#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/61/2236181.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236181_Fobs loop_ _publ_author_name 'Zhao, Shunsheng' 'L\"u, Xingqiang' 'Liu, Xiangrong' _publ_section_title ; {2,2'-[Cyclohexane-1,2-diylbis(nitrilomethanylylidene)]diphenolato}copper(II) ; _journal_coeditor_code FF2080 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1215 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 108.654 _cell_angle_gamma 90.000 _cell_length_a 12.2537 _cell_length_b 24.3018 _cell_length_c 12.2969 _exptl_crystal_F_000 1592.00 _reflns_d_resolution_high 0.8377 _[local]_cod_data_source_file ff2080Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' xb5027_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 379.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1880.97 -4.65 6.21 o 2 0 0 1811.06 1959.27 167.66 o 3 0 0 130600.98 125235.48 8313.76 o 4 0 0 59001.63 49070.08 3254.98 o 5 0 0 9598.83 10249.79 697.70 o 6 0 0 5227.74 4533.41 323.45 o 7 0 0 10842.78 8096.71 559.47 o 8 0 0 3174.77 2635.00 237.49 o 9 0 0 2520.48 2554.35 301.66 o 10 0 0 1529.38 2077.34 395.61 o 11 0 0 23.97 69.81 217.20 o 12 0 0 581.79 465.42 274.60 o 13 0 0 166.93 -32.58 260.64 o 1 1 0 5458.39 4235.36 426.64 o 2 1 0 9521.48 8381.61 426.56 o 3 1 0 27354.49 24459.31 1159.36 o 4 1 0 3340.74 3908.85 195.23 o 5 1 0 13826.96 11818.85 566.28 o 6 1 0 188.99 317.58 48.38 o 7 1 0 2160.90 2304.57 169.51 o 8 1 0 4.03 484.03 139.92 o 9 1 0 1097.77 1753.84 219.21 o 10 1 0 1676.12 1899.93 213.70 o 11 1 0 147.74 -53.88 156.59 o 12 1 0 27.16 454.20 318.04 o 13 1 0 3.26 -13.87 185.39 o 0 2 0 644.30 539.89 58.95 o 1 2 0 36742.84 33482.25 4655.02 o 2 2 0 8338.56 6858.44 380.31 o 3 2 0 4452.09 3490.14 218.13 o 4 2 0 20270.34 17339.63 829.61 o 5 2 0 655.79 611.17 52.34 o 6 2 0 11326.09 9517.39 492.52 o 7 2 0 442.55 497.69 57.54 o 8 2 0 1581.35 1514.03 155.90 o 9 2 0 1062.64 1256.55 129.59 o 10 2 0 690.85 1172.47 192.62 o 11 2 0 2.96 152.99 190.05 o 12 2 0 1.20 69.77 166.32 o 13 2 0 173.12 67.89 175.48 o 1 3 0 10981.66 11269.04 620.01 o 2 3 0 3503.44 3843.07 264.55 o 3 3 0 1459.98 1579.79 129.60 o 4 3 0 2085.11 1613.44 105.54 o 5 3 0 205.34 177.57 32.28 o 6 3 0 4788.51 4856.25 238.91 o 7 3 0 205.27 219.03 48.91 o 8 3 0 1941.59 2021.61 149.50 o 9 3 0 393.20 545.58 95.47 o 10 3 0 28.77 300.68 133.65 o 11 3 0 285.03 247.38 161.46 o 12 3 0 194.43 -165.72 