#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:44:17 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181283 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/61/2236170.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236170_Fobs loop_ _publ_author_name 'Alieva, Guloy' 'Ashurov, Jamshid' 'Mukhamedov, Nasir' 'Parpiev, Nusrat' _publ_section_title ; A new polymorph of 2-(2H-benzotriazol-2-yl)acetic acid ; _journal_coeditor_code DS2205 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2833 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.703 _cell_angle_gamma 90.000 _cell_length_a 11.7190 _cell_length_b 8.3080 _cell_length_c 17.2460 _exptl_crystal_F_000 736.00 _reflns_d_resolution_high 0.8368 _cod_data_source_file ds2205Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' II' _shelx_refln_list_code 4 _shelx_f_calc_maximum 217.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 178.95 162.01 4.00 o 6 0 0 1139.37 1264.22 10.77 o 8 0 0 615.16 714.82 11.54 o 10 0 0 257.92 251.09 9.60 o 12 0 0 718.50 731.65 12.43 o 1 1 0 1633.12 1646.89 7.60 o 3 1 0 1471.10 1290.64 23.89 o 5 1 0 114.10 138.80 4.66 o 7 1 0 236.85 226.84 3.10 o 9 1 0 228.20 217.53 9.76 o 11 1 0 116.05 114.58 3.33 o 13 1 0 0.43 -1.88 3.23 o 0 2 0 14292.77 14269.90 29.68 o 2 2 0 11747.79 11732.94 23.99 o 4 2 0 547.01 603.73 5.52 o 6 2 0 39.70 48.13 1.84 o 8 2 0 107.18 109.43 3.06 o 10 2 0 72.77 73.31 4.28 o 12 2 0 1.11 7.22 2.58 o 1 3 0 1515.47 1647.87 9.43 o 3 3 0 156.37 187.97 3.93 o 5 3 0 3801.90 3802.29 14.15 o 7 3 0 323.22 329.47 5.04 o 9 3 0 0.14 1.50 2.60 o 11 3 0 206.28 184.21 4.34 o 13 3 0 34.50 34.89 4.61 o 0 4 0 80.06 86.61 3.07 o 2 4 0 0.12 0.88 1.70 o 4 4 0 466.67 453.76 4.58 o 6 4 0 352.43 369.80 5.23 o 8 4 0 2.38 -1.54 2.97 o 10 4 0 23.95 22.09 2.84 o 12 4 0 20.12 17.94 3.84 o 1 5 0 427.24 436.70 5.95 o 3 5 0 11.69 16.98 1.91 o 5 5 0 225.75 211.26 4.83 o 7 5 0 354.86 342.95 6.58 o 9 5 0 51.46 44.03 4.69 o 11 5 0 1.21 5.24 3.10 o 0 6 0 2101.76 2056.43 24.94 o 2 6 0 187.51 190.74 5.74 o 4 6 0 0.00 1.53 2.57 o 6 6 0 17.95 13.22 3.65 o 8 6 0 9.08 11.11 2.99 o 10 6 0 12.94 19.90 3.15 o 1 7 0 0.03 -3.09 4.04 o 3 7 0 204.22 181.20 6.11 o 5 7 0 359.55 355.26 5.41 o 7 7 0 37.17 39.49 2.50 o 9 7 0 22.24 21.45 3.00 o 0 8 0 87.00 91.51 7.32 o 2 8 0 33.82 25.77 4.83 o 4 8 0 180.37 194.54 4.34 o 6 8 0 95.56 102.03 2.76 o 8 8 0 10.34 11.89 2.50 o 1 9 0 1.71 4.21 3.93 o 3 9 0 0.44 -1.96 3.19 o 5 9 0 2.15 1.76 2.44 o -13 1 1 25.47 20.03 2.67 o -11 1 1 33.55 26.80 2.47 o -9 1 1 188.77 181.36 4.36 o -7 1 1 3.09 2.91 1.35 o -5 1 1 504.43 531.48 9.61 o -3 1 1 13042.25 12895.59 20.65 o -1 1 1 2638.18 2543.65 7.41 o 1 1 1 4672.66 4593.45 11.06 o 3 1 1 0.25 2.17 0.76 o 5 1 1 175.49 198.99 2.90 o 7 1 1 1324.36 1430.42 17.02 o 9 1 1 36.81 30.93 2.95 o 11 1 1 53.03 48.96 3.21 o 13 1 1 143.60 150.23 4.78 o -12 2 1 39.67 47.57 2.65 o -10 2 1 7.90 7.47 5.20 o -8 2 1 315.28 297.31 4.33 o -6 2 1 375.13 370.72 4.30 o -4 2 1 107.56 110.20 2.11 o -2 2 1 3354.93 3603.00 12.75 o 0 2 1 9142.95 9513.65 17.99 o 2 2 1 2632.61 2730.75 28.83 o 4 2 1 13.85 3.27 1.36 o 6 2 1 972.57 977.11 9.13 o 8 2 1 27.92 25.92 2.39 o 10 2 1 128.99 125.76 3.41 o 12 2 1 103.94 101.19 3.27 o -13 3 1 21.91 22.77 3.40 o -11 3 1 17.00 19.77 2.92 o -9 3 1 5.75 6.90 2.90 o -7 3 1 82.17 77.55 3.79 o -5 3 1 1088.48 1012.48 7.29 o -3 3 1 1965.99 2072.26 23.28 o -1 3 1 1.50 1.45 0.92 o 1 3 1 797.54 816.83 10.96 o 3 3 1 721.75 740.83 48.80 o 5 3 1 50.07 37.80 1.55 o 7 3 1 124.38 103.09 2.94 o 9 3 1 78.83 70.00 3.98 o 11 3 1 0.01 0.35 3.63 o 13 3 1 42.34 41.12 3.02 o -12 4 1 28.49 22.76 2.58 o -10 4 1 2.09 0.17 2.76 o -8 4 1 443.06 416.40 8.05 o -6 4 1 50.38 55.62 3.62 o -4 4 1 344.89 345.00 4.00 o -2 4 1 168.78 140.64 2.71 o 0 4 1 1453.06 1479.47 8.02 o 2 4 1 924.79 940.12 6.52 o 4 4 1 119.86 115.97 3.46 o 6 4 1 71.09 76.61 3.35 o 8 4 1 0.23 -0.36 2.89 o 10 4 1 20.80 16.34 2.80 o 12 4 1 1.55 5.81 2.81 o -11 5 1 36.29 42.76 3.00 o -9 5 1 15.75 12.55 4.27 o -7 5 1 148.09 139.02 4.50 o -5 5 1 20.77 25.04 3.42 o -3 5 1 271.62 293.15 4.47 o -1 5 1 106.96 109.36 3.18 o 1 5 1 1687.35 1670.86 11.60 o 3 5 1 537.08 515.81 11.03 o 5 5 1 638.14 608.46 8.11 o 7 5 1 204.21 215.16 6.51 o 9 5 1 19.43 13.26 4.62 o 11 5 1 4.45 8.86 4.24 o -10 6 1 2.94 -0.87 2.70 o -8 6 1 57.17 51.54 2.64 o -6 6 1 22.76 28.45 4.34 o -4 6 1 808.67 791.68 12.92 o -2 6 1 0.20 0.21 2.71 o 0 6 1 112.07 120.47 10.24 o 2 6 1 162.80 165.79 5.23 o 4 6 1 169.70 169.73 4.71 o 6 6 1 121.62 103.11 3.93 o 8 6 1 9.19 14.79 2.87 o 10 6 1 7.99 2.92 2.97 o -9 7 1 13.51 17.01 4.35 o -7 7 1 69.06 71.25 2.39 o -5 7 1 289.02 297.52 4.98 o -3 7 1 57.20 52.87 4.58 o -1 7 1 58.29 53.39 4.18 o 1 7 1 186.69 192.30 6.21 o 3 7 1 224.68 221.98 6.72 o 5 7 1 1.48 -2.52 3.13 o 7 7 1 2.65 5.95 3.67 o 9 7 1 47.51 46.47 5.22 o -8 8 1 0.05 -1.14 2.73 o -6 8 1 12.71 