53 o 6 6 2 28.82 38.62 5.18 o -35 1 3 30.39 31.39 4.17 o -33 1 3 9.01 6.86 2.73 < -31 1 3 722.29 728.87 10.63 o -29 1 3 749.31 767.32 10.92 o -27 1 3 1618.99 1644.73 15.10 o -25 1 3 109.69 101.23 4.75 o -23 1 3 321.21 306.41 6.95 o -21 1 3 6.24 12.43 2.81 o -19 1 3 253.94 282.87 6.53 o -17 1 3 279.46 342.62 6.60 o -15 1 3 0.50 5.94 3.39 < -13 1 3 2409.86 2626.99 27.74 o -11 1 3 3143.17 3291.78 25.98 o -9 1 3 3742.24 3852.69 33.37 o -7 1 3 1380.07 1489.78 18.47 o -5 1 3 2407.35 2454.09 20.54 o -3 1 3 5327.59 4581.83 25.88 o -1 1 3 933.40 913.09 12.44 o 1 1 3 1918.87 1757.77 18.89 o 3 1 3 6780.52 6727.81 31.95 o 5 1 3 6.34 7.95 3.24 < 7 1 3 199.26 185.88 7.15 o 9 1 3 2394.43 2396.67 22.04 o 11 1 3 12413.60 12865.70 47.40 o 13 1 3 62.11 63.48 4.23 o 15 1 3 63.47 75.93 2.94 o 17 1 3 29.56 42.07 2.99 o 19 1 3 100.79 107.74 3.92 o 21 1 3 456.18 491.55 7.28 o 23 1 3 41.72 50.95 3.32 o 25 1 3 371.02 393.65 6.77 o 27 1 3 744.93 781.18 9.88 o 29 1 3 32.82 31.32 3.70 o 31 1 3 386.33 405.48 7.67 o 33 1 3 117.24 122.75 4.78 o -32 2 3 48.62 44.48 3.11 o -30 2 3 0.00 -1.65 2.43 < -28 2 3 104.57 95.24 4.23 o -26 2 3 545.38 513.68 9.54 o -24 2 3 396.12 352.68 8.48 o -22 2 3 338.05 296.41 7.16 o -20 2 3 260.70 282.21 8.27 o -18 2 3 175.72 198.47 8.34 o -16 2 3 1357.26 1422.30 15.04 o -14 2 3 1852.12 1921.12 15.96 o -12 2 3 3979.74 3941.26 22.94 o -10 2 3 3453.19 3546.22 37.42 o -8 2 3 3072.35 3515.65 32.91 o -6 2 3 2055.61 2176.44 20.11 o -4 2 3 7797.55 8030.10 45.92 o -2 2 3 229.62 231.20 8.52 o 0 2 3 116.72 137.13 5.87 o 2 2 3 842.11 846.64 15.76 o 4 2 3 297.72 254.41 8.27 o 6 2 3 5656.89 6032.93 38.84 o 8 2 3 10949.10 11948.20 62.01 o 10 2 3 2948.54 3420.98 23.22 o 12 2 3 915.32 923.05 9.35 o 14 2 3 577.86 623.04 7.44 o 16 2 3 28.95 25.58 3.06 o 18 2 3 107.20 105.17 4.25 o 20 2 3 43.42 44.17 3.56 o 22 2 3 2342.21 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962.11 11.24 o -11 1 8 697.60 666.60 11.04 o -9 1 8 75.42 78.50 4.19 o -7 1 8 19.33 11.63 2.99 o -5 1 8 4.42 9.06 2.70 o -3 1 8 314.46 303.58 6.13 o -1 1 8 609.95 609.65 7.61 o 1 1 8 1006.89 956.29 8.57 o 3 1 8 410.57 428.01 6.67 o 5 1 8 240.85 240.42 5.34 o 7 1 8 41.72 45.35 3.11 o 9 1 8 1191.77 1205.81 10.83 o 11 1 8 2884.71 2873.90 17.44 o 13 1 8 2737.70 2792.23 16.95 o 15 1 8 44.47 53.45 3.29 o 17 1 8 643.35 632.44 