#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/61/2236195.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236195_Fobs loop_ _publ_author_name 'Reiss, Guido J.' 'J\"orgens, Stefan' _publ_section_title ; (Dimethylphosphoryl)methanaminium chloride ; _journal_coeditor_code FJ2594 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2899 _journal_page_last o2900 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 84.057 _cell_angle_beta 87.691 _cell_angle_gamma 89.016 _cell_length_a 5.2965 _cell_length_b 7.7030 _cell_length_c 8.8035 _exptl_crystal_F_000 152.00 _reflns_d_resolution_high 0.7108 _[local]_cod_data_source_file fj2594Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' dpmaHCl' _shelx_refln_list_code 4 _shelx_f_calc_maximum 70.65 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1324.20 1246.87 10.67 o 2 0 0 406.91 416.04 4.26 o 3 0 0 259.84 236.06 3.04 o 4 0 0 15.09 14.03 0.37 o 5 0 0 77.69 76.90 3.13 o 6 0 0 703.77 713.21 7.67 o 7 0 0 61.47 61.19 2.50 o -7 1 0 61.35 61.02 2.55 o -6 1 0 8.31 8.14 1.21 o -5 1 0 3.63 2.83 0.79 o -4 1 0 581.27 543.76 7.63 o -3 1 0 1.34 2.06 0.40 o -2 1 0 733.68 796.17 4.08 o -1 1 0 151.72 174.52 4.46 o 1 1 0 46.54 52.32 0.49 o 2 1 0 2134.29 2142.98 10.68 o 3 1 0 3.74 6.02 0.25 o 4 1 0 646.55 625.19 10.91 o 5 1 0 0.46 0.44 0.39 o 6 1 0 11.52 9.87 0.89 o 7 1 0 58.55 61.07 2.42 o -7 2 0 6.55 6.64 0.88 o -6 2 0 293.07 295.07 13.21 o -5 2 0 37.63 33.64 2.23 o -4 2 0 202.93 197.74 4.73 o -3 2 0 781.73 770.31 7.15 o -2 2 0 59.79 64.03 0.84 o -1 2 0 87.51 93.28 3.85 o 0 2 0 2519.94 2538.72 12.46 o 1 2 0 284.94 291.85 1.29 o 2 2 0 845.19 890.18 2.40 o 3 2 0 986.57 976.96 3.18 o 4 2 0 78.65 78.97 1.86 o 5 2 0 0.64 1.70 0.72 o 6 2 0 567.01 581.55 10.87 o 7 2 0 81.73 85.39 2.73 o -7 3 0 160.13 161.09 5.60 o -6 3 0 1.31 1.16 0.43 o -5 3 0 7.90 9.06 0.83 o -4 3 0 351.56 347.45 5.48 o -3 3 0 15.58 12.16 0.43 o -2 3 0 1.71 2.01 0.43 o -1 3 0 151.83 130.68 2.07 o 0 3 0 561.04 616.81 2.69 o 1 3 0 53.76 45.63 0.84 o 2 3 0 688.74 710.43 7.95 o 3 3 0 27.47 22.23 0.53 o 4 3 0 126.49 122.02 1.31 o 5 3 0 61.62 62.25 1.86 o 6 3 0 94.45 99.30 2.62 o 7 3 0 130.61 136.17 3.31 o -6 4 0 381.28 377.37 9.18 o -5 4 0 7.76 7.39 0.98 o -4 4 0 21.45 21.74 1.37 o -3 4 0 