#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:45:31 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181286 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/64/2236491.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236491_Fobs loop_ _publ_author_name 'Dayananda, A. S.' 'Dutkiewicz, Grzegorz' 'Yathirajan, H. S.' 'Ramesha, A. R.' 'Kubicki, Maciej' _publ_section_title ; 1-[Bis(4-fluorophenyl)methyl]piperazine ; _journal_coeditor_code MW2085 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2817 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.355 _cell_angle_gamma 90.000 _cell_length_a 12.1574 _cell_length_b 8.8559 _cell_length_c 13.8604 _exptl_crystal_F_000 608.00 _reflns_d_resolution_high 0.7969 _cod_data_source_file mw2085Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' hsy200 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 99.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1219.58 1119.01 2.39 o 2 0 0 1974.84 1872.77 9.62 o 3 0 0 82.07 87.73 0.83 o 4 0 0 1973.09 1819.60 14.60 o 5 0 0 195.39 165.17 2.85 o 6 0 0 334.59 389.42 3.56 o 7 0 0 31.20 31.30 1.13 o 8 0 0 0.12 0.83 0.79 o 9 0 0 170.05 161.39 2.20 o 10 0 0 1.45 2.91 0.29 o 11 0 0 516.62 520.99 4.47 o 12 0 0 206.17 216.80 2.84 o 13 0 0 193.95 202.59 2.53 o 14 0 0 323.69 323.79 5.10 o 15 0 0 15.31 13.74 0.62 o 1 1 0 990.12 949.11 2.30 o 2 1 0 381.64 375.15 1.73 o 3 1 0 171.77 169.43 1.05 o 4 1 0 1501.68 1373.98 3.19 o 5 1 0 3161.65 3094.67 7.80 o 6 1 0 39.56 43.19 0.72 o 7 1 0 90.98 97.31 1.41 o 8 1 0 0.01 0.13 0.15 o 9 1 0 80.82 77.89 1.04 o 10 1 0 313.55 288.53 2.18 o 11 1 0 144.98 150.85 1.69 o 12 1 0 61.84 63.35 0.96 o 13 1 0 8.78 11.73 0.44 o 14 1 0 36.04 39.05 0.65 o 15 1 0 14.15 12.88 0.33 o 0 2 0 270.96 261.57 1.39 o 1 2 0 6111.62 5690.37 7.40 o 2 2 0 135.40 109.05 1.00 o 3 2 0 3002.36 2875.49 18.34 o 4 2 0 1001.69 944.18 4.97 o 5 2 0 789.33 805.05 3.03 o 6 2 0 200.28 180.04 1.51 o 7 2 0 13.82 12.43 0.44 o 8 2 0 136.60 147.38 1.85 o 9 2 0 110.54 106.94 1.42 o 10 2 0 336.06 325.45 2.61 o 11 2 0 85.62 74.87 1.41 o 12 2 0 39.09 39.70 0.86 o 13 2 0 57.64 55.98 0.92 o 14 2 0 0.23 0.76 