#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/65/2236554.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236554_Fobs loop_ _publ_author_name 'Nagarajaiah, H.' 'Begum, Noor Shahina' _publ_section_title ; Ethyl 3-ethoxycarbonylmethyl-7-methyl-5-phenyl-5H-thiazolo[3,2-a]pyrimidine-6-carboxylate ; _journal_coeditor_code PV2584 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2878 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.000 _cell_angle_gamma 90.000 _cell_length_a 10.0861 _cell_length_b 7.7954 _cell_length_c 23.4088 _exptl_crystal_F_000 816.00 _reflns_d_resolution_high 0.7828 _[local]_cod_data_source_file pv2584Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' new_0m in P 21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.74 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 5941.05 5571.89 91.16 o 2 0 0 5992.29 5769.27 82.29 o 3 0 0 6.97 1.27 3.31 o 4 0 0 2317.89 2083.28 38.14 o 5 0 0 205.70 155.18 7.85 o 6 0 0 6107.31 5558.04 97.26 o 7 0 0 958.60 914.41 22.05 o 8 0 0 94.68 88.32 9.20 o 9 0 0 2616.45 2668.07 65.03 o 10 0 0 56.74 62.06 10.36 o 11 0 0 210.07 193.41 21.83 o 12 0 0 987.09 1124.82 50.17 o 1 1 0 6.95 0.69 1.38 o 2 1 0 727.22 571.69 8.15 o 3 1 0 63.74 49.79 2.64 o 4 1 0 721.79 603.09 13.20 o 5 1 0 20.09 19.80 3.11 o 6 1 0 292.44 263.82 7.98 o 7 1 0 1750.95 1655.18 26.57 o 8 1 0 431.07 425.82 12.64 o 9 1 0 2.84 0.00 5.04 o 10 1 0 1010.45 1107.28 27.82 o 11 1 0 57.43 55.75 11.61 o 12 1 0 25.75 19.99 9.65 o 0 2 0 560.21 581.72 10.07 o 1 2 0 16.99 23.53 2.57 o 2 2 0 9212.45 8936.67 106.03 o 3 2 0 7224.44 7192.88 93.84 o 4 2 0 1472.66 1398.94 55.49 o 5 2 0 1217.84 1085.73 24.73 o 6 2 0 69.01 57.63 4.71 o 7 2 0 0.03 5.02 3.99 o 8 2 0 682.27 722.99 19.25 o 9 2 0 2.88 2.90 5.50 o 10 2 0 44.96 46.93 9.26 o 11 2 0 524.74 600.03 22.00 o 12 2 0 0.55 3.28 7.18 o 1 3 0 4200.54 3917.28 48.07 o 2 3 0 110.41 99.80 5.53 o 3 3 0 2216.65 2124.16 37.89 o 4 3 0 215.25 261.71 9.56 o 5 3 0 654.92 573.91 16.81 o 6 3 0 1311.99 1240.33 30.09 o 7 3 0 578.88 541.16 18.31 o 8 3 0 4.68 0.00 7.71 o 9 3 0 699.22 683.54 29.11 o 10 3 0 0.49 0.00 8.55 o 11 3 0 36.26 36.32 12.21 o 12 3 0 4.54 0.00 11.22 o 0 4 0 1219.79 1284.79 24.86 o 1 4 0 599.69 599.31 14.06 o 2 4 0 1998.15 2005.03 32.36 o 3 4 0 1580.05 1499.97 36.10 o 4 4 0 365.14 354.70 10.14 o 5 4 0 0.51 0.00 4.89 o 6 4 0 27.06 19.36 8.15 o 7 4 0 85.38 108.85 13.14 o 8 4 0 1411.98 1425.62 43.35 o 9 4 0 26.59 18.15 10.21 o 10 4 0 121.69 136.68 16.18 o 11 4 0 17.09 25.09 12.49 o 1 5 0 2.26 0.00 7.79 o 2 5 0 6.71 1.71 4.42 o 3 5 0 425.60 436.57 17.79 o 4 5 0 703.53 754.74 21.74 o 5 5 0 2129.42 1936.69 52.34 o 6 5 0 1251.86 1231.27 83.87 o 7 5 0 14.10 9.02 10.53 o 8 5 0 125.59 72.68 13.25 o 9 5 0 170.52 182.34 18.12 o 10 5 0 53.71 68.08 14.34 o 11 5 0 24.31 29.10 14.08 o 0 6 0 34.90 46.34 