#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:45:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181286 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/64/2236485.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236485_Fobs loop_ _publ_author_name 'Li, Dong-jiao' _publ_section_title ; Bis[4,4,5,5-tetramethyl-2-(pyridin-2-yl-\k^2^N)imidazoline-1-oxyl 3-oxide-\kO]tris(nitrato-\k^2^O,O')terbium(III) ; _journal_coeditor_code MW2078 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1341 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 98.367 _cell_angle_gamma 90.000 _cell_length_a 12.2923 _cell_length_b 11.1143 _cell_length_c 23.2644 _exptl_crystal_F_000 1632.00 _reflns_d_resolution_high 0.8405 _cod_data_source_file mw2078Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' shelxl in P21/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 363.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 48307.58 45575.18 635.28 o 4 0 0 4189.66 4293.70 84.46 o 6 0 0 31789.36 32325.42 729.79 o 8 0 0 17267.65 19216.67 903.77 o 10 0 0 2686.00 2738.59 138.17 o 12 0 0 3176.34 3131.32 262.05 o 14 0 0 5234.77 5376.48 469.63 o 1 1 0 2230.37 2398.13 46.31 o 2 1 0 5222.60 5216.14 77.71 o 3 1 0 10592.43 10077.12 226.00 o 4 1 0 19561.84 18519.90 121.33 o 5 1 0 385.96 382.10 26.07 o 6 1 0 705.40 504.81 52.37 o 7 1 0 415.60 500.57 32.15 o 8 1 0 1364.82 1504.46 38.88 o 9 1 0 1623.89 1728.94 59.92 o 10 1 0 11594.49 11900.71 378.60 o 11 1 0 815.72 913.77 71.10 o 12 1 0 3693.75 3302.73 140.95 o 13 1 0 435.57 246.56 70.04 o 14 1 0 163.60 89.41 32.05 o 0 2 0 16465.04 14907.39 361.94 o 1 2 0 30720.85 27910.62 412.19 o 2 2 0 15442.74 14250.44 345.71 o 3 2 0 3526.26 3548.86 59.51 o 4 2 0 1362.83 1438.94 32.49 o 5 2 0 2745.08 1951.74 347.36 o 6 2 0 1211.31 1129.21 39.79 o 7 2 0 13452.66 13639.61 326.49 o 8 2 0 2287.24 2490.47 87.46 o 9 2 0 7338.81 7467.52 292.32 o 10 2 0 1354.45 1261.64 65.19 o 11 2 0 29.66 47.88 40.19 o 12 2 0 2466.31 2024.05 131.08 o 13 2 0 4477.20 3765.15 277.56 o 14 2 0 1019.73 1008.60 206.04 o 1 3 0 10010.12 10054.88 331.97 o 2 3 0 6704.00 6741.95 101.33 o 3 3 0 25358.15 22526.23 305.53 o 4 3 0 619.46 604.07 46.91 o 5 3 0 20917.76 19932.46 697.00 o 6 3 0 748.62 850.94 123.79 o 7 3 0 357.72 282.51 56.86 o 8 3 0 0.47 20.90 29.80 o 9 3 0 9086.26 9133.49 316.08 o 10 3 0 35.85 46.86 64.49 o 11 3 0 10495.90 10832.58 419.93 o 12 3 0 408.86 479.62 74.46 o 13 3 0 