0.15 o 1 3 0 298.74 270.98 1.23 o 2 3 0 115.55 133.73 1.78 o 3 3 0 1245.26 1238.47 4.31 o 4 3 0 4.43 6.47 0.34 o 5 3 0 0.00 0.92 0.26 o 6 3 0 38.26 41.28 0.91 o 7 3 0 706.59 699.90 4.00 o 8 3 0 131.89 124.84 1.79 o 9 3 0 20.20 26.05 0.61 o 10 3 0 3.90 3.02 0.32 o 11 3 0 1.21 1.33 0.21 o 12 3 0 201.85 208.69 1.90 o 13 3 0 60.77 51.75 0.84 o 14 3 0 64.14 59.91 0.84 o 0 4 0 269.49 264.09 2.01 o 1 4 0 220.19 207.47 1.55 o 2 4 0 62.62 56.12 0.73 o 3 4 0 209.61 212.80 1.62 o 4 4 0 54.08 51.69 0.88 o 5 4 0 78.52 84.99 3.22 o 6 4 0 6.67 7.41 0.42 o 7 4 0 146.78 138.42 1.90 o 8 4 0 0.90 0.33 0.12 o 9 4 0 11.99 14.00 0.52 o 10 4 0 18.27 15.94 0.50 o 11 4 0 325.39 318.48 2.39 o 12 4 0 219.60 211.40 1.56 o 13 4 0 41.63 46.58 0.83 o 14 4 0 0.00 0.18 0.10 o 1 5 0 678.43 699.46 4.99 o 2 5 0 369.85 365.94 2.40 o 3 5 0 465.81 492.58 2.59 o 4 5 0 643.16 636.26 3.11 o 5 5 0 96.36 99.57 1.73 o 6 5 0 5.53 4.86 0.34 o 7 5 0 16.31 16.71 0.48 o 8 5 0 43.68 42.24 0.89 o 9 5 0 19.21 21.76 0.58 o 10 5 0 63.16 60.28 0.96 o 11 5 0 87.37 82.02 1.09 o 12 5 0 10.54 5.40 0.31 o 13 5 0 79.72 78.07 1.19 o 0 6 0 243.43 256.10 2.70 o 1 6 0 279.38 298.70 2.41 o 2 6 0 156.67 153.88 1.76 o 3 6 0 1556.05 1560.17 5.73 o 4 6 0 93.87 89.68 1.23 o 5 6 0 0.72 0.39 0.15 o 6 6 0 45.33 43.46 0.89 o 7 6 0 224.33 216.59 2.93 o 8 6 0 0.59 1.01 0.23 o 9 6 0 17.57 17.19 0.65 o 10 6 0 29.07 23.57 0.63 o 11 6 0 2.19 2.93 0.21 o 12 6 0 108.96 119.51 2.11 o 1 7 0 367.34 367.51 2.28 o 2 7 0 0.15 0.55 0.13 o 3 7 0 280.61 272.36 2.35 o 4 7 0 180.30 175.61 2.27 o 5 7 0 179.41 182.97 3.80 o 6 7 0 0.25 0.77 0.26 o 7 7 0 163.29 160.80 1.96 o 8 7 0 41.10 40.83 0.82 o 9 7 0 17.99 17.96 0.52 o 10 7 0 0.31 0.22 0.16 o 11 7 0 0.51 0.51 0.18 o 0 8 0 99.68 90.35 1.87 o 1 8 0 285.83 288.25 2.36 o 2 8 0 203.85 210.33 2.02 o 3 8 0 173.03 171.08 2.10 o 4 8 0 30.90 26.96 1.03 o 5 8 0 350.97 356.02 7.56 o 6 8 0 76.65 73.48 2.37 o 7 8 0 106.79 117.77 2.85 o 8 8 0 88.79 96.61 2.37 o 9 8 0 3.65 5.44 0.54 o 10 8 0 7.68 5.53 0.39 o 1 9 0 77.22 77.37 1.17 o 2 9 0 0.01 0.91 0.42 o 3 9 0 102.93 111.52 1.57 o 4 9 0 201.15 208.94 2.09 o 5 9 0 53.93 54.07 1.02 o 6 9 0 28.80 