#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:45:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181286 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/64/2236408.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236408_Fobs loop_ _publ_author_name 'Li, Hairong' 'Fronczek, Frank R.' 'Watkins, Steven F.' _publ_section_title ; Orthorhombic polymorph of (2E)-2-(2,3-dihydro-1H-inden-1-ylidene)-2,3-dihydro-1H-inden-1-one ; _journal_coeditor_code JJ2149 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2756 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 5.2910 _cell_length_b 17.8090 _cell_length_c 26.6220 _exptl_crystal_F_000 1040.00 _reflns_d_resolution_high 0.8403 _cod_data_source_file jj2149Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' lisfw 2 x C18 H14 O in P 21 21 21' _shelx_refln_list_code 4 _shelx_f_calc_maximum 298.07 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1821.61 1656.17 77.64 o 4 0 0 3.42 18.06 10.95 o 6 0 0 117.15 240.00 32.06 o 1 1 0 2047.73 1770.09 63.91 o 2 1 0 693.06 631.96 22.49 o 3 1 0 644.20 664.17 23.10 o 4 1 0 173.30 197.10 11.81 o 5 1 0 122.24 160.47 12.04 o 6 1 0 101.37 121.99 19.78 o 1 2 0 8788.67 8271.80 302.10 o 2 2 0 601.06 526.76 19.27 o 3 2 0 654.02 718.67 29.99 o 4 2 0 22.90 25.88 12.51 o 5 2 0 8.27 31.28 10.95 o 6 2 0 38.51 46.13 28.85 o 1 3 0 830.49 797.75 28.50 o 2 3 0 83.24 68.04 6.49 o 3 3 0 115.41 103.08 7.98 o 4 3 0 83.02 94.70 8.68 o 5 3 0 2128.56 2025.12 55.44 o 6 3 0 48.47 99.07 31.20 o 0 4 0 493.99 513.16 31.75 o 1 4 0 88845.48 104288.27 7320.65 o 2 4 0 662.00 709.99 26.87 o 3 4 0 254.45 261.37 9.07 o 4 4 0 2580.75 2460.01 66.74 o 5 4 0 3.31 31.28 6.88 o 6 4 0 665.15 780.95 57.83 o 1 5 0 1187.74 1308.93 42.57 o 2 5 0 305.18 315.52 12.91 o 3 5 0 0.71 15.56 6.18 o 4 5 0 665.95 678.48 18.94 o 5 5 0 170.59 181.68 23.38 o 6 5 0 279.53 296.83 45.29 o 0 6 0 109.04 109.98 13.53 o 1 6 0 2.84 -7.04 7.04 o 2 6 0 415.18 427.44 16.20 o 3 6 0 790.69 800.41 23.73 o 4 6 0 25.84 16.42 16.34 o 5 6 0 26.04 63.96 23.22 o 6 6 0 11.26 53.25 40.82 o 1 7 0 4214.94 4333.28 137.07 o 2 7 0 1231.00 1258.79 37.72 o 3 7 0 190.19 202.66 9.54 o 4 7 0 2801.22 2834.78 98.47 o 5 7 0 32.44 21.82 21.19 o 0 8 0 6.41 9.46 12.59 o 1 8 0 385.13 390.09 16.59 o 2 8 0 