1930.07 1718.22 141.07 o 14 3 0 35.82 57.46 45.60 o 0 4 0 10686.71 10713.56 221.15 o 1 4 0 7017.53 7201.54 116.26 o 2 4 0 1033.93 1000.45 35.22 o 3 4 0 44.17 75.09 19.70 o 4 4 0 2662.62 2443.29 97.46 o 5 4 0 9721.09 9587.21 229.67 o 6 4 0 19471.25 19756.90 539.24 o 7 4 0 14615.40 15359.39 414.89 o 8 4 0 7610.09 7910.26 269.51 o 9 4 0 882.50 1001.81 183.30 o 10 4 0 63.21 94.31 59.93 o 11 4 0 776.68 823.75 136.27 o 12 4 0 495.48 497.29 81.27 o 13 4 0 2442.26 2342.75 207.52 o 1 5 0 264.34 236.83 44.23 o 2 5 0 30472.97 29419.30 479.60 o 3 5 0 528.04 535.74 39.85 o 4 5 0 27644.33 28338.41 1223.98 o 5 5 0 3062.87 1968.44 626.77 o 6 5 0 1318.76 1272.77 120.26 o 7 5 0 8.73 27.85 27.75 o 8 5 0 3720.20 3929.23 139.60 o 9 5 0 208.33 194.50 53.89 o 10 5 0 13585.80 13671.78 511.75 o 11 5 0 2646.11 2509.84 141.85 o 12 5 0 5157.19 4751.40 280.70 o 13 5 0 13.65 -2.64 50.45 o 0 6 0 23271.92 22577.42 929.77 o 1 6 0 6.90 -24.07 38.59 o 2 6 0 6505.40 6965.75 196.39 o 3 6 0 78.83 119.92 39.52 o 4 6 0 6.75 33.84 18.69 o 5 6 0 740.46 411.39 168.73 o 6 6 0 15880.35 16458.92 668.99 o 7 6 0 648.82 625.76 95.59 o 8 6 0 10493.71 10966.11 402.56 o 9 6 0 76.68 101.53 52.00 o 10 6 0 1983.16 2132.07 141.28 o 11 6 0 8.86 80.26 55.82 o 12 6 0 2208.28 2268.82 262.17 o 1 7 0 509.50 687.62 153.84 o 2 7 0 12246.95 12449.78 371.09 o 3 7 0 9284.31 9630.79 395.61 o 4 7 0 7741.66 7485.12 264.15 o 5 7 0 8585.44 8607.12 280.33 o 6 7 0 994.79 127.72 282.69 o 7 7 0 4745.90 4534.25 230.78 o 8 7 0 134.12 177.25 78.01 o 9 7 0 4584.97 4430.15 364.39 o 10 7 0 4058.12 3744.38 421.57 o 11 7 0 2394.56 2360.33 268.93 o 12 7 0 2368.09 2358.42 169.05 o 0 8 0 3613.84 3566.20 198.11 o 1 8 0 11498.95 11397.13 472.59 o 2 8 0 1504.35 1425.97 109.47 o 3 8 0 81.71 115.47 36.69 o 4 8 0 640.91 637.98 91.76 o 5 8 0 2515.15 2722.16 109.35 o 6 8 0 2095.44 2080.98 78.66 o 7 8 0 8785.49 8937.91 478.54 o 8 8 0 383.91 291.84 78.82 o 9 8 0 2481.50 2493.36 108.84 o 10 8 0 697.59 708.19 154.82 o 11 8 0 353.58 345.51 82.52 o 1 9 0 2170.83 2133.31 127.73 o 2 9 0 3797.80 4188.44 216.41 o 3 9 0 15102.96 16372.19 582.98 o 4 9 0 3729.51 3861.27 177.68 o 5 9 0 7161.31 7227.05 302.61 o 6 9 0 200.35 292.39 84.56 o 7 9 0 456.94 363.57 90.26 o 8 9 0 386.43 291.29 78.66 o 9 9 0 749.53 728.40 116.44 o 10 9 0 998.59 940.79 190.54 o 0 10 0 6245.35 6755.28 599.52 o 1 10 0 4100.67 4242.35 181.56 o 2 10 0 3989.41 3697.86 298.89 o 3 10 0 125.18 97.25 63.58 o 4 10 0 