#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/62/2236283.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236283_Fobs loop_ _publ_author_name 'Lough, Alan J.' 'Jack, Kelsey' 'Tam, William' _publ_section_title ; Tetramethyl 1,4-dimethyl-13,14-dioxapentacyclo[8.2.1.1^4,7^.0^2,9^.0^3,8^]tetradeca-5,11-diene-5,6,11,12-tetracarboxylate ; _journal_coeditor_code HB6952 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2961 _journal_volume 68 _journal_year 2012 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 11.5170 _cell_length_b 13.9586 _cell_length_c 26.4126 _exptl_crystal_F_000 1888.00 _reflns_d_resolution_high 0.7699 _[local]_cod_data_source_file hb6952Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_d12104_0m in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 275.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' '-x, -y, -z' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' 'x-1/2, y, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 17651.40 17027.21 170.70 o 4 0 0 45671.00 45865.31 396.94 o 6 0 0 883.10 588.81 82.34 o 8 0 0 598.89 439.86 91.27 o 10 0 0 9750.79 9381.86 319.07 o 12 0 0 1076.09 959.14 155.16 o 14 0 0 12.64 16.12 104.67 o 2 1 0 31666.27 30425.88 963.70 o 4 1 0 40.44 50.46 26.00 o 6 1 0 8637.53 9090.39 160.28 o 8 1 0 1158.19 1052.37 81.60 o 10 1 0 3.85 21.27 49.93 o 12 1 0 0.55 68.60 63.71 o 14 1 0 76.23 -13.39 74.50 o 0 2 0 1.88 27.77 19.61 o 2 2 0 21509.72 19509.74 583.85 o 4 2 0 4249.17 3946.94 126.13 o 6 2 0 110.55 122.08 35.78 o 8 2 0 7248.46 7615.42 177.88 o 10 2 0 164.79 155.08 58.70 o 12 2 0 116.97 145.77 69.36 o 14 2 0 564.90 500.55 104.52 o 2 3 0 3275.42 3159.62 70.86 o 4 3 0 19103.38 19388.43 199.39 o 6 3 0 3084.83 3468.37 108.28 o 8 3 0 608.21 604.33 72.02 o 10 3 0 2790.74 2626.79 132.55 o 12 3 0 53.69 136.53 69.04 o 14 3 0 650.56 697.70 118.85 o 0 4 0 23818.21 23196.08 250.71 o 2 4 0 5391.76 5371.07 117.49 o 4 4 0 105.70 103.29 30.85 o 6 4 0 1791.04 1713.97 82.75 o 8 4 0 120.00 157.07 49.75 o 10 4 0 112.41 154.70 61.48 o 12 4 0 2.67 -1.27 67.10 o 14 4 0 10.07 22.28 77.86 o 2 5 0 1004.34 1168.61 63.11 o 4 5 0 3555.59 3726.29 202.45 o 6 5 0 2568.64 2424.62 81.32 o 8 5 0 236.01 218.98 53.92 o 10 5 0 9902.21 9246.27 250.13 o 12 5 0 363.13 359.03 85.56 o 14 5 0 61.16 58.76 80.67 o 0 6 0 577.47 507.24 66.61 o 2 6 0 663.92 644.68 52.57 o 4 6 0 2719.05 2673.68 94.61 o 6 6 0 1680.52 1625.14 88.98 o 8 6 0 4661.00 4282.39 147.97 o 10 6 0 1964.91 1907.06 102.38 o 12 6 0 1611.22 1582.25 107.01 o 14 6 0 1183.11 1397.79 121.17 o 2 7 0 7808.05 7882.95 147.68 o 4 7 0 1107.79 1204.79 74.36 o 6 7 0 752.39 844.68 75.13 o 8 7 0 134.08 109.31 49.82 o 10 7 0 2705.88 2631.90 143.56 o 12 7 0 14.36 14.22 61.40 o 0 8 0 5406.65 5653.86 186.43 o 2 8 0 3453.23 3559.42 132.54 o 4 8 0 2226.50 2444.93 100.65 o 6 8 0 451.23 463.01 68.45 o 8 8 0 124.93 156.60 57.41 o 10 8 0 29.33 53.16 59.01 o 12 8 0 50.18 14.24 64.42 o 2 9 0 1012.54 1198.85 77.72 o 4 9 0 765.02 851.25 79.04 o 6 9 0 315.06 244.38 56.70 o 8 9 0 0.38 -18.57 46.07 o 