8.40 o 19 1 8 12.70 7.18 3.04 < 21 1 8 282.45 278.77 6.90 o 23 1 8 203.54 216.38 5.80 o 25 1 8 860.67 837.72 11.44 o 27 1 8 34.45 37.94 3.07 o -26 2 8 28.53 19.95 2.32 o -24 2 8 172.68 198.14 5.86 o -22 2 8 58.83 59.78 3.83 o -20 2 8 541.30 518.87 9.03 o -18 2 8 362.05 378.47 8.14 o -16 2 8 219.82 217.08 6.41 o -14 2 8 107.26 114.50 5.20 o -12 2 8 0.13 -2.00 4.07 < -10 2 8 861.98 879.17 13.05 o -8 2 8 3492.46 3524.86 21.86 o -6 2 8 1768.05 1755.23 15.57 o -4 2 8 0.02 -2.92 2.88 < -2 2 8 62.06 62.68 3.87 o 0 2 8 209.92 221.00 5.71 o 2 2 8 25.18 23.97 3.28 o 4 2 8 2847.58 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341.33 6.72 o 3 1 9 87.49 76.51 4.19 o 5 1 9 451.22 438.69 7.81 o 7 1 9 722.20 689.24 9.72 o 9 1 9 1904.02 1919.53 15.42 o 11 1 9 1683.14 1760.60 15.30 o 13 1 9 62.78 57.46 3.84 o 15 1 9 397.55 429.32 7.65 o 17 1 9 1.79 9.54 3.62 < 19 1 9 125.70 109.99 5.46 o 21 1 9 472.28 488.45 9.82 o 23 1 9 113.00 124.70 5.55 o 25 1 9 623.22 682.54 11.84 o -24 2 9 616.47 752.90 10.18 o -22 2 9 2.04 3.59 2.26 < -20 2 9 26.23 26.74 3.11 o -18 2 9 51.68 52.80 3.59 o -16 2 9 161.26 169.43 5.93 o -14 2 9 571.46 537.83 9.12 o -12 2 9 478.92 525.71 10.03 o -10 2 9 1836.63 1826.04 19.39 o -8 2 9 3287.43 3428.48 26.43 o -6 2 9 78.30 80.75 4.67 o -4 2 9 467.72 473.56 9.25 o -2 2 9 45.88 47.09 3.73 o 0 2 9 135.01 123.11 4.51 o 2 2 9 2808.64 2894.19 20.94 o 4 2 9 2703.96 2821.01 18.47 o 6 2 9 1605.68 1660.49 15.23 o 8 2 9 388.16 363.63 7.19 o 10 2 9 162.92 147.49 5.54 o 12 2 9 205.61 196.88 5.89 o 14 2 9 2.01 -0.27 2.96 < 16 2 9 7.59 0.71 3.08 < 18 2 9 24.81 18.40 3.31 o 20 2 9 1.86 3.39 2.94 < 22 2 9 18.47 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3.05 o -5 1 10 551.68 489.02 8.25 o -3 1 10 528.30 471.87 8.12 o -1 1 10 20.87 24.30 3.07 o 1 1 10 0.06 0.19 3.35 < 3 1 10 31.94 26.65 3.93 o 5 1 10 186.65 186.14 6.27 o 7 1 10 2073.05 2130.87 17.77 o 9 1 10 0.27 -6.80 3.06 < 11 1 10 3300.37 3387.24 22.81 o 13 1 10 9.39 7.79 3.38 < 15 1 10 0.34 2.68 2.72 < 17 1 10 689.97 718.17 10.52 o 19 1 10 55.98 65.71 4.51 o 21 1 10 1166.83 1215.78 14.77 o 23 1 10 326.65 338.10 9.33 o -22 2 10 10.61 9.53 2.59 o -20 2 10 0.01 0.44 2.73 < -18 2 10 57.19 54.26 3.84 o -16 2 10 86.23 77.16 4.05 o -14 2 10 285.62 234.94 6.10 o -12 2 10 274.61 284.86 6.74 o -10 2 10 103.59 93.99 4.82 o -8 2 10 549.33 559.92 9.17 o -6 2 10 33.90 33.68 3.77 o -4 2 10 243.53 234.18 6.96 o -2 2 10 349.15 339.25 7.25 o 0 2 10 23.49 25.62 3.09 o 2 2 10 2967.12 2975.14 18.95 o 4 2 10 196.28 196.03 6.27 o 6 2 10 95.48 88.11 4.30 o 8 2 10 154.23 150.74 5.57 o 10 2 10 184.04 196.55 5.84 o 12 2 10 481.29 502.28 8.60 o 14 2 10 8.73 4.51 2.94 < 16 2 10 9.53 5.51 2.85 < 18 2 10 40.11 46.19 3.92 o 20 2 10 1.24 0.27 3.05 < -17 3 10 20.46 29.00 2.79 o -15 3 10 34.79 24.26 4.75 o -13 3 10 106.26 112.50 6.04 o -11 3 10 272.71 285.22 8.04 o -9 3 10 96.01 97.03 5.26 o -7 3 10 1062.69 1102.25 14.49 o -5 3 10 5.19 6.12 3.49 < -3 3 10 513.14 537.67 10.49 o -1 3 10 171.08 166.55 6.21 o 1 3 10 166.26 177.14 6.03 o 3 3 10 140.92 135.30 5.69 o 5 3 10 256.46 246.73 6.44 o 7 3 10 105.66 105.72 4.95 o 9 3 10 84.70 87.91 4.30 o 11 3 10 87.23 84.16 3.98 o 13 3 10 150.23 157.55 5.35 o 15 3 10 346.64 432.88 7.87 o 17 3 10 112.70 99.00 5.66 o -10 4 10 6.13 17.33 7.68 < -8 4 10 18.51 20.62 4.38 o -6 4 10 2.03 -1.97 3.66 < -4 4 10 118.28 127.42 6.38 o -2 4 10 255.86 278.37 7.56 o 0 4 10 175.89 180.28 7.10 o 2 4 10 987.31 985.78 15.27 o 4 4 10 765.57 702.05 16.41 o 6 4 10 1159.12 1111.81 15.42 o 8 4 10 1.06 -2.41 2.72 < -21 1 11 7.32 3.31 2.58 < -19 1 11 2.05 4.17 2.67 < -17 1 11 87.97 72.61 3.69 o -15 1 11 5.43 9.15 2.28 o -13 1 11 246.67 249.83 5.93 o -11 1 11 646.20 674.25 8.90 o -9 1 11 621.88 599.06 7.81 o -7 1 11 452.49 426.08 7.46 o -5 1 11 556.62 541.53 7.91 o -3 1 11 270.56 312.32 7.08 o -1 1 11 112.99 109.76 5.41 o 1 1 11 65.60 60.36 4.39 o 3 1 11 421.50 413.72 8.44 o 5 1 11 58.12 51.01 4.38 o 7 1 11 355.63 373.64 8.34 o 9 1 11 0.57 2.61 3.46 < 11 1 11 21.25 11.22 3.04 o 13 1 11 5.70 2.94 2.77 < 15 1 11 10.74 11.77 2.81 o 17 1 11 401.80 404.17 8.55 o 19 1 11 100.91 106.69 4.96 o -18 2 11 259.74 252.71 8.11 o -16 2 11 48.22 39.24 2.91 o -14 2 11 425.03 390.26 6.62 o -12 2 11 556.43 529.79 7.85 o -10 2 11 19.96 19.45 2.55 o -8 2 11 152.89 150.93 5.23 o -6 2 11 154.83 158.96 5.47 o -4 2 11 296.63 300.92 6.72 o -2 2 11 140.40 143.57 5.38 o 0 2 11 58.33 62.14 3.61 o 2 2 11 8.27 12.64 2.82 o 4 2 11 11.43 11.66 2.54 o 6 2 11 42.50 36.43 3.09 o 8 2 11 131.03 139.27 5.20 o 10 2 11 60.07 65.29 4.21 o 12 2 11 202.51 220.33 7.05 o 14 2 11 20.59 16.06 3.28 o 16 2 11 149.05 142.94 6.28 o 18 2 11 0.25 3.16 