#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/65/2236514.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236514_Fobs loop_ _publ_author_name 'Jin, Shouwen' 'Huang, Yanfei' 'Fang, Hao' 'Wang, Tianyi' 'Ding, Liangliang' _publ_section_title ; 3,5,3',5'-Tetramethyl-4,4'-bi(1H-pyrazolyl) hemihydrate ; _journal_coeditor_code NG5290 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2896 _journal_volume 68 _journal_year 2012 _space_group_IT_number 142 _symmetry_space_group_name_Hall '-I 4bd 2c' _symmetry_space_group_name_H-M 'I 41/a c d :2' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 24.9060 _cell_length_b 24.9060 _cell_length_c 14.9684 _exptl_crystal_F_000 3424.00 _reflns_d_resolution_high 0.8404 _[local]_cod_data_source_file ng5290Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 120217b in I4(1)/acd' _shelx_refln_list_code 4 _shelx_f_calc_maximum 592.79 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-y+1/4, x+3/4, z+1/4' 'y+1/4, -x+1/4, z+3/4' '-x+1/2, y, -z' 'x, -y, -z+1/2' 'y+1/4, x+3/4, -z+3/4' '-y+1/4, -x+1/4, -z+1/4' 'x+1/2, y+1/2, z+1/2' '-x+1, -y+1/2, z+1' '-y+3/4, x+5/4, z+3/4' 'y+3/4, -x+3/4, z+5/4' '-x+1, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1' 'y+3/4, x+5/4, -z+5/4' '-y+3/4, -x+3/4, -z+3/4' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'y-1/4, -x-3/4, -z-1/4' '-y-1/4, x-1/4, -z-3/4' 'x-1/2, -y, z' '-x, y, z-1/2' '-y-1/4, -x-3/4, z-3/4' 'y-1/4, x-1/4, z-1/4' '-x+1/2, -y+1/2, -z+1/2' 'x, y+1/2, -z' 'y+1/4, -x-1/4, -z+1/4' '-y+1/4, x+1/4, -z-1/4' 'x, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' '-y+1/4, -x-1/4, z-1/4' 'y+1/4, x+1/4, z+1/4' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 0 4 0 11718.51 11578.75 103.98 o 2 4 0 2145.17 2328.55 51.90 o 4 4 0 351397.19 354774.06 1257.59 o 0 6 0 11029.38 11888.75 128.90 o 2 6 0 1583.75 2442.68 64.44 o 4 6 0 1378.36 1357.98 36.24 o 6 6 0 199137.70 206907.98 1746.58 o 0 8 0 9367.15 7820.90 139.38 o 2 8 0 91369.64 85797.89 370.98 o 4 8 0 12786.91 13301.98 154.90 o 6 8 0 15955.62 16111.92 154.21 o 8 8 0 21043.27 19045.30 315.28 o 0 10 0 1525.21 1411.48 150.74 o 2 10 0 2929.24 2604.15 79.22 o 4 10 0 743.93 650.06 43.47 o 6 10 0 9483.65 8675.79 222.79 o 8 10 0 11345.03 14403.32 168.71 o 10 10 0 19909.33 23759.58 396.15 o 0 12 0 268.97 144.67 40.77 o 2 12 0 1285.55 895.01 50.59 o 4 12 0 4.47 27.43 26.41 o 6 12 0 2487.29 3061.92 