166.06 o 13 3 0 18.29 17.43 185.39 o 0 4 0 292.02 342.86 48.09 o 1 4 0 19138.05 19776.40 1202.49 o 2 4 0 37858.37 34880.64 1930.70 o 3 4 0 8463.49 7608.89 516.66 o 4 4 0 1707.97 1583.21 110.85 o 5 4 0 540.86 425.24 57.99 o 6 4 0 3128.49 2589.52 166.60 o 7 4 0 1283.35 918.96 80.79 o 8 4 0 167.58 390.50 84.54 o 9 4 0 5.67 69.39 80.56 o 10 4 0 20.63 69.09 127.85 o 11 4 0 255.36 400.25 148.97 o 12 4 0 180.14 10.13 169.18 o 13 4 0 0.65 70.24 183.02 o 1 5 0 13917.85 14645.60 900.09 o 2 5 0 20615.90 19467.89 1092.34 o 3 5 0 221.84 256.40 54.94 o 4 5 0 188.40 44.45 82.04 o 5 5 0 353.71 299.65 56.01 o 6 5 0 61.30 49.74 52.97 o 7 5 0 119.92 148.71 74.13 o 8 5 0 2070.44 2156.99 178.66 o 9 5 0 20.98 59.80 84.88 o 10 5 0 40.73 70.60 83.47 o 11 5 0 299.94 503.16 157.65 o 12 5 0 43.72 249.60 176.01 o 13 5 0 0.11 -350.23 233.49 o 0 6 0 9291.85 8025.03 639.35 o 1 6 0 2113.00 2028.16 123.10 o 2 6 0 26782.96 26489.44 1460.35 o 3 6 0 9228.59 9139.38 620.45 o 4 6 0 1638.11 1820.59 181.56 o 5 6 0 35.05 -20.52 62.01 o 6 6 0 4.28 -3.03 71.02 o 7 6 0 1059.22 906.24 113.47 o 8 6 0 628.59 787.89 114.28 o 9 6 0 55.55 111.34 90.21 o 10 6 0 194.16 145.71 94.67 o 11 6 0 1.67 55.54 144.74 o 12 6 0 176.05 260.35 162.93 o 13 6 0 6.32 -214.99 200.91 o 1 7 0 1957.17 1938.39 118.74 o 2 7 0 15679.13 13750.09 777.48 o 3 7 0 12076.68 11548.73 654.54 o 4 7 0 953.70 1102.16 115.00 o 5 7 0 8590.48 7895.07 562.67 o 6 7 0 177.22 106.07 76.90 o 7 7 0 563.99 609.14 146.67 o 8 7 0 257.81 389.38 98.67 o 9 7 0 1278.58 1250.07 167.95 o 10 7 0 3.44 73.79 90.00 o 11 7 0 140.41 -30.33 148.06 o 12 7 0 97.43 324.60 170.55 o 13 7 0 2.19 -86.76 215.65 o 0 8 0 1810.08 1496.16 136.80 o 1 8 0 8062.85 6990.02 398.79 o 2 8 0 16807.76 16034.17 894.72 o 3 8 0 1553.87 1809.07 119.76 o 4 8 0 24.55 30.02 60.55 o 5 8 0 3070.34 3158.51 251.17 o 6 8 0 5201.48 4992.91 375.53 o 7 8 0 1277.54 1262.40 153.17 o 8 8 0 1479.48 1801.73 294.91 o 9 8 0 132.89 282.51 130.55 o 10 8 0 100.35 43.08 94.43 o 11 8 0 95.94 162.36 154.80 o 12 8 0 186.20 90.88 167.46 o 13 8 0 185.03 308.25 212.03 o 1 9 0 9163.47 8506.46 482.02 o 2 9 0 60.99 54.83 26.43 o 3 9 0 22658.86 21041.92 1198.83 o 4 9 0 23575.49 22850.50 1580.59 o 5 9 0 462.15 583.29 124.32 o 6 9 0 1436.34 1601.38 220.21 o 7 9 0 733.77 938.39 136.97 o 8 9 0 2860.53 3014.23 234.33 o 9 9 0 102.43 78.21 96.95 o 10 9 0 1.96 -3.36 101.44 o 11 9 0 648.56 764.98 138.26 o 12 9 0 40.44 67.65 