#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:45:05 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181285 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/63/2236399.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236399_Fobs loop_ _publ_author_name 'Kumar, Mohan' 'Mallesha, L.' 'Sridhar, M. A.' 'Kapoor, Kamini' 'Gupta, Vivek K.' 'Kant, Rajni' _publ_section_title ; N-[2-(5-Bromo-2-morpholin-4-ylpyrimidin-4-ylsulfanyl)-4-methoxyphenyl]-2,4,6-trimethylbenzenesulfonamide ; _journal_coeditor_code IS5200 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3061 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 97.199 _cell_angle_gamma 90.000 _cell_length_a 10.2583 _cell_length_b 17.4727 _cell_length_c 14.4375 _exptl_crystal_F_000 1192.00 _reflns_d_resolution_high 0.8108 _cod_data_source_file is5200Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sria2 in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 486.87 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 91148.29 81401.12 722.25 o 4 0 0 9253.67 9048.50 171.71 o 6 0 0 661.73 694.05 47.04 o 8 0 0 4699.93 4875.49 149.82 o 10 0 0 0.38 -20.60 19.61 o 12 0 0 207.65 288.84 64.22 o 2 1 0 2503.94 2510.40 27.87 o 3 1 0 4266.79 4271.64 41.85 o 4 1 0 38.84 40.73 4.97 o 5 1 0 1129.37 1172.87 38.95 o 6 1 0 1012.29 1015.35 40.48 o 7 1 0 85.85 68.59 10.64 o 8 1 0 1952.87 2077.48 68.95 o 9 1 0 175.66 152.72 14.20 o 10 1 0 404.47 378.86 31.24 o 11 1 0 41.18 9.51 10.98 o 12 1 0 40.27 41.83 17.91 o 2 2 0 84.16 55.06 7.14 o 3 2 0 9827.13 9315.40 85.25 o 4 2 0 2711.32 2745.30 39.29 o 5 2 0 22.66 40.09 10.15 o 6 2 0 2.24 -6.01 8.50 o 7 2 0 6764.72 6757.40 114.10 o 8 2 0 3442.80 3465.45 88.84 o 9 2 0 466.17 490.88 33.55 o 10 2 0 147.99 105.28 17.86 o 11 2 0 605.77 644.77 83.07 o 12 2 0 140.72 113.66 46.76 o 1 3 0 9544.39 9474.22 45.80 o 2 3 0 4330.48 4385.30 33.40 o 3 3 0 254.59 247.49 9.34 o 4 3 0 7577.64 7704.02 64.89 o 5 3 0 65.57 93.22 7.40 o 6 3 0 2094.81 2035.57 44.09 o 7 3 0 157.46 146.28 17.58 o 8 3 0 16.39 13.27 10.50 o 9 3 0 538.29 549.11 28.85 o 10 3 0 18.63 13.16 10.43 o 11 3 0 42.75 52.11 16.59 o 12 3 0 9.18 -7.80 22.58 o 0 4 0 502.90 616.19 14.96 o 1 4 0 9799.22 9528.52 49.58 o 2 4 0 2253.50 2301.13 23.43 o 3 4 0 122.99 129.11 5.19 o 4 4 0 3941.73 