#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/65/2236540.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236540_Fobs loop_ _publ_author_name 'Haehnel, Martin' 'Altenburger, Kai' 'Spannenberg, Anke' 'Arndt, Perdita' 'Rosenthal, Uwe' _publ_section_title ; Di-\m-sulfido-bis{[rac-1,2-bis(\h^5^-4,5,6,7-tetrahydroinden-1-yl)ethane]zirconium(IV)} toluene monosolvate ; _journal_coeditor_code PK2450 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1425 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.092 _cell_angle_gamma 90.000 _cell_length_a 12.6436 _cell_length_b 20.9735 _cell_length_c 14.8855 _exptl_crystal_F_000 1800.00 _reflns_d_resolution_high 0.7587 _[local]_cod_data_source_file pk2450Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ks1248m in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 359.33 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 53829.52 54597.24 1186.77 o 4 0 0 327.74 543.52 53.41 o 6 0 0 54459.73 50630.33 588.16 o 8 0 0 19791.64 19074.79 484.59 o 10 0 0 1601.72 1488.13 52.90 o 12 0 0 6214.77 6633.27 76.82 o 14 0 0 9401.73 10309.50 493.56 o 16 0 0 42.17 70.44 72.35 o 1 1 0 11981.42 14131.83 135.76 o 2 1 0 11098.80 12658.24 109.82 o 3 1 0 910.37 1140.99 40.65 o 4 1 0 2801.57 3331.97 48.90 o 5 1 0 23398.16 23333.94 258.84 o 6 1 0 1931.36 1902.25 45.25 o 7 1 0 131.54 107.47 27.22 o 8 1 0 486.09 585.72 35.41 o 9 1 0 1078.31 1202.69 38.02 o 10 1 0 2515.05 2451.85 38.68 o 11 1 0 14965.02 15110.05 98.19 o 12 1 0 412.28 407.50 41.80 o 13 1 0 3207.30 3224.74 61.41 o 14 1 0 83.29 136.38 37.71 o 15 1 0 258.46 257.43 40.47 o 16 1 0 439.26 377.30 48.79 o 0 2 0 56250.84 58711.20 329.81 o 1 2 0 21530.31 23506.40 176.97 o 2 2 0 30894.11 32159.93 254.33 o 3 2 0 406.26 570.69 30.09 o 4 2 0 105.81 121.44 26.73 o 5 2 0 4167.08 4062.66 46.53 o 6 2 0 30147.44 30862.73 214.15 o 7 2 0 30302.95 30468.38 357.64 o 8 2 0 9391.49 9506.38 109.62 o 9 2 0 353.20 345.31 34.07 o 10 2 0 185.09 224.29 31.59 o 11 2 0 24.00 36.67 34.07 o 12 2 0 13.79 46.54 32.48 o 13 2 0 4126.23 4555.23 52.43 o 14 2 0 2471.48 2798.96 49.10 o 15 2 0 342.13 348.63 37.82 o 16 2 0 30.50 22.65 60.48 o 1 3 0 19829.70 21336.79 120.27 o 2 3 0 18652.74 19798.40 113.38 o 3 3 0 15473.34 16890.71 87.49 o 4 3 0 8418.87 8341.75 60.79 o 5 3 0 744.57 899.71 32.10 o 6 3 0 1453.68 1329.38 33.95 o 7 3 0 3793.39 4443.26 59.95 o 8 3 0 3418.32 3323.24 51.70 o 9 3 0 254.32 