586.97 590.46 3.94 o -2 4 0 96.29 107.21 2.33 o -1 4 0 457.20 461.70 4.51 o 0 4 0 661.47 668.47 4.50 o 1 4 0 4.24 4.65 0.30 o 2 4 0 227.27 226.03 2.29 o 3 4 0 671.04 658.50 7.81 o 4 4 0 7.65 9.63 0.61 o 5 4 0 143.38 145.17 2.71 o 6 4 0 271.39 283.34 4.20 o -6 5 0 7.13 6.05 0.76 o -5 5 0 0.03 0.29 0.49 o -4 5 0 267.97 267.99 4.82 o -3 5 0 19.70 21.78 1.30 o -2 5 0 7.34 9.97 0.85 o -1 5 0 516.92 510.22 5.37 o 0 5 0 0.33 0.54 0.18 o 1 5 0 57.09 54.15 1.06 o 2 5 0 47.65 51.33 1.23 o 3 5 0 91.57 80.83 1.57 o 4 5 0 10.86 12.16 1.08 o 5 5 0 117.50 115.66 3.47 o 6 5 0 43.85 43.90 2.40 o -6 6 0 102.56 99.09 4.93 o -5 6 0 0.05 0.30 0.39 o -4 6 0 310.83 320.50 5.50 o -3 6 0 460.83 484.11 6.36 o -2 6 0 23.86 18.81 1.22 o -1 6 0 104.47 112.79 2.72 o 0 6 0 700.80 698.05 10.58 o 1 6 0 36.39 34.65 0.93 o 2 6 0 160.42 151.98 2.35 o 3 6 0 286.48 282.00 4.61 o 4 6 0 4.00 4.01 0.68 o 5 6 0 157.04 160.90 4.16 o 6 6 0 160.79 170.15 4.68 o -5 7 0 13.17 12.77 1.37 o -4 7 0 148.21 160.19 4.24 o -3 7 0 26.78 27.30 1.69 o -2 7 0 13.57 11.57 1.12 o -1 7 0 289.05 287.64 4.59 o 0 7 0 49.55 48.69 1.69 o 1 7 0 15.18 14.92 0.89 o 2 7 0 119.68 121.37 3.35 o 3 7 0 49.22 47.59 2.10 o 4 7 0 25.04 26.74 1.65 o 5 7 0 27.22 28.03 1.81 o -4 8 0 239.02 237.15 5.48 o -3 8 0 336.75 346.62 6.33 o -2 8 0 11.06 10.61 1.07 o -1 8 0 195.14 193.31 4.02 o 0 8 0 86.08 93.61 2.81 o 1 8 0 44.68 41.50 1.44 o 2 8 0 253.81 239.98 5.15 o 3 8 0 488.55 475.69 7.29 o 4 8 0 10.67 9.13 1.09 o 5 8 0 45.74 45.14 2.45 o -4 9 0 2.44 2.28 0.77 o -3 9 0 14.42 12.80 1.31 o -2 9 0 135.99 137.46 3.85 o -1 9 0 220.94 217.74 4.54 o 0 9 0 54.41 57.29 2.37 o 1 9 0 4.56 3.54 0.49 o 2 9 0 16.48 17.12 1.50 o 3 9 0 68.50 66.01 3.00 o 4 9 0 4.54 5.41 1.00 o -2 10 0 33.63 33.73 2.03 o -1 10 0 254.94 240.78 5.17 o 0 10 0 39.85 40.06 2.15 o 1 10 0 18.76 14.50 1.35 o 2 10 0 122.34 115.67 4.03 o -2 -10 1 3.31 4.79 0.95 o -1 -10 1 16.30 15.53 1.50 o 0 -10 1 22.06 22.92 1.63 o 1 -10 1 8.08 10.73 1.21 o 2 -10 1 1.64 1.84 0.59 o -4 -9 1 205.41 208.24 5.56 o -3 -9 1 89.81 89.46 3.56 o -2 -9 1 2.26 2.53 0.73 o -1 -9 1 97.94 94.76 2.33 o 0 -9 1 101.21 101.70 3.20 o 1 -9 1 57.02 57.23 2.36 o 2 -9 1 318.49 319.96 5.88 o 3 -9 1 43.74 40.75 2.26 o -4 -8 1 95.90 96.75 3.46 o -3 -8 1 2.61 2.50 