4305.83 47.75 o 5 4 0 5525.94 5856.57 56.58 o 6 4 0 62.22 43.42 12.01 o 7 4 0 483.77 503.89 23.25 o 8 4 0 2475.79 2332.77 64.98 o 9 4 0 203.19 230.63 21.34 o 10 4 0 478.57 548.77 47.97 o 11 4 0 95.63 73.59 22.59 o 12 4 0 143.18 162.62 39.41 o 1 5 0 26554.83 26202.15 138.18 o 2 5 0 286.95 292.86 8.44 o 3 5 0 5145.99 5183.49 48.81 o 4 5 0 380.43 375.27 12.46 o 5 5 0 69.34 50.52 7.94 o 6 5 0 16.94 1.77 8.19 o 7 5 0 73.16 93.80 11.36 o 8 5 0 210.64 200.05 21.17 o 9 5 0 33.10 38.52 12.10 o 10 5 0 2.22 -34.26 22.84 o 11 5 0 30.47 22.82 16.17 o 12 5 0 0.62 10.04 25.69 o 0 6 0 6673.42 6809.82 81.55 o 1 6 0 438.19 412.47 10.52 o 2 6 0 16213.42 15900.85 93.77 o 3 6 0 756.66 860.81 19.83 o 4 6 0 6140.87 6177.25 54.60 o 5 6 0 3560.80 3600.90 48.66 o 6 6 0 5513.07 5848.31 75.75 o 7 6 0 16.89 5.28 9.85 o 8 6 0 480.94 517.20 33.13 o 9 6 0 135.41 145.15 22.07 o 10 6 0 379.46 431.26 58.18 o 11 6 0 2.53 3.31 22.32 o 12 6 0 29.73 21.47 37.72 o 1 7 0 5434.84 5774.82 52.56 o 2 7 0 3404.47 3253.20 33.71 o 3 7 0 775.83 843.86 21.53 o 4 7 0 5764.01 5930.28 58.63 o 5 7 0 206.50 217.89 11.36 o 6 7 0 2432.31 2144.36 65.36 o 7 7 0 241.44 223.81 17.90 o 8 7 0 1225.98 1299.93 49.06 o 9 7 0 87.81 66.01 23.43 o 10 7 0 252.15 254.79 47.34 o 11 7 0 56.58 83.49 29.18 o 0 8 0 1103.83 1210.96 29.90 o 1 8 0 514.60 515.13 13.93 o 2 8 0 1953.74 1828.65 27.40 o 3 8 0 2375.33 2388.26 38.03 o 4 8 0 8.67 16.66 4.97 o 5 8 0 804.66 783.13 27.57 o 6 8 0 1291.41 1188.17 31.36 o 7 8 0 1329.36 1354.85 54.39 o 8 8 0 34.67 15.07 21.12 o 9 8 0 190.48 200.60 40.48 o 10 8 0 194.93 178.81 38.87 o 11 8 0 103.33 155.13 43.48 o 1 9 0 10292.20 10994.90 108.36 o 2 9 0 211.69 188.85 10.66 o 3 9 0 4714.78 4613.85 68.62 o 4 9 0 22.98 6.36 8.56 o 5 9 0 1489.32 1470.37 83.40 o 6 9 0 15.48 9.80 8.76 o 7 9 0 171.42 160.97 18.77 o 8 9 0 115.55 82.54 22.48 o 9 9 0 13.22 -2.55 19.90 o 10 9 0 10.07 3.14 37.86 o 11 9 0 106.94 161.61 48.19 o 0 10 0 1321.58 1139.47 35.85 o 1 10 0 173.49 157.68 9.73 o 2 10 0 69.40 74.29 7.75 o 3 10 0 16.83 27.22 8.87 o 4 10 0 1487.22 1298.91 55.91 o 5 10 0 141.12 147.04 15.32 o 6 10 0 14.54 40.03 13.38 o 7 10 0 139.04 112.99 28.82 o 8 10 0 1.29 13.47 26.15 o 9 10 0 23.12 9.92 27.71 o 10 10 0 336.46 428.38 64.80 o 11 10 0 11.03 15.06 29.25 o 1 11 0 1355.65 1296.00 29.07 o 2 