27.61 0.90 o 7 9 0 20.77 24.23 1.10 o 8 9 0 3.54 2.95 0.37 o 0 10 0 10.04 8.77 0.68 o 1 10 0 0.02 0.22 0.13 o 2 10 0 145.36 146.70 1.83 o 3 10 0 47.31 45.51 1.45 o 4 10 0 64.44 62.14 1.64 o 5 10 0 42.52 45.29 1.34 o 6 10 0 31.90 29.78 0.97 o -15 1 1 92.50 87.70 1.06 o -14 1 1 0.00 0.39 0.17 o -13 1 1 39.11 39.99 0.80 o -12 1 1 217.07 217.81 1.76 o -11 1 1 238.24 242.32 1.91 o -10 1 1 0.09 0.17 0.18 o -9 1 1 74.85 72.97 0.94 o -8 1 1 259.42 282.52 2.57 o -7 1 1 81.78 72.75 1.02 o -6 1 1 455.22 419.90 2.22 o -5 1 1 11.67 12.90 0.35 o -4 1 1 161.51 148.33 1.05 o -3 1 1 1884.19 1815.43 4.44 o -2 1 1 1022.57 982.95 2.39 o -1 1 1 2.34 1.83 0.16 o 0 1 1 12.76 14.12 0.20 o 1 1 1 9.09 7.99 0.20 o 3 1 1 464.57 463.26 1.72 o 4 1 1 240.30 241.65 1.76 o 5 1 1 1724.75 1756.43 4.13 o 6 1 1 290.60 289.50 1.91 o 7 1 1 418.84 411.61 2.94 o 8 1 1 8.85 10.45 0.52 o 9 1 1 7.93 7.42 0.31 o 10 1 1 282.77 270.03 1.85 o 11 1 1 0.70 0.39 0.17 o 12 1 1 18.68 16.86 0.56 o 13 1 1 41.69 47.53 0.85 o 14 1 1 78.60 75.16 1.06 o 15 1 1 6.27 4.43 0.23 o -15 2 1 16.22 13.00 0.76 o -14 2 1 0.02 0.31 0.13 o -13 2 1 255.22 262.92 1.97 o -12 2 1 49.20 51.41 0.97 o -11 2 1 565.72 547.21 3.87 o -10 2 1 3.58 2.20 0.29 o -9 2 1 22.09 25.08 0.60 o -8 2 1 70.87 80.72 1.35 o -7 2 1 23.64 28.45 0.66 o -6 2 1 113.57 129.95 1.61 o -5 2 1 474.65 437.10 2.14 o -4 2 1 121.74 102.59 1.03 o -3 2 1 2499.93 2375.01 7.31 o -2 2 1 222.26 206.91 1.18 o -1 2 1 5874.17 5457.69 10.74 o 0 2 1 892.47 917.73 2.95 o 1 2 1 1682.94 1558.40 10.46 o 2 2 1 3377.89 3087.11 19.02 o 3 2 1 2810.07 2759.59 12.23 o 4 2 1 15.72 27.98 0.50 o 5 2 1 4649.77 4778.25 26.03 o 6 2 1 2.79 4.29 0.52 o 7 2 1 24.63 23.88 0.71 o 8 2 1 4.52 5.41 0.42 o 9 2 1 123.93 116.02 1.31 o 10 2 1 228.56 229.31 2.41 o 11 2 1 8.11 6.08 0.44 o 12 2 1 6.91 5.74 0.40 o 13 2 1 37.22 34.44 0.71 o 14 2 1 0.03 0.01 0.12 o -14 3 1 0.22 0.39 0.13 o -13 3 1 20.55 21.42 0.55 o -12 3 1 14.34 17.47 0.57 o -11 3 1 14.10 18.96 0.62 o -10 3 1 93.41 98.65 1.22 o -9 3 1 347.55 340.61 2.74 o -8 3 1 167.87 162.50 2.23 o -7 3 1 202.01 213.11 2.18 o -6 3 1 163.81 197.65 1.95 o -5 3 1 13.25 18.72 0.59 o -4 3 1 