168.94 o 13 9 0 0.02 334.09 280.03 o 0 10 0 2004.40 1558.27 165.23 o 1 10 0 716.55 748.20 62.16 o 2 10 0 758.49 686.11 58.24 o 3 10 0 99.51 156.46 36.51 o 4 10 0 1608.63 1605.81 228.57 o 5 10 0 204.61 94.44 102.71 o 6 10 0 919.37 872.34 133.00 o 7 10 0 2586.34 2870.16 251.76 o 8 10 0 1.26 84.03 109.66 o 9 10 0 30.92 79.98 96.85 o 10 10 0 0.87 21.97 101.93 o 11 10 0 159.24 198.40 118.50 o 12 10 0 0.52 14.80 166.89 o 13 10 0 28.90 168.68 713.65 o 1 11 0 3022.39 2906.89 176.81 o 2 11 0 3335.63 3132.86 216.99 o 3 11 0 886.74 681.22 129.88 o 4 11 0 8.62 -19.13 41.80 o 5 11 0 2155.90 2205.94 201.86 o 6 11 0 39.02 -33.43 87.28 o 7 11 0 75.13 129.41 103.59 o 8 11 0 222.22 320.76 123.96 o 9 11 0 680.90 795.55 134.33 o 10 11 0 157.93 197.92 106.07 o 11 11 0 8.56 -89.16 111.77 o 12 11 0 166.90 361.80 438.27 o 0 12 0 1468.72 1272.39 130.58 o 1 12 0 9.36 -10.35 31.44 o 2 12 0 0.73 -41.50 39.97 o 3 12 0 392.44 306.36 59.79 o 4 12 0 2334.90 2182.73 144.17 o 5 12 0 440.93 521.41 101.78 o 6 12 0 173.33 28.62 90.49 o 7 12 0 52.20 -17.10 102.06 o 8 12 0 43.25 29.20 112.63 o 9 12 0 277.23 447.54 122.02 o 10 12 0 21.68 -27.05 159.66 o 11 12 0 38.32 96.00 114.96 o 12 12 0 7.63 75.46 139.97 o 1 13 0 2040.07 1887.06 132.05 o 2 13 0 2711.66 2434.58 176.13 o 3 13 0 9.47 -1.69 36.94 o 4 13 0 1214.06 1342.69 118.55 o 5 13 0 1321.43 1033.13 282.36 o 6 13 0 139.54 118.24 92.78 o 7 13 0 41.49 -58.92 106.80 o 8 13 0 899.63 989.52 174.73 o 9 13 0 3.89 -105.06 113.99 o 10 13 0 3.09 -105.92 113.93 o 11 13 0 41.07 41.58 133.39 o 12 13 0 1.49 -34.96 141.83 o 0 14 0 5854.45 5150.37 439.56 o 1 14 0 1.10 -16.70 34.86 o 2 14 0 14.56 17.44 38.54 o 3 14 0 1033.88 963.06 93.60 o 4 14 0 290.10 333.14 74.86 o 5 14 0 147.67 -33.15 139.63 o 6 14 0 4.44 -63.65 115.69 o 7 14 0 195.74 380.44 125.90 o 8 14 0 13.10 -39.47 109.02 o 9 14 0 137.29 281.61 135.58 o 10 14 0 0.32 167.50 123.40 o 11 14 0 5.20 -54.11 134.86 o 12 14 0 40.14 95.71 145.59 o 1 15 0 1223.00 1291.41 114.16 o 2 15 0 94.53 35.28 42.55 o 3 15 0 1189.30 1148.73 121.14 o 4 15 0 1131.52 1000.21 248.23 o 5 15 0 15.80 35.43 106.89 o 6 15 0 64.03 8.71 155.92 o 7 15 0 14.67 -15.05 125.83 o 8 15 0 153.44 80.78 121.62 o 9 15 0 40.54 25.59 129.60 o 10 15 0 32.54 -22.59 133.07 o 11 15 0 173.48 277.90 152.10 o 0 16 0 262.66 177.35 93.08 o 1 16 0 4594.13 4236.31 260.90 o 2 16 0 1084.50 1149.61 115.32 o 3 16 0 980.56 1022.54 106.19 o 4 16 0 149.76 -37.69 