10 9 0 1130.74 1246.78 117.49 o 12 9 0 286.25 244.34 84.67 o 0 10 0 9.96 35.34 49.71 o 2 10 0 454.14 514.90 66.39 o 4 10 0 341.59 400.13 66.60 o 6 10 0 218.59 183.23 53.08 o 8 10 0 37.73 60.68 55.30 o 10 10 0 41.26 -1.54 61.28 o 12 10 0 6.01 -61.76 64.68 o 2 11 0 1037.14 966.21 100.01 o 4 11 0 290.03 401.42 107.68 o 6 11 0 906.96 968.71 95.54 o 8 11 0 196.50 88.05 61.96 o 10 11 0 223.69 364.02 85.48 o 0 12 0 2316.83 1894.98 156.33 o 2 12 0 10.14 35.84 45.81 o 4 12 0 1712.83 1662.30 110.56 o 6 12 0 53.30 16.90 51.45 o 8 12 0 253.68 267.32 74.67 o 10 12 0 302.22 213.73 82.04 o 2 13 0 845.79 901.56 94.71 o 4 13 0 2156.48 1868.41 121.59 o 6 13 0 168.23 191.58 72.34 o 8 13 0 67.05 5.37 60.30 o 10 13 0 182.42 174.81 80.88 o 0 14 0 1513.33 1749.52 169.15 o 2 14 0 846.76 843.66 102.44 o 4 14 0 1014.64 942.84 105.30 o 6 14 0 21.80 -7.27 56.85 o 8 14 0 10.88 -36.37 60.22 o 2 15 0 825.93 917.92 105.08 o 4 15 0 525.88 635.88 104.07 o 6 15 0 164.87 153.26 74.01 o 8 15 0 158.12 243.44 83.83 o 0 16 0 44.88 78.65 92.24 o 2 16 0 1.00 12.30 60.15 o 4 16 0 155.78 8.96 61.88 o 6 16 0 101.37 117.30 72.40 o 2 17 0 354.92 360.22 88.63 o 4 17 0 23.19 -45.97 58.90 o 0 18 0 56.41 65.83 108.17 o 1 1 1 15757.95 15112.92 266.37 o 2 1 1 300.22 265.48 20.77 o 3 1 1 14300.79 14270.78 98.60 o 4 1 1 5845.49 5613.31 77.62 o 5 1 1 50.22 58.23 21.08 o 6 1 1 265.33 360.94 36.98 o 7 1 1 18.51 29.70 24.87 o 8 1 1 260.70 273.00 37.32 o 9 1 1 407.15 402.04 47.12 o 10 1 1 1357.60 1344.12 72.10 o 11 1 1 141.48 110.80 43.24 o 12 1 1 119.48 104.71 46.37 o 13 1 1 239.44 283.78 58.09 o 14 1 1 70.10 46.59 52.60 o 0 2 1 398.06 391.67 11.63 o 1 2 1 74641.74 71851.17 309.14 o 2 2 1 2100.20 2021.22 34.57 o 3 2 1 104.07 88.54 18.02 o 4 2 1 5507.42 5382.19 73.98 o 5 2 1 1270.36 1383.42 48.22 o 6 2 1 345.57 363.32 35.87 o 7 2 1 1221.03 1247.36 54.99 o 8 2 1 3494.99 3581.51 90.18 o 9 2 1 2622.65 2524.48 85.02 o 10 2 1 300.26 310.36 48.18 o 11 2 1 65.84 91.70 41.14 o 12 2 1 160.59 185.19 50.88 o 13 2 1 23.35 -3.32 45.72 o 14 2 1 100.31 187.97 61.31 o 1 3 1 23706.59 22743.59 113.49 o 2 3 1 36163.77 35394.21 176.53 o 3 3 1 21.83 23.50 14.62 o 4 3 1 3.17 -0.77 17.81 o 5 3 1 47.92 54.48 22.14 o 6 3 1 650.37 691.99 57.03 o 7 3 1 7394.19 7378.71 141.27 o 8 3 1 968.59 1007.63 68.87 o 9 3 1 408.20 355.44 46.32 o 10 3 1 1168.37 1079.59 70.31 o 11 3 1 120.83 100.42 44.05 o 12 3 1 249.81 250.77 52.71 o 13 3 1 254.24 328.25 62.12 o 14 3 1 2.74 14.15 52.74 o 0 4 1 76031.33 73190.10 583.13 o 1 4 1 1.11 19.30 15.93 o 2 4 1 853.71 738.60 32.14 o 3 4 1 1877.20 2271.62 51.72 o 4 4 1 128.31 116.11 21.11 o 5 4 1 511.92 558.73 39.32 o 6 4 1 571.10 654.38 44.18 o 7 4 1 44.07 43.80 26.24 o 8 4 1 116.70 104.35 33.21 o 9 4 1 67.38 10.63 31.33 o 10 4 1 466.22 459.42 55.52 o 11 4 1 0.11 -16.89 39.10 o 12 4 1 144.55 127.07 47.86 o 13 4 1 929.14 948.00 85.39 o 14 4 1 14.58 39.22 54.91 o 1 5 1 6486.76 6253.38 105.73 o 2 5 1 22.47 29.06 17.96 o 3 5 1 201.48 305.93 30.64 o 4 5 1 274.81 323.88 34.18 o 5 5 1 2118.33 2078.89 61.84 o 6 5 1 163.70 213.93 