1092.76 1062.61 4.30 o -3 3 1 841.46 827.93 3.94 o -2 3 1 0.38 0.72 0.12 o -1 3 1 23.52 19.83 0.34 o 0 3 1 2715.02 2609.86 18.96 o 1 3 1 1422.69 1384.17 4.47 o 2 3 1 605.66 617.74 2.53 o 3 3 1 264.86 253.82 1.99 o 4 3 1 1541.57 1711.17 6.99 o 5 3 1 156.98 171.86 1.72 o 6 3 1 253.82 219.91 2.25 o 7 3 1 6.39 5.18 0.37 o 8 3 1 0.26 0.23 0.15 o 9 3 1 51.37 58.74 0.96 o 10 3 1 3.24 6.48 0.42 o 11 3 1 23.54 22.37 0.76 o 12 3 1 23.73 20.92 0.60 o 13 3 1 16.76 15.84 0.47 o 14 3 1 1.68 2.73 0.18 o -14 4 1 401.04 359.99 23.48 o -13 4 1 32.58 37.07 0.75 o -12 4 1 115.07 119.08 1.18 o -11 4 1 37.35 36.55 0.72 o -10 4 1 108.19 97.24 1.22 o -9 4 1 4.88 4.03 0.27 o -8 4 1 0.17 0.28 0.13 o -7 4 1 294.49 276.52 2.64 o -6 4 1 288.02 326.24 2.71 o -5 4 1 25.40 22.19 0.76 o -4 4 1 0.35 0.33 0.12 o -3 4 1 0.33 0.14 0.11 o -2 4 1 271.54 289.16 1.46 o -1 4 1 240.06 276.36 2.25 o 0 4 1 849.01 845.72 4.20 o 1 4 1 112.63 107.96 1.17 o 2 4 1 416.79 410.60 2.69 o 3 4 1 27.85 20.38 0.47 o 4 4 1 142.02 158.90 2.39 o 5 4 1 2.42 3.99 0.31 o 6 4 1 26.55 33.11 0.81 o 7 4 1 0.10 0.33 0.16 o 8 4 1 58.77 50.61 0.73 o 9 4 1 60.54 61.17 1.23 o 10 4 1 3.04 4.68 0.36 o 11 4 1 0.01 0.00 0.15 o 12 4 1 32.74 35.43 0.73 o 13 4 1 11.89 10.38 0.39 o 14 4 1 215.95 200.03 7.78 o -13 5 1 137.78 139.17 1.52 o -12 5 1 75.74 74.30 1.10 o -11 5 1 2.57 3.57 0.26 o -10 5 1 1.81 0.73 0.15 o -9 5 1 37.70 32.29 0.70 o -8 5 1 53.17 50.97 1.41 o -7 5 1 120.83 120.30 1.26 o -6 5 1 169.03 178.70 1.61 o -5 5 1 177.26 181.58 2.03 o -4 5 1 149.40 155.37 1.96 o -3 5 1 47.06 60.80 1.02 o -2 5 1 835.04 845.15 4.13 o -1 5 1 0.71 1.11 0.16 o 0 5 1 0.95 0.63 0.14 o 1 5 1 14.02 13.36 0.54 o 2 5 1 367.11 388.64 2.33 o 3 5 1 49.51 49.25 0.83 o 4 5 1 89.16 90.15 1.39 o 5 5 1 194.98 173.02 2.26 o 6 5 1 159.41 150.48 1.55 o 7 5 1 23.64 21.70 0.60 o 8 5 1 12.96 14.57 0.60 o 9 5 1 65.84 54.88 0.90 o 10 5 1 162.90 155.37 1.59 o 11 5 1 0.38 0.39 0.22 o 12 5 1 8.89 11.37 0.44 o 13 5 1 92.98 87.68 1.65 o -12 6 1 76.63 71.98 1.35 o -11 6 1 26.56 26.24 0.58 o -10 6 1 11.27 9.88 0.48 o -9 6 1 36.64 34.17 1.12 o -8 6 1 106.00 102.57 2.05 o -7 6 1 29.71 26.61 1.05 o -6 6 1 8.54 