#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/62/2236233.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236233_Fobs loop_ _publ_author_name 'Xu, Wen-jie' 'Qiu, Xue-hui' 'Hua, Huai-jie' 'Tan, Song-de' 'Ding, Hai-yan' _publ_section_title ; 7-[(7S)-7-Azaniumyl-5-azaspiro[2.4]hept-5-yl]-8-chloro-6-fluoro-1-[(1S,2R)-2-fluorocyclopropyl]-4-oxo-1,4-dihydroquinoline-3-carboxylate methanol monosolvate ; _journal_coeditor_code GO2064 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2794 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 104.474 _cell_angle_gamma 90.000 _cell_length_a 8.7455 _cell_length_b 8.2968 _cell_length_c 14.0638 _exptl_crystal_F_000 460.00 _reflns_d_resolution_high 0.8384 _[local]_cod_data_source_file go2064Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' exp_357 in P21 4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 98.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 -9 0 11.09 4.09 4.08 o 5 -8 0 23.67 15.43 7.09 o 1 -7 0 59.71 41.90 8.69 o 6 -7 0 32.59 38.23 8.34 o 7 -7 0 35.23 30.40 6.36 o 1 -6 0 645.58 516.23 26.04 o 2 -6 0 272.02 226.51 17.92 o 3 -6 0 164.35 151.64 15.15 o 4 -6 0 147.49 119.91 12.55 o 5 -6 0 303.49 276.08 18.10 o 6 -6 0 29.99 21.05 7.93 o 7 -6 0 42.21 27.96 6.48 o 2 -5 0 379.55 325.39 18.97 o 3 -5 0 139.15 139.79 14.08 o 4 -5 0 401.06 363.66 20.33 o 5 -5 0 151.09 153.80 13.89 o 6 -5 0 172.85 158.82 16.77 o 7 -5 0 135.56 125.83 14.51 o 2 -4 0 191.44 170.68 12.54 o 3 -4 0 972.13 983.27 31.53 o 4 -4 0 281.49 274.65 16.53 o 5 -4 0 154.27 156.19 9.23 o 6 -4 0 15.56 16.91 7.55 o 7 -4 0 48.01 51.78 8.70 o 2 -3 0 1990.05 1733.45 32.85 o 3 -3 0 1684.45 1670.13 36.26 o 5 -3 0 803.17 767.72 16.31 o 6 -3 0 679.95 678.23 17.16 o 7 -3 0 88.21 87.03 12.03 o 9 -3 0 5.85 -4.76 7.50 o 2 -2 0 689.53 623.64 17.18 o 4 -2 0 191.74 185.78 12.60 o 5 -2 0 99.17 98.98 5.18 o 6 -2 0 43.82 38.13 4.71 o 7 -2 0 35.91 41.79 7.64 o 8 -2 0 150.48 159.94 13.73 o 1 -1 0 1232.68 1041.54 14.74 o 3 -1 0 3002.60 2962.77 36.94 o 4 -1 0 347.88 321.55 14.77 o 5 -1 0 198.53 180.25 10.35 o 6 -1 0 73.15 63.25 11.61 o 7 -1 0 29.53 37.11 5.49 o 8 -1 0 72.24 72.49 7.30 o 9 -1 0 59.78 62.78 9.01 o 1 0 0 11.57 11.22 1.47 o 2 0 0 1230.84 1253.80 17.87 o 3 0 0 866.07 826.82 18.41 