#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:44:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181284 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/62/2236247.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236247_Fobs loop_ _publ_author_name 'Tahir, M. Nawaz' 'Khan, Abdul Haleem' 'Iqbal, Mohammad S.' 'Shad, Hazoor Ahmad' 'Yaqub, Muhammad' _publ_section_title ; 2-[(E)-({4-[(4,6-Dimethylpyrimidin-2-yl)sulfamoyl]phenyl}iminio)methyl]-6-hydroxyphenolate ; _journal_coeditor_code HB6908 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2687 _journal_volume 68 _journal_year 2012 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.7506 _cell_length_b 12.1689 _cell_length_c 12.8408 _exptl_crystal_F_000 1664.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file hb6908Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' SMZEDIH in Pbcn RED PLATE' _shelx_refln_list_code 4 _shelx_f_calc_maximum 453.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 10209.31 10231.06 208.21 o 4 0 0 20463.66 20009.21 405.50 o 6 0 0 54.96 42.39 42.21 o 8 0 0 2791.27 2413.49 141.05 o 10 0 0 399.02 420.76 31.08 o 12 0 0 5.93 -26.77 18.53 o 14 0 0 2127.98 1927.35 109.13 o 16 0 0 954.76 1033.69 94.72 o 18 0 0 2264.62 2271.23 137.96 o 20 0 0 11.30 18.53 51.48 o 22 0 0 292.89 317.11 76.19 o 24 0 0 231.23 234.74 72.07 o 26 0 0 72.84 78.25 70.01 o 28 0 0 36.77 30.89 76.19 o 30 0 0 82.00 49.42 84.42 o 1 1 0 452.84 378.88 9.37 o 3 1 0 1664.82 1331.91 22.13 o 5 1 0 1743.22 1914.34 38.86 o 7 1 0 198.77 205.02 15.63 o 9 1 0 2631.99 2442.65 60.18 o 11 1 0 434.06 398.68 67.95 o 13 1 0 998.91 1083.53 76.19 o 15 1 0 1511.28 1390.71 96.78 o 17 1 0 3.97 -2.46 42.21 o 19 1 0 541.07 542.41 49.46 o 21 1 0 124.96 170.95 47.36 o 23 1 0 146.27 182.22 48.76 o 25 1 0 55.54 31.02 44.25 o 27 1 0 153.48 147.89 56.73 o 29 1 0 3.26 -38.28 73.10 o 0 2 0 752.39 1000.76 34.94 o 2 2 0 7701.03 7173.36 89.51 o 4 2 0 11021.86 10316.73 126.36 o 6 2 0 140.65 122.26 13.58 o 8 2 0 459.51 414.29 26.10 o 10 2 0 260.28 331.67 67.95 o 12 2 0 2721.47 2954.86 123.55 o 14 2 0 1750.25 1742.66 152.38 o 16 2 0 166.72 127.61 33.98 o 18 2 0 12.02 -8.74 23.54 o 20 2 0 68.75 89.19 64.86 o 22 2 0 234.65 249.44 50.45 o 24 2 0 168.43 185.53 51.67 o 26 2 0 144.99 145.04 53.01 o 