#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/63/2236393.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236393_Fobs loop_ _publ_author_name 'Fun, Hoong-Kun' 'Loh, Wan-Sin' 'Viveka, S.' Dinesha 'Nagaraja, G. K.' _publ_section_title ; 2-(4-Methoxyphenyl)-2-oxoethanaminium chloride ; _journal_coeditor_code IS5194 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2987 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.435 _cell_angle_gamma 90.000 _cell_length_a 12.2822 _cell_length_b 7.1605 _cell_length_c 11.1226 _exptl_crystal_F_000 424.00 _reflns_d_resolution_high 0.7072 _[local]_cod_data_source_file is5194Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_gkn5_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.66 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1155.68 1333.79 19.65 o 3 0 0 58.76 87.74 1.46 o 4 0 0 1378.49 1216.27 15.23 o 5 0 0 624.22 517.45 8.63 o 6 0 0 1866.10 1764.06 28.12 o 7 0 0 2151.01 2093.58 26.19 o 8 0 0 1717.68 1827.31 23.07 o 9 0 0 495.31 531.02 7.36 o 10 0 0 1280.10 1295.82 22.75 o 11 0 0 1251.92 1249.60 16.35 o 12 0 0 3.75 6.36 0.83 o 13 0 0 91.87 94.07 3.05 o 14 0 0 25.62 28.64 1.83 o 15 0 0 26.20 40.44 4.40 o 16 0 0 394.43 440.25 8.44 o 17 0 0 132.62 120.63 3.71 o 1 1 0 1359.20 1004.49 15.75 o 2 1 0 150.16 269.41 2.96 o 3 1 0 1108.29 1294.66 13.61 o 4 1 0 2144.39 2328.02 22.33 o 5 1 0 1582.24 1773.18 17.18 o 6 1 0 0.75 3.97 0.43 o 7 1 0 621.63 655.58 6.71 o 8 1 0 64.87 63.68 1.04 o 9 1 0 207.31 182.44 2.17 o 10 1 0 107.57 94.00 1.45 o 11 1 0 30.59 51.26 1.37 o 12 1 0 308.45 302.73 3.80 o 13 1 0 224.41 231.38 3.16 o 14 1 0 320.24 332.72 4.23 o 15 1 0 69.24 61.61 1.60 o 16 1 0 41.10 39.57 1.65 o 17 1 0 13.59 9.68 1.21 o 0 2 0 13439.30 13918.85 216.25 o 1 2 0 2485.48 2634.94 26.01 o 2 2 0 1724.05 1853.66 18.12 o 3 2 0 64.13 43.90 1.81 o 4 2 0 3.93 4.58 0.33 o 5 2 0 702.96 635.37 5.79 o 6 2 0 1543.05 1517.92 15.87 o 7 2 0 275.94 313.59 3.55 o 8 2 0 1026.41 1051.91 10.71 o 9 2 0 472.52 524.79 5.16 o 10 2 0 2573.87 2479.09 22.10 o 11 2 0 40.21 21.55 0.87 o 12 2 0 165.10 159.46 2.71 o 13 2 0 0.08 -0.59 0.60 o 14 2 0 7.57 8.07 0.89 o 15 2 0 4.55 2.98 0.97 o 16 2 0 162.28 175.41 5.10 o 1 3 0 475.76 360.48 11.72 o 2 3 0 1063.70 1093.22 10.07 o 3 3 0 1327.83 1378.20 13.90 o 4 3 0 420.67 485.77 8.18 