11 0 8.26 5.27 5.10 o 3 11 0 2334.30 2320.70 43.04 o 4 11 0 438.79 352.91 21.43 o 5 11 0 548.34 629.09 48.62 o 6 11 0 656.43 563.88 41.98 o 7 11 0 165.03 216.01 39.91 o 8 11 0 151.25 173.83 35.43 o 9 11 0 1.16 -19.16 20.34 o 10 11 0 58.12 72.89 23.26 o 0 12 0 1002.93 984.94 37.08 o 1 12 0 13.77 21.52 5.81 o 2 12 0 1154.83 1230.24 32.49 o 3 12 0 711.88 626.02 20.51 o 4 12 0 461.45 448.25 31.11 o 5 12 0 64.49 57.46 20.20 o 6 12 0 15.61 10.55 12.28 o 7 12 0 742.17 870.46 80.10 o 8 12 0 338.95 373.58 58.93 o 9 12 0 86.10 81.55 29.82 o 10 12 0 287.97 311.51 66.04 o 1 13 0 564.81 526.23 19.29 o 2 13 0 97.69 73.40 9.66 o 3 13 0 909.39 961.99 28.22 o 4 13 0 52.96 25.42 10.68 o 5 13 0 6.62 5.95 12.57 o 6 13 0 128.20 136.27 19.23 o 7 13 0 1.25 -16.60 21.78 o 8 13 0 241.81 302.34 53.67 o 9 13 0 17.79 26.21 47.16 o 10 13 0 160.51 214.20 66.58 o 0 14 0 1742.75 1800.05 64.85 o 1 14 0 116.31 129.54 12.36 o 2 14 0 838.59 834.05 29.77 o 3 14 0 39.04 33.15 8.46 o 4 14 0 32.16 9.25 20.37 o 5 14 0 204.69 219.45 22.32 o 6 14 0 6.44 -4.79 36.95 o 7 14 0 12.76 21.16 44.87 o 8 14 0 121.26 156.68 40.85 o 9 14 0 117.90 86.09 63.42 o 1 15 0 791.59 884.84 35.19 o 2 15 0 203.51 204.58 18.60 o 3 15 0 1145.99 1154.56 41.18 o 4 15 0 6.73 -26.18 17.45 o 5 15 0 729.57 712.57 47.17 o 6 15 0 41.13 32.96 18.53 o 7 15 0 122.01 98.07 21.07 o 8 15 0 32.64 36.87 25.81 o 9 15 0 0.12 18.95 25.32 o 0 16 0 277.26 233.82 24.67 o 1 16 0 106.46 104.27 15.55 o 2 16 0 151.64 192.55 19.02 o 3 16 0 58.25 27.24 12.44 o 4 16 0 23.07 -9.05 16.85 o 5 16 0 271.54 289.13 33.42 o 6 16 0 287.92 255.28 33.35 o 7 16 0 27.12 -16.86 24.83 o 8 16 0 15.20 2.70 25.12 o 1 17 0 45.80 45.11 13.54 o 2 17 0 13.11 17.27 10.95 o 3 17 0 4.85 6.11 16.20 o 4 17 0 79.53 32.34 18.77 o 5 17 0 64.79 61.84 14.08 o 6 17 0 49.70 15.45 18.32 o 7 17 0 52.62 67.88 35.79 o 0 18 0 4.49 47.64 39.60 o 1 18 0 0.09 -8.38 20.95 o 2 18 0 418.87 463.90 40.54 o 3 18 0 2.65 -0.76 12.88 o 4 18 0 0.88 -16.45 15.34 o 5 18 0 109.22 77.44 17.36 o 6 18 0 68.40 20.76 17.31 o 1 19 0 156.14 138.85 38.59 o 2 19 0 8.68 39.46 30.23 o 3 19 0 174.16 204.23 28.06 o 4 19 0 24.99 0.46 13.40 o 5 19 0 62.04 30.53 17.42 o 0 20 0 46.45 63.79 25.10 o 1 20 0 32.19 68.39 29.91 o 2 20 0 37.54 47.16 21.29 o 3 20 0 60.59 56.84 30.62 o 4 20 0 227.30 286.47 