0.64 o -2 -8 1 49.86 50.41 1.70 o -1 -8 1 17.73 17.84 0.80 o 0 -8 1 150.56 153.19 3.61 o 1 -8 1 0.34 0.80 0.48 o 2 -8 1 21.24 18.77 1.33 o 3 -8 1 29.13 28.46 1.88 o 4 -8 1 9.37 9.83 1.26 o -5 -7 1 0.07 -0.56 0.56 o -4 -7 1 585.67 575.81 7.73 o -3 -7 1 248.78 248.47 3.40 o -2 -7 1 0.53 0.73 0.29 o -1 -7 1 206.02 202.88 2.63 o 0 -7 1 30.03 29.04 0.93 o 1 -7 1 1.99 1.22 0.44 o 2 -7 1 601.30 606.60 7.25 o 3 -7 1 281.99 294.30 5.34 o 4 -7 1 25.46 27.58 1.80 o 5 -7 1 101.06 102.83 3.59 o -6 -6 1 23.80 25.20 1.87 o -5 -6 1 33.64 38.45 2.10 o -4 -6 1 0.64 0.57 0.22 o -3 -6 1 39.06 40.27 1.26 o -2 -6 1 638.62 611.59 7.86 o -1 -6 1 293.98 283.08 2.69 o 0 -6 1 320.18 309.51 3.55 o 1 -6 1 31.84 32.53 2.22 o 2 -6 1 6.10 4.75 0.71 o 3 -6 1 44.06 46.45 1.99 o 4 -6 1 149.38 157.99 3.85 o 5 -6 1 21.35 19.48 1.49 o 6 -6 1 115.85 115.51 3.15 o -6 -5 1 1.17 0.81 0.37 o -5 -5 1 31.73 32.56 1.91 o -4 -5 1 612.89 643.41 8.43 o -3 -5 1 53.35 54.86 1.35 o -2 -5 1 34.67 33.54 1.79 o -1 -5 1 971.11 948.20 4.68 o 0 -5 1 5.48 4.01 0.30 o 1 -5 1 19.99 22.70 0.87 o 2 -5 1 909.11 940.56 7.60 o 3 -5 1 296.56 302.51 4.62 o 4 -5 1 35.93 36.93 1.79 o 5 -5 1 239.30 240.53 4.98 o 6 -5 1 8.90 9.61 1.31 o -6 -4 1 1.48 1.21 0.32 o -5 -4 1 186.93 191.02 3.07 o -4 -4 1 2.40 2.41 0.70 o -3 -4 1 55.92 62.51 1.29 o -2 -4 1 401.31 371.34 2.96 o -1 -4 1 20.05 16.46 0.64 o 0 -4 1 41.60 38.46 1.01 o 1 -4 1 517.10 531.62 7.26 o 2 -4 1 56.75 58.90 1.30 o 3 -4 1 607.80 640.85 6.41 o 4 -4 1 70.24 73.03 2.42 o 5 -4 1 60.25 61.16 1.99 o 6 -4 1 31.98 32.79 1.65 o -7 -3 1 117.20 122.46 3.33 o -6 -3 1 3.49 3.31 0.52 o -5 -3 1 48.87 49.56 1.64 o -4 -3 1 598.84 598.10 5.67 o -3 -3 1 47.34 45.67 0.83 o -2 -3 1 216.88 221.33 2.03 o -1 -3 1 1015.18 1006.11 4.08 o 0 -3 1 47.23 55.68 0.98 o 1 -3 1 182.89 176.96 1.83 o 2 -3 1 1694.75 1653.60 6.16 o 3 -3 1 58.31 52.45 0.77 o 4 -3 1 50.54 49.63 2.03 o 5 -3 1 588.98 594.53 6.24 o 6 -3 1 17.06 16.08 1.16 o 7 -3 1 0.07 0.07 0.44 o -7 -2 1 7.09 6.72 0.87 o -6 -2 1 50.13 52.42 1.92 o -5 -2 1 160.09 161.59 3.01 o -4 -2 1 33.00 32.96 0.72 o -3 -2 1 8.13 8.59 0.55 o -2 -2 1 682.19 663.44 3.20 o -1 -2 1 220.86 223.34 1.29 o 0 -2 1 659.28 618.03 3.00 o 1 -2 1 574.11 578.29 2.73 o 2 -2 1 0.08 0.83 0.40 o 3 -2 1 75.35 74.41 