13.81 2.32 o -4 8 1 13.96 17.15 4.35 o -2 8 1 136.13 154.88 5.38 o 0 8 1 58.32 68.15 4.96 o 2 8 1 65.20 78.98 4.73 o 4 8 1 3.26 -0.78 3.27 o 6 8 1 37.68 38.71 2.30 o 8 8 1 33.36 33.72 2.20 o -5 9 1 31.91 29.17 2.86 o -3 9 1 0.07 1.85 3.13 o -1 9 1 56.15 60.59 4.03 o 1 9 1 83.69 80.87 5.38 o 3 9 1 19.54 22.09 3.19 o 5 9 1 2.08 5.57 3.86 o -12 0 2 23.30 24.98 4.61 o -10 0 2 35.04 35.92 5.93 o -8 0 2 545.54 497.66 8.40 o -6 0 2 583.14 596.98 9.64 o -4 0 2 2340.29 2012.69 56.80 o -2 0 2 1854.79 1681.64 10.63 o 0 0 2 2827.12 2602.23 8.51 o 2 0 2 7685.53 7191.94 13.48 o 4 0 2 4312.70 4767.45 21.10 o 6 0 2 1945.02 1949.09 13.52 o 8 0 2 648.55 665.14 8.06 o 10 0 2 10.95 16.89 6.63 o 12 0 2 10.38 11.16 4.12 o -13 1 2 121.22 124.14 3.29 o -11 1 2 0.73 3.20 2.50 o -9 1 2 240.53 251.79 8.88 o -7 1 2 1280.59 1253.14 16.48 o -5 1 2 40.31 48.63 1.83 o -3 1 2 28029.62 27133.56 891.16 o -1 1 2 25356.06 24246.35 365.03 o 1 1 2 371.16 320.94 2.50 o 3 1 2 289.64 292.29 3.21 o 5 1 2 7.83 4.36 1.07 o 7 1 2 337.89 334.62 5.55 o 9 1 2 9.60 12.58 3.06 o 11 1 2 57.90 58.12 2.87 o 13 1 2 41.38 45.65 2.86 o -12 2 2 0.05 -0.97 2.47 o -8 2 2 202.84 207.13 3.69 o -6 2 2 1175.50 1158.12 21.29 o -4 2 2 7520.39 8470.83 89.82 o -2 2 2 47421.88 48087.59 738.41 o 0 2 2 1820.97 1952.86 8.18 o 2 2 2 13.99 18.67 1.85 o 4 2 2 478.41 528.34 7.19 o 6 2 2 199.98 204.51 4.05 o 8 2 2 512.38 477.32 7.06 o 10 2 2 482.14 462.85 6.17 o 12 2 2 87.88 99.80 4.16 o -13 3 2 9.43 4.27 3.55 o -11 3 2 3.80 4.43 2.68 o -9 3 2 696.50 688.65 11.37 o -7 3 2 441.25 445.76 5.10 o -5 3 2 779.94 877.58 6.68 o -3 3 2 34.48 25.86 2.04 o -1 3 2 2673.44 2891.49 32.19 o 1 3 2 991.18 957.50 18.11 o 3 3 2 274.33 318.22 4.57 o 5 3 2 152.42 152.30 3.54 o 7 3 2 22.53 21.63 2.34 o 9 3 2 239.71 251.40 8.25 o 11 3 2 0.01 -2.16 3.49 o 13 3 2 72.57 81.37 6.15 o -12 4 2 55.46 50.76 4.36 o -10 4 2 189.77 171.64 4.35 o -8 4 2 15.41 11.93 2.82 o -6 4 2 14.53 19.36 2.46 o -4 4 2 2772.43 3002.50 22.09 o -2 4 2 7809.30 8343.66 30.59 o 0 4 2 2184.17 2246.21 22.36 o 2 4 2 1100.16 1114.20 7.34 o 4 4 2 461.97 466.43 5.38 o 6 4 2 51.44 55.03 2.68 o 8 4 2 298.11 304.68 6.18 o 10 4 2 325.65 325.55 6.01 o 12 4 2 164.18 175.73 15.82 o -11 5 2 6.38 6.19 3.05 o -9 5 2 0.21 -0.81 3.32 o -7 5 2 43.63 41.34 2.90 o -5 5 2 12.98 10.80 3.25 o -3 5 2 178.75 159.54 3.56 o -1 5 2 157.47 170.01 3.76 o 1 5 2 11.01 10.67 2.12 o 3 5 2 612.70 603.86 9.19 o 5 5 2 79.09 91.46 