231.90 192.52 49.21 o 5 10 0 2153.12 2341.32 201.64 o 6 10 0 3244.58 3023.09 211.90 o 7 10 0 1600.13 1381.98 277.55 o 8 10 0 1745.38 1529.21 348.00 o 9 10 0 1536.89 1263.06 344.34 o 1 11 0 146.50 96.83 69.71 o 2 11 0 3692.99 3750.98 320.84 o 3 11 0 276.95 271.33 63.99 o 4 11 0 5223.79 5441.05 248.81 o 5 11 0 431.24 437.26 104.63 o 6 11 0 1027.77 942.22 205.92 o 7 11 0 37.27 105.33 95.48 o 8 11 0 736.55 638.81 207.76 o 0 12 0 3699.78 3904.04 250.37 o 1 12 0 361.94 406.89 117.14 o 2 12 0 2245.16 2207.53 132.78 o 3 12 0 334.28 345.29 66.36 o 4 12 0 218.12 169.61 68.92 o 5 12 0 240.56 211.99 77.78 o 6 12 0 3460.85 3507.42 601.43 o 1 13 0 122.38 141.86 71.37 o 2 13 0 726.67 670.96 220.24 o -13 0 1 756.22 995.85 183.79 o -11 0 1 2095.28 1692.81 113.70 o -9 0 1 13620.79 15402.42 512.87 o -7 0 1 4788.35 5213.08 224.43 o -5 0 1 67.22 95.18 23.54 o -3 0 1 55843.84 50966.36 1408.99 o 1 0 1 6993.39 4528.89 188.57 o 3 0 1 36495.96 33635.22 362.59 o 5 0 1 79008.66 71549.14 1009.27 o 7 0 1 34282.51 36365.29 866.24 o 9 0 1 1143.08 1074.57 54.27 o 11 0 1 10315.23 11411.01 435.29 o 13 0 1 7550.43 7979.61 613.19 o -14 1 1 779.30 696.64 113.57 o -13 1 1 4624.01 4349.59 237.00 o -12 1 1 945.53 1049.26 154.13 o -11 1 1 2443.79 2229.52 136.60 o -10 1 1 7.53 39.08 24.85 o -9 1 1 1046.26 1146.88 53.95 o -8 1 1 76.51 50.61 29.47 o -7 1 1 23431.95 24178.56 417.30 o -6 1 1 23168.60 24378.53 547.78 o -5 1 1 28500.38 27308.47 365.16 o -4 1 1 2482.31 2809.78 55.99 o -3 1 1 2624.31 2696.33 43.58 o -2 1 1 482.59 441.08 11.34 o -1 1 1 2555.02 2403.40 54.03 o 1 1 1 75010.45 70129.30 1340.41 o 2 1 1 1092.30 1066.73 16.88 o 3 1 1 54206.97 49568.67 496.88 o 4 1 1 2835.65 2899.48 43.57 o 5 1 1 7575.33 8004.20 121.39 o 6 1 1 151.85 183.29 26.51 o 7 1 1 14357.12 14993.43 300.01 o 8 1 1 3856.42 4455.38 161.16 o 9 1 1 6635.60 7137.41 286.39 o 10 1 1 1872.01 2057.73 82.93 o 11 1 1 4180.95 3750.51 116.39 o 12 1 1 436.43 465.04 71.94 o 13 1 1 307.40 275.56 86.51 o 14 1 1 622.56 521.36 88.77 o -14 2 1 1326.55 1245.88 189.94 o -13 2 1 0.30 39.27 34.13 o -12 2 1 592.44 510.07 96.55 o -11 2 1 1123.12 1194.91 201.03 o -10 2 1 13217.76 13398.36 394.68 o -9 2 1 4196.97 4080.07 121.26 o -8 2 1 14391.15 14440.87 320.67 o -7 2 1 2142.06 2114.70 82.06 o -6 2 1 124.53 150.72 48.49 o -5 2 1 11592.11 12929.71 218.02 o -4 2 1 16106.02 16509.07 295.21 o -3 2 1 6556.21 6536.61 100.18 o -2 2 1 17447.43 15787.42 305.21 o -1 2 1 17393.98 15984.72 