4155.72 4126.40 129.94 o 3 8 0 1251.51 1218.57 31.27 o 4 8 0 562.12 607.42 35.84 o 5 8 0 160.53 193.17 36.52 o 1 9 0 109.43 94.71 9.23 o 2 9 0 703.17 850.20 26.07 o 3 9 0 706.64 690.24 22.08 o 4 9 0 0.20 3.91 16.42 o 5 9 0 237.57 222.21 36.68 o 0 10 0 0.12 11.65 13.14 o 1 10 0 1553.85 1588.56 49.11 o 2 10 0 1131.19 1094.74 31.50 o 3 10 0 1155.97 1150.70 41.75 o 4 10 0 0.06 8.60 18.69 o 5 10 0 6.36 10.87 49.10 o 1 11 0 352.97 393.34 18.86 o 2 11 0 9.97 7.82 10.16 o 3 11 0 5326.46 4628.40 145.14 o 4 11 0 34.49 34.48 6.88 o 5 11 0 0.91 47.70 32.06 o 0 12 0 628.34 599.34 31.55 o 1 12 0 0.01 17.12 10.87 o 2 12 0 9.37 45.43 10.16 o 3 12 0 13.84 -3.13 9.38 o 4 12 0 149.82 130.84 24.32 o 1 13 0 5.54 9.46 17.20 o 2 13 0 3.76 19.55 10.87 o 3 13 0 810.82 828.84 28.96 o 4 13 0 51.67 81.09 27.21 o 0 14 0 805.88 819.35 33.67 o 1 14 0 428.62 462.74 20.42 o 2 14 0 548.48 537.77 25.98 o 3 14 0 1.20 23.38 13.29 o 4 14 0 170.28 137.96 41.37 o 1 15 0 27.18 59.58 14.23 o 2 15 0 2.92 25.02 14.86 o 3 15 0 10.78 7.04 30.57 o 4 15 0 347.61 344.89 46.78 o 0 16 0 2.82 31.90 24.32 o 1 16 0 171.88 159.08 15.49 o 2 16 0 222.14 186.23 19.08 o 3 16 0 43.63 12.43 41.37 o 4 16 0 1155.04 968.13 85.34 o 1 17 0 2.04 32.84 17.98 o 2 17 0 360.77 291.08 24.80 o 3 17 0 52.39 66.70 38.39 o 0 18 0 338.58 373.53 57.26 o 1 18 0 385.39 341.79 29.96 o 1 19 0 552.74 490.83 58.21 o 2 19 0 36.64 36.83 29.87 o 1 20 0 119.40 130.83 28.78 o 2 20 0 4.22 16.42 40.58 o 1 0 1 157.12 162.02 7.12 o 2 0 1 417.00 390.24 13.23 o 3 0 1 1933.14 1965.33 59.60 o 4 0 1 12.26 8.60 7.04 o 5 0 1 319.75 340.75 14.47 o 6 0 1 1183.63 1255.02 77.28 o -6 1 1 16.10 36.83 36.67 o -5 1 1 757.17 814.35 30.37 o -4 1 1 119.62 122.00 9.31 o -3 1 1 15.98 35.81 8.68 o -2 1 1 1483.57 1325.78 40.86 o -1 1 1 1987.55 1591.51 51.61 o 1 1 1 1989.71 1657.30 82.48 o 2 1 1 1483.59 1404.51 46.20 o 3 1 1 15.97 31.90 6.33 o 4 1 1 119.94 114.73 8.37 o 5 1 1 757.19 809.58 27.08 o 6 1 1 16.07 82.10 38.47 o -6 2 1 36.31 89.84 32.84 o -5 2 1 6.14 28.23 11.02 o -4 2 1 189.31 190.85 10.79 o -3 2 1 29.43 28.23 6.26 o -2 2 1 425.92 384.75 9.87 o -1 2 1 1002.98 956.60 24.30 o 1 2 1 1001.62 979.31 35.07 o 2 2 1 426.08 412.70 23.88 o 3 2 1 29.37 14.86 9.46 o 4 2 1 189.21 213.92 10.64 o 5 2 1 6.15 3.91 15.64 o 6 2 1 36.18 87.73 