8.30 0.44 o -5 6 1 195.09 190.32 1.80 o -4 6 1 34.26 37.10 0.71 o -3 6 1 64.98 66.51 1.19 o -2 6 1 193.85 192.14 1.98 o -1 6 1 260.50 303.07 2.09 o 0 6 1 312.93 303.81 2.56 o 1 6 1 15.73 12.44 0.50 o 2 6 1 42.75 39.84 0.89 o 3 6 1 840.61 887.32 4.65 o 4 6 1 799.79 775.14 4.15 o 5 6 1 37.31 35.80 0.72 o 6 6 1 81.50 90.59 1.20 o 7 6 1 0.88 0.10 0.21 o 8 6 1 206.93 200.31 3.31 o 9 6 1 52.58 51.67 1.36 o 10 6 1 31.63 33.83 0.80 o 11 6 1 0.44 0.16 0.25 o 12 6 1 3.81 2.90 0.19 o -11 7 1 0.36 0.50 0.12 o -10 7 1 1.23 1.93 0.19 o -9 7 1 48.32 48.19 0.97 o -8 7 1 1.86 2.06 0.26 o -7 7 1 639.31 643.84 4.90 o -6 7 1 18.51 17.87 0.82 o -5 7 1 354.84 360.90 5.30 o -4 7 1 363.94 370.80 3.71 o -3 7 1 28.06 27.85 0.75 o -2 7 1 249.63 257.47 1.72 o -1 7 1 342.83 357.62 2.23 o 0 7 1 5.97 8.39 0.32 o 1 7 1 344.45 339.71 1.99 o 2 7 1 76.49 73.91 1.03 o 3 7 1 151.11 157.67 1.71 o 4 7 1 31.36 33.52 1.15 o 5 7 1 483.66 495.80 5.56 o 6 7 1 50.48 52.70 3.09 o 7 7 1 876.25 840.51 4.85 o 8 7 1 5.26 4.21 0.28 o 9 7 1 91.31 96.92 1.35 o 10 7 1 19.16 22.02 0.57 o 11 7 1 102.18 95.27 1.71 o -10 8 1 58.25 55.24 1.26 o -9 8 1 0.05 0.11 0.26 o -8 8 1 2.74 2.44 0.24 o -7 8 1 26.27 23.95 1.32 o -6 8 1 21.46 19.25 0.83 o -5 8 1 101.55 93.77 1.85 o -4 8 1 75.84 81.44 1.73 o -3 8 1 0.04 0.09 0.15 o -2 8 1 14.34 16.95 0.58 o -1 8 1 89.05 86.45 1.61 o 0 8 1 37.83 36.40 0.84 o 1 8 1 196.22 197.60 1.94 o 2 8 1 484.06 514.25 3.13 o 3 8 1 438.10 451.34 3.40 o 4 8 1 74.85 78.65 1.44 o 5 8 1 0.20 0.34 0.21 o 6 8 1 8.60 7.26 0.52 o 7 8 1 14.55 13.99 0.66 o 8 8 1 7.86 10.23 0.52 o 9 8 1 26.20 19.50 0.60 o -8 9 1 0.24 1.31 0.28 o -7 9 1 2.52 3.91 0.50 o -6 9 1 75.98 81.20 1.47 o -5 9 1 8.87 7.95 0.41 o -4 9 1 13.54 14.33 0.55 o -3 9 1 5.10 4.90 0.38 o -2 9 1 34.31 34.02 0.68 o -1 9 1 20.83 22.22 0.56 o 0 9 1 4.28 4.36 0.29 o 1 9 1 423.31 423.35 2.69 o 2 9 1 8.22 7.93 0.39 o 3 9 1 79.17 80.17 1.16 o 4 9 1 159.16 168.14 2.34 o 5 9 1 46.32 49.02 1.54 o 6 9 1 77.54 70.70 1.38 o 7 9 1 7.21 8.82 0.67 o 8 9 1 70.45 77.83 1.58 o -6 10 1 1.24 2.41 0.31 o -5 10 1 0.21 0.28 0.22 o -4 10 1 20.97 20.70 0.66 o -3 10 1 21.92 26.05 1.08 o -2 10 1 76.78 