265.21 o 0 2 1 294.60 305.62 16.94 o 1 2 1 61.80 90.56 20.00 o 2 2 1 16960.43 17129.79 338.80 o 3 2 1 776.31 570.23 76.49 o 4 2 1 32374.05 27319.13 1453.76 o 5 2 1 6466.24 6095.37 185.52 o 6 2 1 10473.52 9765.83 195.48 o 7 2 1 3118.92 3435.98 97.30 o 8 2 1 4239.03 4517.34 132.46 o 9 2 1 126.59 172.40 39.10 o 10 2 1 3872.61 4141.87 183.68 o 11 2 1 4000.37 3508.10 142.34 o 12 2 1 4112.81 3903.35 224.22 o 13 2 1 760.25 704.61 118.43 o 14 2 1 2515.69 2336.21 343.53 o -14 3 1 3730.71 3931.77 248.70 o -13 3 1 219.50 140.73 57.95 o -12 3 1 8345.12 8476.59 348.51 o -11 3 1 16.06 -50.41 50.56 o -10 3 1 673.60 767.84 137.54 o -9 3 1 213.06 214.11 65.20 o -8 3 1 4781.01 5038.26 195.35 o -7 3 1 263.08 315.24 57.63 o -6 3 1 36493.21 36747.80 668.28 o -5 3 1 78.35 95.19 24.13 o -4 3 1 18713.32 18816.11 352.48 o -3 3 1 902.43 1044.69 29.48 o -2 3 1 11838.52 12667.75 271.19 o -1 3 1 6865.57 6959.90 120.61 o 0 3 1 5865.80 5630.30 95.03 o 1 3 1 12029.97 12425.53 207.65 o 2 3 1 3099.71 2879.83 52.27 o 3 3 1 900.13 849.20 15.44 o 4 3 1 21932.96 22205.20 392.49 o 5 3 1 92.23 112.31 31.83 o 6 3 1 6854.21 6566.60 133.86 o 7 3 1 326.09 361.08 78.06 o 8 3 1 13366.73 13625.25 417.45 o 9 3 1 1673.42 1566.20 114.53 o 10 3 1 4611.05 4865.00 174.27 o 11 3 1 772.12 538.27 124.98 o 12 3 1 43.51 102.58 38.70 o 13 3 1 27.99 84.23 43.81 o 14 3 1 2451.61 2489.95 167.74 o -13 4 1 4.33 28.74 50.67 o -12 4 1 93.46 120.50 45.84 o -11 4 1 920.31 663.52 133.79 o -10 4 1 12825.81 13191.51 400.54 o -9 4 1 7713.32 7563.51 289.86 o -8 4 1 13859.79 14173.17 432.39 o -7 4 1 4372.83 4293.80 157.04 o -6 4 1 23.89 60.93 29.00 o -5 4 1 980.73 1051.84 63.77 o -4 4 1 15015.61 15140.05 415.95 o -3 4 1 4184.38 3923.84 88.90 o -2 4 1 4828.79 4894.09 75.50 o -1 4 1 20588.69 18186.59 429.03 o 0 4 1 3353.91 3263.55 68.83 o 1 4 1 7620.53 8082.94 145.78 o 2 4 1 5681.86 5697.82 142.35 o 3 4 1 3379.22 3503.40 88.96 o 4 4 1 38543.64 36031.93 843.78 o 5 4 1 5031.41 4629.26 109.17 o 6 4 1 15589.38 15937.28 438.25 o 7 4 1 2986.04 2959.42 121.46 o 8 4 1 22.25 78.80 51.43 o 9 4 1 161.32 202.15 61.21 o 10 4 1 7166.62 7603.57 356.72 o 11 4 1 1871.19 1860.64 161.87 o 12 4 1 3079.84 3023.80 133.77 o 13 4 1 2159.80 2082.17 136.34 o -13 5 1 5324.05 5410.77 257.47 o -12 5 1 1592.05 1255.06 195.50 o -11 5 1 3669.11 3443.82 201.63 o -10 5 1 72.08 135.36 65.43 o -9 5 1 261.98 227.95 57.49 o -8 5 1 1356.77 1338.96 179.87 o -7 5 1 8944.52 9146.58 308.27 