34.56 o -6 3 1 62.56 87.74 47.70 o -5 3 1 46.91 84.61 10.32 o -4 3 1 71.55 69.44 8.37 o -3 3 1 543.09 544.53 14.33 o -2 3 1 1230.26 1259.87 31.79 o -1 3 1 15477.28 15290.03 522.94 o 0 3 1 188.90 211.72 8.93 o 1 3 1 15478.34 15026.16 624.88 o 2 3 1 1229.34 1328.38 51.09 o 3 3 1 542.97 570.91 24.03 o 4 3 1 71.54 96.34 13.14 o 5 3 1 46.97 51.61 10.87 o 6 3 1 62.66 69.44 33.55 o -6 4 1 517.92 526.07 51.32 o -5 4 1 146.29 226.33 27.76 o -4 4 1 299.34 317.45 9.94 o -3 4 1 86.32 93.06 4.85 o -2 4 1 4812.55 4730.34 112.31 o -1 4 1 19008.45 19128.93 658.41 o 0 4 1 4147.97 3975.90 139.04 o 1 4 1 19013.62 19581.54 658.00 o 2 4 1 4812.15 4418.13 239.52 o 3 4 1 86.16 80.55 11.57 o 4 4 1 299.34 336.62 14.39 o 5 4 1 146.12 197.86 13.37 o 6 4 1 517.74 637.96 77.69 o -6 5 1 76.83 24.24 34.41 o -5 5 1 476.98 480.95 33.10 o -4 5 1 668.13 685.76 35.15 o -3 5 1 54.74 55.36 7.04 o -2 5 1 17.16 36.83 4.77 o -1 5 1 6916.85 6994.80 246.25 o 0 5 1 384.65 409.40 15.82 o 1 5 1 6915.02 7066.02 223.72 o 2 5 1 17.02 25.88 5.40 o 3 5 1 54.65 66.70 17.36 o 4 5 1 668.70 669.72 20.27 o 5 5 1 477.00 444.80 15.34 o 6 5 1 76.80 186.97 45.90 o -6 6 1 0.86 -25.02 37.53 o -5 6 1 299.26 257.74 27.85 o -4 6 1 6.70 6.18 20.17 o -3 6 1 114.72 111.13 5.32 o -2 6 1 1588.60 1705.57 55.58 o -1 6 1 479.97 497.44 17.46 o 0 6 1 3327.09 3099.75 93.95 o 1 6 1 480.59 512.55 17.78 o 2 6 1 1588.39 1671.02 61.86 o 3 6 1 114.63 97.99 18.85 o 4 6 1 6.70 0.00 7.82 o 5 6 1 298.84 302.64 35.04 o 6 6 1 0.85 -11.65 45.98 o -5 7 1 84.28 89.85 23.30 o -4 7 1 591.36 596.43 34.12 o -3 7 1 497.46 513.48 13.93 o -2 7 1 5865.12 6102.66 197.89 o -1 7 1 614.87 633.05 18.33 o 0 7 1 100.92 82.13 7.59 o 1 7 1 614.92 573.92 21.46 o 2 7 1 5865.21 5889.08 168.48 o 3 7 1 496.96 472.47 20.66 o 4 7 1 591.38 646.67 25.59 o 5 7 1 84.33 83.59 22.52 o -5 8 1 247.73 269.53 30.27 o -4 8 1 1244.09 1208.40 35.02 o -3 8 1 67.16 68.03 6.96 o -2 8 1 11455.22 11849.21 338.93 o -1 8 1 859.34 892.18 30.09 o 0 8 1 1374.90 1371.79 41.52 o 1 8 1 859.80 907.30 30.33 o 2 8 1 11455.30 11806.12 387.48 o 3 8 1 67.15 57.87 7.66 o 4 8 1 1243.25 1183.18 38.54 o 5 8 1 247.60 230.58 39.11 o -5 9 1 38.89 113.54 32.14 o -4 9 1 319.17 289.20 12.36 o -3 9 1 178.47 172.07 8.84 o -2 9 1 1367.20 1463.06 47.12 o -1 9 1 83.32 94.71 