#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:44:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181284 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/62/2236294.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236294_Fobs loop_ _publ_author_name 'Guentner, Christian' 'Korber, Nikolaus' _publ_section_title ; Tetraamminelithium triamminelithium trisulfide, [Li(NH~3~)~4~][Li(NH~3~)~3~S~3~] ; _journal_coeditor_code HB6966 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first i84 _journal_page_last i85 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.457 _cell_angle_gamma 90.000 _cell_length_a 12.4218 _cell_length_b 9.3721 _cell_length_c 22.2692 _exptl_crystal_F_000 992.00 _reflns_d_resolution_high 0.8250 _cod_data_source_file hb6966Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 1 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 248.36 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1506.39 2404.77 362.39 o 3 0 0 4.37 268.90 323.96 o 4 0 0 5729.34 5969.75 219.16 o 5 0 0 1527.93 1619.59 182.82 o 6 0 0 0.06 94.59 200.02 o 7 0 0 1462.30 1285.40 145.24 o 8 0 0 13922.30 13022.85 176.99 o 9 0 0 216.05 321.75 120.39 o 10 0 0 8958.00 8327.08 145.47 o 11 0 0 631.59 636.65 131.20 o 12 0 0 2497.86 2522.27 122.27 o 13 0 0 3.55 130.40 116.06 o 14 0 0 158.03 3.27 116.77 o 1 1 0 2138.28 3579.91 303.29 o 2 1 0 186.85 288.69 263.84 o 3 1 0 28751.29 34446.86 436.00 o 4 1 0 1609.23 1664.57 129.14 o 5 1 0 607.16 554.86 137.51 o 6 1 0 307.50 303.37 133.07 o 7 1 0 17195.24 16252.18 149.12 o 8 1 0 39.92 50.70 100.42 o 9 1 0 302.21 362.84 91.96 o 10 1 0 1507.10 1482.16 97.58 o 11 1 0 2626.32 2645.33 96.56 o 12 1 0 1424.14 1511.60 81.36 o 13 1 0 289.13 325.47 84.88 o 14 1 0 111.29 137.85 80.71 o 0 2 0 4171.74 4875.96 363.73 o 1 2 0 137.55 184.21 263.05 o 2 2 0 763.35 274.69 211.64 o 3 2 0 19641.45 21656.90 215.99 o 4 2 0 4125.10 4474.22 154.74 o 5 2 0 29.44 131.44 155.58 o 6 2 0 7183.19 6537.08 133.29 o 7 2 0 2.88 -33.72 106.76 o 8 2 0 417.59 458.50 97.41 o 9 2 0 589.83 557.30 95.74 o 10 2 0 170.04 175.80 88.89 o 11 2 0 672.60 719.56 92.22 o 12 2 0 468.77 495.82 85.87 o 13 2 0 3343.14 3265.68 91.00 o 14 2 0 51.51 125.53 71.49 o 1 3 0 2702.98 2799.48 186.45 o 2 3 0 10065.71 10379.66 209.46 o 3 3 0 535.30 486.81 165.78 o 4 3 0 637.52 690.87 176.20 o 5 3 0 5.32 60.49 144.17 o 6 3 0 2790.90 2759.18 129.22 o 7 3 0 754.73 726.14 102.47 o 8 3 0 548.64 592.55 