o 5 3 0 1618.18 1654.90 26.37 o 6 3 0 1180.06 1177.65 11.57 o 7 3 0 3.21 6.69 0.36 o 8 3 0 3.25 5.25 0.44 o 9 3 0 0.03 0.11 0.37 o 10 3 0 55.51 51.83 1.30 o 11 3 0 0.66 0.60 0.52 o 12 3 0 303.77 298.27 4.45 o 13 3 0 413.14 438.42 7.28 o 14 3 0 262.85 257.14 4.60 o 15 3 0 59.99 55.68 2.90 o 16 3 0 5.54 10.88 1.22 o 0 4 0 373.24 430.57 7.50 o 1 4 0 353.10 385.66 4.33 o 2 4 0 1292.61 1212.83 11.25 o 3 4 0 34.68 39.01 0.79 o 4 4 0 4.31 2.25 0.36 o 5 4 0 370.85 358.37 4.52 o 6 4 0 114.93 99.37 3.65 o 7 4 0 11.57 18.95 1.11 o 8 4 0 516.61 534.59 6.73 o 9 4 0 389.64 393.07 8.01 o 10 4 0 1020.85 939.61 10.80 o 11 4 0 247.51 230.62 3.84 o 12 4 0 57.91 52.73 1.54 o 13 4 0 29.93 32.30 1.91 o 14 4 0 1.65 1.42 1.34 o 15 4 0 0.89 0.23 0.90 o 1 5 0 40.86 39.99 0.98 o 2 5 0 103.95 121.40 1.67 o 3 5 0 329.39 338.33 3.95 o 4 5 0 1169.49 1152.11 13.10 o 5 5 0 517.68 514.33 5.76 o 6 5 0 115.53 128.93 2.02 o 7 5 0 260.99 265.05 3.86 o 8 5 0 0.34 0.65 0.70 o 9 5 0 76.55 66.28 2.69 o 10 5 0 2.86 2.43 1.19 o 11 5 0 2.10 1.93 1.22 o 12 5 0 339.28 342.90 7.67 o 13 5 0 163.66 161.78 4.90 o 14 5 0 104.01 107.54 4.04 o 15 5 0 121.44 121.99 4.49 o 0 6 0 1405.22 1434.92 23.40 o 1 6 0 77.64 68.38 1.41 o 2 6 0 37.20 39.28 1.01 o 3 6 0 0.03 -0.14 0.39 o 4 6 0 3.54 1.58 0.44 o 5 6 0 3.36 4.64 0.80 o 6 6 0 29.60 26.48 1.73 o 7 6 0 2.62 3.49 0.89 o 8 6 0 108.85 112.79 3.57 o 9 6 0 53.60 48.12 2.49 o 10 6 0 35.29 28.85 2.23 o 11 6 0 6.08 5.40 1.41 o 12 6 0 0.00 -1.24 1.24 o 13 6 0 2.76 4.34 1.59 o 1 7 0 12.59 12.58 0.73 o 2 7 0 38.92 39.06 1.08 o 3 7 0 154.43 159.99 3.67 o 4 7 0 147.43 155.37 2.24 o 5 7 0 382.65 372.50 6.17 o 6 7 0 1.33 1.69 0.87 o 7 7 0 17.46 17.28 1.80 o 8 7 0 0.27 -0.42 0.92 o 9 7 0 13.81 10.50 1.68 o 10 7 0 0.31 1.73 1.41 o 11 7 0 80.78 83.03 3.57 o 12 7 0 10.97 9.86 4.01 o 0 8 0 151.12 157.49 2.92 o 1 8 0 0.23 0.35 0.52 o 2 8 0 4.27 6.83 0.70 o 3 8 0 35.55 41.86 1.83 o 4 8 0 35.93 33.66 1.79 o 5 8 0 324.07 346.55 6.08 o 6 8 0 144.74 153.03 5.56 o 7 8 0 5.49 5.78 1.19 o 8 8 0 13.79 12.71 1.84 o 9 8 0 6.04 7.07 1.83 o 10 8 0 18.75 16.37 2.14 o 1 9 0 0.61 1.18 0.70 o 2 9 0 7.76 7.48 1.04 o 3 9 0 2.82 3.09 0.97 o 4 9 0 4.87 3.88 1.13 o 5 9 0 75.81 86.56 2.79 o 6 9 0 0.15 2.22 1.13 o 7 9 0 45.84 53.22 2.35 o 1 10 0 0.46 1.87 1.43 o 2 10 0 0.18 -0.18 1.33 o -17 1 1 