3.17 < -13 3 11 3.20 5.28 3.14 < -11 3 11 35.49 31.28 3.33 o -9 3 11 10.39 7.73 2.78 < -7 3 11 413.25 425.91 8.32 o -5 3 11 0.01 3.62 2.45 < -3 3 11 0.07 2.19 2.44 < -1 3 11 312.72 321.61 7.62 o 1 3 11 55.11 56.10 3.79 o 3 3 11 55.35 53.76 4.03 o 5 3 11 62.33 57.50 3.86 o 7 3 11 74.83 61.66 4.18 o 9 3 11 124.30 128.86 5.17 o 11 3 11 21.09 21.22 3.57 o -18 0 12 266.43 329.48 12.75 o -16 0 12 606.96 681.42 15.57 o -14 0 12 290.19 283.78 7.77 o -12 0 12 379.55 391.24 8.88 o -10 0 12 214.75 237.65 7.62 o -8 0 12 0.26 5.69 3.27 < -6 0 12 2030.15 2039.24 24.76 o -4 0 12 188.11 172.76 7.56 o -2 0 12 4453.70 4335.63 31.11 o 0 0 12 273.90 299.04 8.36 o 2 0 12 203.39 178.10 9.52 o 4 0 12 6.23 9.95 5.46 < 6 0 12 187.12 187.55 9.26 o 8 0 12 127.35 136.47 7.98 o 10 0 12 52.05 52.81 5.51 o 12 0 12 548.09 512.98 13.70 o 14 0 12 515.31 486.35 14.33 o 16 0 12 14.25 18.85 4.62 o -17 1 12 282.58 311.85 7.85 o -15 1 12 94.33 92.71 3.60 o -13 1 12 0.92 1.56 1.92 < -11 1 12 8.64 17.63 2.46 o -9 1 12 74.65 85.82 3.50 o -7 1 12 1604.89 1561.77 13.06 o -5 1 12 76.65 76.66 4.11 o -3 1 12 5.51 0.69 2.90 < -1 1 12 59.37 54.08 3.98 o 1 1 12 5.06 1.35 3.02 < 3 1 12 1432.14 1430.09 14.78 o 5 1 12 148.45 168.15 5.41 o 7 1 12 6.00 11.59 2.88 o 9 1 12 272.83 254.62 6.78 o 11 1 12 6.88 4.20 3.10 < 13 1 12 331.73 330.83 8.26 o 15 1 12 17.54 19.70 3.93 o -14 2 12 48.32 60.41 4.66 o -12 2 12 341.80 307.70 6.80 o -10 2 12 28.78 19.25 2.35 o -8 2 12 74.78 78.22 3.73 o -6 2 12 198.73 212.48 5.62 o -4 2 12 0.06 -0.19 2.52 < -2 2 12 3.73 3.25 2.92 < 0 2 12 111.57 101.42 4.54 o 2 2 12 3.39 -2.55 2.25 < 4 2 12 164.71 170.59 4.89 o 6 2 12 314.08 323.89 6.71 o 8 2 12 1160.37 1171.89 12.77 o 10 2 12 0.11 -0.57 2.38 < 12 2 12 0.63 1.92 2.53 < -5 3 12 128.78 126.32 5.55 o -3 3 12 778.71 838.57 13.34 o -1 3 12 55.91 50.95 4.14 o 1 3 12 0.11 -0.46 2.27 < 3 3 12 376.17 356.93 12.32 o -11 1 13 383.07 405.02 8.65 o -9 1 13 17.73 23.14 2.60 o -7 1 13 52.60 39.06 3.08 o -5 1 13 415.40 492.03 7.87 o -3 1 13 9.91 18.88 2.45 o -1 1 13 258.39 253.22 5.72 o 1 1 13 231.17 233.18 5.96 o 3 1 13 1452.96 1461.93 13.67 o 5 1 13 3.67 3.34 2.30 < 7 1 13 265.39 260.17 8.44 o 9 1 13 163.51 193.40 7.10 o -4 2 13 45.92 46.27 3.77 o -2 2 13 91.53 96.57 5.04 o 0 2 13 353.01 391.30 9.06 o 2 2 13 609.72 689.31 13.28 o 4 2 13 2.60 5.84 3.74 <