100.61 o 9 3 0 1166.91 1260.69 98.86 o 10 3 0 3232.85 3195.07 97.32 o 11 3 0 0.56 34.85 83.12 o 12 3 0 682.35 796.82 85.79 o 13 3 0 149.82 218.70 79.58 o 14 3 0 111.21 142.94 80.32 o 0 4 0 8500.87 8836.98 253.05 o 1 4 0 595.95 658.64 167.80 o 2 4 0 3457.90 3339.71 174.96 o 3 4 0 979.02 901.00 166.31 o 4 4 0 717.65 707.44 148.17 o 5 4 0 38.57 181.65 129.78 o 6 4 0 4263.48 4081.73 127.53 o 7 4 0 4409.08 4220.71 111.38 o 8 4 0 19.65 86.91 93.30 o 9 4 0 57.19 -20.19 86.48 o 10 4 0 4.15 127.95 95.49 o 11 4 0 43.34 50.92 90.84 o 12 4 0 45.87 -8.24 82.71 o 13 4 0 33.50 167.17 76.53 o 14 4 0 3.58 295.83 237.83 o 1 5 0 187.03 135.29 140.65 o 2 5 0 308.80 259.78 135.93 o 3 5 0 9892.74 9228.18 140.74 o 4 5 0 5745.00 5501.80 123.56 o 5 5 0 3872.65 3718.80 122.19 o 6 5 0 352.94 281.97 109.17 o 7 5 0 135.88 95.28 110.99 o 8 5 0 1146.28 1152.89 100.14 o 9 5 0 239.47 249.92 99.77 o 10 5 0 68.49 90.29 92.96 o 11 5 0 147.34 198.52 81.26 o 12 5 0 68.13 87.24 82.18 o 13 5 0 353.45 325.13 83.46 o 0 6 0 1938.95 1872.65 171.04 o 1 6 0 6653.17 6275.38 136.83 o 2 6 0 1793.15 1697.36 111.57 o 3 6 0 4991.65 4768.39 112.19 o 4 6 0 133.09 220.36 106.60 o 5 6 0 673.96 690.27 104.79 o 6 6 0 1334.17 1225.37 115.26 o 7 6 0 142.54 186.58 105.07 o 8 6 0 109.32 136.10 102.02 o 9 6 0 2062.18 2135.26 101.56 o 10 6 0 297.70 391.34 95.92 o 11 6 0 232.48 299.15 88.94 o 12 6 0 1.93 81.64 88.57 o 1 7 0 403.28 453.15 112.68 o 2 7 0 350.40 397.28 107.54 o 3 7 0 68.00 153.17 116.34 o 4 7 0 200.42 236.87 101.82 o 5 7 0 1459.12 1463.81 102.43 o 6 7 0 1371.31 1440.90 97.56 o 7 7 0 1135.00 1098.36 93.21 o 8 7 0 3647.16 3677.37 103.20 o 9 7 0 715.13 848.08 92.99 o 10 7 0 24.04 75.51 85.37 o 11 7 0 395.42 386.06 89.47 o 0 8 0 1347.59 1419.98 146.12 o 1 8 0 480.19 599.06 117.36 o 2 8 0 285.71 327.80 105.70 o 3 8 0 447.27 443.88 104.76 o 4 8 0 0.12 36.18 102.80 o 5 8 0 815.88 778.26 102.76 o 6 8 0 1020.19 1087.08 98.63 o 7 8 0 10.98 4.09 86.03 o 8 8 0 0.29 78.51 86.34 o 9 8 0 185.48 190.38 83.11 o 10 8 0 863.62 928.11 87.41 o 1 9 0 55.32 120.72 101.31 o 2 9 0 2139.77 2195.12 109.00 o 3 9 0 93.37 131.70 92.78 o 4 9 0 2579.27 2490.57 98.24 o 5 9 0 464.17 568.09 95.68 o 6 9 0 490.82 593.08 89.17 o 7 9 0 192.38 176.38 93.63 o 8 9 0 2.07 -40.48 81.15 o 9 9 0 12.62 32.04 106.92 o 0 10 0 63.71 85.59 172.84 o 1 10 0 1109.10 1201.46 98.69 o 2 10 0 52.07 52.84 92.36 o 3 10 0 1004.32 1116.67 97.17 o 4 10 0 339.04 379.90 87.39 o 5 10 0 3.42 