8.68 o 0 9 1 124.68 113.57 10.17 o 1 9 1 83.37 83.13 10.17 o 2 9 1 1366.86 1435.31 44.53 o 3 9 1 179.05 165.50 12.98 o 4 9 1 319.18 302.66 14.63 o 5 9 1 38.95 72.72 34.33 o -5 10 1 5.21 118.93 59.19 o -4 10 1 36.76 33.47 7.74 o -3 10 1 393.09 411.23 15.88 o -2 10 1 47.99 31.28 7.82 o -1 10 1 186.01 193.21 12.44 o 0 10 1 601.32 609.07 24.90 o 1 10 1 186.46 185.54 11.42 o 2 10 1 48.01 47.70 8.52 o 3 10 1 393.11 454.26 17.92 o 4 10 1 36.94 29.71 10.09 o 5 10 1 5.23 23.38 33.54 o -4 11 1 25.35 11.65 19.47 o -3 11 1 8318.74 8514.98 238.93 o -2 11 1 29.37 22.60 10.87 o -1 11 1 21.50 18.77 11.65 o 0 11 1 376.99 426.16 20.81 o 1 11 1 21.52 28.23 8.60 o 2 11 1 29.34 20.25 10.09 o 3 11 1 8319.44 8293.16 271.64 o 4 11 1 25.38 21.03 11.03 o 5 11 1 8.09 -6.18 35.11 o -5 12 1 0.66 50.82 32.68 o -4 12 1 87.08 80.55 26.59 o -3 12 1 528.35 493.30 18.62 o -2 12 1 2912.89 3052.33 77.39 o -1 12 1 292.17 327.48 16.19 o 0 12 1 18.04 17.12 9.23 o 1 12 1 292.13 304.64 16.59 o 2 12 1 2913.94 2932.75 81.95 o 3 12 1 528.92 515.92 21.60 o 4 12 1 86.99 60.84 24.01 o -4 13 1 181.47 200.21 38.01 o -3 13 1 494.27 479.72 19.64 o -2 13 1 203.67 205.00 14.39 o -1 13 1 92.86 90.95 13.84 o 0 13 1 19.31 30.34 12.67 o 1 13 1 92.81 96.89 13.22 o 2 13 1 203.84 228.08 15.17 o 3 13 1 494.09 495.76 22.46 o 4 13 1 181.63 116.53 33.79 o -4 14 1 678.17 493.33 58.38 o -3 14 1 123.21 129.51 14.00 o -2 14 1 108.92 93.61 14.62 o -1 14 1 124.33 120.20 13.45 o 0 14 1 363.65 357.54 19.01 o 1 14 1 124.28 118.95 14.62 o 2 14 1 108.71 116.52 15.09 o 3 14 1 123.41 95.25 14.15 o 4 14 1 678.41 636.69 56.50 o -3 15 1 908.97 854.86 44.15 o -2 15 1 1839.63 1835.16 59.97 o -1 15 1 306.97 323.39 18.07 o 0 15 1 12.90 36.83 14.93 o 1 15 1 307.03 334.58 19.48 o 2 15 1 1839.92 1854.37 55.43 o 3 15 1 909.11 718.49 68.97 o 4 15 1 929.38 731.98 75.69 o -4 16 1 692.41 519.76 52.27 o -3 16 1 13.01 -3.91 45.51 o -2 16 1 420.35 423.80 21.91 o -1 16 1 679.49 706.36 28.25 o 0 16 1 1.35 46.91 16.50 o 1 16 1 679.89 666.75 27.47 o 2 16 1 419.81 483.34 24.57 o 4 16 1 692.64 672.43 72.54 o -3 17 1 4.05 18.06 30.65 o -2 17 1 142.17 143.90 24.17 o -1 17 1 36.80 41.36 15.48 o 0 17 1 122.06 152.81 17.99 o 1 17 1 36.70 20.25 20.41 o 2 17 1 142.20 145.30 20.26 o 3 17 1 4.04 52.47 44.57 o -2 18 1 1.64 -24.32 