27.99 o 7 5 1 352.45 339.66 46.51 o 8 5 1 5.75 -2.28 27.60 o 9 5 1 4.80 17.57 32.93 o 10 5 1 97.56 65.33 37.93 o 11 5 1 2122.21 2066.63 93.73 o 12 5 1 14.72 15.37 43.66 o 13 5 1 12.93 26.89 49.26 o 14 5 1 244.41 288.17 67.43 o 0 6 1 1616.24 1562.96 33.89 o 1 6 1 5203.09 5788.11 81.86 o 2 6 1 762.04 710.17 37.28 o 3 6 1 349.68 304.00 33.70 o 4 6 1 2353.04 2346.45 62.74 o 5 6 1 5762.59 6278.29 104.94 o 6 6 1 1592.19 1566.98 61.43 o 7 6 1 271.53 249.03 36.11 o 8 6 1 844.52 870.09 60.11 o 9 6 1 232.86 246.70 36.69 o 10 6 1 1.99 16.84 29.69 o 11 6 1 65.40 79.20 35.42 o 12 6 1 73.62 83.36 39.21 o 13 6 1 201.28 252.37 48.44 o 14 6 1 39.99 31.96 44.54 o 1 7 1 5707.83 5624.85 109.43 o 2 7 1 119.32 90.75 23.47 o 3 7 1 3943.09 4129.67 114.59 o 4 7 1 264.16 250.96 31.60 o 5 7 1 56.30 36.22 24.59 o 6 7 1 26.63 25.27 26.81 o 7 7 1 629.19 721.74 54.45 o 8 7 1 273.54 265.64 43.29 o 9 7 1 850.09 812.12 65.91 o 10 7 1 664.34 609.28 64.41 o 11 7 1 900.24 822.89 75.17 o 12 7 1 357.00 431.67 64.01 o 13 7 1 1.20 31.73 49.75 o 0 8 1 2377.33 2289.85 88.14 o 1 8 1 860.39 865.83 45.40 o 2 8 1 1046.70 1096.53 49.89 o 3 8 1 1153.48 1282.28 53.00 o 4 8 1 86.23 104.54 27.43 o 5 8 1 902.71 885.56 53.17 o 6 8 1 883.33 912.83 57.55 o 7 8 1 1176.41 1179.50 66.03 o 8 8 1 152.39 160.15 39.51 o 9 8 1 924.05 875.74 68.86 o 10 8 1 144.09 115.73 43.39 o 11 8 1 0.28 -38.24 38.24 o 12 8 1 1.88 3.93 46.29 o 13 8 1 20.92 36.18 52.03 o 1 9 1 2251.48 2421.06 47.92 o 2 9 1 740.56 654.76 44.20 o 3 9 1 2633.39 2771.12 86.58 o 4 9 1 234.77 182.15 33.90 o 5 9 1 117.45 122.77 32.73 o 6 9 1 6.35 -14.29 29.28 o 7 9 1 129.81 172.53 39.91 o 8 9 1 57.43 29.40 35.59 o 9 9 1 698.18 745.63 68.25 o 10 9 1 3.07 2.46 41.03 o 11 9 1 21.33 17.82 43.52 o 12 9 1 116.62 91.37 52.30 o 0 10 1 1228.30 1196.63 112.15 o 1 10 1 432.76 389.79 25.64 o 2 10 1 8.84 1.12 24.17 o 3 10 1 53.11 46.42 27.57 o 4 10 1 0.09 4.90 28.63 o 5 10 1 1925.07 1805.69 73.60 o 6 10 1 135.47 95.38 36.80 o 7 10 1 451.11 453.93 54.96 o 8 10 1 3.21 -9.91 35.25 o 9 10 1 373.56 349.89 55.42 o 10 10 1 14.29 37.27 44.01 o 11 10 1 634.40 767.41 81.30 o 12 10 1 28.18 20.96 50.58 o 1 11 1 5.83 -2.30 27.07 o 2 11 1 239.27 220.42 28.01 o 3 11 1 801.18 841.68 58.53 o 4 11 1 16.17 7.53 31.28 o 5 11 1 710.88 643.97 58.73 o 6 11 1 9.14 23.64 33.31 o 7 11 1 57.32 34.71 38.18 o 8 11 1 371.54 409.87 57.89 o 9 11 1 79.72 80.36 45.97 o 10 11 1 19.56 -0.89 42.05 o 11 11 1 149.66 117.92 54.92 o 0 12 1 157.89 175.44 54.57 o 1 12 1 1024.00 976.69 63.38 o 2 12 1 8.65 -12.54 29.70 o 3 12 1 1865.82 1812.59 79.09 o 4 12 1 43.61 48.61 34.91 o 5 12 1 560.32 603.50 61.59 o 6 12 1 32.12 -9.04 36.00 o 7 12 1 1062.87 1056.33 76.09 o 8 12 1 30.12 61.99 42.51 o 9 12 1 25.51 35.74 44.64 o 10 12 1 3.85 0.37 45.51 o 11 12 1 56.69 26.02 52.84 o 1 13 1 589.35 573.25 59.55 o 2 13 1 148.40 225.61 43.30 o 3 13 1 802.40 841.62 65.65 o 4 13 1 12.93 49.81 37.19 o 5 13 1 1346.80 1308.79 78.49 o 6 13 1 0.06 0.30 37.40 o 7 13 1 472.62 530.00 66.02 o 8 13 1 52.35 -3.57 41.92 o 9 13 1 0.03 -22.24 45.49 o 10 13 1 