362.62 30.70 o 10 3 0 85.46 86.94 33.76 o 11 3 0 81.30 29.44 34.79 o 12 3 0 3564.01 3424.21 73.73 o 13 3 0 2024.92 2258.66 45.90 o 14 3 0 17.04 48.50 36.74 o 15 3 0 855.21 861.03 46.51 o 0 4 0 28.15 72.08 37.29 o 1 4 0 672.95 718.82 32.31 o 2 4 0 5514.78 5898.75 62.37 o 3 4 0 449.83 374.68 27.13 o 4 4 0 23224.37 23470.50 119.53 o 5 4 0 9915.22 11528.88 70.54 o 6 4 0 144.74 237.30 25.63 o 7 4 0 1143.79 1273.32 32.23 o 8 4 0 65.96 98.02 28.21 o 9 4 0 538.75 535.94 34.66 o 10 4 0 2791.66 2931.99 45.70 o 11 4 0 310.56 336.56 35.81 o 12 4 0 88.54 151.02 40.97 o 13 4 0 1063.90 1062.32 36.72 o 14 4 0 244.38 317.64 46.45 o 15 4 0 124.15 154.57 49.45 o 1 5 0 711.61 815.05 30.55 o 2 5 0 1249.81 1229.49 35.85 o 3 5 0 3532.54 3863.79 42.27 o 4 5 0 267.12 389.11 25.06 o 5 5 0 2665.96 2834.30 36.50 o 6 5 0 0.67 3.53 23.33 o 7 5 0 13358.42 13382.79 116.32 o 8 5 0 2177.47 2341.88 36.27 o 9 5 0 5567.34 5509.87 49.51 o 10 5 0 752.12 599.94 29.47 o 11 5 0 1.50 22.90 34.94 o 12 5 0 155.33 121.56 41.10 o 13 5 0 490.94 548.88 44.60 o 14 5 0 1247.65 1230.70 45.90 o 15 5 0 3434.27 3258.93 172.60 o 0 6 0 20658.67 21794.85 138.96 o 1 6 0 20451.38 21769.28 119.56 o 2 6 0 12891.61 12440.43 68.33 o 3 6 0 7942.71 7668.60 56.46 o 4 6 0 35363.26 34756.61 165.60 o 5 6 0 434.72 707.84 26.37 o 6 6 0 7880.76 7565.50 51.95 o 7 6 0 4150.84 4226.28 39.21 o 8 6 0 3644.04 3398.85 37.36 o 9 6 0 202.59 260.74 29.08 o 10 6 0 8386.26 8201.02 54.01 o 11 6 0 53.17 61.45 32.69 o 12 6 0 2231.27 2254.16 44.81 o 13 6 0 633.82 729.45 42.22 o 14 6 0 93.96 142.95 42.23 o 15 6 0 3.25 46.54 40.87 o 1 7 0 2602.58 2960.59 42.02 o 2 7 0 15495.67 15341.66 121.06 o 3 7 0 2215.39 2222.14 30.56 o 4 7 0 1258.65 1148.89 27.84 o 5 7 0 13778.84 14382.12 64.54 o 6 7 0 546.17 541.16 25.37 o 7 7 0 1654.89 1841.83 30.99 o 8 7 0 6469.43 6235.08 45.83 o 9 7 0 79.71 77.67 28.03 o 10 7 0 1351.27 1244.37 34.35 o 11 7 0 940.45 864.84 38.06 o 12 7 0 1189.89 1356.64 43.09 o 13 7 0 2123.53 2083.18 44.85 o 14 7 0 1894.90 1823.32 52.43 o 15 7 0 270.42 243.42 46.30 o 0 8 0 25318.67 23481.61 213.63 o 1 8 0 3694.89 4069.26 37.49 o 2 8 0 10592.92 10613.04 125.84 o 3 8 0 13463.37 12219.70 85.31 o 4 8 0 467.41 516.87 24.51 o 5 8 0 3555.00 3405.95 35.48 o 6 8 0 29871.18 30151.54 152.50 o 7 8 0 23.97 31.92 23.18 o 8 8 0 11942.56 11803.80 90.72 o 9 8 0 3160.82 3207.27 43.67 o 10 8 0 43.86 49.91 28.33 o 11 8 0 3225.40 3333.19 44.45 o 12 8 0 