2.20 o 4 -2 1 181.19 198.20 4.89 o 5 -2 1 55.87 54.43 2.85 o 6 -2 1 214.07 213.10 7.65 o 7 -2 1 59.68 62.68 2.48 o -7 -1 1 294.37 303.86 5.23 o -6 -1 1 2.05 1.48 0.40 o -5 -1 1 17.95 16.94 1.02 o -4 -1 1 601.11 591.73 4.71 o -3 -1 1 18.16 18.65 0.62 o -2 -1 1 207.15 205.90 1.70 o -1 -1 1 1688.58 1796.19 3.58 o 0 -1 1 195.71 186.43 0.89 o 1 -1 1 742.48 718.27 1.71 o 2 -1 1 953.03 916.24 4.08 o 3 -1 1 6.00 15.97 4.40 o 4 -1 1 168.43 160.86 4.01 o 5 -1 1 716.87 706.73 9.96 o 6 -1 1 2.37 2.16 0.84 o 7 -1 1 29.54 28.13 1.74 o -7 0 1 0.41 -0.49 0.49 o -6 0 1 27.99 27.64 1.52 o -5 0 1 608.40 618.02 8.53 o -4 0 1 20.95 24.21 0.81 o -3 0 1 281.76 294.00 3.05 o -2 0 1 648.42 630.24 3.05 o -1 0 1 417.28 381.24 1.82 o 1 0 1 266.47 334.13 0.94 o 2 0 1 176.52 176.26 0.99 o 3 0 1 89.48 85.87 2.10 o 4 0 1 205.58 195.28 1.15 o 5 0 1 54.19 52.30 2.65 o 6 0 1 70.40 73.67 2.51 o 7 0 1 50.54 53.19 2.36 o -7 1 1 239.15 238.72 4.95 o -6 1 1 1.21 0.69 0.44 o -5 1 1 153.10 158.16 4.51 o -4 1 1 371.13 357.00 2.42 o -3 1 1 163.37 177.36 3.88 o -2 1 1 218.90 220.99 1.69 o -1 1 1 3861.33 4102.05 14.93 o 0 1 1 443.22 429.22 1.46 o 1 1 1 480.84 504.13 5.47 o 2 1 1 866.01 849.43 18.44 o 3 1 1 10.92 10.94 0.65 o 4 1 1 180.45 172.47 2.90 o 5 1 1 467.31 462.61 5.41 o 6 1 1 3.10 2.69 0.52 o 7 1 1 133.16 135.35 3.64 o -7 2 1 58.25 61.50 3.42 o -6 2 1 68.40 65.19 3.15 o -5 2 1 870.90 846.81 10.73 o -4 2 1 15.89 15.95 1.62 o -3 2 1 0.31 0.73 0.18 o -2 2 1 45.68 37.60 0.82 o -1 2 1 1603.21 1661.90 6.69 o 0 2 1 3.66 7.62 0.25 o 1 2 1 4991.16 5050.80 7.53 o 2 2 1 172.46 202.82 1.40 o 3 2 1 137.49 130.42 2.11 o 4 2 1 0.83 2.37 0.92 o 5 2 1 166.09 159.98 3.08 o 6 2 1 2.30 1.82 0.47 o 7 2 1 118.93 120.91 3.31 o -7 3 1 115.29 118.42 10.66 o -6 3 1 16.79 15.71 1.14 o -5 3 1 354.61 355.71 4.80 o -4 3 1 130.16 128.73 3.39 o -3 3 1 335.39 319.39 2.60 o -2 3 1 386.43 398.21 2.81 o -1 3 1 2816.64 2831.16 9.92 o 0 3 1 212.73 216.86 3.74 o 1 3 1 1124.99 1156.25 4.52 o 2 3 1 900.59 911.16 3.74 o 3 3 1 156.16 153.43 1.43 o 4 3 1 66.76 66.80 1.72 o 5 3 1 517.31 517.07 5.40 o 6 3 1 52.68 52.32 1.94 o 7 3 1 129.90 138.10 3.44 o -6 4 1 14.90 16.31 1.21 o -5 4 1 163.86 161.34 4.15 o -4 4 1 1.61 0.93 0.43 o -3 4 1 307.72 290.08 12.15 o -2 4 1 440.55 