43.54 o 1 21 0 33.19 72.59 30.71 o 2 21 0 10.65 28.25 18.78 o -11 0 1 4.16 -13.12 25.83 o -9 0 1 2127.85 2196.57 108.04 o -7 0 1 121.67 100.96 15.77 o -5 0 1 533.49 617.89 39.98 o -3 0 1 45.61 47.13 5.75 o 3 0 1 26470.64 24646.43 164.55 o 5 0 1 7907.15 7632.38 142.66 o 7 0 1 5712.71 5796.34 153.94 o 9 0 1 13.33 -4.86 19.81 o 11 0 1 1234.84 1300.56 226.21 o -12 1 1 45.08 17.75 19.73 o -11 1 1 140.67 112.79 16.27 o -10 1 1 486.30 456.19 40.06 o -9 1 1 1039.42 1152.73 55.53 o -8 1 1 3713.93 3683.79 91.99 o -7 1 1 609.26 613.10 33.53 o -6 1 1 3796.60 3862.55 79.95 o -5 1 1 24.76 26.32 9.67 o -4 1 1 4360.31 4487.43 79.77 o -3 1 1 725.19 734.86 17.38 o -2 1 1 1715.61 1794.85 24.25 o 2 1 1 982.32 889.66 14.43 o 3 1 1 7080.29 7296.41 58.91 o 4 1 1 15.76 16.49 6.92 o 5 1 1 241.82 266.41 17.79 o 6 1 1 1914.76 1999.91 56.82 o 7 1 1 632.28 624.24 34.99 o 8 1 1 1802.83 1910.90 65.40 o 9 1 1 372.22 371.46 29.67 o 10 1 1 1105.32 1039.13 103.48 o 11 1 1 0.12 0.77 16.06 o 12 1 1 66.42 63.67 29.15 o -12 2 1 112.71 103.42 27.55 o -11 2 1 151.76 156.08 20.65 o -10 2 1 0.45 -2.46 16.64 o -9 2 1 372.32 435.23 33.61 o -8 2 1 102.35 108.65 16.29 o -7 2 1 63.44 51.87 7.23 o -6 2 1 163.15 158.49 15.64 o -5 2 1 8925.34 9002.87 139.04 o -4 2 1 9952.03 9847.66 84.56 o -3 2 1 4653.32 4689.84 50.14 o -2 2 1 328.74 360.40 11.94 o 2 2 1 4073.53 4170.23 30.48 o 3 2 1 6730.71 6564.64 55.06 o 4 2 1 15188.93 16151.14 215.47 o 5 2 1 1248.28 1389.53 36.82 o 6 2 1 405.96 444.37 25.29 o 7 2 1 2732.89 2762.50 72.49 o 8 2 1 477.01 504.87 33.18 o 9 2 1 67.60 59.64 11.97 o 10 2 1 110.10 103.61 16.96 o 11 2 1 321.55 294.14 35.58 o 12 2 1 17.00 18.41 32.93 o -12 3 1 3.61 -19.90 29.83 o -11 3 1 1.56 7.44 18.86 o -10 3 1 25.30 17.83 10.16 o -9 3 1 0.06 0.33 12.79 o -8 3 1 408.00 396.16 29.20 o -7 3 1 1141.03 1347.79 37.59 o -6 3 1 3171.94 3408.85 54.55 o -5 3 1 4560.53 4690.59 61.50 o -4 3 1 13219.08 13982.82 77.16 o -3 3 1 4589.85 4433.43 51.74 o -2 3 1 74.81 68.83 8.04 o -1 3 1 2886.29 2982.09 26.08 o 0 3 1 1791.86 1780.57 18.17 o 1 3 1 7930.00 7721.55 53.21 o 2 3 1 255.90 280.03 7.51 o 3 3 1 10273.99 10053.19 53.46 o 4 3 1 4.64 5.89 2.92 o 5 3 1 7662.92 8123.01 89.18 o 6 3 1 193.20 247.36 15.94 o 7 3 1 1815.95 1952.83 49.01 o 8 3 1 447.92 424.53 24.08 o 9 3 1 97.28 103.41 