95.36 o 8 12 0 17541.64 18469.40 251.77 o 10 12 0 12906.87 10725.76 201.44 o 12 12 0 646.61 706.84 86.88 o 0 14 0 596.82 811.40 68.33 o 2 14 0 1518.69 2105.27 77.70 o 4 14 0 8315.99 8261.00 140.89 o 6 14 0 0.21 -37.38 34.76 o 8 14 0 17000.31 16146.36 282.53 o 10 14 0 20137.58 20483.55 292.74 o 12 14 0 40.29 -11.84 52.64 o 14 14 0 1371.54 1537.82 142.12 o 0 16 0 3752.70 3167.48 167.39 o 2 16 0 3142.43 3398.15 117.49 o 4 16 0 91.88 27.27 31.95 o 6 16 0 1.89 29.99 36.30 o 8 16 0 1204.13 939.86 88.42 o 10 16 0 399.25 479.81 74.65 o 12 16 0 611.90 662.95 81.84 o 14 16 0 9235.94 9230.46 222.54 o 16 16 0 10.47 8.94 106.22 o 0 18 0 135.55 77.44 66.13 o 2 18 0 217.28 279.58 51.00 o 4 18 0 10891.13 11720.45 176.19 o 6 18 0 266.54 176.70 58.38 o 8 18 0 2813.00 3092.48 128.50 o 10 18 0 106.97 98.34 58.53 o 12 18 0 360.49 375.94 78.30 o 14 18 0 6394.63 6060.07 264.06 o 16 18 0 0.66 100.09 92.91 o 18 18 0 1142.06 830.27 305.81 o 0 20 0 12090.09 12085.82 467.88 o 2 20 0 5.76 78.19 50.84 o 4 20 0 5363.99 5525.79 162.69 o 6 20 0 1099.71 851.27 118.10 o 8 20 0 3272.15 2610.42 150.68 o 10 20 0 1363.71 1305.21 136.13 o 12 20 0 444.60 37.98 102.11 o 14 20 0 419.35 486.83 136.29 o 16 20 0 402.38 281.10 109.44 o 18 20 0 914.60 755.23 128.87 o 20 20 0 131.45 243.02 230.70 o 0 22 0 5283.43 5531.90 346.46 o 2 22 0 9840.22 9051.67 243.07 o 4 22 0 3941.81 3547.02 169.50 o 6 22 0 905.39 811.51 96.24 o 8 22 0 8.59 82.83 82.51 o 10 22 0 2507.85 2115.30 171.02 o 12 22 0 45.97 130.63 92.97 o 14 22 0 10.99 92.54 109.52 o 16 22 0 152.26 188.55 101.70 o 18 22 0 64.07 32.91 119.25 o 0 24 0 3.58 72.64 277.19 o 2 24 0 421.65 434.10 86.64 o 4 24 0 1956.75 1891.27 140.59 o 6 24 0 223.88 350.47 100.67 o 8 24 0 593.37 747.10 160.16 o 10 24 0 1538.12 1362.35 161.78 o 12 24 0 470.73 659.51 124.98 o 14 24 0 72.25 179.63 133.19 o 16 24 0 76.10 215.22 103.53 o 0 26 0 905.29 664.37 149.28 o 2 26 0 2364.56 2425.34 172.16 o 4 26 0 5.58 -40.47 98.84 o 6 26 0 4.75 133.33 130.61 o 8 26 0 10.65 -102.57 108.64 o 10 26 0 736.07 804.92 167.80 o 12 26 0 123.29 171.65 128.53 o 14 26 0 77.25 112.38 115.92 o 0 28 0 174.08 383.24 138.49 o 2 28 0 296.82 372.34 104.27 o 4 28 0 110.89 -14.03 104.79 o 6 28 0 77.78 131.89 116.14 o 8 28 0 77.20 243.03 111.84 o 2 3 1 96203.84 94249.12 403.41 o 1 4 1 27021.30 26490.05 118.22 o 3 4 1 52876.16 49910.45 148.87 o 2 5 1 2909.04 3286.67 39.45 o 4 5 1 101437.95 