2551.33 2705.83 40.73 o 13 8 0 669.27 726.67 41.09 o 14 8 0 5754.93 5940.99 157.35 o 15 8 0 218.48 147.23 47.25 o 1 9 0 7681.96 7999.51 54.85 o 2 9 0 8222.38 8400.93 72.17 o 3 9 0 3919.14 4420.45 38.55 o 4 9 0 104.61 142.77 23.22 o 5 9 0 20022.24 19762.90 108.61 o 6 9 0 11.86 12.30 21.05 o 7 9 0 130.87 128.26 24.51 o 8 9 0 3233.91 3206.36 40.26 o 9 9 0 4805.17 4524.92 55.93 o 10 9 0 4183.47 4025.80 51.59 o 11 9 0 4863.59 5325.20 90.49 o 12 9 0 97.12 87.45 34.11 o 13 9 0 1851.41 2005.13 56.02 o 14 9 0 782.22 798.16 50.67 o 15 9 0 565.42 465.09 43.61 o 0 10 0 10544.64 9802.31 189.96 o 1 10 0 16215.39 15216.09 130.38 o 2 10 0 1654.39 1876.53 27.28 o 3 10 0 1462.18 1431.68 26.71 o 4 10 0 1978.47 2016.63 29.77 o 5 10 0 8333.76 8367.52 61.01 o 6 10 0 20120.30 20115.52 160.03 o 7 10 0 4051.47 3968.64 35.96 o 8 10 0 5795.29 5617.50 51.30 o 9 10 0 4949.68 4831.97 64.27 o 10 10 0 3041.31 3145.50 41.50 o 11 10 0 1094.72 1249.18 38.23 o 12 10 0 1523.44 1502.28 42.29 o 13 10 0 2226.41 2516.38 78.56 o 14 10 0 2919.90 2884.93 100.73 o 1 11 0 8657.81 8710.96 85.81 o 2 11 0 2.90 31.09 21.07 o 3 11 0 148.27 102.11 19.46 o 4 11 0 3927.69 3790.93 34.49 o 5 11 0 6850.78 6855.91 50.07 o 6 11 0 4423.96 4718.66 37.78 o 7 11 0 120.19 157.91 25.88 o 8 11 0 6.55 34.37 26.20 o 9 11 0 806.15 790.01 31.15 o 10 11 0 325.88 377.40 30.26 o 11 11 0 2717.32 2734.93 49.47 o 12 11 0 2732.05 2869.99 62.74 o 13 11 0 535.33 552.40 42.42 o 14 11 0 314.39 316.48 38.91 o 0 12 0 7328.19 8169.42 136.95 o 1 12 0 9868.58 10064.15 62.78 o 2 12 0 328.87 327.01 22.76 o 3 12 0 27.64 29.13 22.49 o 4 12 0 33.12 13.16 21.24 o 5 12 0 76.78 89.19 23.61 o 6 12 0 264.48 201.74 23.42 o 7 12 0 1257.76 1306.48 28.55 o 8 12 0 11.45 24.69 26.62 o 9 12 0 58.23 44.10 24.30 o 10 12 0 190.45 223.11 28.80 o 11 12 0 259.70 237.85 32.66 o 12 12 0 148.05 204.86 36.68 o 13 12 0 2543.34 2438.53 43.39 o 14 12 0 292.31 252.69 45.26 o 1 13 0 6956.15 7519.42 59.38 o 2 13 0 1170.40 1011.58 26.88 o 3 13 0 1480.66 1536.39 27.87 o 4 13 0 549.10 562.34 24.04 o 5 13 0 1073.69 1175.87 27.15 o 6 13 0 8156.99 7757.81 89.10 o 7 13 0 833.96 868.53 26.08 o 8 13 0 9.43 29.95 25.45 o 9 13 0 288.26 224.53 25.18 o 10 13 0 666.05 638.03 31.82 o 11 13 0 165.31 166.03 32.18 o 12 13 0 3079.05 3190.89 62.14 o 13 13 0 80.85 83.78 41.75 o 14 13 0 223.31 181.56 42.19 o 0 14 0 79.41 26.68 25.44 o 1 14 0 194.05 226.48 21.03 o 2 14 0 1566.34 1512.09 25.95 