12.58 o 10 3 1 24.64 24.95 10.60 o 11 3 1 13.74 7.60 13.96 o 12 3 1 30.97 37.67 28.73 o -12 4 1 274.26 297.83 56.28 o -11 4 1 409.96 477.85 62.22 o -10 4 1 66.87 56.09 15.62 o -9 4 1 1315.71 1398.32 59.38 o -8 4 1 511.61 409.25 27.22 o -7 4 1 3999.74 4013.31 63.11 o -6 4 1 135.97 120.27 8.53 o -5 4 1 3699.72 3415.12 59.01 o -4 4 1 418.43 437.42 15.76 o -3 4 1 7691.35 7766.56 92.56 o -2 4 1 9707.60 9905.80 97.37 o -1 4 1 24134.89 23849.13 96.76 o 0 4 1 4543.32 4550.21 30.96 o 1 4 1 3678.73 3516.09 26.09 o 2 4 1 8720.41 8523.87 49.48 o 3 4 1 241.72 218.42 7.25 o 4 4 1 3464.46 3887.71 38.91 o 5 4 1 77.55 119.83 7.17 o 6 4 1 3354.01 3317.91 52.35 o 7 4 1 32.37 19.55 8.69 o 8 4 1 289.96 277.01 19.53 o 9 4 1 995.93 932.83 39.74 o 10 4 1 348.88 365.75 39.93 o 11 4 1 2.98 2.65 38.14 o 12 4 1 154.38 175.58 55.63 o -12 5 1 210.11 263.83 48.85 o -11 5 1 18.53 1.62 24.93 o -10 5 1 269.77 349.09 38.39 o -9 5 1 1.99 -9.34 12.53 o -8 5 1 263.22 266.30 36.15 o -7 5 1 35.11 53.11 8.98 o -6 5 1 901.78 937.35 36.47 o -5 5 1 30.55 15.92 8.13 o -4 5 1 1447.10 1285.84 32.22 o -3 5 1 710.91 706.73 18.38 o -2 5 1 2172.88 2067.55 31.21 o -1 5 1 367.15 417.79 9.82 o 0 5 1 147.26 159.29 6.25 o 1 5 1 855.69 944.83 13.92 o 2 5 1 1128.06 1138.80 19.69 o 3 5 1 4268.92 4175.36 37.83 o 4 5 1 7274.03 7519.91 67.22 o 5 5 1 329.26 351.47 14.06 o 6 5 1 3285.42 3411.36 51.79 o 7 5 1 137.01 128.27 8.93 o 8 5 1 1743.96 1911.61 50.55 o 9 5 1 294.35 255.55 30.25 o 10 5 1 450.20 543.62 65.46 o 11 5 1 25.28 24.09 26.37 o 12 5 1 100.16 123.96 40.81 o -12 6 1 244.63 343.94 58.69 o -11 6 1 31.04 32.30 38.11 o -10 6 1 0.44 -0.41 23.14 o -9 6 1 508.98 464.67 36.83 o -8 6 1 248.11 224.37 21.25 o -7 6 1 59.75 44.08 16.47 o -6 6 1 1083.04 1007.70 39.84 o -5 6 1 55.25 60.17 8.80 o -4 6 1 85.24 90.66 5.59 o -3 6 1 5254.31 5707.44 68.57 o -2 6 1 2295.52 2232.12 35.02 o -1 6 1 254.86 271.44 7.93 o 0 6 1 232.28 229.37 8.65 o 1 6 1 1696.39 1566.82 21.69 o 2 6 1 2032.91 2070.84 28.26 o 3 6 1 80.83 52.94 5.64 o 4 6 1 1882.90 1861.49 37.13 o 5 6 1 767.20 699.58 20.25 o 6 6 1 1396.45 1371.28 35.78 o 7 6 1 1131.17 1169.92 41.79 o 8 6 1 0.98 -7.30 10.79 o 9 6 1 1802.85 2088.82 87.10 o 10 6 1 0.25 18.75 21.28 o 11 6 1 87.14 99.74 37.31 o -11 7 1 10.01 17.91 23.96 o -10 7 1 6.96 -27.40 30.15 o -9 