99843.05 318.14 o 1 6 1 14901.60 14919.02 88.24 o 3 6 1 77541.70 73893.19 345.92 o 5 6 1 71603.13 70779.13 235.35 o 2 7 1 47833.57 45079.39 206.77 o 4 7 1 972.90 773.19 28.24 o 6 7 1 8771.43 9744.26 76.57 o 1 8 1 4532.60 3921.31 46.26 o 3 8 1 4009.14 4086.16 54.88 o 5 8 1 24278.30 22895.86 140.41 o 7 8 1 7018.85 8587.79 76.01 o 2 9 1 9489.72 9485.68 81.32 o 4 9 1 6400.64 7727.26 80.90 o 6 9 1 916.68 731.62 33.59 o 8 9 1 7.79 17.28 18.73 o 1 10 1 2939.02 3160.68 44.32 o 3 10 1 32.29 23.93 14.41 o 5 10 1 10458.41 9773.48 98.98 o 7 10 1 4899.16 5916.41 72.65 o 9 10 1 16552.66 18425.55 152.88 o 2 11 1 300.52 374.11 20.66 o 4 11 1 1135.50 1241.81 34.73 o 6 11 1 1551.81 1931.37 52.66 o 8 11 1 10.55 41.81 34.80 o 10 11 1 108.38 80.17 26.04 o 1 12 1 10651.55 10817.27 94.65 o 3 12 1 14876.90 15555.43 129.61 o 5 12 1 1528.00 1438.53 46.89 o 7 12 1 17991.09 20478.56 214.94 o 9 12 1 12587.74 11790.71 113.14 o 11 12 1 10.52 -1.44 27.91 o 2 13 1 7224.94 7906.58 97.48 o 4 13 1 317.54 470.94 31.71 o 6 13 1 1004.55 1524.45 49.16 o 8 13 1 19669.38 19457.80 184.15 o 10 13 1 3309.43 3682.57 75.77 o 12 13 1 1060.16 1138.15 55.13 o 1 14 1 219.45 228.77 28.31 o 3 14 1 133.42 87.28 21.03 o 5 14 1 1037.84 926.48 40.52 o 7 14 1 90.83 128.87 25.58 o 9 14 1 1622.99 1611.62 53.27 o 11 14 1 8530.33 7908.77 131.04 o 13 14 1 453.42 698.33 49.98 o 2 15 1 453.14 424.74 29.99 o 4 15 1 18.67 25.13 27.42 o 6 15 1 2337.93 2933.77 69.50 o 8 15 1 47.70 27.66 27.85 o 10 15 1 338.76 381.72 41.12 o 12 15 1 25.73 13.32 34.95 o 14 15 1 409.05 396.15 51.46 o 1 16 1 8349.40 7574.81 120.84 o 3 16 1 317.96 410.78 40.49 o 5 16 1 203.69 177.15 27.68 o 7 16 1 5927.39 6491.21 103.82 o 9 16 1 52.24 51.28 33.59 o 11 16 1 1.12 85.93 36.35 o 13 16 1 6020.70 5686.31 133.04 o 15 16 1 10041.71 9211.10 186.82 o 2 17 1 4323.21 4759.85 93.96 o 4 17 1 1202.01 1065.86 45.12 o 6 17 1 42.66 39.35 31.46 o 8 17 1 1065.41 935.81 56.34 o 10 17 1 672.91 753.01 52.88 o 12 17 1 377.53 309.86 66.23 o 14 17 1 88.14 -17.83 49.22 o 16 17 1 105.54 208.91 70.63 o 1 18 1 4984.61 5171.62 107.31 o 3 18 1 0.13 30.01 27.29 o 5 18 1 1387.31 1472.24 52.92 o 7 18 1 1405.05 1466.48 60.38 o 9 18 1 975.90 906.60 67.92 o 11 18 1 806.35 903.46 64.39 o 13 18 1 143.72 157.72 49.08 o 15 18 1 377.47 325.98 66.87 o 17 18 1 142.68 268.88 67.27 o 2 19 1 258.82 268.30 38.38 o 4 19 1 181.24 205.39 32.45 o 6 19 1 1535.81 1624.61 