o 3 14 0 34.20 16.17 21.80 o 4 14 0 2764.68 2741.95 33.34 o 5 14 0 3530.44 3333.43 32.35 o 6 14 0 41.11 43.35 25.94 o 7 14 0 2036.74 1790.36 31.70 o 8 14 0 197.86 200.66 25.16 o 9 14 0 632.82 694.20 27.85 o 10 14 0 1941.50 1896.67 35.08 o 11 14 0 176.87 178.80 29.16 o 12 14 0 0.70 11.49 29.70 o 13 14 0 22.65 48.96 38.06 o 1 15 0 1425.75 1438.52 26.16 o 2 15 0 2138.60 2004.10 26.61 o 3 15 0 426.98 503.15 24.48 o 4 15 0 16.62 33.08 24.60 o 5 15 0 4941.97 4904.17 41.28 o 6 15 0 96.62 75.57 23.89 o 7 15 0 842.34 953.96 27.29 o 8 15 0 5910.34 5777.32 57.71 o 9 15 0 90.00 126.27 25.34 o 10 15 0 780.71 793.54 31.40 o 11 15 0 160.65 144.99 30.26 o 12 15 0 20.15 29.06 33.44 o 13 15 0 17.42 14.65 33.97 o 0 16 0 1150.25 1139.45 35.95 o 1 16 0 3315.70 3191.05 31.36 o 2 16 0 797.37 668.42 24.64 o 3 16 0 17184.17 17191.98 180.05 o 4 16 0 1954.04 1945.11 31.66 o 5 16 0 3930.68 4179.39 40.09 o 6 16 0 173.14 197.57 27.32 o 7 16 0 1.02 17.18 25.99 o 8 16 0 432.74 410.93 29.61 o 9 16 0 5797.82 5840.24 55.94 o 10 16 0 533.62 579.91 32.72 o 11 16 0 5140.95 5239.90 58.22 o 12 16 0 196.79 189.96 38.30 o 13 16 0 603.14 556.86 40.94 o 1 17 0 729.79 679.90 24.68 o 2 17 0 3559.53 3530.83 32.38 o 3 17 0 1954.81 1683.31 27.66 o 4 17 0 1717.77 1863.81 31.07 o 5 17 0 711.76 741.55 28.69 o 6 17 0 106.75 82.62 25.39 o 7 17 0 35.81 55.02 24.26 o 8 17 0 6013.74 6018.86 89.33 o 9 17 0 204.65 237.57 29.11 o 10 17 0 923.21 1036.60 35.36 o 11 17 0 305.40 316.00 35.55 o 12 17 0 6.26 20.56 36.09 o 0 18 0 3269.93 3595.41 80.95 o 1 18 0 5207.07 4992.35 34.55 o 2 18 0 2071.11 1935.23 27.94 o 3 18 0 10536.12 10539.22 123.58 o 4 18 0 5502.94 5554.08 62.81 o 5 18 0 3639.90 3743.90 35.95 o 6 18 0 4245.51 4012.54 35.25 o 7 18 0 539.43 551.21 27.49 o 8 18 0 148.57 182.26 27.48 o 9 18 0 4956.95 4998.69 89.76 o 10 18 0 1758.53 1874.72 33.46 o 11 18 0 3736.03 3685.18 84.91 o 12 18 0 37.02 33.75 35.24 o 1 19 0 3146.99 3205.13 49.77 o 2 19 0 1890.94 1752.99 28.69 o 3 19 0 292.14 279.58 25.65 o 4 19 0 2.24 15.72 26.64 o 5 19 0 5138.08 5208.21 56.36 o 6 19 0 208.54 271.26 28.35 o 7 19 0 83.67 123.14 28.59 o 8 19 0 1926.69 2094.92 35.15 o 9 19 0 3164.91 3323.53 37.84 o 10 19 0 444.26 439.45 31.46 o 11 19 0 1484.90 1377.84 37.59 o 0 20 0 475.23 486.48 31.39 o 1 20 0 5186.94 5182.04 36.10 o 2 20 0 4872.80 4863.30 35.16 o 3 20 0 450.19 456.71 26.26 o 4 20 0 5854.18 5920.96 84.52 o 5 20 0 1087.39 1171.06 28.82 o 