28 2 0 30.16 87.31 54.24 o 30 2 0 4.55 10.40 56.73 o 1 3 0 2377.19 2298.38 42.33 o 3 3 0 19049.59 20257.87 240.65 o 5 3 0 245.23 267.77 16.20 o 7 3 0 2215.02 2220.25 50.43 o 9 3 0 294.43 319.95 32.54 o 11 3 0 2886.14 2953.07 93.05 o 13 3 0 139.40 129.49 29.61 o 15 3 0 1023.36 1006.99 61.56 o 17 3 0 18.35 23.17 25.13 o 19 3 0 34.08 53.15 30.67 o 21 3 0 213.72 265.04 44.18 o 23 3 0 74.00 93.14 45.30 o 25 3 0 0.16 -28.66 33.05 o 27 3 0 411.55 442.69 70.34 o 29 3 0 6.24 42.45 59.78 o 0 4 0 2181.34 2166.21 96.78 o 2 4 0 634.50 740.08 38.06 o 4 4 0 392.59 490.97 58.45 o 6 4 0 1994.84 1776.92 73.31 o 8 4 0 93.34 83.96 20.98 o 10 4 0 175.48 169.09 31.08 o 12 4 0 5862.48 6047.91 333.58 o 14 4 0 178.77 204.11 71.04 o 16 4 0 397.10 424.54 61.77 o 18 4 0 1810.24 1824.83 83.51 o 20 4 0 46.58 64.09 35.01 o 22 4 0 35.45 -2.32 31.78 o 24 4 0 130.26 87.00 38.07 o 26 4 0 137.51 199.74 88.54 o 28 4 0 28.73 32.95 82.37 o 1 5 0 94.79 60.40 20.21 o 3 5 0 375.03 414.13 70.92 o 5 5 0 2920.88 2759.33 82.97 o 7 5 0 3114.29 3319.97 83.97 o 9 5 0 1365.44 1321.77 51.09 o 11 5 0 2940.49 3101.34 104.04 o 13 5 0 973.77 954.88 91.63 o 15 5 0 1119.36 1273.30 81.34 o 17 5 0 279.96 286.64 43.03 o 19 5 0 78.09 104.28 40.15 o 21 5 0 0.50 -55.99 41.18 o 23 5 0 4.41 81.11 39.91 o 25 5 0 136.54 407.71 98.84 o 27 5 0 33.64 127.67 88.54 o 0 6 0 1196.95 1225.36 59.48 o 2 6 0 4467.21 4483.08 104.16 o 4 6 0 4380.06 4642.88 107.31 o 6 6 0 2776.12 2899.13 80.37 o 8 6 0 2668.78 2530.82 76.23 o 10 6 0 720.64 883.96 51.09 o 12 6 0 4617.25 4284.61 135.39 o 14 6 0 1298.74 1419.02 79.09 o 16 6 0 291.35 268.72 45.98 o 18 6 0 548.98 549.18 58.85 o 20 6 0 27.37 17.38 35.62 o 22 6 0 541.51 462.33 61.24 o 24 6 0 1.86 152.38 86.48 o 26 6 0 75.81 140.02 90.60 o 1 7 0 10.04 21.94 20.84 o 3 7 0 1706.17 1641.45 60.47 o 5 7 0 72.79 72.78 25.63 o 7 7 0 44.66 70.74 25.94 o 9 7 0 2476.55 2685.83 84.01 o 11 7 0 351.30 330.32 39.28 o 13 7 0 14.62 56.42 36.05 o 15 7 0 194.26 189.62 43.03 o 17 7 0 83.00 50.69 38.46 o 19 7 0 67.10 29.17 56.63 o 21 7 0 467.75 598.38 67.69 o 23 7 0 104.02 96.78 84.42 o 25 7 0 121.70 156.49 90.60 o 27 7 0 10.53 47.36 90.60 o 0 8 0 1557.35 1782.61 84.11 o 2 8 0 1542.73 1466.86 63.45 o 4 8 0 98.80 99.62 28.91 o 6 8 0 29.54 8.55 24.81 o 8 8 0 335.43 372.71 40.31 o 10 8 0 