66.34 o 8 19 1 644.56 501.14 50.46 o 10 19 1 406.98 446.08 54.37 o 12 19 1 1522.79 1381.46 80.97 o 14 19 1 881.20 1061.00 84.04 o 16 19 1 236.76 365.72 74.82 o 18 19 1 160.69 268.13 74.91 o 1 20 1 34.95 43.31 43.75 o 3 20 1 189.93 133.75 40.45 o 5 20 1 52.73 45.67 38.05 o 7 20 1 63.80 43.04 43.95 o 9 20 1 214.23 86.84 51.47 o 11 20 1 2291.62 2230.92 94.01 o 13 20 1 23.05 77.94 57.79 o 15 20 1 765.89 707.22 88.62 o 17 20 1 310.34 328.27 79.58 o 19 20 1 1549.85 1663.02 122.24 o 2 21 1 466.68 474.56 53.26 o 4 21 1 127.08 117.78 42.72 o 6 21 1 202.26 206.40 46.56 o 8 21 1 199.17 271.80 53.88 o 10 21 1 52.37 73.89 52.68 o 12 21 1 887.67 1078.76 103.36 o 14 21 1 0.85 67.12 69.83 o 16 21 1 66.72 56.36 71.27 o 18 21 1 316.22 448.84 84.03 o 20 21 1 112.51 284.79 114.32 o 1 22 1 908.43 963.60 75.47 o 3 22 1 669.92 538.06 57.65 o 5 22 1 1099.83 953.39 77.09 o 7 22 1 27.58 7.21 48.71 o 9 22 1 20.31 49.62 54.73 o 11 22 1 309.51 310.19 67.21 o 13 22 1 350.68 305.19 96.04 o 15 22 1 84.10 -96.39 76.00 o 17 22 1 18.17 64.48 71.90 o 19 22 1 10.56 119.41 80.38 o 2 23 1 1000.15 1010.93 72.55 o 4 23 1 309.55 292.36 59.04 o 6 23 1 446.63 303.59 57.91 o 8 23 1 38.80 168.33 63.36 o 10 23 1 647.03 626.73 74.39 o 12 23 1 59.27 13.86 66.27 o 14 23 1 171.96 117.80 69.40 o 16 23 1 10.27 -11.23 78.62 o 18 23 1 18.90 37.49 78.77 o 1 24 1 462.08 440.19 94.53 o 3 24 1 1738.53 1754.15 94.62 o 5 24 1 218.87 226.51 60.35 o 7 24 1 708.18 869.33 92.27 o 9 24 1 142.45 275.85 75.28 o 11 24 1 360.30 431.71 79.24 o 13 24 1 398.48 465.13 94.63 o 15 24 1 360.95 271.94 85.30 o 17 24 1 72.12 60.28 72.01 o 2 25 1 1323.79 1268.58 86.38 o 4 25 1 1143.84 1122.14 90.69 o 6 25 1 640.41 416.28 73.74 o 8 25 1 666.12 775.83 89.40 o 10 25 1 378.11 308.30 78.31 o 12 25 1 52.71 119.06 74.21 o 14 25 1 157.70 99.85 88.44 o 1 26 1 80.21 157.94 61.13 o 3 26 1 0.05 52.12 56.41 o 5 26 1 1.72 29.01 68.87 o 7 26 1 426.97 295.84 77.52 o 9 26 1 218.07 329.33 82.01 o 11 26 1 8.21 158.91 89.58 o 13 26 1 98.55 278.14 83.79 o 2 27 1 897.15 782.11 87.11 o 4 27 1 227.86 277.43 71.99 o 6 27 1 297.74 329.24 81.13 o 8 27 1 238.86 334.45 85.33 o 10 27 1 3.95 -36.49 76.59 o 12 27 1 40.16 6.23 82.65 o 1 28 1 237.52 416.98 70.54 o 3 28 1 18.44 114.26 78.55 o 5 28 1 139.79 220.23 78.52 o 7 28 1 193.91 73.71 78.95 o 9 28 1 0.01 26.50 77.66 o 2 29 1 195.41 284.23 72.17 o 4 29 1 0.76 40.20 78.29 o 1 1 2 25687.03 25912.43 