6 20 0 0.77 14.35 26.92 o 7 20 0 2429.02 2531.34 32.26 o 8 20 0 156.32 167.35 30.28 o 9 20 0 339.29 319.44 29.09 o 10 20 0 2021.58 1776.11 36.66 o 11 20 0 33.28 33.98 34.55 o 1 21 0 43.29 77.42 24.11 o 2 21 0 515.25 480.27 26.56 o 3 21 0 3.98 6.27 26.11 o 4 21 0 660.45 640.27 33.28 o 5 21 0 20.57 52.13 27.21 o 6 21 0 681.12 577.13 27.61 o 7 21 0 41.11 79.42 27.49 o 8 21 0 0.67 7.40 29.60 o 9 21 0 220.30 211.80 33.90 o 10 21 0 1948.41 1744.03 47.18 o 0 22 0 785.35 854.44 39.39 o 1 22 0 1564.30 1689.21 30.09 o 2 22 0 26.31 28.45 26.34 o 3 22 0 55.89 79.91 25.06 o 4 22 0 31.36 15.12 31.06 o 5 22 0 1327.70 1420.04 31.12 o 6 22 0 188.98 220.63 27.87 o 7 22 0 1538.83 1671.60 36.27 o 8 22 0 22.73 41.09 31.77 o 9 22 0 2.39 37.56 33.74 o 1 23 0 1038.44 1026.69 27.21 o 2 23 0 147.94 188.35 27.74 o 3 23 0 0.28 -0.55 26.51 o 4 23 0 40.30 41.51 29.37 o 5 23 0 1116.94 1149.42 31.24 o 6 23 0 530.18 557.99 29.61 o 7 23 0 82.27 136.54 30.35 o 8 23 0 418.78 440.95 34.47 o 0 24 0 506.59 630.77 40.70 o 1 24 0 906.40 946.09 30.04 o 2 24 0 80.67 101.87 27.29 o 3 24 0 5525.02 5837.73 84.02 o 4 24 0 276.31 314.67 33.81 o 5 24 0 1329.81 1309.76 35.23 o 6 24 0 678.46 684.55 33.98 o 7 24 0 16.71 14.01 35.21 o 1 25 0 355.76 370.50 30.14 o 2 25 0 2045.04 2111.57 33.95 o 3 25 0 25.80 47.70 30.30 o 4 25 0 474.41 444.66 32.93 o 5 25 0 312.40 276.11 33.49 o 6 25 0 11.12 5.51 32.33 o 0 26 0 53.27 18.10 42.44 o 1 26 0 4.88 15.01 31.56 o 2 26 0 907.20 839.24 34.81 o 3 26 0 8081.60 7931.48 129.17 o 4 26 0 1563.32 1563.93 39.81 o 5 26 0 3004.19 2656.54 46.83 o 1 27 0 737.39 766.46 35.16 o 2 27 0 1021.67 936.80 35.05 o 3 27 0 191.76 146.35 33.71 o -15 0 1 240.88 299.65 54.93 o -13 0 1 8660.95 9446.02 104.29 o -11 0 1 1043.31 1269.20 52.57 o -9 0 1 7.59 25.22 41.56 o -7 0 1 13280.42 12633.69 114.57 o -5 0 1 37038.46 36878.07 422.28 o -3 0 1 1805.96 2221.22 69.57 o -1 0 1 28918.54 31651.21 1056.26 o 1 0 1 129115.04 107453.30 1057.87 o 3 0 1 58.33 42.73 46.74 o 5 0 1 705.93 402.02 45.87 o 7 0 1 51551.51 48256.02 400.81 o 9 0 1 11561.34 11471.75 172.70 o 11 0 1 1204.29 1356.47 60.09 o 13 0 1 5755.06 6042.07 83.33 o 15 0 1 6415.91 6089.58 86.59 o -16 1 1 303.18 303.67 52.17 o -15 1 1 350.08 307.18 47.79 o -14 1 1 47.28 60.61 39.30 o -13 1 1 37.21 34.45 41.43 o -12 1 1 5530.41 5616.31 80.62 o -11 1 1 1389.83 1453.59 50.68 o -10 1 1 7316.01 7325.11 116.65 o -9 1 1 892.97 957.16 36.68 o -8 1 1 918.49 