o 4 0 0 4.63 6.29 2.99 o 5 0 0 732.09 769.35 37.01 o 6 0 0 35.10 35.64 5.32 o 7 0 0 241.43 224.14 13.66 o 8 0 0 151.86 143.06 12.51 o 9 0 0 20.61 18.65 6.87 o 10 0 0 45.11 44.19 7.15 o 2 1 0 1005.05 984.08 16.06 o 3 1 0 3076.53 3220.40 35.87 o 4 1 0 386.80 412.28 15.62 o 5 1 0 221.90 213.61 9.58 o 6 1 0 82.55 94.78 6.32 o 7 1 0 30.24 25.71 5.92 o 8 1 0 74.21 93.07 11.66 o 9 1 0 69.15 69.83 10.37 o 10 1 0 39.36 57.80 6.77 o 1 2 0 3198.51 2963.29 18.21 o 2 2 0 681.13 721.58 14.02 o 5 2 0 92.99 93.87 9.91 o 6 2 0 62.08 58.19 6.17 o 7 2 0 38.20 51.21 6.30 o 8 2 0 130.62 142.32 7.74 o 9 2 0 60.17 57.03 11.43 o 1 3 0 1649.35 1637.93 16.54 o 2 3 0 2066.89 2086.80 25.97 o 3 3 0 1669.30 1710.17 27.23 o 4 3 0 192.84 212.80 7.20 o 5 3 0 832.74 902.77 14.21 o 6 3 0 657.88 701.96 20.39 o 7 3 0 90.33 93.32 6.97 o 8 3 0 52.75 46.26 5.37 o 9 3 0 1.37 -0.10 3.54 o 0 4 0 642.52 727.00 18.16 o 1 4 0 2400.46 2550.00 24.08 o 2 4 0 182.47 208.79 9.65 o 3 4 0 975.44 1131.69 20.60 o 4 4 0 294.84 308.60 9.92 o 5 4 0 162.25 162.36 10.91 o 6 4 0 18.32 22.26 5.52 o 7 4 0 68.27 74.26 6.50 o 8 4 0 15.38 12.67 3.64 o 9 4 0 14.03 8.27 4.16 o 1 5 0 222.52 229.45 10.07 o 2 5 0 348.55 375.36 10.29 o 3 5 0 124.11 143.14 6.10 o 4 5 0 411.72 423.69 12.37 o 5 5 0 140.53 147.73 7.17 o 6 5 0 163.52 163.06 8.86 o 7 5 0 134.26 137.34 7.99 o 8 5 0 92.34 101.45 7.25 o 0 6 0 296.07 294.48 18.17 o 1 6 0 617.27 646.68 14.60 o 2 6 0 282.85 291.77 10.26 o 3 6 0 152.40 172.28 8.37 o 4 6 0 136.52 145.65 8.10 o 5 6 0 292.87 301.20 31.73 o 6 6 0 28.93 28.84 5.24 o 7 6 0 29.91 24.78 4.99 o 8 6 0 95.72 96.75 9.05 o 1 7 0 72.88 63.83 7.42 o 2 7 0 248.04 266.57 12.94 o 3 7 0 33.60 25.92 4.30 o 4 7 0 89.05 88.06 5.83 o 5 7 0 34.41 43.71 5.53 o 6 7 0 28.66 28.50 3.94 o 7 7 0 33.58 34.78 5.29 o 0 8 0 89.95 100.92 11.17 o 1 8 0 31.34 28.31 4.51 o 2 8 0 229.35 256.35 10.01 o 3 8 0 54.76 51.59 6.58 o 4 8 0 58.45 48.18 8.05 o 5 8 0 20.70 14.45 5.17 o 1 9 0 4.62 2.03 4.89 o 2 9 0 83.55 76.33 7.32 o 3 9 0 159.41 162.69 12.24 o -4 -9 1 78.04 65.04 8.20 o -6 -8 1 29.17 32.94 5.95 o -5 -8 1 10.35 7.96 5.45 o 5 -8 1 37.37 39.28 7.53 o -7 -7 1 74.18 73.26 9.02 o -6 -7 1 6.88 5.67 6.07 o 0 -7 1 828.48 672.10 30.98 o 4 -7 1 106.43 103.20 11.52 o 5 -7 1 18.46 15.53 4.34 o 6 -7 1 73.61 62.86 9.69 o -7 -6 1 154.69 156.11 14.92 o -6 -6 1 152.43 132.41 15.65 o -3 -6 1 573.35 587.29 29.65 o -2 -6 1 69.42 81.85 11.05 o -1 -6 1 54.78 44.23 7.80 o 0 -6 1 213.89 159.46 13.82 o 1 -6 1 43.30 28.24 7.08 o 2 -6 1 147.29 127.05 14.19 o 3 -6 1 146.54 136.89 15.33 o 4 -6 1 171.97 154.07 15.15 o 5 -6 1 61.17 59.37 10.00 o 6 -6 1 179.55 193.42 16.82 o 7 -6 1 4.71 -4.74 4.74 o -7 -5 1 211.33 202.89 17.69 o -6 -5 1 197.57 172.40 17.60 o -5 -5 1 174.37 181.98 11.03 o -4 -5 1 221.44 219.92 15.02 o -3 -5 1 83.39 74.45 10.66 o -2 -5 1 2079.57 1872.53 43.57 o -1 -5 1 302.97 269.49 15.82 o 2 -5 1 246.00 204.39 15.76 o 3 -5 1 107.26 85.98 11.00 o 4 -5 1 61.71 47.46 9.01 o 5 -5 1 292.28 281.21 19.81 o 6 -5 1 47.14 40.91 6.73 o 7 -5 1 191.69 166.34 15.02 o -9 -4 1 33.15 20.61 6.27 o -7 -4 1 377.17 349.99 23.11 o -6 -4 1 395.41 372.81 41.42 o -5 -4 1 299.93 293.05 17.16 o -4 -4 1 625.90 532.02 21.32 o -3 -4 1 1242.46 1219.13 34.44 o -2 -4 1 184.49 161.91 11.72 o 2 -4 1 305.82 256.35 15.40 o 3 -4 1 336.24 271.39 17.53 o 4 -4 1 97.79 97.28 7.22 o 5 -4 1 62.06 50.91 5.21 o 6 -4 1 315.44 310.46 12.00 o 7 -4 1 88.86 56.72 10.73 o -9 -3 1 187.59 178.18 14.38 o -7 -3 1 62.62 53.85 10.05 o -6 -3 1 791.10 713.26 22.01 o -5 -3 1 347.08 317.20 9.11 o -4 -3 1 901.71 847.70 27.86 o -3 -3 1 401.59 448.25 18.82 o -2 -3 1 1383.01 1316.32 27.96 o 2 -3 1 219.07 200.63 11.69 o 3 -3 1 268.45 231.84 14.38 o 4 -3 1 65.54 64.34 5.60 o 5 -3 1 2.25 -0.14 3.55 o 6 -3 1 2.25 -0.38 3.18 o 7 -3 1 444.99 433.11 24.05 o -9 -2 1 20.15 23.26 7.49 o -7 -2 1 218.29 202.46 18.30 o -6 -2 1 195.41 182.22 21.70 o -5 -2 1 676.98 669.48 19.47 o -4 -2 1 1503.87 1470.69 33.31 o -2 -2 1 376.10 316.54 12.19 o -1 -2 1 6876.49 5943.30 43.36 o 2 -2 1 588.10 541.41 16.33 o 3 -2 1 86.40 79.18 7.87 o 4 -2 1 951.48 895.05 26.27 o 5 -2 1 183.16 167.10 6.61 o 6 -2 1 438.09 432.69 13.27 o 8 -2 1 114.15 86.60 10.61 o -10 -1 1 153.64 135.25 10.57 o -9 -1 1 113.59 112.36 12.41 o -8 -1 1 1.37 -1.10 3.92 o -7 -1 1 35.01 41.15 8.03 o -6 -1 1 273.70 270.53 9.84 o -5 -1 1 825.44 899.27 18.93 o -4 -1 1 445.89 438.99 17.32 o -3 -1 1 57.82 68.65 6.34 o -1 -1 1 5653.47 5320.52 32.36 o 2 -1 1 865.53 828.60 17.20 o 3 -1 1 550.14 470.01 37.95 o 4 -1 1 731.69 715.06 