130.75 o 0 2 2 190820.92 188263.30 491.82 o 1 3 2 16614.54 16733.43 74.26 o 3 3 2 85737.12 82234.57 341.50 o 0 4 2 3269.57 3144.69 61.06 o 2 4 2 86006.91 88206.48 282.99 o 1 5 2 27629.30 27291.96 121.35 o 3 5 2 7875.99 8620.78 74.75 o 5 5 2 435.63 349.41 31.64 o 0 6 2 57792.36 54653.51 324.44 o 2 6 2 297.80 285.44 16.63 o 4 6 2 1072.39 895.15 32.61 o 1 7 2 775.31 660.74 26.92 o 3 7 2 12046.49 11692.23 78.27 o 5 7 2 167.33 174.65 17.23 o 7 7 2 2798.31 2880.60 64.93 o 0 8 2 69942.31 68473.73 621.41 o 2 8 2 21.52 18.84 17.35 o 4 8 2 13942.28 13296.45 87.47 o 6 8 2 14812.58 13278.23 106.10 o 1 9 2 11052.71 10763.43 109.23 o 3 9 2 288.90 232.92 18.23 o 5 9 2 10368.53 11561.02 108.39 o 7 9 2 20313.57 18353.88 124.86 o 9 9 2 26742.90 28361.95 250.05 o 0 10 2 1164.77 1235.49 57.19 o 2 10 2 34353.07 35353.68 183.71 o 4 10 2 11.92 72.50 16.24 o 6 10 2 33681.27 34764.90 176.04 o 8 10 2 8755.53 7122.83 78.96 o 1 11 2 346.22 339.41 21.70 o 3 11 2 229.78 264.29 19.18 o 5 11 2 1145.20 774.23 25.07 o 7 11 2 1.39 30.03 18.48 o 9 11 2 1710.51 1742.30 48.88 o 11 11 2 10307.74 12452.13 194.16 o 0 12 2 11669.37 9793.81 120.12 o 2 12 2 561.43 483.79 25.95 o 4 12 2 5704.13 6131.59 83.89 o 6 12 2 578.82 637.80 31.88 o 8 12 2 819.89 1066.29 44.09 o 10 12 2 252.32 318.52 29.33 o 1 13 2 2.14 19.36 24.50 o 3 13 2 1610.32 1486.26 37.20 o 5 13 2 7427.13 6694.15 77.27 o 7 13 2 2338.87 2596.18 65.20 o 9 13 2 680.92 694.86 39.08 o 11 13 2 4299.48 4311.07 85.98 o 13 13 2 762.55 660.85 64.80 o 0 14 2 3887.08 3688.20 86.02 o 2 14 2 582.44 607.86 25.61 o 4 14 2 3727.32 3704.62 56.10 o 6 14 2 2106.40 1962.89 51.07 o 8 14 2 187.11 214.17 27.81 o 10 14 2 1999.77 2048.48 61.63 o 12 14 2 3576.38 3590.04 90.98 o 1 15 2 4725.21 4732.11 77.49 o 3 15 2 159.58 325.17 24.17 o 5 15 2 197.21 270.25 27.30 o 7 15 2 2522.60 2332.84 66.33 o 9 15 2 2043.21 2203.26 69.43 o 11 15 2 108.91 160.57 35.84 o 13 15 2 689.95 647.16 61.55 o 15 15 2 1189.30 1001.05 102.94 o 0 16 2 1047.96 850.10 76.51 o 2 16 2 39.73 85.83 24.38 o 4 16 2 852.35 951.99 40.54 o 6 16 2 336.96 332.02 28.09 o 8 16 2 105.32 120.49 28.06 o 10 16 2 227.68 280.89 37.78 o 12 16 2 3565.77 3014.65 107.37 o 14 16 2 4294.81 4048.40 127.47 o 1 17 2 1316.07 1480.53 59.15 o 3 17 2 593.91 513.69 35.25 o 5 17 2 1761.35 2184.40 58.82 o 7 17 2 1347.26 1468.01 63.21 o 9 17 2 82.15 30.53 42.30 o 11 17 2 5423.94 4972.01 136.11 o 13 17 2 