142.61 131.69 55.28 o 0 14 1 85.76 173.87 61.45 o 1 14 1 655.29 629.19 63.30 o 2 14 1 79.56 77.79 38.95 o 3 14 1 226.36 165.35 45.25 o 4 14 1 3.10 -5.08 37.04 o 5 14 1 94.69 135.88 45.13 o 6 14 1 272.22 176.94 50.66 o 7 14 1 2.51 -39.04 39.04 o 8 14 1 138.22 124.16 50.22 o 9 14 1 52.63 76.53 51.13 o 1 15 1 0.03 -36.02 36.02 o 2 15 1 1.04 -8.95 38.89 o 3 15 1 82.31 46.84 41.81 o 4 15 1 32.22 18.25 40.56 o 5 15 1 184.41 214.61 51.91 o 6 15 1 3.51 -40.46 40.46 o 7 15 1 73.08 68.03 49.34 o 8 15 1 0.68 -8.91 46.68 o 0 16 1 3.76 46.04 59.72 o 1 16 1 0.03 -4.91 40.22 o 2 16 1 80.57 77.04 45.22 o 3 16 1 93.22 84.86 47.36 o 4 16 1 42.34 -0.37 44.69 o 5 16 1 27.57 9.10 44.84 o 6 16 1 101.90 92.98 50.78 o 1 17 1 96.69 52.72 49.10 o 2 17 1 67.50 86.45 50.09 o 3 17 1 364.36 382.20 64.57 o 4 17 1 0.88 -26.62 44.28 o 5 17 1 109.78 102.26 53.19 o 0 18 1 97.03 101.37 74.84 o 1 18 1 142.88 150.93 54.10 o 0 0 2 10862.45 8212.60 76.90 o 1 0 2 17327.53 17252.91 86.32 o 2 0 2 7249.16 7101.22 86.61 o 3 0 2 23735.68 22332.45 451.61 o 4 0 2 1090.44 1077.03 54.38 o 5 0 2 4342.54 4329.53 104.02 o 6 0 2 862.21 981.47 61.93 o 7 0 2 1105.16 1231.28 77.14 o 8 0 2 7.19 26.97 38.04 o 9 0 2 971.54 1003.11 85.02 o 10 0 2 88.72 32.44 51.64 o 11 0 2 3.05 -19.66 51.49 o 12 0 2 130.20 31.53 100.50 o 13 0 2 133.19 113.90 70.51 o 14 0 2 65.99 214.14 86.50 o 1 1 2 15794.61 14904.95 63.07 o 2 1 2 10036.30 9351.87 84.45 o 3 1 2 2698.59 2687.76 46.99 o 4 1 2 41.02 26.03 17.74 o 5 1 2 2887.86 3172.77 64.32 o 6 1 2 894.36 1120.69 53.68 o 7 1 2 2209.48 2292.97 68.44 o 8 1 2 194.09 221.96 34.43 o 9 1 2 1155.71 1231.65 65.67 o 10 1 2 1124.49 1175.05 70.74 o 11 1 2 38.12 0.48 37.24 o 12 1 2 2.79 41.16 40.88 o 13 1 2 112.58 170.99 52.94 o 14 1 2 86.01 52.30 55.61 o 0 2 2 691.67 714.85 16.75 o 1 2 2 4673.98 4529.43 47.26 o 2 2 2 602.48 594.68 24.32 o 3 2 2 2483.68 2355.89 46.35 o 4 2 2 6360.89 6409.24 131.82 o 5 2 2 1967.71 2046.08 55.54 o 6 2 2 408.60 444.99 38.41 o 7 2 2 2036.39 1988.95 65.34 o 8 2 2 500.25 551.33 48.80 o 9 2 2 904.25 892.23 59.63 o 10 2 2 11.70 20.05 34.24 o 11 2 2 918.44 1035.23 73.96 o 12 2 2 5.53 -7.76 40.13 o 13 2 2 30.02 48.05 47.42 o 14 2 2 42.28 80.38 55.39 o 1 3 2 8202.93 7709.02 88.87 o 2 3 2 6547.17 6132.60 74.32 o 3 3 2 4767.97 4873.52 77.79 o 4 3 2 78.28 48.30 19.56 o 5 3 2 396.38 358.82 35.09 o 6 3 2 7.38 7.48 22.50 o 7 3 2 688.00 760.42 47.76 o 8 3 2 17.87 26.51 27.32 o 9 3 2 1135.65 1120.27 65.90 o 10 3 2 107.28 93.61 37.66 o 11 3 2 603.63 639.99 63.54 o 12 3 2 9.30 24.01 42.49 o 13 3 2 168.12 113.81 53.46 o 14 3 2 68.13 112.28 57.85 o 0 4 2 8414.54 7853.74 75.94 o 1 4 2 96.66 87.77 12.20 o 2 4 2 6041.26 5773.64 87.82 o 3 4 2 2340.83 2406.67 52.35 o 4 4 2 3288.94 3005.18 55.85 o 5 4 2 459.24 394.40 32.16 o 6 4 2 1262.92 1277.63 53.54 o 7 4 2 786.54 813.05 51.07 o 8 4 2 53.30 49.55 29.89 o 9 4 2 27.35 2.43 31.85 o 10 4 2 99.73 115.24 40.43 o 11 4 2 16.65 -17.06 38.87 o 12 4 2 58.74 84.83 45.94 o 13 4 2 3.51 29.49 47.30 o 14 4 2 21.07 25.83 55.37 o 1 5 2 0.24 7.54 15.55 o 2 5 2 1994.78 