21.67 o 5 -1 1 10.74 8.13 2.63 o 6 -1 1 12.69 17.40 4.51 o 7 -1 1 68.36 63.36 9.72 o 8 -1 1 14.92 17.95 7.19 o 9 -1 1 123.83 111.84 10.82 o -10 0 1 141.82 128.25 11.09 o -9 0 1 32.34 26.63 4.80 o -8 0 1 548.07 517.31 18.22 o -7 0 1 1135.12 1167.06 21.58 o -6 0 1 333.88 319.46 12.64 o -5 0 1 172.80 175.77 12.35 o -4 0 1 5715.55 6235.34 60.51 o -3 0 1 387.06 396.69 13.14 o -2 0 1 581.51 567.82 12.48 o -1 0 1 3520.50 3541.28 21.95 o 0 0 1 998.02 1029.00 7.10 o 1 0 1 594.76 629.81 8.29 o 2 0 1 200.75 221.63 4.44 o 3 0 1 11.17 17.82 3.39 o 4 0 1 15.66 30.83 4.88 o 5 0 1 9.00 17.38 2.78 o 6 0 1 14.53 13.34 5.34 o 7 0 1 97.33 87.60 11.22 o 8 0 1 0.77 6.79 5.45 o 9 0 1 17.03 14.13 6.49 o -10 1 1 154.00 155.21 11.58 o -9 1 1 115.57 117.18 8.66 o -8 1 1 5.04 1.78 5.90 o -7 1 1 33.65 27.68 5.14 o -6 1 1 332.76 339.24 9.21 o -5 1 1 813.36 892.02 22.02 o -4 1 1 465.17 512.46 17.83 o -3 1 1 38.36 55.67 5.60 o -2 1 1 6433.13 6291.14 42.81 o -1 1 1 5539.54 5468.17 29.85 o 0 1 1 469.20 502.00 4.18 o 1 1 1 401.29 407.34 9.69 o 2 1 1 906.91 938.06 14.75 o 3 1 1 554.29 546.76 14.42 o 4 1 1 739.81 772.76 20.45 o 5 1 1 2.51 -0.52 2.35 o 6 1 1 15.78 15.19 6.84 o 7 1 1 72.97 83.93 11.46 o 8 1 1 19.63 27.72 9.16 o 9 1 1 140.10 122.86 8.96 o -10 2 1 28.49 20.15 5.71 o -9 2 1 18.63 19.09 4.89 o -8 2 1 118.09 112.95 6.30 o -7 2 1 226.96 223.24 8.58 o -6 2 1 189.73 189.23 7.32 o -5 2 1 697.36 756.13 14.34 o -4 2 1 1342.63 1479.66 28.95 o -3 2 1 755.58 810.73 18.56 o -2 2 1 374.46 339.93 10.55 o -1 2 1 7232.05 6826.64 40.97 o 0 2 1 735.25 731.95 8.20 o 1 2 1 2005.24 2052.18 32.41 o 2 2 1 642.87 643.15 12.34 o 5 2 1 184.01 212.16 14.24 o 6 2 1 462.22 493.07 24.01 o 7 2 1 416.23 447.25 24.66 o 8 2 1 99.30 106.01 7.51 o 9 2 1 69.48 73.08 6.83 o -9 3 1 184.62 187.75 10.35 o -8 3 1 224.81 233.68 10.15 o -7 3 1 57.04 55.20 5.69 o -6 3 1 775.40 798.55 13.34 o -5 3 1 382.78 405.51 9.91 o -4 3 1 901.38 1031.27 15.48 o -3 3 1 450.38 506.59 15.61 o -2 3 1 1556.06 1651.47 25.41 o -1 3 1 5248.32 5064.80 42.52 o 0 3 1 2534.31 2567.43 27.70 o 1 3 1 346.56 379.11 8.65 o 2 3 1 281.35 292.40 9.01 o 3 3 1 279.72 256.89 10.10 o 4 3 1 56.90 54.44 3.44 o 5 3 1 11.69 13.68 6.22 o 6 3 1 0.46 -2.18 8.02 o 7 3 1 427.73 428.81 13.69 o 8 3 1 119.94 125.60 7.36 