24.32 o -1 18 1 803.16 851.44 37.57 o 0 18 1 238.58 242.62 19.16 o 1 18 1 803.14 804.79 42.89 o 2 18 1 1.65 -26.51 27.37 o -1 19 1 939.17 876.29 48.07 o 0 19 1 5.75 21.03 20.25 o 1 19 1 939.86 1006.71 85.25 o 2 19 1 301.99 236.61 42.16 o -2 20 1 32.92 5.55 36.13 o 1 20 1 67.71 54.11 33.70 o 2 20 1 32.94 7.82 37.53 o 0 21 1 383.81 337.62 53.43 o 1 0 2 57.48 50.06 3.99 o 2 0 2 48.92 59.59 6.49 o 3 0 2 19.12 16.42 5.47 o 4 0 2 55.22 72.72 9.54 o 5 0 2 364.89 387.71 16.51 o 6 0 2 4679.72 4878.94 199.79 o -6 1 2 93.00 147.33 30.58 o -5 1 2 1162.87 1253.23 45.58 o -4 1 2 60.62 82.11 9.62 o -3 1 2 908.79 948.01 29.30 o -2 1 2 424.54 360.95 11.67 o -1 1 2 585.10 560.21 19.93 o 1 1 2 585.26 540.52 16.95 o 2 1 2 424.16 371.68 16.21 o 3 1 2 909.54 920.67 32.28 o 4 1 2 60.54 68.97 8.84 o 5 1 2 1162.82 1229.58 37.28 o 6 1 2 92.96 92.51 19.39 o -6 2 2 48.66 111.12 29.48 o -5 2 2 115.23 121.37 9.23 o -4 2 2 504.81 473.69 15.81 o -3 2 2 744.49 690.53 17.62 o -2 2 2 397.42 363.10 8.53 o -1 2 2 1393.28 1355.95 45.45 o 0 2 2 7179.96 7099.89 384.03 o 1 2 2 1393.20 1335.39 53.33 o 2 2 2 397.92 398.02 18.95 o 3 2 2 744.72 739.95 27.41 o 4 2 2 504.46 488.40 19.80 o 5 2 2 115.49 123.25 11.18 o 6 2 2 48.53 54.89 19.47 o -6 3 2 270.70 320.37 55.06 o -5 3 2 125.76 123.25 21.12 o -4 3 2 1521.63 1484.21 38.80 o -3 3 2 309.09 288.24 7.59 o -2 3 2 695.63 698.21 20.69 o -1 3 2 41916.50 44132.68 1749.94 o 0 3 2 3763.82 3743.31 131.62 o 1 3 2 41920.14 41615.45 3175.41 o 2 3 2 695.34 674.78 27.66 o 3 3 2 309.93 355.45 15.80 o 4 3 2 1521.64 1534.22 46.09 o 5 3 2 125.76 137.95 15.09 o 6 3 2 270.58 276.88 36.29 o -6 4 2 131.41 190.81 66.47 o -5 4 2 2238.10 2242.67 119.37 o -4 4 2 195.59 205.00 18.46 o -3 4 2 153.97 159.09 8.45 o -2 4 2 272.23 265.04 10.96 o -1 4 2 5119.24 5049.35 160.62 o 0 4 2 21017.35 22410.90 704.17 o 1 4 2 5119.91 4925.71 162.61 o 2 4 2 272.03 315.51 15.88 o 3 4 2 153.73 138.60 19.79 o 4 4 2 195.86 188.58 19.94 o 5 4 2 2237.48 2094.05 58.98 o 6 4 2 131.31 203.40 51.07 o -6 5 2 5.69 58.72 41.60 o -5 5 2 265.05 251.47 26.59 o -4 5 2 355.43 358.55 15.88 o -3 5 2 165.93 172.78 8.84 o -2 5 2 701.40 693.66 17.70 o -1 5 2 3508.01 3663.40 102.22 o 0 5 2 25.03 30.34 6.18 o 1 5 2 3511.80 3548.56 107.29 o 2 5 2 702.00 727.98 22.64 o 3 5 2 165.99 