2673.83 2681.44 89.92 o 12 8 0 827.90 883.22 59.44 o 14 8 0 155.12 106.46 42.53 o 16 8 0 48.46 26.14 37.77 o 18 8 0 77.42 -31.12 36.53 o 20 8 0 197.41 105.84 47.97 o 22 8 0 97.47 113.14 48.32 o 24 8 0 6.14 20.59 84.42 o 1 9 0 18.32 -7.39 21.73 o 3 9 0 84.38 68.65 30.40 o 5 9 0 1245.29 1235.05 67.61 o 7 9 0 1016.21 915.65 72.96 o 9 9 0 467.41 426.50 46.09 o 11 9 0 299.99 274.43 43.03 o 13 9 0 22.72 73.39 34.31 o 15 9 0 944.05 910.54 79.92 o 17 9 0 443.20 528.28 67.41 o 19 9 0 7.92 -4.15 39.58 o 21 9 0 99.08 175.42 51.94 o 23 9 0 13.29 16.47 84.42 o 0 10 0 19.10 11.85 35.65 o 2 10 0 524.04 425.80 40.40 o 4 10 0 618.04 618.69 46.73 o 6 10 0 364.86 394.31 91.98 o 8 10 0 493.27 511.76 63.32 o 10 10 0 1279.86 1377.19 78.82 o 12 10 0 486.45 531.48 69.46 o 14 10 0 41.54 42.68 68.30 o 16 10 0 9.47 -39.16 91.63 o 18 10 0 82.26 39.03 85.45 o 20 10 0 90.76 185.96 56.28 o 22 10 0 7.05 -117.37 78.25 o 1 11 0 113.78 62.82 33.58 o 3 11 0 1.24 -11.53 27.21 o 5 11 0 109.50 51.12 30.72 o 7 11 0 7.62 -2.19 34.17 o 9 11 0 30.11 10.53 35.86 o 11 11 0 17.27 -15.70 35.43 o 13 11 0 1.09 20.35 37.16 o 15 11 0 22.89 -0.10 37.04 o 17 11 0 2.95 53.95 47.97 o 19 11 0 11.76 -11.44 46.61 o 0 12 0 67.15 42.26 45.71 o 2 12 0 279.63 311.82 41.98 o 4 12 0 124.64 132.13 36.45 o 6 12 0 884.72 939.99 63.01 o 8 12 0 7.04 -32.63 34.17 o 10 12 0 264.55 239.55 49.10 o 12 12 0 2.93 -6.29 38.79 o 14 12 0 30.23 54.42 43.18 o 16 12 0 188.54 166.55 62.15 o 18 12 0 3.92 29.18 66.92 o 1 13 0 123.47 89.83 40.94 o 3 13 0 256.33 312.71 56.77 o 5 13 0 28.75 36.42 34.98 o 7 13 0 21.47 13.89 33.58 o 9 13 0 119.86 88.92 38.86 o 11 13 0 63.06 109.22 46.96 o 13 13 0 0.68 -1.80 43.00 o 15 13 0 0.29 16.97 42.80 o 0 14 0 241.07 192.75 63.02 o 2 14 0 41.72 2.31 36.26 o 4 14 0 39.08 28.57 37.52 o 6 14 0 26.15 38.20 36.57 o 8 14 0 6.10 10.29 36.45 o 10 14 0 9.53 44.53 38.74 o 1 15 0 14.42 -35.11 37.10 o 1 1 1 21549.00 22458.95 199.43 o 2 1 1 792.00 522.88 11.49 o 3 1 1 63.09 115.78 5.61 o 4 1 1 29646.89 29513.47 251.15 o 5 1 1 3817.53 3571.31 36.80 o 6 1 1 605.61 589.01 16.59 o 7 1 1 980.31 812.45 17.88 o 8 1 1 1159.31 1353.52 28.31 o 9 1 1 4243.56 4259.85 61.78 o 10 1 1 997.79 1023.64 25.91 o 11 1 1 254.07 301.79 24.62 o 12 1 1 246.02 287.36 18.81 o 13 1 1 108.15 157.62 20.24 o 14 1 1 168.82 191.41 