5.47 o 7 5 2 13.38 10.59 3.32 o 9 5 2 115.42 99.39 4.08 o 11 5 2 0.35 4.76 3.68 o -10 6 2 0.38 1.88 3.30 o -8 6 2 183.51 173.88 4.08 o -6 6 2 110.76 106.68 9.20 o -4 6 2 8.98 8.48 3.19 o -2 6 2 4.98 3.30 2.43 o 0 6 2 5.11 11.16 2.58 o 2 6 2 0.02 1.96 2.69 o 4 6 2 209.85 207.78 6.33 o 6 6 2 38.73 40.77 3.11 o 8 6 2 18.95 12.87 2.75 o 10 6 2 29.55 33.66 2.61 o -9 7 2 4.81 6.98 5.23 o -7 7 2 73.30 83.24 4.77 o -5 7 2 0.31 5.64 4.71 o -3 7 2 526.90 525.01 9.75 o -1 7 2 235.02 218.89 6.62 o 1 7 2 3.94 2.19 4.41 o 3 7 2 360.00 298.23 38.40 o 5 7 2 110.81 121.85 3.33 o 7 7 2 3.52 8.55 2.94 o 9 7 2 109.71 107.82 2.52 o -8 8 2 0.07 -3.13 3.13 o -6 8 2 19.80 17.23 2.69 o -4 8 2 3.33 2.08 4.51 o -2 8 2 0.00 -0.52 4.60 o 0 8 2 2.96 4.59 3.80 o 2 8 2 91.71 102.24 5.07 o 4 8 2 27.80 31.79 3.21 o 6 8 2 26.25 34.06 2.49 o -5 9 2 53.28 49.41 3.37 o -3 9 2 30.91 32.03 3.00 o -1 9 2 10.78 11.98 3.23 o 1 9 2 95.18 91.32 3.64 o 3 9 2 282.54 310.61 5.75 o 5 9 2 102.96 113.89 4.10 o -13 1 3 30.99 26.38 3.05 o -11 1 3 43.51 44.05 2.99 o -9 1 3 0.55 8.06 3.75 o -7 1 3 1274.90 1188.02 7.68 o -5 1 3 6.47 10.69 1.73 o -3 1 3 3032.09 3207.87 67.14 o -1 1 3 2729.07 2664.41 14.61 o 1 1 3 762.62 674.98 4.02 o 3 1 3 4124.29 4155.03 58.56 o 5 1 3 3478.66 3851.41 12.82 o 7 1 3 12.68 15.95 2.09 o 9 1 3 7.33 8.48 3.19 o 11 1 3 29.46 24.66 3.06 o 13 1 3 0.00 10.35 3.38 o -12 2 3 0.92 3.02 3.04 o -10 2 3 1.08 2.61 4.83 o -8 2 3 157.81 163.20 4.68 o -6 2 3 749.85 783.42 8.55 o -4 2 3 67.17 56.12 2.46 o -2 2 3 37322.20 36077.89 48.28 o 0 2 3 11631.08 11446.65 43.51 o 2 2 3 2022.51 2025.88 49.10 o 4 2 3 1318.94 1411.48 8.03 o 6 2 3 0.00 3.31 1.74 o 8 2 3 33.41 31.55 3.45 o 10 2 3 739.87 745.55 7.63 o 12 2 3 356.41 393.14 6.44 o -13 3 3 21.51 20.78 4.79 o -11 3 3 52.52 43.75 3.05 o -9 3 3 35.16 32.75 3.09 o -7 3 3 19.93 21.61 2.18 o -5 3 3 1055.95 1048.53 14.90 o -3 3 3 2.42 4.80 1.54 o -1 3 3 1154.78 1215.50 13.21 o 1 3 3 1691.71 1718.68 69.89 o 3 3 3 369.91 408.84 7.96 o 5 3 3 87.57 112.81 3.21 o 7 3 3 126.95 116.04 7.07 o 9 3 3 100.76 96.36 4.51 o 11 3 3 0.21 2.14 7.78 o -12 4 3 0.19 0.30 3.52 o -10 4 3 29.32 25.55 2.83 o -8 4 3 3.03 -0.20 3.04 o -6 4 3 115.73 121.16 4.85 o -4 4 3 1908.30 1963.57 35.11 o -2 4 3 754.77 786.84 6.20 o 0 4 3 95.40 103.50 2.75 o 2 4 3 141.81 136.95 4.57 o 4 4 3 395.92 389.56 7.94 o 6 4 3 105.23 130.29 3.93 o 8 4 3 7.29 5.02 3.92 o 10 4 3 9.72 7.26 3.00 o 12 4 3 21.36 27.35 