4.50 87.19 o 6 10 0 356.43 321.06 91.70 o 7 10 0 935.17 708.75 250.60 o 1 11 0 687.18 717.98 107.20 o 2 11 0 222.86 276.07 92.03 o 3 11 0 90.39 70.77 94.74 o -14 1 1 327.47 338.75 76.44 o -13 1 1 204.72 284.19 84.30 o -12 1 1 268.17 319.62 82.16 o -11 1 1 456.71 468.97 93.47 o -10 1 1 175.29 304.60 96.03 o -9 1 1 2138.48 2056.61 100.37 o -8 1 1 534.23 651.08 93.08 o -7 1 1 2096.86 1872.98 117.98 o -6 1 1 13.68 109.06 124.51 o -5 1 1 2.72 112.70 139.12 o -4 1 1 35796.96 38647.41 444.37 o -3 1 1 1752.14 1778.01 170.44 o -2 1 1 1768.73 2357.30 268.70 o -1 1 1 562.32 839.18 275.97 o 0 1 1 1.87 59.34 265.07 o 1 1 1 23.70 19.75 242.07 o 2 1 1 841.51 1297.32 232.70 o 3 1 1 347.49 150.78 180.41 o 4 1 1 8149.94 8510.74 165.43 o 5 1 1 3036.61 3252.01 152.13 o 6 1 1 1988.95 2020.75 142.97 o 7 1 1 598.99 624.95 108.62 o 8 1 1 58.39 159.70 90.74 o 9 1 1 2013.60 2004.12 98.12 o 10 1 1 822.28 879.68 96.57 o 11 1 1 147.34 169.30 94.74 o 12 1 1 446.35 577.47 74.23 o 13 1 1 288.98 407.98 79.68 o 14 1 1 74.14 139.66 81.52 o -14 2 1 5.56 13.17 74.53 o -13 2 1 12.22 3.22 70.94 o -12 2 1 34.98 118.65 86.18 o -11 2 1 1753.29 1808.92 88.16 o -10 2 1 2485.89 2499.37 95.53 o -9 2 1 1192.20 1177.00 84.12 o -8 2 1 18.80 88.86 93.59 o -7 2 1 3177.49 2996.54 123.54 o -6 2 1 646.14 504.01 133.17 o -5 2 1 2684.19 2682.38 160.68 o -4 2 1 1509.48 1573.12 148.73 o -3 2 1 16965.93 18466.43 345.55 o -2 2 1 233.06 105.26 208.02 o -1 2 1 1922.50 2307.95 262.20 o 0 2 1 86.00 162.65 274.69 o 1 2 1 372.45 409.62 271.77 o 2 2 1 1627.68 1647.92 190.57 o 3 2 1 7572.47 7984.21 179.31 o 4 2 1 2049.01 2087.65 151.26 o 5 2 1 32.40 100.19 152.36 o 6 2 1 20.52 2.72 127.18 o 7 2 1 1854.89 1792.75 107.53 o 8 2 1 604.11 541.01 100.69 o 9 2 1 59.31 64.34 90.11 o 10 2 1 291.53 227.64 96.98 o 11 2 1 192.35 215.92 90.59 o 12 2 1 72.77 20.46 75.36 o 13 2 1 750.93 779.00 84.75 o 14 2 1 149.09 218.86 75.12 o -14 3 1 39.12 74.18 79.99 o -13 3 1 229.04 239.32 85.37 o -12 3 1 7.85 25.12 83.70 o -11 3 1 188.57 298.62 91.37 o -10 3 1 754.47 742.29 97.79 o -9 3 1 0.24 47.80 93.87 o -8 3 1 1074.02 1052.94 97.84 o -7 3 1 1678.86 1672.74 112.63 o -6 3 1 5840.31 5471.66 124.26 o -5 3 1 1468.00 1400.01 137.11 o -4 3 1 1022.48 989.51 174.93 o -3 3 1 1502.69 1452.60 168.57 o -2 3 1 997.29 1008.59 167.13 o -1 3 1 21.37 -4.33 166.76 o 0 3 1 906.85 966.09 168.20 o 1 3 1 1703.33 1658.19 176.36 o 2 3 1 158.45 107.87 171.59 o 3 3 1 126.33 36.69 156.70 