1901.29 48.29 o 3 5 2 1756.34 1777.61 49.96 o 4 5 2 9259.43 9416.36 110.95 o 5 5 2 155.08 152.81 27.98 o 6 5 2 8.00 27.44 22.23 o 7 5 2 2278.79 2172.80 65.47 o 8 5 2 0.03 5.49 29.60 o 9 5 2 1026.70 1021.37 65.10 o 10 5 2 209.68 228.96 45.30 o 11 5 2 92.11 117.74 44.50 o 12 5 2 366.75 399.18 59.95 o 13 5 2 403.17 460.63 68.37 o 14 5 2 21.17 3.74 54.11 o 0 6 2 298.03 286.77 23.85 o 1 6 2 2673.76 2902.48 64.30 o 2 6 2 1381.00 1439.30 50.65 o 3 6 2 64.42 28.53 20.75 o 4 6 2 990.97 929.42 45.80 o 5 6 2 10.82 17.90 21.70 o 6 6 2 636.22 683.91 46.88 o 7 6 2 121.07 134.49 32.72 o 8 6 2 3612.88 3585.50 87.97 o 9 6 2 3614.64 3620.44 94.10 o 10 6 2 256.85 237.90 38.50 o 11 6 2 2.09 -10.93 34.87 o 12 6 2 207.39 261.48 50.10 o 13 6 2 0.40 2.37 39.49 o 14 6 2 55.42 88.01 47.92 o 1 7 2 264.42 298.20 32.11 o 2 7 2 173.91 185.66 26.58 o 3 7 2 1642.26 1671.49 55.99 o 4 7 2 267.15 310.55 35.25 o 5 7 2 480.94 520.74 43.33 o 6 7 2 194.77 164.03 32.72 o 7 7 2 610.77 758.33 56.67 o 8 7 2 44.44 62.07 34.93 o 9 7 2 94.97 50.83 36.98 o 10 7 2 177.54 144.74 45.60 o 11 7 2 407.95 381.12 82.91 o 12 7 2 0.00 55.61 45.36 o 13 7 2 275.74 306.75 64.19 o 0 8 2 603.50 585.73 28.01 o 1 8 2 385.10 400.59 26.87 o 2 8 2 1.14 5.35 21.35 o 3 8 2 387.94 402.86 38.98 o 4 8 2 9.19 -5.97 22.37 o 5 8 2 60.10 42.96 27.23 o 6 8 2 321.99 361.91 43.98 o 7 8 2 208.49 133.15 36.63 o 8 8 2 2.60 -30.85 30.85 o 9 8 2 214.46 210.65 44.33 o 10 8 2 0.23 8.71 40.02 o 11 8 2 15.23 -16.24 40.92 o 12 8 2 7.34 -1.73 45.29 o 13 8 2 85.95 93.39 54.54 o 1 9 2 33.21 16.30 16.30 o 2 9 2 531.05 493.85 41.46 o 3 9 2 1286.52 1404.58 58.86 o 4 9 2 362.62 339.00 39.53 o 5 9 2 14.53 12.22 26.57 o 6 9 2 28.35 8.32 29.92 o 7 9 2 18.16 60.77 33.88 o 8 9 2 208.61 203.01 43.56 o 9 9 2 219.42 219.01 47.51 o 10 9 2 750.62 796.95 72.74 o 11 9 2 18.16 -5.32 42.02 o 12 9 2 69.87 57.31 49.13 o 0 10 2 82.72 71.56 39.41 o 1 10 2 46.65 45.16 16.94 o 2 10 2 125.17 91.41 28.77 o 3 10 2 0.11 -21.60 23.13 o 4 10 2 297.52 384.23 45.68 o 5 10 2 100.69 164.37 37.34 o 6 10 2 0.33 -1.75 31.24 o 7 10 2 22.88 64.53 36.73 o 8 10 2 81.04 53.94 38.31 o 9 10 2 3.23 -3.83 38.97 o 10 10 2 0.26 -26.30 39.71 o 11 10 2 40.87 21.03 47.86 o 12 10 2 31.12 28.21 50.18 o 1 11 2 14.20 2.77 15.28 o 2 11 2 1270.90 1149.52 44.97 o 3 11 2 278.66 265.10 40.63 o 4 11 2 30.81 42.97 32.23 o 5 11 2 149.77 114.90 37.76 o 6 11 2 82.80 106.44 38.30 o 7 11 2 285.27 343.12 51.59 o 8 11 2 115.76 144.98 44.43 o 9 11 2 39.99 13.29 41.73 o 10 11 2 48.83 48.09 45.82 o 11 11 2 235.71 236.85 60.35 o 0 12 2 1839.21 1922.66 110.28 o 1 12 2 508.61 465.49 51.41 o 2 12 2 76.11 107.90 35.13 o 3 12 2 295.54 318.75 45.49 o 4 12 2 318.96 362.88 48.21 o 5 12 2 41.23 44.57 35.12 o 6 12 2 181.75 181.24 44.16 o 7 12 2 275.13 263.13 50.06 o 8 12 2 0.83 -26.25 38.65 o 9 12 2 3.25 31.10 43.50 o 10 12 2 63.98 86.12 50.29 o 11 12 2 398.10 442.50 70.67 o 1 13 2 13.64 10.19 33.25 o 2 13 2 8.30 30.20 34.24 o 3 13 2 1.79 -18.72 31.79 o 4 13 2 185.55 162.99 42.60 o 5 13 2 17.29 37.61 38.02 o 6 13 2 178.32 142.84 46.60 