o -6 5 1 791.59 869.83 163.13 o -5 5 1 26797.97 24938.32 1862.19 o -4 5 1 8131.48 7725.94 385.48 o -3 5 1 7511.71 7758.93 300.74 o -2 5 1 3080.89 3415.28 99.96 o -1 5 1 729.10 665.20 35.55 o 0 5 1 127.05 101.00 23.12 o 1 5 1 29511.17 29129.85 1025.28 o 2 5 1 1039.93 937.61 65.16 o 3 5 1 7665.74 6845.57 172.28 o 4 5 1 6431.87 7123.57 110.63 o 5 5 1 993.65 764.07 151.27 o 6 5 1 69.72 69.93 56.17 o 7 5 1 10857.90 11519.27 401.64 o 8 5 1 209.78 265.53 55.32 o 9 5 1 17854.99 18705.03 596.88 o 10 5 1 2629.14 2948.32 259.63 o 11 5 1 2192.24 1996.82 264.96 o 12 5 1 18.51 39.40 54.42 o 13 5 1 1275.31 1342.13 188.17 o -12 6 1 45.44 107.38 61.37 o -11 6 1 5344.37 4981.77 255.06 o -10 6 1 13.85 41.12 43.77 o -9 6 1 15839.83 16322.68 524.37 o -8 6 1 466.11 440.02 116.04 o -7 6 1 1754.12 1711.74 183.36 o -6 6 1 8.92 102.74 65.97 o -5 6 1 4738.34 4941.19 165.25 o -4 6 1 3569.40 3450.32 100.90 o -3 6 1 18935.98 20148.43 452.12 o -2 6 1 108.52 46.03 33.18 o -1 6 1 16120.81 16112.62 366.69 o 0 6 1 2782.24 2974.37 81.17 o 1 6 1 2403.27 2395.48 105.06 o 2 6 1 73.59 54.34 43.81 o 3 6 1 17174.63 16978.26 532.00 o 4 6 1 6.40 33.41 22.13 o 5 6 1 28742.57 31292.24 1168.08 o 6 6 1 172.28 187.48 54.56 o 7 6 1 1639.31 1678.40 76.30 o 8 6 1 141.42 137.01 46.81 o 9 6 1 294.61 420.03 72.52 o 10 6 1 580.46 585.01 129.48 o 11 6 1 3475.40 3275.44 236.76 o 12 6 1 202.37 193.68 54.94 o -12 7 1 3348.85 3195.73 195.90 o -11 7 1 2253.20 2185.73 124.21 o -10 7 1 807.03 832.10 177.46 o -9 7 1 538.44 409.88 95.52 o -8 7 1 3200.83 3321.98 150.67 o -7 7 1 2538.15 2480.37 129.43 o -6 7 1 11090.15 11475.52 803.85 o -5 7 1 4862.48 4922.36 142.72 o -4 7 1 1935.41 1827.71 60.80 o -3 7 1 612.52 528.25 84.32 o -2 7 1 0.34 56.42 31.66 o -1 7 1 4660.32 4460.47 151.61 o 0 7 1 2922.18 2902.44 121.30 o 1 7 1 23629.68 24717.22 1123.81 o 2 7 1 11239.55 11320.56 340.42 o 3 7 1 12694.57 12296.11 580.40 o 4 7 1 4681.74 4971.34 146.44 o 5 7 1 216.44 191.74 35.04 o 6 7 1 556.06 345.75 172.93 o 7 7 1 8940.97 9502.34 451.13 o 8 7 1 5063.61 6138.76 311.43 o 9 7 1 4740.09 4834.90 270.19 o 10 7 1 1460.32 1468.65 161.36 o 11 7 1 1805.98 1951.73 194.96 o 12 7 1 9.85 -58.92 107.92 o -11 8 1 70.15 32.38 56.76 o -10 8 1 4935.87 4902.27 322.79 o -9 8 1 785.75 740.75 176.41 o -8 8 1 4617.30 4125.89 258.09 o -7 8 1 1914.62 1809.35 146.65 o -6 8 1 27.01 19.35 33.57 o -5 8 1 128.90 129.16 47.45 o -4 8 1 9993.43 10251.57 476.90 o -3 8 1 274.31 340.48 