o 4 3 1 547.21 619.63 152.24 o 5 3 1 662.44 617.90 138.13 o 6 3 1 575.21 465.15 121.71 o 7 3 1 742.78 773.42 101.29 o 8 3 1 562.32 621.49 93.56 o 9 3 1 1202.64 1156.29 95.06 o 10 3 1 1077.60 1154.88 96.93 o 11 3 1 17.81 25.16 85.42 o 12 3 1 410.29 374.50 86.78 o 13 3 1 266.23 227.07 71.53 o 14 3 1 172.09 149.11 74.77 o -14 4 1 1568.51 1478.77 116.45 o -13 4 1 512.43 506.73 85.71 o -12 4 1 45.70 88.61 80.82 o -11 4 1 623.79 720.30 91.22 o -10 4 1 85.96 132.00 82.41 o -9 4 1 198.13 255.14 87.95 o -8 4 1 868.75 874.01 105.64 o -7 4 1 5832.84 5664.83 122.10 o -6 4 1 12347.75 11835.36 145.47 o -5 4 1 8314.05 7974.84 149.66 o -4 4 1 12.72 53.57 145.54 o -3 4 1 6.09 65.12 143.23 o -2 4 1 3929.44 3872.31 174.31 o -1 4 1 5.99 92.98 150.70 o 0 4 1 2.33 88.75 154.08 o 1 4 1 8600.48 8784.09 195.80 o 2 4 1 175.87 276.47 169.17 o 3 4 1 9301.36 9228.22 189.71 o 4 4 1 3318.17 3064.11 150.48 o 5 4 1 3089.13 2973.32 136.96 o 6 4 1 3102.62 2961.37 116.35 o 7 4 1 0.50 66.53 100.76 o 8 4 1 1002.10 1147.18 99.83 o 9 4 1 360.00 329.47 90.77 o 10 4 1 15.51 90.56 93.65 o 11 4 1 165.47 118.83 90.00 o 12 4 1 255.96 240.34 79.83 o 13 4 1 455.15 326.81 82.22 o -13 5 1 1021.83 1068.10 89.30 o -12 5 1 271.35 303.84 85.23 o -11 5 1 537.96 697.93 93.55 o -10 5 1 982.55 1043.73 99.82 o -9 5 1 542.09 556.85 96.27 o -8 5 1 2566.65 2512.63 110.60 o -7 5 1 798.06 794.94 112.71 o -6 5 1 30.24 152.99 108.68 o -5 5 1 3113.43 3006.16 121.39 o -4 5 1 17.00 -38.03 111.73 o -3 5 1 13241.60 12699.18 150.13 o -2 5 1 6509.01 6188.82 157.48 o -1 5 1 311.75 313.48 131.46 o 0 5 1 1720.62 1501.99 135.82 o 1 5 1 6198.62 6032.11 152.14 o 2 5 1 519.27 506.21 129.18 o 3 5 1 287.10 363.11 127.21 o 4 5 1 193.12 154.00 121.85 o 5 5 1 6138.08 5663.10 125.82 o 6 5 1 2103.03 1951.36 115.33 o 7 5 1 1326.22 1351.80 111.02 o 8 5 1 766.58 758.01 105.71 o 9 5 1 18.87 71.35 88.78 o 10 5 1 10.88 -11.25 85.99 o 11 5 1 825.01 899.46 87.56 o 12 5 1 202.13 289.76 83.71 o 13 5 1 502.00 513.96 82.48 o -12 6 1 0.29 6.72 87.90 o -11 6 1 1466.70 1464.49 86.52 o -10 6 1 2172.45 2204.73 99.04 o -9 6 1 181.24 220.28 93.93 o -8 6 1 2357.50 2321.34 103.40 o -7 6 1 170.79 173.95 102.98 o -6 6 1 935.17 998.31 112.15 o -5 6 1 79.07 36.05 105.21 o -4 6 1 17.56 -10.08 105.04 o -3 6 1 915.61 979.51 109.72 o -2 6 1 727.11 715.86 114.49 o -1 6 1 3450.74 3385.30 128.19 o 0 6 1 4497.14 4239.51 117.85 o 1 6 1 1497.90 1429.75 122.14 o 2 6 1 4113.89 3901.77 119.96 o 3 