2357.98 2395.22 100.44 o 15 17 2 6.44 22.75 49.35 o 17 17 2 14.44 -71.52 72.87 o 0 18 2 2958.39 2596.55 134.16 o 2 18 2 3101.79 2898.06 77.12 o 4 18 2 60.51 171.71 34.41 o 6 18 2 321.12 242.06 34.79 o 8 18 2 201.72 247.83 44.29 o 10 18 2 9596.37 9085.82 171.35 o 12 18 2 1045.00 1048.30 71.48 o 14 18 2 1136.90 1195.51 80.90 o 16 18 2 308.23 364.76 65.66 o 1 19 2 28.27 16.56 41.30 o 3 19 2 154.56 96.84 36.26 o 5 19 2 555.71 611.31 49.10 o 7 19 2 2119.61 2049.58 80.93 o 9 19 2 406.87 381.55 51.63 o 11 19 2 1614.11 1697.17 84.40 o 13 19 2 101.16 133.75 58.56 o 15 19 2 33.30 94.37 61.70 o 17 19 2 426.77 410.21 74.12 o 19 19 2 15.73 165.56 104.66 o 0 20 2 3636.23 3785.15 169.81 o 2 20 2 295.43 165.59 37.87 o 4 20 2 1422.91 1327.75 64.71 o 6 20 2 1882.59 1842.37 77.33 o 8 20 2 1786.96 1489.73 78.87 o 10 20 2 2844.26 2731.72 105.77 o 12 20 2 533.09 579.43 59.61 o 14 20 2 819.15 806.23 77.32 o 16 20 2 192.72 154.56 68.72 o 18 20 2 85.25 96.67 66.48 o 1 21 2 36.14 46.15 48.13 o 3 21 2 4083.98 3983.53 112.20 o 5 21 2 440.52 293.72 50.06 o 7 21 2 4040.49 3494.17 113.42 o 9 21 2 1986.60 1865.96 88.20 o 11 21 2 8.27 50.34 47.24 o 13 21 2 442.13 323.98 64.05 o 15 21 2 411.51 338.70 75.00 o 17 21 2 178.94 372.12 89.36 o 19 21 2 645.67 630.52 97.92 o 0 22 2 1523.40 1281.43 105.07 o 2 22 2 516.17 437.46 49.60 o 4 22 2 1118.87 1023.36 71.86 o 6 22 2 591.72 498.41 60.81 o 8 22 2 508.46 496.51 60.40 o 10 22 2 3203.93 3116.36 115.88 o 12 22 2 27.82 -64.60 60.10 o 14 22 2 85.89 106.66 73.57 o 16 22 2 2248.85 2492.27 143.92 o 18 22 2 101.11 155.57 81.72 o 1 23 2 130.73 106.95 43.86 o 3 23 2 374.81 236.62 52.36 o 5 23 2 0.32 -22.03 56.67 o 7 23 2 5.28 20.71 55.42 o 9 23 2 4.03 96.05 53.57 o 11 23 2 211.18 303.73 73.68 o 13 23 2 216.59 74.16 72.49 o 15 23 2 126.36 118.37 71.71 o 17 23 2 316.88 425.92 93.38 o 0 24 2 176.28 320.70 81.56 o 2 24 2 69.56 195.79 58.54 o 4 24 2 5.13 75.10 56.80 o 6 24 2 4046.16 4190.88 155.06 o 8 24 2 0.21 14.09 58.30 o 10 24 2 325.49 321.96 89.36 o 12 24 2 0.01 49.87 68.70 o 14 24 2 1549.52 1756.55 126.17 o 16 24 2 0.60 82.12 79.06 o 1 25 2 25.39 -1.41 48.06 o 3 25 2 1224.27 1226.63 83.90 o 5 25 2 12.42 66.59 83.16 o 7 25 2 48.81 213.38 66.15 o 9 25 2 41.08 232.90 79.91 o 11 25 2 1053.86 843.13 97.65 o 13 25 2 62.02 141.39 101.72 o 15 25 2 4.88 -105.29 80.30 o 0 26 2 2188.23 2107.18 152.27 o 2 26 2 6.28 67.97 57.91 o 4 26 2 112.53 