o 9 3 1 225.86 244.67 10.93 o -9 4 1 34.83 44.50 7.11 o -8 4 1 3.45 2.30 3.30 o -7 4 1 359.37 363.28 12.90 o -6 4 1 369.63 375.15 12.78 o -5 4 1 285.74 294.34 11.19 o -4 4 1 617.04 626.86 10.30 o -3 4 1 1304.67 1510.29 17.10 o -2 4 1 187.02 196.16 10.45 o -1 4 1 1196.18 1222.01 24.37 o 0 4 1 565.85 642.62 11.81 o 1 4 1 74.98 75.27 4.30 o 3 4 1 297.10 318.67 9.29 o 4 4 1 69.72 69.26 5.11 o 5 4 1 61.24 65.52 5.56 o 6 4 1 345.45 346.60 21.41 o 7 4 1 86.61 91.51 6.79 o 8 4 1 75.71 73.18 5.80 o -8 5 1 32.74 31.64 3.65 o -7 5 1 221.65 237.13 8.89 o -6 5 1 161.95 167.54 9.05 o -5 5 1 142.04 144.56 8.33 o -4 5 1 208.41 227.75 10.60 o -3 5 1 83.91 94.74 6.39 o -2 5 1 2152.82 2409.54 20.83 o -1 5 1 269.34 304.72 9.38 o 0 5 1 1061.27 1178.97 20.32 o 1 5 1 268.68 237.64 9.29 o 2 5 1 247.15 256.72 9.04 o 3 5 1 102.52 109.85 6.25 o 4 5 1 78.92 80.45 6.05 o 5 5 1 315.48 328.30 10.12 o 6 5 1 55.39 57.98 5.94 o 7 5 1 198.86 216.13 9.51 o 8 5 1 282.43 319.44 10.88 o -8 6 1 33.86 35.19 6.31 o -7 6 1 142.12 147.16 7.73 o -6 6 1 154.85 170.77 9.03 o -5 6 1 23.41 18.34 4.91 o -4 6 1 172.43 179.53 9.05 o -3 6 1 552.85 615.57 15.25 o -2 6 1 70.45 76.40 5.76 o -1 6 1 42.06 44.39 5.72 o 0 6 1 264.28 275.27 9.77 o 1 6 1 42.66 51.38 5.06 o 2 6 1 163.37 176.96 8.03 o 3 6 1 153.54 154.44 8.22 o 4 6 1 197.09 221.10 10.30 o 5 6 1 58.91 61.82 5.87 o 6 6 1 169.20 166.92 23.89 o 7 6 1 0.66 0.40 2.32 o -7 7 1 76.52 92.17 6.46 o -6 7 1 12.34 20.72 3.52 o -5 7 1 22.50 22.74 3.78 o -4 7 1 117.02 124.72 6.79 o -3 7 1 50.81 49.06 5.11 o -2 7 1 481.57 489.79 13.81 o -1 7 1 356.75 361.90 11.85 o 0 7 1 846.51 917.82 16.15 o 1 7 1 191.80 193.24 8.99 o 2 7 1 63.56 79.16 11.20 o 3 7 1 141.02 133.52 9.57 o 4 7 1 93.30 101.84 6.95 o 5 7 1 20.25 24.76 3.97 o 6 7 1 85.87 95.86 7.05 o -6 8 1 23.26 27.49 5.72 o -5 8 1 14.39 12.96 5.05 o -4 8 1 91.33 91.73 10.48 o -3 8 1 180.62 184.33 11.53 o -2 8 1 19.42 16.88 3.59 o -1 8 1 7.10 5.68 3.72 o 0 8 1 215.42 233.21 10.20 o 1 8 1 31.70 20.40 4.93 o 2 8 1 2.13 -2.59 2.59 o 3 8 1 147.26 160.99 9.88 o 4 8 1 110.96 115.22 8.31 o 5 8 1 39.54 40.03 6.94 o -4 9 1 74.01 72.21 8.87 o -3 9 1 33.03 33.85 7.14 o -2 9 1 14.25 22.17 4.83 o -1 9 1 391.34 370.72 10.67 o 0 9 1 1.36 6.77 6.15 o 1 9 1 39.00 52.26 9.16 o 2 9 1 