76.11 1.92 o -1 10 1 28.31 28.56 1.21 o 0 10 1 27.56 28.89 0.70 o 1 10 1 0.22 0.69 0.21 o 2 10 1 0.00 0.22 0.23 o 3 10 1 3.25 1.95 0.37 o 4 10 1 4.00 3.36 0.42 o 5 10 1 23.52 23.75 0.97 o 6 10 1 12.14 11.85 0.60 o -15 0 2 4.89 8.07 0.46 o -14 0 2 29.62 33.99 0.89 o -13 0 2 2.82 4.27 0.42 o -12 0 2 123.31 121.59 2.14 o -11 0 2 364.12 373.57 3.80 o -10 0 2 10.05 8.31 0.51 o -9 0 2 118.30 122.55 1.75 o -8 0 2 83.34 100.16 2.11 o -7 0 2 393.31 377.83 3.78 o -6 0 2 81.10 86.71 1.64 o -5 0 2 30.12 34.33 0.93 o -4 0 2 1878.57 1854.04 4.39 o -3 0 2 0.68 2.02 0.46 o -1 0 2 7912.22 7071.29 8.75 o 0 0 2 783.86 687.93 2.88 o 1 0 2 1354.40 1326.21 7.58 o 2 0 2 288.76 235.67 2.41 o 3 0 2 950.99 918.91 4.05 o 4 0 2 2318.21 2094.18 13.58 o 5 0 2 150.77 159.65 2.19 o 6 0 2 3200.26 3114.10 10.67 o 7 0 2 2636.13 2732.40 10.95 o 8 0 2 466.34 448.37 4.82 o 9 0 2 0.68 0.64 0.15 o 10 0 2 826.43 824.48 6.42 o 11 0 2 14.83 11.20 0.74 o 12 0 2 2153.91 2142.56 8.71 o 13 0 2 63.11 69.12 1.43 o 14 0 2 0.05 0.31 0.15 o -15 1 2 32.69 29.54 0.73 o -14 1 2 5.69 5.20 0.26 o -13 1 2 3.96 5.65 0.32 o -12 1 2 29.32 29.17 0.65 o -11 1 2 866.62 872.84 4.44 o -10 1 2 12.30 13.28 0.40 o -9 1 2 3.73 3.54 0.23 o -8 1 2 436.57 436.26 3.14 o -7 1 2 3.57 2.86 0.25 o -6 1 2 499.60 523.19 3.07 o -5 1 2 460.46 411.36 1.96 o -4 1 2 2606.99 2492.96 6.83 o -3 1 2 2821.84 2610.34 6.11 o -2 1 2 3060.22 2865.53 6.14 o -1 1 2 1252.92 1198.82 7.45 o 0 1 2 2133.50 1967.09 11.65 o 2 1 2 7957.52 7492.66 9.14 o 3 1 2 166.32 148.54 0.92 o 4 1 2 208.88 210.06 1.28 o 5 1 2 58.47 72.92 0.86 o 6 1 2 34.11 34.99 2.71 o 7 1 2 203.53 247.56 2.33 o 8 1 2 58.20 46.83 1.34 o 9 1 2 16.48 17.98 0.42 o 10 1 2 28.38 26.35 0.59 o 11 1 2 7.76 5.64 0.35 o 12 1 2 17.99 15.63 0.53 o 13 1 2 0.13 0.50 0.13 o 14 1 2 6.02 4.63 0.27 o -14 2 2 0.01 0.11 0.17 o -13 2 2 1.22 0.91 0.20 o -12 2 2 26.96 31.27 0.66 o -11 2 2 196.30 194.93 1.60 o -10 2 2 690.32 670.53 2.82 o -9 2 2 74.43 69.50 1.02 o -8 2 2 198.81 213.55 2.14 o -7 2 2 25.78 17.70 0.52 o -6 2 2 256.18 284.95 1.91 o -5 2 2 753.76 745.75 2.81 o -4 2 2 168.86 169.85 1.52 o -3 2 2 1994.90 1946.33 9.35 o -2 2 2 22.12 