106.33 62.20 o 6 26 2 0.00 48.61 68.79 o 8 26 2 1805.14 1974.22 128.69 o 10 26 2 4.39 70.45 75.81 o 12 26 2 57.34 40.37 72.55 o 1 27 2 140.07 146.67 65.63 o 3 27 2 49.85 -24.69 66.70 o 5 27 2 60.75 122.14 75.20 o 7 27 2 8.55 78.23 74.70 o 9 27 2 135.20 68.74 79.89 o 11 27 2 30.28 138.72 86.35 o 0 28 2 378.20 464.88 112.86 o 2 28 2 151.76 176.38 66.27 o 4 28 2 518.10 607.67 96.39 o 6 28 2 448.39 542.82 90.44 o 8 28 2 25.27 61.28 76.75 o 1 29 2 55.46 113.71 64.43 o 3 29 2 23.12 116.05 76.75 o 5 29 2 205.34 122.81 77.54 o 1 2 3 14646.91 14298.23 51.24 o 2 3 3 15187.64 16087.64 60.56 o 1 4 3 18415.71 17153.77 78.16 o 3 4 3 19306.43 18627.28 85.79 o 2 5 3 26074.08 25543.69 113.99 o 4 5 3 4767.11 5331.76 56.16 o 1 6 3 465.30 545.38 22.15 o 3 6 3 10208.79 9464.77 65.81 o 5 6 3 7146.73 8063.83 72.69 o 2 7 3 26028.01 26434.23 138.63 o 4 7 3 17.54 32.41 15.94 o 6 7 3 1910.97 2131.90 39.04 o 1 8 3 26637.15 27716.34 162.33 o 3 8 3 10305.75 10215.05 93.77 o 5 8 3 5586.86 4734.00 72.89 o 7 8 3 20080.48 19610.70 121.88 o 2 9 3 2578.34 2931.89 56.22 o 4 9 3 2418.36 2451.35 47.33 o 6 9 3 15328.43 15924.11 128.88 o 8 9 3 454.09 489.89 23.31 o 1 10 3 770.11 834.34 33.90 o 3 10 3 462.73 413.28 25.90 o 5 10 3 5144.49 5501.65 73.51 o 7 10 3 29.45 -3.15 20.42 o 9 10 3 1308.94 1433.13 36.81 o 2 11 3 96.67 191.67 22.94 o 4 11 3 670.45 508.98 30.39 o 6 11 3 11021.72 12887.87 106.35 o 8 11 3 2701.39 2996.11 53.28 o 10 11 3 380.76 514.90 57.67 o 1 12 3 104.83 203.08 25.37 o 3 12 3 4674.00 5878.40 84.24 o 5 12 3 6192.72 6458.44 85.35 o 7 12 3 338.35 372.67 26.76 o 9 12 3 12190.55 12364.64 109.44 o 11 12 3 1002.40 860.01 34.24 o 2 13 3 249.48 143.04 23.78 o 4 13 3 4397.56 5124.56 86.96 o 6 13 3 3937.14 3689.63 79.61 o 8 13 3 2544.43 3028.33 61.24 o 10 13 3 2679.37 3313.49 62.88 o 12 13 3 3802.50 3574.10 91.19 o 1 14 3 7407.41 7399.44 101.89 o 3 14 3 4643.02 3975.88 65.68 o 5 14 3 15.14 12.94 25.76 o 7 14 3 9.90 45.05 21.95 o 9 14 3 221.75 228.72 40.57 o 11 14 3 813.55 720.04 54.11 o 13 14 3 670.12 743.13 59.62 o 2 15 3 4540.68 4768.53 83.50 o 4 15 3 7465.08 6975.66 105.35 o 6 15 3 13083.73 12631.08 143.41 o 8 15 3 5712.34 5266.37 90.63 o 10 15 3 135.44 150.66 34.33 o 12 15 3 687.63 775.27 61.22 o 14 15 3 1.37 -15.12 49.51 o 1 16 3 353.44 300.30 31.18 o 3 16 3 89.85 50.51 25.25 o 5 16 3 2322.15 2268.26 66.16 o 7 16 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