421.07 4.66 o -1 4 1 680.46 715.80 5.72 o 0 4 1 49.67 55.05 1.10 o 1 4 1 762.49 792.09 4.20 o 2 4 1 2.62 13.15 0.87 o 3 4 1 97.45 117.41 4.36 o 4 4 1 186.00 195.70 2.81 o 5 4 1 243.48 245.93 3.60 o 6 4 1 81.11 85.24 2.36 o -6 5 1 0.18 0.53 0.41 o -5 5 1 225.25 222.65 4.86 o -4 5 1 186.09 203.89 4.30 o -3 5 1 5.35 4.51 0.41 o -2 5 1 208.93 221.01 3.74 o -1 5 1 102.87 102.31 2.44 o 0 5 1 8.24 8.73 0.53 o 1 5 1 1624.66 1577.93 6.81 o 2 5 1 618.19 584.03 5.57 o 3 5 1 86.98 83.80 2.32 o 4 5 1 100.47 102.20 2.91 o 5 5 1 208.85 210.02 4.57 o 6 5 1 4.03 3.49 0.49 o -6 6 1 70.70 70.56 3.97 o -5 6 1 223.93 222.88 4.99 o -4 6 1 4.97 5.15 0.85 o -3 6 1 31.94 33.37 1.17 o -2 6 1 145.43 136.14 3.25 o -1 6 1 10.77 17.59 1.16 o 0 6 1 169.86 168.99 2.37 o 1 6 1 119.54 119.14 2.07 o 2 6 1 170.22 156.91 3.24 o 3 6 1 43.69 49.20 1.88 o 4 6 1 156.44 152.03 3.58 o 5 6 1 89.19 90.89 3.09 o 6 6 1 0.76 1.16 0.57 o -5 7 1 90.82 89.68 3.40 o -4 7 1 91.55 98.07 3.34 o -3 7 1 3.50 5.90 0.57 o -2 7 1 360.49 382.73 5.89 o -1 7 1 133.27 136.68 3.21 o 0 7 1 2.19 1.81 0.45 o 1 7 1 274.35 280.00 7.38 o 2 7 1 129.90 132.56 3.41 o 3 7 1 18.34 20.07 1.36 o 4 7 1 402.83 400.90 6.18 o 5 7 1 66.69 62.58 2.64 o -4 8 1 2.85 3.59 0.86 o -3 8 1 101.26 97.55 3.37 o -2 8 1 138.37 142.84 3.79 o -1 8 1 21.18 20.46 1.31 o 0 8 1 47.66 49.48 2.05 o 1 8 1 95.87 94.19 4.08 o 2 8 1 10.18 9.95 1.09 o 3 8 1 32.74 32.68 1.90 o 4 8 1 9.12 7.70 0.97 o 5 8 1 45.95 45.06 2.41 o -4 9 1 17.71 17.15 1.62 o -3 9 1 9.05 9.85 1.19 o -2 9 1 211.23 214.52 4.86 o -1 9 1 117.42 119.45 3.40 o 0 9 1 3.89 3.89 0.60 o 1 9 1 167.64 163.62 3.03 o 2 9 1 36.24 35.53 2.14 o 3 9 1 1.38 0.81 0.47 o 4 9 1 183.43 184.14 5.08 o -2 10 1 119.86 121.13 3.84 o -1 10 1 0.96 1.49 0.57 o 0 10 1 65.49 67.24 2.79 o 1 10 1 22.37 20.87 1.63 o 2 10 1 42.18 37.77 2.26 o -2 -10 2 182.47 177.68 5.18 o -1 -10 2 25.30 25.80 1.97 o 0 -10 2 3.97 3.54 0.68 o 1 -10 2 261.92 263.36 5.44 o 2 -10 2 75.21 73.02 2.88 o -3 -9 2 49.10 53.22 1.95 o -2 -9 2 0.42 0.76 0.33 o -1 -9 2 19.87 19.93 1.17 o 0 -9 2 166.79 172.81 3.19 o 1 -9 2 31.54 32.38 1.78 o 2 -9 2 73.82 76.49 2.83 o 3 -9 2 9.28 8.73 1.08 o -4 -8 2 1.03 1.65 0.66 o -3 -8 2 43.46 43.32 1.63 o -2 -8 2 394.62 388.72 4.80 o -1 -8 2 21.91 22.11 1.15 o 