25.99 34.32 1.57 o -16 1 1 16.56 20.70 1.26 o -15 1 1 4.93 6.22 1.41 o -14 1 1 20.37 18.05 0.98 o -13 1 1 19.31 20.76 1.07 o -12 1 1 36.83 34.10 1.23 o -11 1 1 2.51 2.11 0.48 o -10 1 1 38.53 39.75 0.94 o -9 1 1 13.01 12.04 0.57 o -8 1 1 1.50 0.63 0.28 o -7 1 1 15.68 20.68 0.57 o -6 1 1 662.85 635.19 5.89 o -5 1 1 202.59 163.44 1.74 o -4 1 1 758.21 613.92 6.23 o -3 1 1 565.03 536.36 14.66 o -2 1 1 91.97 122.91 1.58 o -1 1 1 2203.84 1805.66 22.67 o 0 1 1 385.15 330.24 4.12 o 1 1 1 3.61 1.93 0.14 o 2 1 1 0.38 -0.19 0.19 o 3 1 1 2.68 0.62 0.18 o 4 1 1 3.97 5.08 0.33 o 5 1 1 2.11 0.92 0.20 o 6 1 1 31.50 36.62 1.39 o 7 1 1 453.95 419.71 4.11 o 8 1 1 79.72 90.69 1.30 o 9 1 1 206.65 197.66 2.31 o 10 1 1 187.71 165.31 2.18 o 11 1 1 74.02 66.17 1.27 o 12 1 1 0.40 -0.46 0.46 o 13 1 1 3.14 3.49 0.67 o 14 1 1 0.10 -0.53 0.61 o 15 1 1 0.37 0.50 0.74 o 16 1 1 0.10 -1.00 1.05 o 17 1 1 32.78 39.74 1.89 o -16 2 1 89.41 89.71 3.04 o -15 2 1 80.07 86.15 2.10 o -14 2 1 1.38 1.70 0.71 o -13 2 1 16.05 14.16 1.12 o -12 2 1 36.11 37.14 1.56 o -11 2 1 450.71 423.52 4.84 o -10 2 1 1369.58 1296.96 12.95 o -9 2 1 25.80 29.54 0.81 o -8 2 1 0.73 2.72 0.60 o -7 2 1 159.10 186.12 2.32 o -6 2 1 703.30 652.25 6.27 o -5 2 1 4022.35 3857.74 34.30 o -4 2 1 192.56 177.12 2.03 o -3 2 1 219.03 183.75 2.31 o -2 2 1 39.54 29.64 0.85 o -1 2 1 3.52 5.18 0.50 o 0 2 1 2231.13 1923.11 21.14 o 1 2 1 17334.15 17788.17 192.02 o 2 2 1 1267.71 1211.78 15.68 o 3 2 1 2.98 0.28 0.36 o 4 2 1 57.17 58.31 0.99 o 5 2 1 1940.74 1865.08 15.14 o 6 2 1 44.10 37.95 1.29 o 7 2 1 27.93 28.21 0.66 o 8 2 1 478.68 438.72 4.84 o 9 2 1 140.81 139.68 1.98 o 10 2 1 8.88 6.54 0.51 o 11 2 1 7.71 16.69 0.82 o 12 2 1 491.89 477.49 7.98 o 13 2 1 114.76 119.89 2.74 o 14 2 1 3.27 4.97 0.96 o 15 2 1 18.98 26.12 1.57 o 16 2 1 10.36 15.31 1.72 o -16 3 1 3.39 3.53 1.02 o -15 3 1 47.40 47.42 1.84 o -14 3 1 2.29 0.58 0.69 o -13 3 1 42.03 41.75 1.39 o -12 3 1 78.76 78.74 2.41 o -11 3 1 3.08 3.77 0.63 o -10 3 1 69.60 82.10 1.67 o -9 3 1 43.80 45.15 1.53 o -8 3 1 0.72 0.40 0.27 o -7 3 1 60.40 56.65 1.51 o -6 3 1 63.14 58.77 0.78 o -5 3 1 9.66 8.47 0.66 o -4 3 1 4.64 2.93 0.31 o -3 3 1 278.39 301.60 3.30 o -2 3 1 118.61 141.25 2.02 o -1 3 1 1.71 6.05 0.39 o 0 3 1 7.63 3.73 0.32 o 1 3 1 15.45 12.49 1.11 o 2 3 1 314.36 302.12 3.76 o 3 3 