5.29 o -11 5 3 2.36 0.05 3.70 o -9 5 3 22.26 27.35 3.95 o -7 5 3 181.72 182.37 4.37 o -5 5 3 15.73 12.11 4.73 o -3 5 3 1.12 0.82 2.02 o -1 5 3 772.32 805.07 10.83 o 1 5 3 224.89 221.58 4.45 o 3 5 3 382.57 375.44 7.66 o 5 5 3 28.92 33.57 3.06 o 7 5 3 238.47 217.93 5.55 o 9 5 3 5.56 -0.90 3.66 o 11 5 3 19.39 20.30 4.74 o -10 6 3 40.19 37.62 4.60 o -8 6 3 129.45 126.26 3.03 o -6 6 3 1191.90 1174.71 17.12 o -4 6 3 602.84 568.08 10.05 o -2 6 3 2.87 1.94 2.46 o 0 6 3 432.40 396.82 6.52 o 2 6 3 9.79 6.66 2.98 o 4 6 3 0.47 8.98 4.63 o 6 6 3 381.71 391.87 6.20 o 8 6 3 1.78 2.69 2.74 o 10 6 3 14.99 10.70 2.91 o -9 7 3 3.56 5.30 4.74 o -7 7 3 6.90 6.97 2.81 o -5 7 3 36.44 39.69 3.41 o -3 7 3 293.94 272.56 7.18 o -1 7 3 83.31 68.89 4.38 o 1 7 3 109.50 107.52 3.95 o 3 7 3 182.90 196.05 6.27 o 5 7 3 198.07 208.92 4.60 o 7 7 3 16.55 23.36 3.81 o 9 7 3 8.99 5.56 2.10 o -8 8 3 1.51 0.61 2.77 o -6 8 3 0.56 -1.83 2.80 o -4 8 3 122.95 126.00 4.22 o -2 8 3 171.96 178.13 6.14 o 0 8 3 39.66 27.05 4.21 o 2 8 3 15.24 17.10 3.93 o 4 8 3 119.65 120.93 3.66 o 6 8 3 0.72 1.08 2.30 o -5 9 3 60.48 58.32 3.27 o -3 9 3 25.85 26.85 3.93 o -1 9 3 60.70 73.42 2.79 o 1 9 3 10.75 16.70 2.73 o 3 9 3 33.57 34.03 2.98 o 5 9 3 0.04 2.69 3.37 o -12 0 4 164.11 165.72 10.21 o -10 0 4 685.53 658.41 15.28 o -8 0 4 795.61 720.85 14.68 o -6 0 4 1105.60 1191.41 11.05 o -4 0 4 158.26 159.64 5.00 o -2 0 4 5525.99 5513.43 37.16 o 0 0 4 1095.02 1053.41 36.10 o 2 0 4 86.08 110.53 2.57 o 4 0 4 597.54 538.37 9.26 o 6 0 4 1898.42 1771.62 20.48 o 8 0 4 593.17 568.22 9.67 o 10 0 4 225.27 238.74 7.17 o 12 0 4 36.51 44.55 5.56 o -13 1 4 30.42 30.62 3.13 o -11 1 4 77.49 83.52 3.10 o -9 1 4 21.62 29.13 3.07 o -7 1 4 534.31 585.18 11.39 o -5 1 4 284.62 309.02 4.10 o -3 1 4 115.42 96.47 2.33 o -1 1 4 915.95 926.66 5.41 o 1 1 4 2068.49 1958.10 27.69 o 3 1 4 81.55 73.12 2.02 o 5 1 4 137.37 138.80 4.63 o 7 1 4 114.89 115.94 3.58 o 9 1 4 113.00 110.65 3.90 o 11 1 4 480.84 494.99 8.41 o 13 1 4 147.31 152.84 6.84 o -12 2 4 32.10 29.48 2.74 o -10 2 4 172.47 150.76 6.72 o -8 2 4 136.55 150.10 3.64 o -6 2 4 0.65 -1.47 1.47 o -4 2 4 1762.95 1985.15 12.98 o -2 2 4 47.81 66.24 12.19 o 0 2 4 3660.34 3388.27 13.95 o 2 2 4 702.38 783.96 16.02 o 4 2 4 530.03 527.63 9.07 o 6 2 4 1444.63 1560.01 12.61 o 8 2 4 189.48 212.68 6.39 o 10 2 4 13.14 15.77 2.91 o 12 2 4 29.97 36.51 2.61 o -13 3 4 24.70 33.76 4.71 o -11 3 4 96.63 93.68 3.77 o -9 3 4 9.61 