0 -8 2 20.73 22.80 1.07 o 1 -8 2 325.97 324.13 7.45 o 2 -8 2 15.74 14.26 1.18 o 3 -8 2 27.64 25.46 1.74 o 4 -8 2 366.26 369.41 6.80 o -5 -7 2 20.63 19.54 1.60 o -4 -7 2 2.11 2.28 0.62 o -3 -7 2 198.74 193.17 4.10 o -2 -7 2 7.33 8.45 1.44 o -1 -7 2 20.07 20.58 0.81 o 0 -7 2 123.85 123.24 1.93 o 1 -7 2 0.23 0.22 0.26 o 2 -7 2 19.82 16.73 1.22 o 3 -7 2 175.50 179.71 4.20 o 4 -7 2 0.05 -0.01 0.43 o 5 -7 2 89.55 93.62 3.41 o -5 -6 2 385.66 387.57 6.70 o -4 -6 2 44.67 44.63 1.41 o -3 -6 2 14.71 15.82 0.84 o -2 -6 2 201.06 194.54 3.44 o -1 -6 2 5.14 5.26 0.41 o 0 -6 2 203.36 189.20 2.84 o 1 -6 2 741.49 740.36 5.22 o 2 -6 2 13.97 15.06 0.82 o 3 -6 2 51.64 55.50 2.15 o 4 -6 2 398.72 405.94 6.19 o 5 -6 2 9.32 8.72 1.11 o -6 -5 2 136.10 143.17 4.41 o -5 -5 2 11.11 11.64 1.20 o -4 -5 2 25.27 26.18 1.01 o -3 -5 2 547.70 535.84 4.24 o -2 -5 2 194.86 186.92 3.51 o -1 -5 2 0.05 0.47 0.22 o 0 -5 2 70.23 68.53 1.51 o 1 -5 2 81.78 84.50 1.62 o 2 -5 2 41.10 43.40 1.25 o 3 -5 2 257.81 264.94 4.28 o 4 -5 2 1.50 2.04 0.52 o 5 -5 2 8.78 8.60 1.00 o 6 -5 2 65.56 65.05 2.48 o -6 -4 2 0.24 -0.10 0.48 o -5 -4 2 337.85 355.05 6.39 o -4 -4 2 55.90 58.57 3.11 o -3 -4 2 433.26 432.40 3.85 o -2 -4 2 775.00 742.36 4.32 o -1 -4 2 198.80 208.62 2.26 o 0 -4 2 62.05 75.08 1.95 o 1 -4 2 846.19 845.65 14.87 o 2 -4 2 458.28 481.21 3.69 o 3 -4 2 588.13 616.31 9.38 o 4 -4 2 365.51 368.75 5.33 o 5 -4 2 44.16 42.29 2.61 o 6 -4 2 16.83 16.80 1.20 o -6 -3 2 210.44 218.84 3.34 o -5 -3 2 58.18 58.48 1.43 o -4 -3 2 0.65 0.48 0.24 o -3 -3 2 903.06 879.90 4.78 o -2 -3 2 88.17 90.52 2.33 o -1 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26.26 1.07 o 4 1 10 117.17 117.65 4.14 o -4 2 10 0.00 -0.72 0.72 o -3 2 10 4.21 3.69 0.72 o -2 2 10 265.76 267.72 5.13 o -1 2 10 18.59 19.61 1.39 o 0 2 10 30.61 29.94 1.69 o 1 2 10 392.98 406.20 24.09 o 2 2 10 0.32 0.39 0.19 o 3 2 10 38.44 37.00 1.59 o 4 2 10 102.95 105.93 3.05 o -3 3 10 19.14 17.35 1.93 o -2 3 10 25.83 23.65 2.23 o -1 3 10 130.22 136.59 5.16 o 0 3 10 7.27 7.73 0.98 o 1 3 10 62.78 64.06 3.73 o 2 3 10 162.21 164.08 8.20 o 3 3 10 35.26 32.87 1.51 o 4 3 10 16.85 17.39 1.17 o -3 4 10 24.12 22.65 2.18 o -2 4 10 175.27 176.80 6.13 o -1 4 10 1.57 1.05 0.62 o 0 4 10 43.22 44.53 3.02 o 1 4 10 269.02 