104.78 o 5 16 0 839.71 808.11 161.35 o 6 16 0 1576.28 1402.43 212.08 o 7 16 0 221.63 119.89 144.23 o 8 16 0 165.66 314.08 173.84 o 9 16 0 101.08 208.06 171.95 o 10 16 0 108.60 203.62 146.01 o 11 16 0 3.91 162.26 148.65 o 1 17 0 37.37 71.19 46.05 o 2 17 0 1504.79 1589.88 122.33 o 3 17 0 820.65 1027.90 148.99 o 4 17 0 279.18 151.70 114.16 o 5 17 0 1675.30 1602.98 252.10 o 6 17 0 44.10 117.42 136.11 o 7 17 0 40.12 20.17 144.14 o 8 17 0 71.04 -111.11 157.37 o 9 17 0 245.57 349.28 186.18 o 10 17 0 138.32 337.66 197.94 o 11 17 0 32.63 186.21 197.28 o 0 18 0 3650.82 3503.59 327.35 o 1 18 0 181.77 277.02 76.16 o 2 18 0 24.84 56.02 49.14 o 3 18 0 1675.93 1786.85 222.60 o 4 18 0 736.65 658.38 148.20 o 5 18 0 202.65 357.55 207.89 o 6 18 0 39.72 -44.77 127.72 o 7 18 0 648.34 944.27 200.34 o 8 18 0 132.45 193.49 170.84 o 9 18 0 29.27 45.13 219.52 o 10 18 0 103.67 280.20 198.15 o 1 19 0 24.49 28.92 52.09 o 2 19 0 182.42 155.75 59.62 o 3 19 0 686.39 859.99 232.71 o 4 19 0 63.46 84.62 112.54 o 5 19 0 186.78 207.68 180.74 o 6 19 0 37.27 161.58 150.77 o 7 19 0 139.72 209.15 160.26 o 8 19 0 0.03 -73.87 167.05 o 9 19 0 2.22 299.53 197.57 o 10 19 0 52.26 -157.16 174.55 o 0 20 0 75.21 67.28 85.18 o 1 20 0 137.75 171.28 65.22 o 2 20 0 4.97 52.49 119.15 o 3 20 0 45.27 27.47 105.11 o 4 20 0 55.83 178.39 119.07 o 5 20 0 44.84 387.29 145.40 o 6 20 0 29.47 -20.29 148.24 o 7 20 0 2.85 19.75 147.06 o 8 20 0 20.59 133.10 184.62 o 9 20 0 15.48 51.43 180.12 o 10 20 0 10.16 -58.44 172.98 o 1 21 0 40.67 5.00 57.35 o 2 21 0 6.56 77.34 81.49 o 3 21 0 60.98 -58.95 221.08 o 4 21 0 234.90 347.47 183.84 o 5 21 0 157.59 213.50 189.27 o 6 21 0 29.68 -53.20 138.92 o 7 21 0 72.44 158.01 163.09 o 8 21 0 11.87 186.62 181.37 o 9 21 0 5.45 -80.47 178.91 o 0 22 0 33.10 -30.64 83.89 o 1 22 0 2.43 -31.88 56.94 o 2 22 0 5.14 108.77 97.00 o 3 22 0 96.17 2.67 123.34 o 4 22 0 3.85 -87.17 117.36 o 5 22 0 11.26 -148.41 255.21 o 6 22 0 21.70 216.37 168.33 o 7 22 0 36.16 -25.01 162.54 o 8 22 0 30.54 67.45 181.50 o 9 22 0 2.27 43.70 179.01 o 1 23 0 144.20 192.31 69.63 o 2 23 0 51.77 -85.59 206.34 o 3 23 0 82.85 -18.97 161.35 o 4 23 0 56.88 55.21 128.62 o 5 23 0 1.52 -98.15 249.00 o 6 23 0 0.95 24.44 154.87 o 7 23 0 8.82 119.48 257.53 o 8 23 0 7.18 8.95 228.06 o 0 24 0 179.41 108.60 100.84 o 1 24 0 14.43 -9.78 60.19 o 2 24 0 12.08 118.84 149.71 o 3 24 0 10.51 125.42 119.19 o 4 24 0 2.08 -56.08 126.43 o 5 24 0 