107.08 20.26 o 4 5 2 355.68 401.11 16.82 o 5 5 2 264.88 288.16 14.24 o 6 5 2 5.67 50.04 38.39 o -6 6 2 31.80 59.58 36.67 o -5 6 2 18.41 43.94 22.60 o -4 6 2 196.63 203.44 11.97 o -3 6 2 68.01 73.67 8.68 o -2 6 2 2171.29 2174.03 54.87 o -1 6 2 817.42 777.67 23.44 o 0 6 2 186.07 195.61 10.17 o 1 6 2 817.23 787.08 23.60 o 2 6 2 2170.29 2208.14 73.81 o 3 6 2 68.02 23.38 17.83 o 4 6 2 196.73 208.29 12.91 o 5 6 2 18.41 25.02 7.82 o 6 6 2 31.70 82.10 42.07 o -5 7 2 23.39 77.57 20.17 o -4 7 2 173.56 180.20 12.75 o -3 7 2 1648.52 1619.56 45.10 o -2 7 2 9079.77 9021.21 268.33 o -1 7 2 2130.00 2123.45 59.47 o 0 7 2 484.77 455.92 19.11 o 1 7 2 2129.83 2044.08 63.40 o 2 7 2 9081.64 9406.34 323.32 o 3 7 2 1648.92 1881.83 99.60 o 4 7 2 173.55 172.77 12.51 o 5 7 2 23.46 21.03 28.23 o -5 8 2 47.94 29.71 20.41 o -4 8 2 1105.36 1083.15 44.17 o -3 8 2 277.67 263.16 13.61 o -2 8 2 2126.13 2063.92 58.60 o -1 8 2 2210.61 2339.80 73.29 o 0 8 2 563.10 545.99 18.33 o 1 8 2 2212.26 2312.76 72.81 o 2 8 2 2125.84 2185.35 68.10 o 3 8 2 277.97 268.64 11.03 o 4 8 2 1105.60 1109.07 35.40 o 5 8 2 47.94 21.82 30.57 o -5 9 2 42.72 46.13 32.69 o -4 9 2 223.13 177.94 25.34 o -3 9 2 134.12 114.11 16.11 o -2 9 2 336.70 365.01 12.83 o -1 9 2 571.49 565.68 18.63 o 0 9 2 1399.01 1410.97 40.02 o 1 9 2 571.22 620.17 22.31 o 2 9 2 336.60 320.49 16.04 o 3 9 2 134.08 166.90 8.68 o 4 9 2 223.16 201.87 15.88 o 5 9 2 42.73 43.95 40.04 o -5 10 2 189.42 147.35 31.91 o -4 10 2 17.13 22.60 9.30 o -3 10 2 469.12 483.43 15.96 o -2 10 2 263.50 251.51 14.16 o -1 10 2 224.48 230.62 12.75 o 0 10 2 212.37 234.06 13.69 o 1 10 2 224.19 240.94 13.06 o 2 10 2 263.86 275.99 12.99 o 3 10 2 468.91 481.00 20.89 o 4 10 2 17.08 11.65 17.20 o 5 10 2 189.24 308.46 43.25 o -4 11 2 89.15 93.61 13.53 o -3 11 2 444.41 447.17 20.11 o -2 11 2 131.41 130.84 11.50 o -1 11 2 16.10 17.12 10.17 o 0 11 2 806.78 821.26 28.90 o 1 11 2 16.19 21.82 9.38 o 2 11 2 131.30 126.39 11.97 o 3 11 2 443.81 449.59 19.01 o 4 11 2 89.34 106.51 16.19 o 5 11 2 4.64 57.00 39.25 o -5 12 2 66.09 109.94 38.16 o -4 12 2 167.16 161.89 29.88 o -3 12 2 268.98 243.58 17.44 o -2 12 2 470.20 472.41 23.08 o -1 12 2 74.84 73.67 11.50 o 0 12 2 568.22 570.86 22.70 o 1 12 2 74.77 109.95 11.73 o 2 12 2 470.24 488.37 19.80 o 3 12 2 