5.84 3.45 o -7 3 4 6.68 14.11 2.79 o -5 3 4 9087.23 10029.99 33.32 o -3 3 4 3317.65 3507.03 17.15 o -1 3 4 117.74 133.43 3.19 o 1 3 4 274.87 280.54 40.77 o 3 3 4 540.60 512.40 9.18 o 5 3 4 484.26 503.10 7.86 o 7 3 4 145.92 118.12 4.88 o 9 3 4 478.76 472.53 9.62 o 11 3 4 20.78 29.60 3.78 o -12 4 4 31.68 30.93 5.41 o -10 4 4 111.31 103.61 3.11 o -8 4 4 4.20 2.35 4.51 o -6 4 4 812.55 843.27 12.70 o -4 4 4 3986.88 4036.71 37.72 o -2 4 4 139.78 130.67 2.71 o 0 4 4 275.14 260.83 5.12 o 2 4 4 20.56 23.02 2.30 o 4 4 4 18.61 24.32 3.77 o 6 4 4 383.12 347.60 12.60 o 8 4 4 300.78 278.36 9.56 o 10 4 4 27.92 31.12 3.48 o 12 4 4 0.63 2.79 2.85 o -11 5 4 4.82 -1.00 6.79 o -9 5 4 44.72 49.67 2.96 o -7 5 4 668.09 676.93 12.57 o -5 5 4 1059.57 1008.33 12.83 o -3 5 4 410.03 412.46 11.31 o -1 5 4 173.10 187.45 3.56 o 1 5 4 1325.77 1353.33 9.39 o 3 5 4 34.66 34.11 3.10 o 5 5 4 123.54 116.78 3.99 o 7 5 4 503.33 510.14 7.22 o 9 5 4 172.64 165.14 6.52 o 11 5 4 73.20 71.72 3.99 o -10 6 4 8.52 12.25 3.75 o -8 6 4 31.45 36.64 2.56 o -6 6 4 307.69 319.83 4.64 o -4 6 4 0.01 2.17 3.87 o -2 6 4 18.65 21.39 2.47 o 0 6 4 1.22 1.17 2.42 o 2 6 4 38.11 32.80 3.04 o 4 6 4 22.28 25.46 5.22 o 6 6 4 3.49 6.33 3.37 o 8 6 4 4.07 4.39 2.80 o 10 6 4 3.90 6.40 2.77 o -9 7 4 3.99 2.56 3.02 o -7 7 4 4.14 7.66 2.73 o -5 7 4 1.99 2.78 3.49 o -3 7 4 2.83 1.34 3.78 o -1 7 4 10.70 8.66 4.87 o 1 7 4 52.74 61.59 3.58 o 3 7 4 40.55 40.00 4.74 o 5 7 4 0.40 4.58 3.76 o 7 7 4 24.93 26.32 2.97 o 9 7 4 5.11 10.07 2.01 o -8 8 4 0.09 -1.64 2.57 o -6 8 4 91.44 97.40 3.41 o -4 8 4 127.47 133.13 3.74 o -2 8 4 22.90 26.43 3.22 o 0 8 4 53.01 53.81 4.11 o 2 8 4 216.97 231.29 9.54 o 4 8 4 76.57 91.97 3.56 o 6 8 4 14.59 16.96 2.43 o -5 9 4 0.49 -2.65 2.65 o -3 9 4 8.41 6.94 3.04 o -1 9 4 0.11 -1.55 2.70 o 1 9 4 91.74 90.87 3.61 o 3 9 4 7.80 9.26 2.80 o -13 1 5 5.30 5.18 3.08 o -11 1 5 166.17 169.18 3.83 o -9 1 5 497.05 468.62 7.59 o -7 1 5 385.89 405.14 6.13 o -5 1 5 913.10 935.62 9.65 o -3 1 5 13421.67 14003.28 39.79 o -1 1 5 1322.66 1468.12 52.60 o 1 1 5 538.29 436.58 45.04 o 3 1 5 2031.26 2187.21 12.45 o 5 1 5 1002.85 1007.52 10.42 o 7 1 5 53.74 54.09 3.20 o 9 1 5 297.20 312.28 6.34 o 11 1 5 70.92 80.71 3.12 o -12 2 5 196.20 195.75 3.82 o -10 2 5 7.08 7.26 2.74 o -8 2 5 58.87 54.40 3.00 o -6 2 5 44.60 38.98 2.24 o -4 2 5 1210.57 1307.45 9.56 o -2 2 5 5511.91 5801.29 20.07 o 0 2 5 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