26.25 0.50 o -1 2 2 4523.03 4246.73 11.32 o 0 2 2 68.52 95.57 0.72 o 1 2 2 9567.74 8802.84 27.65 o 2 2 2 2260.65 2124.14 17.53 o 3 2 2 796.30 803.68 3.78 o 4 2 2 774.25 753.89 4.59 o 5 2 2 20.91 20.41 0.75 o 6 2 2 3375.03 3534.39 8.88 o 7 2 2 36.49 35.83 1.09 o 8 2 2 23.96 26.60 1.06 o 9 2 2 8.93 9.37 0.39 o 10 2 2 0.90 0.28 0.17 o 11 2 2 26.22 21.39 0.75 o 12 2 2 8.21 7.38 0.44 o 13 2 2 14.32 13.54 0.44 o 14 2 2 0.97 0.62 0.24 o -14 3 2 38.56 42.31 0.70 o -13 3 2 26.87 30.64 0.64 o -12 3 2 109.75 115.97 1.23 o -11 3 2 15.59 14.25 0.48 o -10 3 2 18.18 16.76 0.52 o -9 3 2 1136.03 1132.33 4.23 o -8 3 2 321.78 326.85 2.31 o -7 3 2 155.49 161.26 2.35 o -6 3 2 256.97 234.02 1.89 o -5 3 2 144.92 151.05 1.50 o -4 3 2 544.85 559.47 3.03 o -3 3 2 12.67 14.10 0.46 o -2 3 2 408.26 398.81 1.94 o -1 3 2 1169.14 1160.73 3.09 o 0 3 2 1983.41 1919.61 5.61 o 1 3 2 326.80 285.72 1.67 o 2 3 2 7.19 7.05 0.28 o 3 3 2 23.68 24.72 0.67 o 4 3 2 285.06 277.55 3.41 o 5 3 2 167.34 186.31 2.01 o 6 3 2 17.68 19.84 0.65 o 7 3 2 139.42 152.78 2.19 o 8 3 2 30.52 32.43 0.66 o 9 3 2 22.76 20.97 0.56 o 10 3 2 48.33 48.66 1.11 o 11 3 2 37.77 39.93 1.00 o 12 3 2 12.08 9.68 0.47 o 13 3 2 3.31 1.82 0.18 o 14 3 2 2.84 3.03 0.23 o -14 4 2 28.20 20.66 0.71 o -13 4 2 4.10 4.49 0.23 o -12 4 2 133.10 129.70 1.23 o -11 4 2 639.60 637.00 3.10 o -10 4 2 186.95 175.31 1.64 o -9 4 2 23.24 21.14 0.58 o -8 4 2 14.92 14.27 0.42 o -7 4 2 442.77 454.71 3.32 o -6 4 2 69.30 73.27 1.43 o -5 4 2 98.74 109.69 2.12 o -4 4 2 31.64 33.39 0.75 o -3 4 2 1282.42 1295.54 10.06 o -2 4 2 13.88 7.32 0.27 o -1 4 2 72.14 62.69 0.69 o 0 4 2 2830.18 3008.04 13.22 o 1 4 2 1351.03 1355.86 5.04 o 2 4 2 807.14 800.13 4.36 o 3 4 2 264.27 286.06 1.77 o 4 4 2 3.34 1.24 0.18 o 5 4 2 59.96 59.18 1.09 o 6 4 2 253.42 261.54 2.65 o 7 4 2 81.06 69.54 1.09 o 8 4 2 7.90 6.47 0.32 o 9 4 2 9.08 4.57 0.43 o 10 4 2 10.84 7.36 0.44 o 11 4 2 48.85 48.33 1.04 o 12 4 2 7.13 8.69 0.37 o 13 4 2 0.02 -0.04 0.12 o -13 5 2 51.38 44.08 1.39 o -12 5 2 116.89 121.97 1.42 o -11 5 2 19.53 19.26 0.65 o -10 5 2 51.42 57.52 0.91 o -9 5 2 4.64 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