20.56 o 15 1 1 48.18 51.25 23.48 o 16 1 1 303.75 353.02 39.53 o 17 1 1 32.17 19.31 20.89 o 18 1 1 12.50 12.55 21.31 o 19 1 1 65.19 58.51 24.37 o 20 1 1 359.56 335.02 37.45 o 21 1 1 259.57 231.22 29.18 o 22 1 1 278.70 251.01 35.37 o 23 1 1 98.21 86.85 31.03 o 24 1 1 0.88 11.98 29.75 o 25 1 1 55.72 16.80 49.93 o 26 1 1 156.40 120.99 40.12 o 27 1 1 78.90 68.07 36.29 o 28 1 1 48.64 -24.02 37.45 o 29 1 1 14.62 32.55 39.78 o 30 1 1 0.02 -29.82 37.67 o 0 2 1 70546.82 70808.70 802.45 o 1 2 1 28946.79 25773.55 219.59 o 2 2 1 7294.03 7142.65 69.09 o 3 2 1 60.77 90.43 7.35 o 4 2 1 1813.60 1503.80 20.74 o 5 2 1 15624.65 14507.16 128.81 o 6 2 1 3975.15 4034.99 43.10 o 7 2 1 8064.90 7220.95 77.88 o 8 2 1 555.80 561.01 22.12 o 9 2 1 15.63 39.65 11.71 o 10 2 1 107.92 119.27 14.56 o 11 2 1 963.67 784.40 47.96 o 12 2 1 1166.64 1093.95 32.82 o 13 2 1 344.55 387.56 26.06 o 14 2 1 0.67 2.67 14.51 o 15 2 1 1.83 -8.53 14.57 o 16 2 1 1046.68 955.94 61.23 o 17 2 1 34.22 42.58 18.15 o 18 2 1 1.91 -23.09 15.39 o 19 2 1 59.25 74.47 20.93 o 20 2 1 0.57 -21.71 16.88 o 21 2 1 8.69 -16.62 23.91 o 22 2 1 9.68 -13.30 26.86 o 23 2 1 39.23 51.42 27.21 o 24 2 1 396.99 461.07 42.95 o 25 2 1 43.62 70.13 33.40 o 26 2 1 242.66 299.23 44.41 o 27 2 1 0.02 53.41 36.54 o 28 2 1 40.36 -4.46 35.42 o 29 2 1 2.65 46.62 40.18 o 30 2 1 7.38 -10.13 38.71 o 1 3 1 1148.49 1106.81 19.16 o 2 3 1 735.56 881.48 18.11 o 3 3 1 80.87 76.87 8.78 o 4 3 1 1101.32 1089.97 21.35 o 5 3 1 921.53 799.51 22.47 o 6 3 1 2402.29 2412.78 42.39 o 7 3 1 630.44 619.50 22.57 o 8 3 1 449.61 455.80 20.36 o 9 3 1 1444.79 1528.83 35.77 o 10 3 1 1505.87 1471.61 37.42 o 11 3 1 683.05 743.80 30.30 o 12 3 1 3353.83 3246.05 70.60 o 13 3 1 0.44 -3.16 16.35 o 14 3 1 1170.18 1230.12 56.17 o 15 3 1 268.86 287.65 30.02 o 16 3 1 0.18 3.24 23.78 o 17 3 1 76.60 111.00 21.10 o 18 3 1 74.76 33.37 19.74 o 19 3 1 201.45 192.50 35.36 o 20 3 1 23.68 24.31 21.81 o 21 3 1 25.67 50.88 21.96 o 22 3 1 50.51 39.03 23.01 o 23 3 1 0.15 -11.03 32.10 o 24 3 1 0.01 6.67 30.83 o 25 3 1 16.30 47.87 35.68 o 26 3 1 71.01 76.33 37.20 o 27 3 1 0.45 18.30 29.94 o 28 3 1 8.36 -25.28 35.24 o 29 3 1 3.31 53.47 41.49 o 0 4 1 21.89 21.66 14.90 o 1 4 1 420.63 354.66 16.22 o 2 4 1 6312.81 6410.54 81.52 o 3 4 1 913.78 952.90 36.15 o 4 4 1 3425.92 3432.31 