260.03 7.19 o 2 4 10 0.59 0.05 0.37 o 3 4 10 3.72 2.65 0.86 o 4 4 10 165.59 160.91 5.64 o -3 5 10 0.49 0.64 0.65 o -2 5 10 36.99 39.76 3.03 o -1 5 10 37.27 43.46 3.13 o 0 5 10 31.64 34.99 2.80 o 1 5 10 56.83 58.60 3.58 o 2 5 10 136.94 135.65 5.43 o 3 5 10 1.05 0.91 0.66 o -2 6 10 169.75 179.13 6.56 o -1 6 10 2.28 1.54 0.75 o 0 6 10 19.74 20.03 2.22 o 1 6 10 114.86 113.22 5.18 o 2 6 10 0.03 -0.21 0.52 o 0 7 10 0.67 0.24 0.60 o 1 7 10 41.92 41.73 3.33 o -1 -3 11 5.10 5.34 1.02 o 0 -3 11 201.83 199.33 5.65 o 1 -3 11 15.54 16.18 1.56 o 2 -3 11 0.46 0.59 0.38 o -2 -2 11 40.18 40.36 2.79 o -1 -2 11 8.16 7.55 1.24 o 0 -2 11 35.19 35.37 2.45 o 1 -2 11 158.73 163.04 4.92 o 2 -2 11 6.77 6.82 1.00 o -2 -1 11 0.64 2.01 0.74 o -1 -1 11 16.80 16.55 1.81 o 0 -1 11 244.03 260.59 6.67 o 1 -1 11 18.60 19.68 1.76 o 2 -1 11 18.55 18.79 1.66 o 3 -1 11 158.37 163.71 4.38 o -3 0 11 12.49 12.35 1.69 o -2 0 11 43.15 46.80 3.22 o -1 0 11 12.20 13.48 1.73 o 0 0 11 19.32 20.03 1.91 o 1 0 11 56.12 59.34 3.21 o 2 0 11 11.24 11.24 1.00 o 3 0 11 54.89 52.13 3.08 o -3 1 11 182.82 186.33 6.63 o -2 1 11 60.77 60.54 3.72 o -1 1 11 75.19 76.45 2.85 o 0 1 11 150.61 162.58 9.67 o 1 1 11 1.15 0.82 0.41 o 2 1 11 21.15 20.46 1.34 o 3 1 11 181.65 172.85 5.64 o -3 2 11 45.40 42.23 3.16 o -2 2 11 133.23 138.09 4.92 o -1 2 11 15.19 15.28 1.33 o 0 2 11 0.66 0.43 0.43 o 1 2 11 12.79 14.08 1.24 o 2 2 11 9.46 7.88 0.89 o 3 2 11 96.06 90.48 4.24 o -2 3 11 0.01 0.10 0.44 o -1 3 11 153.54 161.90 10.04 o 0 3 11 469.94 479.40 17.78 o 1 3 11 2.08 2.07 0.51 o 2 3 11 1.60 0.82 0.43 o 3 3 11 28.65 26.82 2.40 o -2 4 11 72.21 75.64 4.24 o -1 4 11 19.44 16.60 2.06 o 0 4 11 27.02 24.60 2.42 o 1 4 11 7.06 6.07 0.89 o 2 4 11 59.99 65.69 2.63 o 3 4 11 57.26 54.08 3.49 o -1 5 11 78.78 83.47 4.52 o 0 5 11 233.50 237.66 7.60 o 1 5 11 2.07 1.09 0.64 o 2 5 11 57.61 57.24 3.06 o 0 -1 12 32.09 37.87 2.72 o 1 -1 12 5.08 3.99 0.91 o -1 0 12 143.52 151.16 5.69 o 0 0 12 0.77 0.67 0.59 o 1 0 12 45.24 43.69 2.84 o -1 1 12 87.81 91.34 4.58 o 0 1 12 22.26 24.20 1.67 o 1 1 12 51.35 51.62 2.46 o 2 1 12 22.12 22.58 1.47 o -1 2 12 89.58 99.11 7.21 o 0 2 12 0.01 -0.09 0.41 o 1 2 12 130.07 127.51 4.74 o 2 2 12 127.45 128.88 3.58 o 0 3 12 2.69 2.08 0.63 o 1 3 12 9.75 9.65 1.08 o