o 7 13 2 7.89 2.06 40.31 o 8 13 2 208.86 204.83 53.58 o 9 13 2 0.03 -19.99 44.40 o 10 13 2 254.41 373.80 65.93 o 0 14 2 447.08 458.49 91.95 o 1 14 2 712.84 764.63 66.86 o 2 14 2 663.25 716.79 65.57 o 3 14 2 100.35 55.03 40.01 o 4 14 2 611.58 603.64 65.32 o 5 14 2 6.27 -2.96 37.97 o 6 14 2 1.53 -5.62 38.84 o 7 14 2 224.97 361.83 59.70 o 8 14 2 1.35 9.69 44.98 o 9 14 2 47.24 85.90 52.18 o 1 15 2 0.03 17.93 38.51 o 2 15 2 19.74 6.63 38.89 o 3 15 2 604.11 566.81 66.27 o 4 15 2 520.50 538.86 65.50 o 5 15 2 22.81 43.14 43.87 o 6 15 2 97.00 72.94 48.09 o 7 15 2 772.28 841.23 81.74 o 8 15 2 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141.61 98.33 38.94 o 6 6 27 84.13 73.30 39.54 o 7 6 27 0.00 -9.12 28.35 o 1 7 27 385.38 423.25 44.26 o 2 7 27 219.72 194.55 39.09 o 3 7 27 488.32 481.50 53.49 o 4 7 27 73.08 62.62 39.61 o 5 7 27 25.98 20.98 36.96 o 6 7 27 26.91 -24.42 37.02 o 7 7 27 123.02 111.48 43.59 o 0 8 27 863.89 938.10 82.03 o 1 8 27 668.53 670.76 52.72 o 2 8 27 65.64 64.70 35.22 o 3 8 27 152.84 136.64 39.34 o 4 8 27 3.87 -8.76 37.02 o 5 8 27 150.22 239.03 50.17 o 6 8 27 82.70 135.54 46.19 o 1 9 27 62.36 64.10 35.62 o 2 9 27 883.95 960.19 66.65 o 3 9 27 3.10 -22.39 33.15 o 4 9 27 45.84 43.36 40.80 o 5 9 27 18.97 38.76 41.09 o 0 10 27 1112.86 1034.96 113.83 o 1 10 27 18.65 37.32 36.46 o 2 10 27 294.32 401.46 52.09 o 3 10 27 51.16 90.60 39.61 o 4 10 27 433.14 595.68 102.51 o 1 11 27 126.82 199.60 50.73 o 0 0 28 4.36 6.80 74.38 o 1 0 28 801.56 836.74 100.89 o 2 0 28 2.72 20.22 56.02 o 3 0 28 34.05 45.32 24.13 o 4 0 28 101.00 121.93 37.45 o 5 0 28 7.77 -32.03 32.03 o 6 0 28 4.75 -7.09 27.19 o 7 0 28 71.94 128.10 38.05 o 8 0 28 1960.94 2031.54 92.82 o 1 1 28 149.96 179.31 45.69 o 2 1 28 33.97 45.88 23.23 o 3 1 28 17.97 7.51 24.89 o 4 1 28 196.93 249.61 26.90 o 5 1 28 49.55 36.14 21.72 o 6 1 28 2.08 0.13 23.39 o 7 1 28 274.30 266.35 37.68 o 8 1 28 2.86 2.47 25.76 o 0 2 28 140.80 201.05 39.76 o 1 2 28 170.92 165.84 26.59 o 2 2 28 188.78 200.50 27.41 o 3 2 28 173.42 196.04 28.60 o 4 2 28 1.33 -23.30 23.30 o 5 2 28 38.99 32.59 21.79 o 6 2 28 415.08 444.29 42.42 o 7 2 28 602.21 716.45 52.43 o 8 2 28 32.71 9.30 30.31 o 1 3 28 110.19 143.97 27.79 o 2 3 28 3.70 13.16 23.04 o 3 3 28 14.63 2.02 24.13 o 4 3 28 52.00 71.82 29.84 o 5 3 28 57.00 66.64 32.67 o 6 3 28 23.90 37.06 25.56 o 7 3 28 445.81 421.29 45.49 o 8 3 28 112.22 147.62 36.54 o 0 4 28 271.31 243.42 46.42 o 1 4 28 584.40 642.90 46.08 o 2 4 28 8.66 27.84 25.53 o 3 4 28 215.65 255.78 38.77 o 4 4 28 5.89 17.97 28.79 o 5 4 28 432.91 493.14 53.87 o 6 4 28 37.09 55.13 36.13 o 7 4 28 0.28 -10.50 27.51 o 1 5 28 538.18 551.38 46.20 o 2 5 28 1617.77 1508.00 62.34 o 3 5 28 4.73 8.29 29.46 o 4 5 28 3.44 8.12 30.86 o 5 5 28 16.59 24.58 34.24 o 6 5 28 184.23 170.88 43.06 o 7 5 28 4.27 -31.89 35.13 o 0 6 28 273.31 307.21 54.55 o 1 6 28 275.92 309.27 39.51 o 2 6 28 448.33 447.79 45.99 o 3 6 28 81.86 69.72 33.90 o 4 6 28 150.75 184.67 44.03 o 5 6 28 56.38 60.19 37.86 o 6 6 28 79.29 84.90 40.38 o 7 6 28 172.84 212.47 58.52 o 1 7 28 