1 2.88 1.97 0.29 o 4 3 1 700.61 680.86 9.21 o 5 3 1 155.20 125.06 10.76 o 6 3 1 21.15 33.06 0.85 o 7 3 1 90.36 94.92 1.18 o 8 3 1 46.45 52.95 1.06 o 9 3 1 106.21 114.39 1.76 o 10 3 1 4.11 6.10 0.55 o 11 3 1 37.36 38.22 1.43 o 12 3 1 0.10 0.90 0.80 o 13 3 1 0.03 0.14 0.89 o 14 3 1 11.53 9.74 1.07 o 15 3 1 15.28 13.67 1.24 o 16 3 1 0.30 2.23 1.62 o -15 4 1 181.39 181.47 3.52 o -14 4 1 35.56 32.02 1.97 o -13 4 1 57.67 56.77 2.99 o -12 4 1 39.79 33.97 1.12 o -11 4 1 34.54 32.59 1.99 o -10 4 1 0.08 -0.33 0.33 o -9 4 1 401.49 387.21 6.06 o -8 4 1 391.70 399.90 7.77 o -7 4 1 394.59 406.17 7.01 o -6 4 1 62.20 68.00 1.42 o -5 4 1 3110.39 3094.70 33.70 o -4 4 1 52.33 45.24 1.72 o -3 4 1 55.40 57.51 1.07 o -2 4 1 0.00 -0.12 0.24 o -1 4 1 8.44 11.96 0.52 o 0 4 1 2523.81 2476.25 27.46 o 1 4 1 239.99 255.88 3.05 o 2 4 1 1003.63 1001.00 10.34 o 3 4 1 1221.56 1141.60 13.46 o 4 4 1 322.27 343.71 3.95 o 7 4 1 69.57 68.44 1.34 o 8 4 1 95.84 97.14 2.20 o 9 4 1 155.13 149.68 2.28 o 10 4 1 32.73 27.26 2.00 o 11 4 1 1029.04 1003.27 17.34 o 12 4 1 9.88 10.87 1.23 o 13 4 1 104.14 102.00 2.35 o 14 4 1 50.06 48.54 1.79 o 15 4 1 35.14 42.80 1.99 o -15 5 1 6.27 8.09 1.88 o -14 5 1 0.20 -1.03 1.43 o -13 5 1 84.27 74.16 3.24 o -12 5 1 262.78 246.99 6.13 o -11 5 1 79.02 79.34 6.97 o -10 5 1 36.87 43.55 1.74 o -9 5 1 84.11 82.56 2.25 o -8 5 1 22.68 23.51 1.86 o -7 5 1 6.42 6.84 0.84 o -6 5 1 129.26 131.81 2.34 o -5 5 1 62.83 66.56 1.32 o -4 5 1 209.72 224.82 2.61 o -3 5 1 201.24 226.67 2.95 o -2 5 1 178.41 202.92 2.40 o -1 5 1 547.99 561.28 6.11 o 0 5 1 5.80 11.93 0.63 o 1 5 1 104.42 110.38 1.73 o 2 5 1 2.74 3.91 0.44 o 3 5 1 18.70 18.97 0.69 o 4 5 1 292.01 303.35 3.68 o 5 5 1 38.12 44.78 1.11 o 6 5 1 10.01 17.89 0.81 o 7 5 1 910.09 910.98 11.00 o 8 5 1 97.37 101.23 4.04 o 9 5 1 21.06 24.74 1.90 o 10 5 1 98.42 87.96 4.51 o 11 5 1 17.30 15.86 1.77 o 12 5 1 45.41 48.28 2.72 o 13 5 1 46.01 45.06 3.13 o 14 5 1 99.88 99.37 6.95 o 15 5 1 1.79 1.06 2.14 o -13 6 1 27.01 25.92 7.23 o -12 6 1 2.77 4.69 2.35 o -11 6 1 2.84 3.58 1.40 o -10 6 1 10.94 10.69 1.58 o -9 6 1 123.87 115.42 3.79 o -8 6 1 352.00 344.03 5.78 o -7 6 1 412.46 413.54 6.58 o -6 6 1 383.31 393.78 5.38 o -5 6 1 60.62 66.85 1.68 o -4 6 1 207.10 212.62 2.63 o -3 6 1 146.56 145.48 2.00 o -2 6 1 17.25 13.77 0.67 o -1 6 1 279.04 