269.04 251.48 14.16 o 4 12 2 167.06 179.41 29.95 o 5 12 2 66.10 34.48 33.47 o -4 13 2 219.50 204.99 39.26 o -3 13 2 1383.61 1330.13 40.82 o -2 13 2 74.49 118.32 12.75 o -1 13 2 188.98 190.85 13.92 o 0 13 2 1.75 12.43 12.43 o 1 13 2 188.88 197.10 14.94 o 2 13 2 74.78 80.55 11.57 o 3 13 2 1383.33 1303.73 46.46 o 4 13 2 219.44 278.75 42.00 o -4 14 2 1003.06 793.83 74.14 o -3 14 2 30.77 34.48 15.80 o -2 14 2 278.89 304.60 19.56 o -1 14 2 444.78 487.08 22.22 o 0 14 2 218.86 247.95 16.74 o 1 14 2 445.10 430.82 19.72 o 2 14 2 278.86 288.17 15.18 o 3 14 2 30.75 20.25 11.81 o 4 14 2 1002.29 827.34 78.84 o -3 15 2 220.85 201.87 20.65 o -2 15 2 42.91 75.61 16.50 o -1 15 2 198.33 212.27 14.70 o 0 15 2 3.13 23.38 14.07 o 1 15 2 198.31 203.43 17.52 o 2 15 2 42.89 16.42 13.37 o 3 15 2 221.53 317.39 45.83 o 4 15 2 341.80 371.32 51.71 o -4 16 2 135.88 171.26 39.49 o -3 16 2 69.49 23.38 37.61 o -2 16 2 411.94 395.47 30.04 o -1 16 2 75.72 83.59 15.87 o 0 16 2 26.27 63.96 18.77 o 1 16 2 75.64 62.64 16.34 o 2 16 2 412.05 410.10 23.78 o 3 16 2 69.52 55.36 19.55 o -3 17 2 103.70 374.50 252.20 o -2 17 2 305.64 263.14 31.76 o -1 17 2 76.21 28.86 17.13 o 0 17 2 2.68 -3.91 18.84 o 1 17 2 76.30 79.61 21.97 o 2 17 2 305.54 316.41 27.85 o 3 17 2 103.80 154.13 34.72 o -2 18 2 6.46 16.42 31.98 o -1 18 2 44.58 14.86 22.68 o 0 18 2 220.49 234.01 21.35 o 1 18 2 44.68 101.89 25.96 o 2 18 2 6.42 -3.91 30.65 o 3 18 2 1.90 -14.07 42.14 o -1 19 2 27.57 4.61 18.69 o 0 19 2 43.03 35.81 31.12 o 1 19 2 27.53 -18.77 33.70 o 2 19 2 29.68 3.13 36.67 o -2 20 2 83.17 71.32 40.58 o 0 20 2 2.73 86.17 35.81 o 1 20 2 641.81 643.69 38.34 o 2 20 2 83.11 200.19 137.71 o 0 21 2 125.71 169.85 43.01 o 1 0 3 2.56 7.04 3.83 o 2 0 3 2245.26 2005.89 65.36 o 3 0 3 125.49 141.25 7.98 o 4 0 3 12.14 22.60 7.74 o 5 0 3 8.20 23.38 12.43 o 6 0 3 304.87 474.63 36.53 o -6 1 3 20.69 75.61 28.23 o -5 1 3 43.21 72.72 13.37 o -4 1 3 157.96 160.49 14.86 o -3 1 3 82.24 79.06 9.93 o -2 1 3 714.07 605.46 17.95 o -1 1 3 3253.14 3126.08 100.91 o 0 1 3 1279.67 1211.55 84.24 o 1 1 3 3254.83 2967.35 104.49 o 2 1 3 714.05 646.13 29.86 o 3 1 3 82.27 88.29 6.80 o 4 1 3 157.79 159.08 9.85 o 5 1 3 43.15 57.00 12.67 o 6 1 3 20.72 60.83 20.96 o -6 2 3 43.58 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