27.70 -17.22 201.68 o 6 24 0 5.72 24.93 160.10 o 7 24 0 44.92 12.01 182.82 o 1 25 0 18.19 65.16 90.76 o 2 25 0 334.40 385.55 122.63 o 3 25 0 31.92 128.21 172.98 o 4 25 0 1.90 -15.64 202.46 o 5 25 0 143.32 214.34 159.19 o 6 25 0 1.66 57.83 170.91 o 7 25 0 9.76 -79.43 165.66 o 0 26 0 8.04 20.17 94.64 o 1 26 0 98.94 7.46 93.80 o 2 26 0 17.83 36.30 106.07 o 3 26 0 4.83 -55.88 279.25 o 4 26 0 1.84 -150.88 309.51 o 5 26 0 17.03 151.45 158.86 o 6 26 0 27.26 244.76 176.03 o 1 27 0 67.62 150.49 110.15 o 2 27 0 1.03 -34.93 100.98 o 3 27 0 3.38 8.10 155.92 o 4 27 0 22.55 -32.29 152.81 o 5 27 0 8.84 79.59 195.48 o 1 28 0 17.75 139.63 105.50 o 2 28 0 0.40 -22.17 113.70 o 3 28 0 0.02 -4.77 122.21 o -14 1 1 21.02 -74.20 193.34 o -13 1 1 346.77 199.36 183.20 o -12 1 1 204.31 401.16 180.34 o -11 1 1 280.02 5.27 154.13 o -10 1 1 1617.00 1499.20 230.69 o -9 1 1 1429.01 1284.09 176.51 o -8 1 1 12.22 -3.86 46.02 o -7 1 1 22254.16 16064.97 811.08 o -6 1 1 14734.60 12660.93 592.60 o -5 1 1 39.39 68.41 36.31 o -4 1 1 36764.10 31754.91 1484.01 o -3 1 1 143730.02 146728.77 7979.09 o -2 1 1 358.60 318.13 28.34 o -1 1 1 4473.74 4389.31 455.34 o 0 1 1 59883.92 84509.86 5934.85 o 1 1 1 708.47 759.54 68.90 o 2 1 1 5199.43 4997.05 243.32 o 3 1 1 23637.61 19979.80 967.52 o 4 1 1 3121.31 2445.02 131.09 o 5 1 1 7834.53 7073.85 341.24 o 6 1 1 1968.53 1466.93 96.70 o 7 1 1 1870.03 1603.23 103.99 o 8 1 1 32.03 14.82 42.93 o 9 1 1 577.66 779.16 138.39 o 10 1 1 378.33 503.81 163.55 o 11 1 1 10.69 -102.80 242.80 o 12 1 1 267.61 262.21 181.62 o 13 1 1 49.36 -54.21 177.71 o -14 2 1 123.23 162.12 187.59 o -13 2 1 69.11 219.47 189.01 o -12 2 1 601.24 792.47 207.78 o -11 2 1 84.25 230.81 169.10 o -10 2 1 1804.87 2137.08 236.95 o -9 2 1 1944.62 2058.66 219.22 o -8 2 1 27.40 89.56 90.72 o -7 2 1 1933.50 1996.10 288.38 o -6 2 1 0.67 472.68 433.57 o -5 2 1 2523.00 2235.96 130.17 o -4 2 1 477.62 488.50 98.32 o -3 2 1 6198.64 5821.57 401.06 o -2 2 1 8534.91 6886.89 639.17 o -1 2 1 1257.05 1260.51 123.34 o 0 2 1 991.69 1097.86 83.37 o 1 2 1 6379.77 5628.31 389.42 o 2 2 1 37356.63 34577.02 1641.10 o 3 2 1 3736.46 3475.38 176.01 o 4 2 1 133.10 115.79 32.46 o 5 2 1 5855.29 4710.28 236.55 o 6 2 1 1020.07 1033.53 88.92 o 7 2 1 1154.78 933.90 94.82 o 8 2 1 1.05 24.33 67.44 o 9 2 1 736.91 705.10 131.22 o 10 2 1 600.67 988.03 217.52 o 11 2 1 0.97 0.05 156.30 o 12 2 1 66.65 88.63 171.85 o 13 2 1 2.10 47.66 183.34 o -14 3 1 4.57 -75.54 185.54 o -13 3 1 128.32 56.00 178.94 o -12 3 1 9.19 249.86 174.87 o -11 3 1 32.01 219.46 165.44 o -10 3 1 957.32 1456.77 266.94 o -9 3 1 396.41 604.82 95.63 o -8 3 1 973.17 996.86 159.21 o -7 3 1 48.41 92.23 36.30 o -6 3 1 11909.15 10010.52 679.04 o -5 3 1 2827.22 2593.41 200.12 o -4 3 1 277.18 330.29 84.51 o -3 3 1 709.67 639.08 67.80 o -2 3 1 50593.84 43710.39 3972.38 o -1 3 1 50331.14 51328.00 3118.75 o 0 3 1 2585.17 2863.79 296.32 o 1 3 1 22540.86 19248.24 1746.12 o 2 3 1 1152.70 1335.95 123.61 o 3 3 1 843.55 940.33 65.22 o 4 3 1 1648.84 1500.51 86.15 o 5 3 1 616.46 597.48 55.44 o 6 3 1 3209.50 2851.23 178.96 o 7 3 1 7.48 -24.25 61.29 o 8 3 1 929.98 792.33 90.93 o 9 3 1 694.53 708.23 102.44 o 10 3 1 679.68 728.72 155.24 o 11 3 1 28.41 218.79 143.03 o 12 3 1 1.94 141.95 174.43 o 13 3 1 126.89 -90.79 183.67 o -14 4 1 0.01 -84.86 179.56 o -13 4 1 1.24 233.31 190.82 o -12 4 1 16.34 211.42 174.87 o -11 4 1 685.42 580.37 162.51 o -10 4 1 1063.25 1250.75 192.42 o -9 4 1 848.44 809.64 106.70 o -8 4 1 4042.87 3781.15 260.29 o -7 4 1 1011.72 1086.30 93.62 o -6 4 1 235.53 300.38 56.32 o -5 4 1 1530.44 1601.69 151.97 o -4 4 1 2590.09 2039.59 159.48 o -3 4 1 30108.30 28902.88 1905.88 o -2 4 1 45828.82 40876.42 2698.72 o -1 4 1 214.96 323.48 36.50 o 0 4 1 2429.74 2536.21 189.22 o 1 4 1 10099.93 7976.66 655.21 o 2 4 1 72.45 41.11 52.85 o 3 4 1 8311.04 7288.02 421.78 o 4 4 1 10043.00 8477.51 414.30 o 5 4 1 9.13 65.90 56.66 o 6 4 1 3142.21 2860.54 156.25 o 7 4 1 357.15 380.78 77.01 o 8 4 1 1022.29 977.00 102.35 o 9 4 1 70.41 136.18 108.93 o 10 4 1 1.29 99.94 130.87 o 11 4 1 201.73 189.37 146.10 o 12 4 1 4.00 -29.01 174.87 o 13 4 1 26.84 -42.00 192.78 o -13 5 1 165.43 187.77 183.33 o -12 5 1 345.79 368.47 185.83 o -11 5 1 93.07 337.15 203.56 o -10 5 1 227.74 503.88 101.82 o -9 5 1 309.03 498.35 97.31 o -8 5 1 790.14 888.29 107.81 o -7 5 1 5292.52 4865.04 318.28 o -6 5 1 222.23 143.78 64.71 o -5 5 1 4832.18 4257.49 310.00 o -4 5 1 604.10 671.71 80.41 o -3 5 1 153.93 255.88 46.62 o -2 5 1 662.28 667.17 50.80 o -1 5 1 4406.57 4383.59 276.06 o 0 5 1 15916.63 15441.43 847.23 o 1 5 1 30164.84 30042.97 1859.71 o 2 5 1 28.87 -10.04 29.55 o 3 5 1 1642.75 1566.24 117.09 o 4 5 1 906.79 920.95 108.83 o 5 5 1 1405.85 1271.16 102.76 o 6 5 1 1211.70 1250.91 87.65 o 7 5 1 3033.88 2845.04 185.77 o 8 5 1 1072.53 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