273.63 3.17 o 0 6 1 443.43 465.63 5.42 o 1 6 1 256.59 277.66 3.55 o 2 6 1 215.65 239.26 3.16 o 3 6 1 722.24 740.36 7.37 o 4 6 1 350.19 346.01 4.24 o 5 6 1 1029.46 1000.61 12.02 o 6 6 1 822.49 799.91 9.90 o 7 6 1 95.16 96.22 2.82 o 8 6 1 1.40 0.57 0.80 o 9 6 1 73.46 75.65 3.08 o 10 6 1 274.21 265.12 6.40 o 11 6 1 416.32 400.35 8.73 o 12 6 1 34.51 29.15 2.40 o 13 6 1 25.75 21.99 2.31 o -12 7 1 187.17 192.69 5.69 o -11 7 1 166.09 157.21 9.24 o -10 7 1 128.35 115.79 4.01 o -9 7 1 102.04 101.86 5.04 o -8 7 1 65.68 60.76 2.82 o -7 7 1 93.74 93.51 3.29 o -6 7 1 515.63 521.95 6.93 o -5 7 1 52.08 57.87 1.69 o -4 7 1 24.03 27.56 1.27 o -3 7 1 769.30 765.62 7.70 o -2 7 1 572.06 568.07 5.95 o -1 7 1 264.33 248.60 2.87 o 0 7 1 230.87 222.18 2.85 o 1 7 1 83.62 86.03 1.73 o 2 7 1 0.29 0.82 0.47 o 3 7 1 37.50 36.11 1.22 o 4 7 1 178.41 177.59 3.12 o 5 7 1 316.71 317.48 4.72 o 6 7 1 151.91 155.17 3.45 o 7 7 1 359.21 350.48 6.10 o 8 7 1 282.73 281.42 5.29 o 9 7 1 199.82 202.63 5.58 o 10 7 1 1.21 2.05 1.44 o 11 7 1 5.30 6.70 1.70 o 12 7 1 11.98 16.83 2.19 o -10 8 1 121.99 128.05 4.45 o -9 8 1 34.40 31.40 2.60 o -8 8 1 84.53 71.75 3.25 o -7 8 1 230.51 216.91 5.67 o -6 8 1 25.62 18.48 1.82 o -5 8 1 677.80 700.36 10.48 o -4 8 1 36.02 42.26 1.60 o -3 8 1 29.63 29.97 1.40 o -2 8 1 2.60 3.02 0.70 o -1 8 1 71.82 69.50 1.42 o 0 8 1 32.32 33.76 1.08 o 1 8 1 386.31 392.53 4.55 o 2 8 1 128.50 132.68 2.40 o 3 8 1 129.28 120.67 2.41 o 4 8 1 148.16 142.16 3.40 o 5 8 1 322.38 317.82 5.73 o 6 8 1 63.25 66.23 2.39 o 7 8 1 3.47 3.42 1.14 o 8 8 1 24.19 19.93 1.68 o 9 8 1 23.81 18.20 2.18 o 10 8 1 39.12 34.65 2.71 o -7 9 1 0.32 -1.16 1.36 o -6 9 1 70.99 71.99 3.88 o -5 9 1 43.71 43.70 2.14 o -4 9 1 64.00 60.01 2.01 o -3 9 1 425.98 440.10 9.84 o -2 9 1 344.74 340.10 7.35 o -1 9 1 286.70 291.65 7.28 o 0 9 1 148.03 145.69 2.46 o 1 9 1 0.69 0.19 0.67 o 2 9 1 63.73 74.00 1.76 o 3 9 1 16.51 15.66 1.51 o 4 9 1 491.81 527.55 8.55 o 5 9 1 5.52 6.01 1.70 o 6 9 1 290.77 301.91 5.82 o 7 9 1 225.50 227.68 4.92 o -2 10 1 4.22 2.87 1.50 o -1 10 1 4.18 2.00 1.42 o 0 10 1 14.05 8.09 1.70 o 1 10 1 199.67 197.07 5.24 o 2 10 1 76.77 71.31 2.31 o -17 0 2 14.59 14.40 1.74 o -16 0 2 71.16 60.82 2.63 o -15 0 2 555.99 592.75 11.98 o -14 0 2 248.53 235.90 5.16 o -13 0 2 210.38 226.67 8.43 o -12 0 2 570.05 571.79 