6 1 447.48 464.01 101.48 o 4 6 1 1915.78 1882.08 104.81 o 5 6 1 168.03 197.28 104.78 o 6 6 1 474.03 500.49 112.45 o 7 6 1 37.73 -7.27 101.02 o 8 6 1 838.95 887.24 103.94 o 9 6 1 511.31 543.90 100.52 o 10 6 1 1503.43 1448.14 95.32 o 11 6 1 839.57 968.09 93.34 o 12 6 1 629.04 657.06 84.25 o -11 7 1 145.67 159.92 88.38 o -10 7 1 146.84 189.00 88.93 o -9 7 1 78.97 171.02 98.88 o -8 7 1 8.12 26.71 95.82 o -7 7 1 2031.68 2071.90 97.97 o -6 7 1 29.77 45.93 96.58 o -5 7 1 193.15 188.90 95.45 o -4 7 1 264.10 350.50 103.92 o -3 7 1 107.21 171.96 108.73 o -2 7 1 308.71 307.33 119.88 o -1 7 1 1422.72 1403.29 117.87 o 0 7 1 591.38 545.12 100.16 o 1 7 1 771.52 1600.48 379.71 o 2 7 1 71.25 135.61 115.19 o 3 7 1 229.19 225.81 104.06 o 4 7 1 17.04 46.01 108.01 o 5 7 1 527.42 549.48 100.66 o 6 7 1 344.06 289.05 96.62 o 7 7 1 415.29 505.24 97.36 o 8 7 1 539.99 549.26 100.92 o 9 7 1 600.56 676.11 97.00 o 10 7 1 123.55 152.47 86.94 o 11 7 1 45.85 89.84 90.99 o -10 8 1 28.81 93.21 80.17 o -9 8 1 361.68 490.19 87.33 o -8 8 1 83.18 107.95 87.14 o -7 8 1 6.23 72.41 89.64 o -6 8 1 284.97 296.53 93.42 o -5 8 1 988.00 960.15 100.16 o -4 8 1 3.32 -18.21 94.75 o -3 8 1 15.83 9.76 103.82 o -2 8 1 710.10 810.98 109.11 o -1 8 1 682.27 730.02 110.15 o 0 8 1 100.01 147.47 122.97 o 1 8 1 0.24 35.30 105.96 o 2 8 1 1367.44 1421.10 105.85 o 3 8 1 364.03 370.36 95.95 o 4 8 1 51.00 96.30 91.37 o 5 8 1 1177.37 1227.35 101.19 o 6 8 1 40.36 38.74 96.80 o 7 8 1 47.39 73.59 90.72 o 8 8 1 66.88 65.02 85.14 o 9 8 1 150.61 204.78 84.14 o 10 8 1 48.47 25.69 81.97 o -9 9 1 383.33 335.06 90.73 o -8 9 1 599.11 674.38 88.37 o -7 9 1 25.70 28.36 91.93 o -6 9 1 2.63 115.83 94.17 o -5 9 1 4.63 78.74 86.17 o -4 9 1 1550.49 1575.18 97.68 o -3 9 1 69.92 139.71 94.91 o -2 9 1 206.60 214.37 112.04 o -1 9 1 497.88 521.15 107.79 o 0 9 1 138.37 181.41 109.45 o 1 9 1 0.90 43.02 101.50 o 2 9 1 1155.42 1192.68 110.22 o 3 9 1 0.33 148.17 97.09 o 4 9 1 64.48 87.12 92.71 o 5 9 1 463.85 522.01 92.30 o 6 9 1 1668.31 1703.31 95.55 o 7 9 1 223.23 175.82 89.59 o 8 9 1 42.22 119.55 84.68 o 9 9 1 36.12 -32.91 188.49 o -7 10 1 145.64 299.63 167.08 o -6 10 1 642.98 629.16 87.82 o -5 10 1 1050.10 966.13 91.08 o -4 10 1 0.76 34.37 86.72 o -3 10 1 72.33 187.95 89.36 o -2 10 1 123.42 172.51 100.70 o -1 10 1 40.98 92.18 100.43 o 0 10 1 65.60 120.08 112.01 o 1 10 1 77.37 145.52 99.16 o 2 10 1 498.87 638.41 104.45 o 3 10 1 544.96 616.01 92.02 o 4 10 1 453.81 