352.16 395.79 43.76 o 2 7 28 164.90 205.50 41.46 o 3 7 28 149.06 117.02 38.09 o 4 7 28 189.98 247.38 47.18 o 5 7 28 42.68 59.06 40.18 o 6 7 28 95.58 92.94 44.15 o 0 8 28 11.09 -25.66 41.36 o 1 8 28 2887.55 2903.52 94.54 o 2 8 28 226.49 264.03 44.65 o 3 8 28 38.32 30.94 35.80 o 4 8 28 1.90 -16.84 36.02 o 5 8 28 665.06 768.20 71.74 o 1 9 28 60.92 97.64 37.70 o 2 9 28 543.80 602.13 59.09 o 3 9 28 195.44 159.78 43.27 o 4 9 28 45.57 38.25 40.33 o 0 10 28 243.81 152.25 67.69 o 1 10 28 132.93 134.03 41.88 o 2 10 28 0.02 7.01 35.74 o 1 1 29 38.96 55.62 38.49 o 2 1 29 365.69 355.69 55.35 o 3 1 29 61.34 71.08 27.98 o 4 1 29 262.46 281.20 48.92 o 5 1 29 18.28 -6.57 24.69 o 6 1 29 15.82 2.99 23.02 o 7 1 29 6.52 -6.10 25.96 o 0 2 29 890.42 904.42 81.60 o 1 2 29 165.88 168.08 24.46 o 2 2 29 8.65 13.39 19.80 o 3 2 29 96.59 106.00 25.83 o 4 2 29 0.05 -8.64 23.93 o 5 2 29 28.40 27.82 28.97 o 6 2 29 14.72 25.98 24.12 o 7 2 29 0.68 11.03 27.00 o 1 3 29 35.19 21.42 22.87 o 2 3 29 398.69 446.35 39.26 o 3 3 29 33.23 20.56 23.95 o 4 3 29 614.06 650.79 51.51 o 5 3 29 0.23 -26.46 28.81 o 6 3 29 199.15 192.94 42.50 o 7 3 29 41.98 22.15 28.84 o 0 4 29 0.54 -3.23 34.53 o 1 4 29 609.19 670.86 46.26 o 2 4 29 151.46 165.68 31.98 o 3 4 29 154.20 141.08 34.24 o 4 4 29 58.65 57.35 31.95 o 5 4 29 256.49 284.74 46.32 o 6 4 29 27.19 -32.48 32.48 o 7 4 29 3.81 -9.18 35.66 o 1 5 29 82.86 111.16 31.11 o 2 5 29 4.52 -25.24 25.24 o 3 5 29 324.01 325.58 43.92 o 4 5 29 2.99 -21.81 32.86 o 5 5 29 12.79 31.79 35.48 o 6 5 29 0.77 48.19 37.14 o 0 6 29 684.38 725.25 72.08 o 1 6 29 1.95 37.32 28.48 o 2 6 29 29.94 32.87 29.71 o 3 6 29 103.16 108.58 36.79 o 4 6 29 117.60 163.75 43.13 o 5 6 29 263.71 237.96 48.39 o 6 6 29 154.80 194.01 46.05 o 1 7 29 44.73 33.99 31.55 o 2 7 29 27.90 25.02 34.32 o 3 7 29 120.71 186.72 41.00 o 4 7 29 4.81 23.74 38.01 o 5 7 29 255.89 271.46 51.31 o 0 8 29 120.67 67.40 48.46 o 1 8 29 180.86 237.74 43.60 o 2 8 29 135.85 137.78 40.58 o 3 8 29 3.00 -3.62 34.35 o 4 8 29 6.00 -13.94 38.01 o 1 9 29 13.90 11.46 36.05 o 2 9 29 230.99 252.40 47.26 o 0 0 30 11.51 29.52 80.98 o 1 0 30 2.60 31.73 59.07 o 2 0 30 23.53 45.90 75.83 o 3 0 30 238.55 178.65 74.43 o 4 0 30 557.42 475.39 132.25 o 5 0 30 322.22 332.46 56.49 o 6 0 30 14.51 37.15 41.15 o 7 0 30 460.24 387.22 75.24 o 1 1 30 55.26 58.47 39.46 o 2 1 30 209.92 245.59 51.44 o 3 1 30 32.48 14.18 41.01 o 4 1 30 156.89 220.04 45.09 o 5 1 30 113.07 99.38 39.65 o 6 1 30 267.88 266.77 39.25 o 7 1 30 6.73 27.71 32.52 o 0 2 30 62.18 49.38 60.15 o 1 2 30 98.36 59.43 43.43 o 2 2 30 103.18 85.91 29.77 o 3 2 30 117.66 113.12 33.57 o 4 2 30 84.42 97.15 40.89 o 5 2 30 165.79 200.12 36.22 o 6 2 30 150.08 195.02 39.92 o 7 2 30 207.00 203.16 52.87 o 1 3 30 1.11 -14.90 21.50 o 2 3 30 46.47 60.55 25.04 o 3 3 30 1037.70 1146.49 53.79 o 4 3 30 485.44 636.40 53.71 o 5 3 30 478.34 460.84 61.61 o 6 3 30 35.34 41.02 34.28 o 0 4 30 3.10 17.27 35.60 o 1 4 30 45.73 39.39 26.03 o 2 4 30 59.48 74.40 28.69 o 3 4 30 336.46 358.66 45.34 o 4 4 30 359.75 440.36 52.72 o 5 4 30 33.29 