9.89 o -11 0 2 119.44 136.64 2.93 o -10 0 2 4732.57 4398.59 54.67 o -9 0 2 2809.34 2538.41 31.85 o -8 0 2 607.59 652.91 8.74 o -7 0 2 334.80 319.95 4.57 o -6 0 2 211.15 284.78 4.05 o -5 0 2 3922.64 3969.86 68.32 o -4 0 2 9837.96 10286.99 256.51 o -3 0 2 4366.22 4302.65 260.78 o -2 0 2 1763.91 1758.32 28.53 o -1 0 2 223.95 234.90 3.74 o 0 0 2 915.27 768.84 11.50 o 1 0 2 762.43 781.15 11.60 o 2 0 2 9487.11 9894.68 148.87 o 3 0 2 9881.08 10636.73 100.88 o 4 0 2 1242.57 1402.68 18.56 o 5 0 2 0.44 7.63 1.06 o 6 0 2 10546.66 11113.74 173.44 o 7 0 2 326.72 331.54 6.53 o 8 0 2 484.26 455.30 6.37 o 9 0 2 236.89 217.16 3.53 o 10 0 2 304.22 316.51 4.87 o 11 0 2 1031.17 909.77 12.25 o 12 0 2 1.36 6.49 0.86 o 13 0 2 653.34 648.92 9.29 o 14 0 2 516.74 545.73 10.88 o 15 0 2 164.96 167.28 4.71 o 16 0 2 41.49 42.24 2.93 o 17 0 2 12.09 9.33 2.09 o -17 1 2 111.38 110.11 3.43 o -16 1 2 1.23 0.30 0.79 o -15 1 2 157.73 165.90 3.95 o -14 1 2 7.18 8.26 0.87 o -13 1 2 153.38 153.21 2.39 o -12 1 2 310.45 312.93 3.86 o -11 1 2 386.56 378.12 4.42 o -10 1 2 5.04 18.38 0.70 o -9 1 2 201.35 255.91 2.82 o -8 1 2 1025.64 1025.56 9.40 o -7 1 2 526.91 553.45 5.26 o -6 1 2 29.70 41.97 1.26 o -5 1 2 6.21 12.67 0.46 o -4 1 2 582.64 594.38 6.59 o -3 1 2 24.75 58.74 1.07 o -2 1 2 1668.27 1845.61 22.83 o -1 1 2 6844.00 7354.68 166.66 o 0 1 2 5555.21 3913.99 268.62 o 1 1 2 2027.60 2400.50 29.88 o 2 1 2 2596.28 2662.23 27.63 o 3 1 2 1262.40 1335.51 10.73 o 4 1 2 8.11 12.00 0.33 o 5 1 2 1505.13 1432.40 10.95 o 6 1 2 151.67 163.84 1.84 o 7 1 2 250.37 289.88 3.00 o 8 1 2 122.77 149.90 1.84 o 9 1 2 462.54 503.51 5.00 o 10 1 2 297.69 329.85 3.56 o 11 1 2 113.80 126.67 1.84 o 12 1 2 253.17 236.49 2.89 o 13 1 2 10.34 11.57 0.75 o 14 1 2 8.24 7.97 0.80 o 15 1 2 146.54 158.28 2.94 o 16 1 2 34.56 26.31 1.82 o -16 2 2 22.64 15.72 1.33 o -15 2 2 363.17 389.43 6.24 o -14 2 2 145.96 139.00 2.65 o -13 2 2 184.11 183.70 3.07 o -12 2 2 372.98 375.69 5.08 o -11 2 2 352.78 341.69 4.08 o -10 2 2 430.59 400.30 4.56 o -9 2 2 179.39 163.29 3.29 o -8 2 2 172.89 184.93 2.61 o -7 2 2 988.19 1011.55 11.42 o -6 2 2 943.08 1035.71 8.58 o -5 2 2 189.85 222.62 2.25 o -4 2 2 4544.74 4723.24 40.60 o -3 2 2 1101.75 1237.98 16.35 o -2 2 2 2436.91 2451.66 30.34 o -1 2 2 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