7 1 1.61 -14.95 23.22 o -8 7 1 61.99 51.63 12.72 o -7 7 1 3.11 -5.13 16.47 o -6 7 1 516.20 476.33 32.26 o -5 7 1 923.89 843.51 26.27 o -4 7 1 1378.12 1400.81 31.71 o -3 7 1 4240.65 3912.51 61.13 o -2 7 1 37.33 29.40 5.20 o -1 7 1 8521.95 8414.10 54.98 o 0 7 1 1065.46 1080.19 20.42 o 1 7 1 892.45 737.54 16.62 o 2 7 1 880.22 886.82 17.80 o 3 7 1 1786.66 1838.12 32.61 o 4 7 1 15.46 28.89 5.27 o 5 7 1 695.74 717.41 17.99 o 6 7 1 82.88 66.09 7.69 o 7 7 1 23.44 24.45 10.61 o 8 7 1 7.63 3.06 22.69 o 9 7 1 0.26 24.24 24.88 o 10 7 1 5.37 13.30 34.05 o 11 7 1 5.74 14.30 29.13 o -11 8 1 43.90 33.92 21.34 o -10 8 1 10.38 17.83 19.68 o -9 8 1 296.72 279.57 54.82 o -8 8 1 366.99 333.63 31.61 o -7 8 1 184.37 129.38 24.37 o -6 8 1 629.66 687.48 28.15 o -5 8 1 1112.17 1128.58 26.78 o -4 8 1 2810.88 2675.14 85.52 o -3 8 1 59.26 54.50 7.44 o -2 8 1 4214.96 4395.28 43.87 o -1 8 1 3336.10 3523.51 35.50 o 0 8 1 10860.84 11568.86 71.64 o 1 8 1 1698.88 1677.55 27.19 o 2 8 1 4767.57 4679.62 44.69 o 3 8 1 166.59 170.74 9.37 o 4 8 1 2840.34 2787.58 42.40 o 5 8 1 6990.37 6396.08 127.87 o 6 8 1 811.23 791.99 24.44 o 7 8 1 605.03 590.61 25.30 o 8 8 1 356.95 338.30 47.75 o 9 8 1 1093.67 1207.60 95.74 o 10 8 1 7.32 -3.43 29.76 o 11 8 1 0.95 -17.19 38.13 o -11 9 1 3.03 3.81 26.44 o -10 9 1 94.15 111.75 46.26 o -9 9 1 0.72 4.40 19.60 o -8 9 1 540.41 516.34 60.01 o -7 9 1 20.10 9.35 15.43 o -6 9 1 127.66 108.13 10.94 o -5 9 1 275.82 296.23 13.72 o -4 9 1 376.94 293.44 20.18 o -3 9 1 1922.98 1982.41 52.86 o -2 9 1 390.61 311.62 15.26 o -1 9 1 73.98 138.32 7.87 o 0 9 1 220.22 261.17 11.46 o 1 9 1 4138.68 4310.16 49.98 o 2 9 1 9.69 36.63 5.51 o 3 9 1 1223.92 1267.78 26.54 o 4 9 1 121.77 77.35 6.76 o 5 9 1 485.89 439.99 20.45 o 6 9 1 1278.26 1298.75 55.43 o 7 9 1 97.65 80.77 44.89 o 8 9 1 247.07 273.61 46.43 o 9 9 1 68.21 59.66 77.64 o 10 9 1 41.19 68.11 31.18 o 11 9 1 14.66 51.35 29.77 o -11 10 1 548.82 647.95 133.78 o -10 10 1 9.87 -9.86 21.11 o -9 10 1 191.66 182.81 40.01 o -8 10 1 63.10 28.75 20.11 o -7 10 1 3824.50 3933.19 123.37 o -6 10 1 46.79 39.19 12.94 o -5 10 1 3567.71 3376.57 63.51 o -4 10 1 231.06 194.85 14.93 o -3 10 1 4894.74 4614.77 71.37 o -2 10 1 1502.35 1556.22 32.24 o -1 10 1 79.45 79.77 6.85 o 0 10 1 178.26 193.80 9.99 o 1 10 1 827.61 732.10 23.28 