55.52 o 5 4 1 129.11 112.27 14.37 o 6 4 1 5603.34 5544.37 80.79 o 7 4 1 3180.30 3025.16 52.76 o 8 4 1 746.63 859.20 32.50 o 9 4 1 1425.92 1361.95 37.87 o 10 4 1 301.84 291.94 22.10 o 11 4 1 3586.23 3634.80 77.82 o 12 4 1 2239.58 2407.38 61.26 o 13 4 1 594.83 575.34 34.71 o 14 4 1 1195.63 1214.77 45.81 o 15 4 1 0.32 12.88 18.40 o 16 4 1 230.63 221.57 26.82 o 17 4 1 671.20 733.31 41.74 o 18 4 1 62.73 56.59 21.89 o 19 4 1 61.40 45.06 22.03 o 20 4 1 2.26 -27.79 18.53 o 21 4 1 2.96 -7.83 21.73 o 22 4 1 1.51 0.82 20.00 o 23 4 1 163.63 179.39 29.86 o 24 4 1 15.03 -10.86 42.09 o 25 4 1 5.16 27.53 34.45 o 26 4 1 32.83 6.72 33.72 o 27 4 1 13.43 83.33 93.69 o 28 4 1 29.51 131.92 64.78 o 29 4 1 0.02 16.00 71.72 o 1 5 1 3050.18 2974.33 52.99 o 2 5 1 1302.59 1511.24 39.11 o 3 5 1 342.19 436.16 30.24 o 4 5 1 53.98 67.43 14.29 o 5 5 1 61.37 98.10 15.44 o 6 5 1 10.16 6.99 13.08 o 7 5 1 2799.65 2610.20 50.79 o 8 5 1 284.61 258.65 20.45 o 9 5 1 1592.44 1517.19 38.78 o 10 5 1 1664.97 1757.77 47.17 o 11 5 1 854.19 876.04 37.72 o 12 5 1 256.92 267.24 24.30 o 13 5 1 1617.65 1703.81 54.64 o 14 5 1 158.38 143.82 25.24 o 15 5 1 556.08 522.14 36.83 o 16 5 1 719.49 731.92 42.76 o 17 5 1 316.86 303.87 31.80 o 18 5 1 11.22 -23.58 20.05 o 19 5 1 92.05 118.10 26.09 o 20 5 1 186.44 161.95 28.47 o 21 5 1 220.35 275.35 32.39 o 22 5 1 341.56 426.36 39.50 o 23 5 1 36.43 25.63 31.64 o 24 5 1 19.43 109.68 39.20 o 25 5 1 37.44 45.88 44.03 o 26 5 1 30.65 -4.15 73.10 o 27 5 1 5.17 35.47 61.10 o 28 5 1 53.80 62.48 63.02 o 0 6 1 5527.82 5791.19 125.46 o 1 6 1 476.05 471.52 25.45 o 2 6 1 151.40 110.88 18.72 o 3 6 1 197.97 157.93 18.09 o 4 6 1 43.95 40.23 18.72 o 5 6 1 3305.32 3521.19 63.70 o 6 6 1 3.69 16.67 17.22 o 7 6 1 106.59 116.20 18.23 o 8 6 1 34.85 31.09 20.72 o 9 6 1 468.86 495.02 27.65 o 10 6 1 202.72 216.47 24.59 o 11 6 1 170.88 152.73 22.94 o 12 6 1 641.93 613.24 38.96 o 13 6 1 462.86 497.65 33.34 o 14 6 1 43.58 61.43 23.15 o 15 6 1 117.91 83.37 24.63 o 16 6 1 491.27 534.93 39.95 o 17 6 1 1.90 -14.60 27.64 o 18 6 1 112.67 100.78 33.03 o 19 6 1 33.21 33.75 33.58 o 20 6 1 18.41 30.87 26.25 o 21 6 1 25.60 46.46 26.77 o 22 6 1 0.12 -14.20 24.50 o 23 6 1 74.38 85.07 38.47 o 24 6 1 6.44 13.22 33.90 o 25 6 1 1.15 -40.55 38.68 o 26 6 1 0.17 -3.06 56.73 o 27 6 1 8.23 -2.79 81.34 o 1 7 1 179.38 194.13 21.03 o 2 7 1 1528.33 1494.18 38.27 o 3 7 1 230.14 235.28 20.56 o 4 7 1 169.01 182.46 20.66 o 5 7 1 10.07 4.39 15.89 o 6 7 1 52.80 85.40 18.02 o 7 7 1 1640.14 1644.40 45.03 o 8 7 1 1122.19 1096.89 41.00 o 9 7 1 1388.33 1579.38 51.42 o 10 7 1 354.65 370.25 27.56 o 11 7 1 399.79 395.36 28.52 o 12 7 1 227.47 271.89 28.32 o 13 7 1 8.29 22.25 20.96 o 14 7 1 591.95 543.05 36.44 o 15 7 1 12.09 47.43 25.12 o 16 7 1 552.82 550.44 43.02 o 17 7 1 1.45 24.08 25.81 o 18 7 1 101.08 107.15 28.62 o 19 7 1 2.05 14.32 25.18 o 20 7 1 45.25 11.17 26.45 o 21 7 1 90.53 54.66 30.61 o 22 7 1 3.33 32.33 36.19 o 23 7 1 21.79 -12.96 36.22 o 24 7 1 105.16 118.94 43.44 o 25 7 1 11.86 64.43 60.41 o 26 7 1 2.35 -8.66 60.10 o 0 8 1 86.86 75.30 28.33 o 1 8 1 10.79 -21.26 14.63 o 2 8 1 328.30 289.18 23.14 o 3 8 1 1.14 -16.72 14.82 o 4 8 1 280.97 266.92 23.25 o 5 8 1 263.72 247.24 24.56 o 6 8 1 615.32 550.52 32.84 o 7 8 1 596.61 543.10 32.33 o 8 8 1 0.44 -5.97 23.14 o 9 8 1 17.22 5.12 18.98 o 10 8 1 330.56 322.11 28.26 o 11 8 1 873.04 866.30 41.17 o 12 8 1 709.48 667.72 39.60 o 13 8 1 339.40 309.36 32.88 o 14 8 1 411.79 356.05 40.96 o 15 8 1 20.77 53.97 27.54 o 16 8 1 24.15 23.58 27.04 o 17 8 1 462.15 452.71 50.23 o 18 8 1 93.50 212.43 34.43 o 19 8 1 50.71 66.32 32.40 o 20 8 1 65.70 81.85 37.75 o 21 8 1 42.69 -6.27 38.78 o 22 8 1 68.57 81.61 42.72 o 23 8 1 15.16 48.65 40.60 o 24 8 1 1.95 -53.54 63.83 o 25 8 1 11.86 -14.29 67.95 o 1 9 1 59.45 28.60 18.48 o 2 9 1 430.30 384.99 27.78 o 3 9 1 694.45 610.45 32.81 o 4 9 1 43.38 45.56 18.59 o 5 9 1 323.27 333.18 27.04 o 6 9 1 174.64 189.85 25.85 o 7 9 1 1401.52 1306.20 59.40 o 8 9 1 3.54 -9.16 20.02 o 9 9 1 3.75 19.96 21.12 o 10 9 1 289.06 246.23 29.83 o 11 9 1 286.62 285.66 30.38 o 12 9 1 28.16 41.95 23.32 o 13 9 1 254.41 248.10 33.10 o 14 9 1 38.04 27.84 25.71 o 15 9 1 111.03 33.54 26.83 o 16 9 1 115.00 179.76 46.07 o 17 9 1 8.66 61.16 30.00 o 18 9 1 6.83 -12.18 28.38 o 19 9 1 4.47 -14.34 29.11 o 20 9 1 6.95 -6.45 37.88 o 21 9 1 5.30 12.25 37.81 o 22 9 1 21.72 -13.09 41.43 o 23 9 1 0.05 -15.54 61.10 o 24 9 1 0.02 69.80 64.68 o 0 10 1 32.66 21.18 26.31 o 1 10 1 335.55 311.11 26.02 o 2 10 1 141.40 115.90 23.07 o 3 10 1 123.49 89.53 22.62 o 4 10 1 6.95 34.84 20.91 o 5 10 1 1086.25 934.44 