496.44 86.92 o 5 10 1 7.37 23.23 88.09 o 6 10 1 74.52 134.96 86.47 o 7 10 1 318.70 221.02 223.12 o -3 11 1 302.80 291.25 96.24 o -2 11 1 47.32 88.40 105.83 o -1 11 1 1238.95 1229.27 113.23 o 0 11 1 33.67 80.68 100.12 o 1 11 1 143.78 229.94 101.93 o 2 11 1 10.53 58.10 88.77 o 3 11 1 0.10 -51.69 91.06 o -15 0 2 97.72 404.66 222.65 o -14 0 2 228.95 321.28 112.41 o -13 0 2 2467.63 2472.77 124.79 o -12 0 2 1922.32 2020.00 127.95 o -11 0 2 4477.04 4520.01 143.11 o -10 0 2 1696.68 1920.92 126.40 o -9 0 2 133.70 148.62 125.90 o -8 0 2 449.74 577.20 116.03 o -7 0 2 181.92 241.97 158.68 o -6 0 2 10660.68 10124.70 224.77 o -5 0 2 6555.41 6564.10 219.82 o -4 0 2 18721.18 19422.34 262.25 o -3 0 2 2266.38 2411.03 277.77 o -2 0 2 9490.96 12386.75 421.81 o -1 0 2 108.88 209.40 355.43 o 1 0 2 121.03 243.92 351.61 o 3 0 2 1.82 -117.84 277.48 o 4 0 2 6879.78 7415.24 231.16 o 5 0 2 3339.58 3666.81 222.27 o 6 0 2 3281.55 3461.00 209.86 o 7 0 2 226.40 139.52 142.41 o 8 0 2 3506.45 3378.82 163.69 o 9 0 2 331.40 333.97 135.60 o 10 0 2 1573.69 1611.72 125.55 o 11 0 2 48.84 28.84 131.25 o 12 0 2 5019.85 5016.51 140.81 o 13 0 2 934.82 949.81 121.59 o 14 0 2 36.03 57.86 113.30 o -14 1 2 390.00 414.78 77.78 o -13 1 2 338.56 335.19 70.69 o -12 1 2 630.68 626.16 86.00 o -11 1 2 183.41 342.75 85.11 o -10 1 2 969.44 966.59 97.58 o -9 1 2 6399.73 5898.28 103.32 o -8 1 2 181.96 203.27 99.68 o -7 1 2 3212.85 2882.39 117.49 o -6 1 2 1495.84 1301.34 130.11 o -5 1 2 168.25 212.95 149.83 o -4 1 2 17256.57 17888.97 187.77 o -3 1 2 265.05 165.76 176.11 o -2 1 2 287.48 468.10 227.57 o -1 1 2 7208.74 10000.73 356.57 o 0 1 2 216.03 282.03 278.07 o 2 1 2 101.09 211.83 261.41 o 3 1 2 34.24 -9.28 183.45 o 4 1 2 25801.72 28320.55 550.07 o 5 1 2 4973.40 4962.66 147.55 o 6 1 2 58.89 86.92 137.69 o 7 1 2 1028.42 1059.92 109.77 o 8 1 2 2397.77 2328.71 101.29 o 9 1 2 3176.11 3005.40 103.52 o 10 1 2 121.83 193.47 89.62 o 11 1 2 0.17 134.70 82.07 o 12 1 2 1237.06 1241.39 84.70 o 13 1 2 826.06 906.88 84.55 o 14 1 2 10.13 39.98 80.99 o -14 2 2 184.36 266.38 74.61 o -13 2 2 2.41 141.50 83.47 o -12 2 2 81.94 163.26 75.50 o -11 2 2 444.22 433.87 84.16 o -10 2 2 3154.80 3072.41 95.66 o -9 2 2 1078.94 1058.52 94.65 o -8 2 2 6046.31 5702.56 95.11 o -7 2 2 6.78 54.48 103.84 o -6 2 2 725.95 669.20 128.60 o -5 2 2 201.36 238.35 154.09 o -4 2 2 1907.29 1874.23 135.94 o -3 2 2 6160.36 6187.96 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