916.04 33.13 o -7 1 1 4376.27 4977.84 51.87 o -6 1 1 1264.94 1133.35 35.02 o -5 1 1 4714.02 4555.15 48.77 o -4 1 1 13359.07 13498.75 147.97 o -3 1 1 6.99 42.60 32.56 o -2 1 1 13149.57 14264.83 380.11 o -1 1 1 17783.88 20252.65 214.69 o 0 1 1 11840.75 13728.79 135.71 o 1 1 1 2321.96 2410.20 57.87 o 2 1 1 128.60 179.98 32.25 o 3 1 1 5316.22 5069.75 60.28 o 4 1 1 5.26 24.20 26.43 o 5 1 1 2228.44 2244.71 43.92 o 6 1 1 32620.64 33115.79 387.82 o 7 1 1 871.11 995.43 35.08 o 8 1 1 92.61 105.40 32.79 o 9 1 1 2762.38 2670.39 52.76 o 10 1 1 392.61 417.16 35.52 o 11 1 1 8.02 -4.11 34.58 o 12 1 1 13418.87 13762.80 129.99 o 13 1 1 1085.18 1018.47 39.94 o 14 1 1 1963.46 1947.93 44.95 o 15 1 1 81.45 95.93 44.93 o -16 2 1 389.76 360.04 43.50 o -15 2 1 115.67 124.67 43.37 o -14 2 1 640.25 696.52 41.98 o -13 2 1 3514.99 3473.62 106.61 o -12 2 1 4410.79 4937.82 101.79 o -11 2 1 931.65 920.59 38.18 o -10 2 1 614.77 601.30 30.34 o -9 2 1 596.05 644.52 32.70 o -8 2 1 0.02 31.09 32.37 o -7 2 1 6113.95 5714.29 85.02 o -6 2 1 23777.43 24062.32 270.54 o -5 2 1 11053.74 10626.81 105.10 o -4 2 1 88.88 98.63 26.39 o -3 2 1 5371.57 6220.61 59.34 o -2 2 1 16730.51 17880.73 153.34 o -1 2 1 55171.98 57954.92 496.85 o 0 2 1 28172.39 32079.17 161.08 o 1 2 1 52042.59 52939.13 247.97 o 2 2 1 13732.76 14550.10 95.13 o 3 2 1 2121.98 2444.70 43.43 o 4 2 1 21.37 24.62 25.96 o 5 2 1 6577.15 7206.68 69.86 o 6 2 1 7825.27 7595.12 57.41 o 7 2 1 14376.58 14280.21 149.72 o 8 2 1 10136.89 10141.46 102.49 o 9 2 1 7417.19 8038.74 61.32 o 10 2 1 2024.21 2300.17 42.97 o 11 2 1 554.47 641.75 34.65 o 12 2 1 96.98 59.55 33.40 o 13 2 1 1356.71 1551.67 48.06 o 14 2 1 4016.56 4255.27 130.86 o 15 2 1 1396.39 1343.51 54.52 o -16 3 1 983.45 958.05 53.90 o -15 3 1 26.14 39.11 42.60 o -14 3 1 2093.53 2121.30 51.37 o -13 3 1 8.35 31.04 34.84 o -12 3 1 4717.69 4666.54 83.84 o -11 3 1 1134.06 1208.34 42.58 o -10 3 1 2272.56 2292.65 41.63 o -9 3 1 785.18 746.55 31.34 o -8 3 1 3233.08 3466.67 42.30 o -7 3 1 5066.17 5088.50 57.55 o -6 3 1 11121.57 11748.57 137.48 o -5 3 1 6.11 11.60 27.35 o -4 3 1 217.68 290.59 24.99 o -3 3 1 2.07 16.20 25.62 o -2 3 1 313.39 316.13 30.99 o -1 3 1 34625.47 36638.73 138.44 o 0 3 1 31050.71 33208.27 138.42 o 1 3 1 49878.42 52359.98 265.39 o 2 3 1 1421.26 1914.03 40.05 o 3 3 1 18460.24 20117.53 131.08 o 4 3 1 1583.24 1469.71 37.14 o 5 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