62.69 o -2 8 1 19478.67 21192.73 706.01 o -1 8 1 2560.53 2404.34 116.67 o 0 8 1 3334.42 3250.78 132.08 o 1 8 1 322.01 367.95 96.28 o 2 8 1 93.82 96.29 68.82 o 3 8 1 426.00 439.71 77.87 o 4 8 1 13732.49 14302.64 447.56 o 5 8 1 1021.01 876.46 139.35 o 6 8 1 5706.81 6153.13 272.85 o 7 8 1 34.03 57.92 41.43 o 8 8 1 241.04 194.58 64.42 o 9 8 1 425.17 374.58 74.21 o 10 8 1 1910.87 1823.80 121.14 o 11 8 1 651.37 517.66 169.66 o -10 9 1 628.77 632.34 132.44 o -9 9 1 119.74 40.55 65.70 o -8 9 1 2792.75 2491.92 132.34 o -7 9 1 128.74 134.55 49.40 o -6 9 1 9640.90 10119.52 497.96 o -5 9 1 284.26 239.34 63.05 o -4 9 1 2478.36 2681.22 137.69 o -3 9 1 1799.03 1998.86 93.32 o -2 9 1 747.74 721.32 167.08 o -1 9 1 357.27 465.56 97.50 o 0 9 1 9707.57 10602.84 362.16 o 1 9 1 2771.10 2605.18 164.13 o 2 9 1 19700.77 20100.95 725.71 o 3 9 1 576.48 635.08 88.73 o 4 9 1 2612.71 2792.15 286.68 o 5 9 1 217.37 184.16 68.73 o 6 9 1 3119.78 3125.60 160.31 o 7 9 1 972.03 1004.44 237.89 o 8 9 1 3489.84 3652.47 157.30 o 9 9 1 643.21 553.01 125.35 o 10 9 1 3895.61 4225.56 336.07 o -9 10 1 2995.30 3133.71 383.90 o -8 10 1 1248.98 1032.24 248.51 o -7 10 1 1048.63 1146.91 201.56 o -6 10 1 439.14 437.49 113.66 o -5 10 1 76.14 132.27 71.33 o -4 10 1 1043.96 1183.68 108.24 o -3 10 1 8438.77 8298.45 356.38 o -2 10 1 4234.85 4293.01 247.84 o -1 10 1 7180.81 8013.25 365.61 o 0 10 1 5846.74 6200.60 314.29 o 1 10 1 1603.11 1727.63 278.84 o 2 10 1 94.04 114.05 51.71 o 3 10 1 2130.20 2181.81 126.66 o 4 10 1 981.86 1299.74 111.01 o 5 10 1 4384.59 4419.18 242.60 o 6 10 1 1613.33 1420.73 331.68 o 7 10 1 1245.62 1104.87 249.48 o 8 10 1 9.40 149.01 117.26 o 9 10 1 150.09 169.10 78.19 o -8 11 1 2.91 87.45 104.14 o -7 11 1 2761.61 2908.66 210.15 o -6 11 1 232.46 139.45 69.94 o -5 11 1 5086.92 5084.73 253.40 o -4 11 1 1.77 78.83 64.20 o -3 11 1 847.53 786.57 137.96 o -2 11 1 294.26 313.90 66.65 o -1 11 1 2802.05 2879.09 321.25 o 0 11 1 8.67 66.92 59.54 o 1 11 1 8259.65 9087.82 531.13 o 2 11 1 1259.37 1138.27 221.37 o 3 11 1 3193.49 3523.28 273.77 o 4 11 1 443.42 480.19 100.55 o 5 11 1 19.21 17.06 62.02 o 6 11 1 99.09 177.11 139.85 o 7 11 1 3324.18 3164.71 686.25 o -6 12 1 0.62 98.20 66.37 o -5 12 1 133.68 159.84 51.24 o -4 12 1 220.67 143.33 99.34 o -3 12 1 6302.32 6440.29 349.43 o -2 12 1 327.51 354.34 86.41 o -1 12 1 4702.14 4382.99 581.07 o 0 12 1 184.03 225.88 117.12 o 1 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