o 2 10 1 10.95 -0.50 4.29 o 3 10 1 1279.18 1139.93 43.42 o 4 10 1 533.72 450.34 36.66 o 5 10 1 37.01 18.27 9.31 o 6 10 1 106.90 77.98 74.92 o 7 10 1 869.62 879.19 88.31 o 8 10 1 37.03 22.46 52.67 o 9 10 1 13.94 13.01 26.49 o 10 10 1 93.49 112.95 44.48 o 11 10 1 209.09 261.31 111.07 o -10 11 1 161.29 206.82 47.12 o -9 11 1 169.28 106.28 32.16 o -8 11 1 70.69 47.28 19.97 o -7 11 1 69.49 73.76 21.14 o -6 11 1 650.67 610.27 44.92 o -5 11 1 113.61 78.81 17.36 o -4 11 1 28.67 -10.17 9.69 o -3 11 1 476.95 439.37 27.23 o -2 11 1 346.97 316.72 16.54 o -1 11 1 1047.56 1020.93 25.46 o 0 11 1 16.11 9.68 5.39 o 1 11 1 1271.25 1190.99 31.50 o 2 11 1 232.62 233.41 10.52 o 3 11 1 2183.13 2131.29 93.02 o 4 11 1 282.30 281.15 21.20 o 5 11 1 1161.50 1284.72 59.71 o 6 11 1 242.93 186.32 34.93 o 7 11 1 8.99 -7.20 19.50 o 8 11 1 179.97 137.98 67.44 o 9 11 1 84.55 103.98 56.00 o 10 11 1 183.18 272.18 53.72 o -10 12 1 33.72 39.84 25.44 o -9 12 1 6.97 0.22 24.82 o -8 12 1 297.30 286.41 52.86 o -7 12 1 251.24 272.47 37.66 o -6 12 1 2.24 -6.83 13.87 o -5 12 1 52.65 85.26 20.44 o -4 12 1 4086.21 4054.80 85.92 o -3 12 1 919.82 967.09 40.49 o -2 12 1 162.08 172.47 11.85 o -1 12 1 8.08 17.15 8.30 o 0 12 1 4493.18 4427.11 55.81 o 1 12 1 157.06 149.65 13.46 o 2 12 1 1820.48 1708.33 41.22 o 3 12 1 163.29 145.38 14.46 o 4 12 1 1599.78 1670.74 57.28 o 5 12 1 539.07 518.91 32.68 o 6 12 1 3.78 -34.85 23.23 o 7 12 1 13.15 20.34 94.28 o 8 12 1 204.79 232.52 129.63 o 9 12 1 11.51 -2.92 25.08 o 10 12 1 63.07 51.23 46.54 o -10 13 1 104.63 130.76 32.46 o -9 13 1 23.66 45.51 20.49 o -8 13 1 36.87 15.97 24.98 o -7 13 1 12.11 8.08 15.44 o -6 13 1 107.12 77.99 14.02 o -5 13 1 50.27 59.29 24.61 o -4 13 1 191.28 184.48 18.40 o -3 13 1 888.20 987.33 36.19 o -2 13 1 921.85 832.55 38.47 o -1 13 1 972.55 1010.06 27.64 o 0 13 1 8.92 25.69 8.75 o 1 13 1 3038.35 3077.70 55.23 o 2 13 1 84.25 77.43 11.71 o 3 13 1 88.12 83.00 15.20 o 4 13 1 745.26 683.62 53.33 o 5 13 1 46.60 41.21 14.23 o 6 13 1 142.68 104.61 31.04 o 7 13 1 224.99 203.71 60.16 o 8 13 1 140.74 169.15 43.75 o 9 13 1 72.06 73.10 42.29 o -9 14 1 42.01 29.26 24.43 o -8 14 1 25.91 -5.20 36.41 o -7 14 1 675.67 632.46 56.96 o -6 14 1 556.00 554.68 41.12 o -5 14 1 493.98 508.25 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