19.61 34.28 o 6 4 30 32.66 46.41 36.88 o 1 5 30 300.47 342.22 42.27 o 2 5 30 33.85 18.16 27.92 o 3 5 30 205.56 242.83 41.18 o 4 5 30 302.07 325.42 52.28 o 5 5 30 3.04 41.47 37.81 o 0 6 30 462.20 503.41 70.58 o 1 6 30 27.94 14.06 29.82 o 2 6 30 1.29 -15.38 30.62 o 3 6 30 37.70 47.22 34.43 o 4 6 30 528.82 647.56 64.23 o 5 6 30 110.59 95.13 43.22 o 1 7 30 511.51 594.79 53.66 o 2 7 30 39.36 -16.48 33.17 o 3 7 30 3.70 -19.08 33.80 o 4 7 30 89.58 123.98 44.42 o 0 8 30 141.84 190.93 55.49 o 1 8 30 214.50 346.87 49.93 o 2 8 30 3.38 4.18 34.97 o 3 8 30 29.70 -19.24 48.34 o 1 1 31 688.58 645.36 70.67 o 2 1 31 60.23 70.84 45.42 o 3 1 31 545.44 650.30 73.04 o 4 1 31 94.15 47.32 62.82 o 5 1 31 447.49 530.68 64.09 o 6 1 31 0.68 -31.04 35.21 o 0 2 31 922.29 1013.20 110.43 o 1 2 31 14.64 -0.98 39.13 o 2 2 31 0.67 -9.05 41.81 o 3 2 31 1449.22 1424.99 65.59 o 4 2 31 0.02 -5.09 34.45 o 5 2 31 405.84 461.19 62.90 o 6 2 31 352.78 331.09 81.43 o 1 3 31 1.55 1.41 27.09 o 2 3 31 1.08 19.06 30.87 o 3 3 31 172.28 182.66 41.68 o 4 3 31 53.16 80.92 31.44 o 5 3 31 811.27 905.96 62.88 o 0 4 31 0.50 -6.93 35.21 o 1 4 31 63.48 88.15 28.68 o 2 4 31 110.91 106.40 30.89 o 3 4 31 31.02 13.61 29.42 o 4 4 31 99.18 49.41 35.04 o 5 4 31 1281.85 1477.05 75.94 o 1 5 31 41.92 38.81 29.14 o 2 5 31 52.36 23.14 29.36 o 3 5 31 166.05 197.03 40.65 o 4 5 31 5.33 -25.37 33.34 o 0 6 31 249.92 321.13 58.29 o 1 6 31 20.29 34.84 30.49 o 2 6 31 358.07 349.20 47.13 o 3 6 31 226.76 245.70 43.85 o 4 6 31 40.09 59.55 39.42 o 1 7 31 173.56 166.84 38.32 o 2 7 31 4.10 25.07 35.16 o 0 0 32 34.45 -5.63 76.13 o 1 0 32 228.54 196.29 77.65 o 2 0 32 577.43 668.61 108.13 o 3 0 32 7.51 61.85 68.17 o 4 0 32 920.48 1151.01 179.63 o 5 0 32 2711.57 2888.88 250.90 o 1 1 32 415.16 455.56 64.91 o 2 1 32 33.63 15.12 43.42 o 3 1 32 0.96 -8.83 42.91 o 4 1 32 214.08 291.55 82.78 o 5 1 32 2.85 14.34 63.61 o 0 2 32 1385.78 1643.38 139.24 o 1 2 32 1.20 -40.97 40.97 o 2 2 32 190.82 218.44 54.49 o 3 2 32 2.57 17.75 45.21 o 4 2 32 581.28 558.32 98.29 o 5 2 32 8.86 69.18 40.18 o 1 3 32 9.27 20.45 40.34 o 2 3 32 369.42 452.92 66.96 o 3 3 32 197.60 221.14 43.84 o 4 3 32 146.87 171.69 47.78 o 0 4 32 108.35 124.99 42.79 o 1 4 32 97.70 112.35 29.66 o 2 4 32 359.84 360.56 40.75 o 3 4 32 17.79 -21.60 27.94 o 4 4 32 377.69 480.02 54.71 o 1 5 32 340.98 314.51 41.25 o 2 5 32 23.23 40.44 29.10 o 3 5 32 221.75 255.90 42.40 o 0 6 32 235.65 231.93 55.65 o 1 6 32 16.75 27.27 31.07 o 2 6 32 3.58 -19.03 31.31 o 1 1 33 0.25 81.11 47.32 o 2 1 33 1.66 16.23 41.88 o 3 1 33 94.45 131.44 52.11 o 4 1 33 256.50 294.01 126.42 o 0 2 33 1148.07 1367.06 187.89 o 1 2 33 423.32 417.61 66.38 o 2 2 33 4.64 7.84 41.68 o 3 2 33 270.93 272.05 59.16 o 1 3 33 317.45 372.48 62.74 o 2 3 33 211.39 248.48 58.97 o 3 3 33 179.92 157.26 63.48 o 0 4 33 5.34 -56.83 56.83 o 1 4 33 659.23 729.02 77.18 o 2 4 33 3.47 43.71 33.83 o 0 0 34 414.14 457.53 142.15 o 1 0 34 3.09 -31.36 55.96 o 2 0 34 2.13 -30.42 59.23 o 1 1 34 111.75 101.33 50.55 o 0 2 34 1445.22 1588.21 143.15 o 1 2 34 16.38 14.67 47.60 o