49.38 o 6 10 1 1682.99 1686.03 54.35 o 7 10 1 129.08 167.60 27.86 o 8 10 1 349.85 374.07 33.42 o 9 10 1 581.81 496.57 36.93 o 10 10 1 1202.32 1224.55 52.49 o 11 10 1 561.85 581.15 39.11 o 12 10 1 20.39 6.49 23.65 o 13 10 1 47.88 61.07 26.36 o 14 10 1 142.23 104.78 30.23 o 15 10 1 50.88 49.53 29.12 o 16 10 1 135.03 125.09 34.13 o 17 10 1 12.44 8.63 30.94 o 18 10 1 2.42 2.30 31.55 o 19 10 1 33.08 66.13 46.89 o 20 10 1 0.95 -53.15 38.69 o 21 10 1 32.10 -27.43 40.22 o 22 10 1 4.49 8.24 64.07 o 1 11 1 0.07 -0.34 19.36 o 2 11 1 248.87 243.00 26.62 o 3 11 1 138.32 140.54 23.26 o 4 11 1 79.86 44.63 22.50 o 5 11 1 0.02 3.75 21.09 o 6 11 1 38.16 10.41 21.08 o 7 11 1 21.23 38.78 23.05 o 8 11 1 66.67 55.89 24.00 o 9 11 1 12.73 -27.13 23.92 o 10 11 1 398.29 461.16 38.13 o 11 11 1 0.10 -8.09 25.08 o 12 11 1 406.68 459.04 38.92 o 13 11 1 17.51 57.45 27.93 o 14 11 1 3.16 -24.85 27.33 o 15 11 1 309.96 304.88 39.61 o 16 11 1 61.91 138.33 34.28 o 17 11 1 112.02 133.03 38.93 o 18 11 1 6.00 -6.01 33.85 o 19 11 1 11.76 10.79 70.49 o 20 11 1 13.55 57.82 46.39 o 0 12 1 142.01 173.45 36.55 o 1 12 1 69.82 17.36 21.96 o 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27.54 119.91 52.42 o 1 8 13 0.30 -10.22 31.98 o 2 8 13 27.13 31.99 32.41 o 3 8 13 0.42 -27.23 35.80 o 4 8 13 5.53 24.22 32.82 o 5 8 13 68.59 114.38 37.60 o 6 8 13 102.27 81.39 39.40 o 0 0 14 709.31 805.12 107.08 o 1 0 14 9.93 45.94 40.02 o 2 0 14 443.31 448.36 60.10 o 3 0 14 62.89 15.56 52.51 o 4 0 14 52.97 64.33 167.82 o 5 0 14 17.79 -24.71 53.54 o 6 0 14 382.18 529.20 102.96 o 7 0 14 27.27 86.48 67.95 o 8 0 14 45.50 -51.48 51.48 o 9 0 14 8.24 -59.72 53.54 o 10 0 14 6.44 20.59 63.83 o 11 0 14 0.27 -32.95 61.77 o 12 0 14 129.05 28.83 67.95 o 13 0 14 37.92 37.06 70.01 o 14 0 14 34.60 109.13 78.25 o 1 1 14 16.38 12.25 26.26 o 2 1 14 15.10 8.39 27.09 o 3 1 14 3.81 -14.25 24.82 o 4 1 14 4.92 8.32 31.03 o 5 1 14 48.01 29.86 42.22 o 6 1 14 64.06 124.52 49.44 o 7 1 14 5.41 50.21 43.61 o 8 1 14 32.17 13.13 44.25 o 9 1 14 16.22 -21.76 41.92 o 10 1 14 5.87 -27.64 41.32 o 11 1 14 69.03 -39.46 44.25 o 12 1 14 0.48 -37.53 41.92 o 13 1 14 22.02 7.68 48.63 o 14 1 14 7.91 34.06 65.89 o 0 2 14 215.32 140.48 79.28 o 1 2 14 0.23 93.27 33.94 o 2 2 14 49.14 38.46 32.30 o 3 2 14 81.94 82.42 36.20 o 4 2 14 1.86 -5.09 35.17 o 5 2 14 0.72 -22.94 29.69 o 6 2 14 39.48 22.65 41.32 o 7 2 14 3.09 -2.79 40.69 o 8 2 14 0.24 31.85 43.61 o 9 2 14 42.26 -1.37 43.61 o 10 2 14 0.02 23.73 44.25 o 11 2 14 25.55 -13.48 91.63 o 12 2 14 35.60 52.79 50.22 o 13 2 14 0.63 -23.65 49.44 o 1 3 14 174.63 134.00 49.44 o 2 3 14 1.30 -32.09 38.07 o 3 3 14 14.83 31.75 41.32 o 4 3 14 124.60 159.58 50.96 o 5 3 14 5.45 4.74 40.69 o 6 3 14 12.92 -14.41 39.31 o 7 3 14 134.01 146.20 74.13 o 8 3 14 4.17 -26.77 63.83 o 9 3 14 256.44 302.69 92.66 o 10 3 14 0.20 -2.06 70.01 o 11 3 14 98.26 55.60 76.19 o 12 3 14 4.84 92.66 78.25 o 0 4 14 15.12 24.71 59.72 o 1 4 14 77.81 0.00 42.22 o 2 4 14 35.10 69.03 45.71 o 3 4 14 25.04 59.85 43.54 o 4 4 14 1.64 18.64 41.32 o 5 4 14 31.42 9.32 42.49 o 6 4 14 28.75 50.90 48.39 o 7 4 14 0.72 12.35 61.77 o 8 4 14 0.95 86.48 74.13 o 9 4 14 5.32 -43.24 61.77 o 10 4 14 77.34 51.48 72.07 o 11 4 14 37.94 61.77 78.25 o 1 5 14 154.34 138.92 53.13 o 2 5 14 4.40 -47.09 40.15 o 3 5 14 98.31 120.29 63.83 o 4 5 14 0.11 -22.44 43.03 o 5 5 14 83.76 64.29 45.02 o 6 5 14 0.11 -22.65 62.80 o 7 5 14 76.99 63.15 47.00 o 8 5 14 0.21 -45.72 38.03 o 9 5 14 2.15 -61.77 41.18 o 10 5 14 8.30 4.56 45.32 o 0 6 14 183.49 121.94 57.66 o 1 6 14 134.09 171.69 36.98 o 2 6 14 64.88 56.70 32.12 o 3 6 14 0.02 -7.84 27.78 o 4 6 14 0.01 -29.97 34.21 o 5 6 14 9.98 30.17 32.25 o 6 6 14 139.34 149.64 37.42 o 7 6 14 4.30 14.73 31.85 o 1 7 14 0.20 -3.62 30.44 o 1 1 15 1.82 -11.97 30.13 o 2 1 15 140.40 146.61 58.14 o 3 1 15 28.81 82.12 49.25 o 4 1 15 26.31 -8.62 81.34 o 5 1 15 19.59 -51.63 39.23 o 6 1 15 1.06 -3.29 43.03 o 7 1 15 3.02 25.87 47.36 o 8 1 15 17.72 8.45 86.48 o 9 1 15 10.64 7.05 47.98 o 0 2 15 116.98 187.38 74.13 o 1 2 15 20.78 -3.21 86.48 o 2 2 15 13.16 -15.27 38.40 o 3 2 15 81.08 86.59 38.27 o 4 2 15 3.54 27.78 44.39 o 5 2 15 199.74 173.79 54.24 o 6 2 15 25.71 53.06 47.17 o 7 2 15 24.74 117.48 53.13 o 8 2 15 6.40 -55.60 42.93 o 1 3 15 19.76 37.48 43.61 o 2 3 15 99.75 124.14 51.48 o 3 3 15 4.71 22.58 45.07 o 4 3 15 0.06 7.21 54.57 o 5 3 15 6.07 -80.31 53.54 o 6 3 15 10.80 -86.48 57.66 o 7 3 15 19.82 142.08 78.25 o 0 4 15 123.34 189.44 76.19 o 1 4 15 95.39 19.18 110.16 o 2 4 15 20.27 -29.94 45.85 o 3 4 15 0.10 0.14 42.79 o 4 4 15 9.76 19.42 47.17 o 5 4 15 145.11 115.31 80.31 o