39.22 48.58 8.33 o 3 9 1 16.51 16.65 6.48 o -4 -9 2 33.55 21.80 5.57 o -6 -8 2 38.19 36.55 6.54 o -5 -8 2 10.70 7.50 5.88 o 3 -8 2 27.61 29.62 6.71 o 4 -8 2 97.73 77.75 8.94 o 5 -8 2 52.57 47.00 7.73 o -7 -7 2 87.59 86.87 9.70 o -6 -7 2 48.87 45.14 9.65 o -5 -7 2 16.36 29.93 6.95 o 4 -7 2 50.55 39.34 8.01 o 5 -7 2 130.10 108.78 10.92 o 6 -7 2 123.74 110.96 10.83 o -7 -6 2 21.78 29.04 7.60 o -6 -6 2 49.46 58.04 10.63 o -2 -6 2 234.58 225.64 16.76 o -1 -6 2 186.07 189.32 14.66 o 1 -6 2 179.87 150.10 14.63 o 2 -6 2 440.16 377.48 23.76 o 3 -6 2 243.72 265.72 20.50 o 4 -6 2 2.90 5.79 5.15 o 5 -6 2 107.69 114.79 13.09 o 6 -6 2 22.16 26.44 7.46 o 7 -6 2 127.91 135.95 11.35 o -7 -5 2 52.84 32.58 8.60 o -6 -5 2 284.20 286.34 22.52 o -5 -5 2 27.82 24.37 9.15 o -2 -5 2 1396.37 1315.58 35.75 o -1 -5 2 118.96 121.13 10.71 o 2 -5 2 95.05 93.62 11.07 o 3 -5 2 27.69 30.78 7.64 o 4 -5 2 220.47 195.50 10.97 o 5 -5 2 516.17 486.77 17.63 o 6 -5 2 46.21 41.87 7.05 o 7 -5 2 9.74 3.28 4.50 o -7 -4 2 96.31 107.05 14.03 o -6 -4 2 78.20 98.36 31.79 o -5 -4 2 220.75 218.55 17.69 o -4 -4 2 76.60 54.99 8.91 o -2 -4 2 78.69 74.77 8.33 o -1 -4 2 662.37 609.55 19.73 o 2 -4 2 735.80 631.01 24.20 o 3 -4 2 385.90 332.46 30.22 o 4 -4 2 13.58 5.09 8.51 o 5 -4 2 471.39 434.71 13.85 o 6 -4 2 46.49 42.95 5.35 o 7 -4 2 752.82 764.84 29.64 o -9 -3 2 63.06 56.59 9.41 o -7 -3 2 12.50 7.53 5.95 o -6 -3 2 315.88 314.25 15.25 o -5 -3 2 14.99 18.96 3.67 o -4 -3 2 261.48 257.66 15.89 o -2 -3 2 37.95 37.95 5.32 o -1 -3 2 1718.89 1575.93 26.40 o 2 -3 2 978.26 875.70 24.81 o 3 -3 2 264.37 228.12 14.33 o 4 -3 2 92.68 84.54 6.79 o 5 -3 2 310.86 289.97 9.32 o 6 -3 2 202.07 179.54 9.70 o 7 -3 2 249.76 236.80 17.57 o 8 -3 2 89.64 101.69 11.05 o -9 -2 2 52.84 50.45 10.71 o -7 -2 2 13.90 7.12 8.50 o -6 -2 2 158.42 138.66 9.81 o -5 -2 2 119.80 122.62 8.04 o -4 -2 2 170.34 165.29 11.83 o -3 -2 2 2308.33 2147.67 34.60 o -1 -2 2 6633.88 5933.94 41.63 o 2 -2 2 2382.23 2167.34 33.11 o 3 -2 2 1348.62 1332.04 29.81 o 4 -2 2 227.95 208.38 10.20 o 5 -2 2 831.59 786.68 14.08 o 6 -2 2 372.31 359.77 12.16 o 8 -2 2 38.51 36.52 8.37 o 9 -2 2 39.81 44.66 6.80 o -10 -1 2 16.35 3.53 4.89 o -9 -1 2 215.36 214.94 17.36 o -8 -1 2 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