16.85 o 1 6 0 42.23 44.30 10.97 o 2 6 0 137.75 129.09 15.32 o 3 6 0 23.80 2.14 7.21 o 4 6 0 100.02 80.12 12.81 o 5 6 0 770.43 704.84 29.59 o 6 6 0 187.34 157.79 26.81 o 7 6 0 129.15 113.75 24.89 o 8 6 0 8.97 0.00 16.47 o 9 6 0 35.09 6.51 18.00 o 10 6 0 17.16 27.96 22.21 o 1 7 0 1412.18 1483.46 49.15 o 2 7 0 74.09 83.36 20.68 o 3 7 0 909.90 939.08 37.30 o 4 7 0 108.22 98.41 15.32 o 5 7 0 3.32 21.06 17.62 o 6 7 0 268.72 264.64 34.85 o 7 7 0 0.11 8.04 19.15 o 8 7 0 308.76 237.45 34.85 o 9 7 0 172.92 180.00 32.55 o 0 8 0 641.73 708.52 48.64 o 1 8 0 209.12 216.25 22.33 o 2 8 0 27.12 24.30 14.47 o 3 8 0 43.40 41.49 14.78 o 4 8 0 12.48 0.00 11.78 o 5 8 0 71.71 46.34 23.36 o 6 8 0 7.06 0.00 18.38 o 7 8 0 344.14 375.70 44.43 o 1 9 0 17.21 0.13 17.62 o 2 9 0 15.21 0.00 14.49 o 3 9 0 3.76 1.15 14.35 o 4 9 0 2.49 0.38 21.83 o 5 9 0 51.33 86.55 27.96 o -12 1 1 40.06 42.94 17.81 o -11 1 1 46.06 46.76 8.53 o -10 1 1 592.40 614.73 17.26 o -9 1 1 56.48 54.69 6.88 o -8 1 1 142.47 137.53 7.28 o -7 1 1 1137.20 1089.80 19.34 o -6 1 1 286.47 235.08 7.76 o -5 1 1 229.14 186.29 9.44 o -4 1 1 18.67 11.51 2.53 o -3 1 1 15.54 23.59 2.78 o -2 1 1 4.29 0.00 1.82 o -1 1 1 2970.78 2964.14 30.67 o 0 1 1 505.45 391.64 6.33 o 1 1 1 934.49 743.73 9.93 o 2 1 1 2621.16 2620.49 27.53 o 3 1 1 4987.87 4615.64 89.46 o 4 1 1 19.28 15.23 2.96 o 5 1 1 11.61 8.75 3.01 o 6 1 1 8.82 4.48 4.35 o 7 1 1 38.35 57.12 8.84 o 8 1 1 188.57 197.04 9.10 o 9 1 1 177.21 181.92 12.05 o 10 1 1 55.89 56.36 11.00 o 11 1 1 145.10 145.93 11.58 o 12 1 1 255.12 314.35 20.11 o -12 2 1 321.69 402.33 24.05 o -11 2 1 588.19 701.38 21.20 o -10 2 1 2.19 0.00 5.76 o -9 2 1 493.43 500.69 14.17 o -8 2 1 31.08 27.74 6.97 o -7 2 1 71.95 75.69 7.30 o -6 2 1 904.45 882.23 23.28 o -5 2 1 6832.11 6993.50 104.20 o -4 2 1 519.30 545.97 12.32 o -3 2 1 3294.11 3351.34 41.12 o -2 2 1 392.55 327.16 5.76 o -1 2 1 4333.57 4127.34 60.15 o 0 2 1 14510.27 14487.23 169.58 o 1 2 1 60.80 88.02 5.25 o 2 2 1 197.12 140.21 6.11 o 3 2 1 3345.53 3208.66 71.19 o 4 2 1 139.05 146.99 10.27 o 5 2 1 266.63 265.40 22.21 o 6 2 1 193.40 165.14 6.51 o 7 2 1 1243.81 1228.76 26.89 o 8 2 1 43.53 31.44 5.12 o 9 2 1 178.82 209.38 11.39 o 10 2 1 0.81 0.00 6.31 o 11 2 1 180.87 200.80 12.23 o 12 2 1 1.44 0.00 7.43 o -12 3 1 27.99 32.27 12.97 o -11 3 1 89.41 80.94 14.16 o -10 3 1 0.07 10.55 9.75 o -9 3 1 659.81 679.32 27.70 o -8 3 1 933.99 920.47 25.60 o -7 3 1 626.64 586.59 18.85 o -6 3 1 117.37 114.17 8.80 o -5 3 1 24.95 7.75 4.67 o -4 3 1 7.16 0.00 3.48 o -3 3 1 1391.23 1471.95 23.22 o -2 3 1 240.64 279.14 9.95 o -1 3 1 411.54 371.78 7.81 o 0 3 1 66.96 50.37 2.26 o 1 3 1 424.85 388.91 8.46 o 2 3 1 2958.05 3136.09 57.93 o 3 3 1 668.62 781.67 13.71 o 4 3 1 4821.56 4966.17 91.43 o 5 3 1 557.41 466.94 18.75 o 6 3 1 28.34 24.78 7.63 o 7 3 1 55.34 41.24 9.27 o 8 3 1 176.86 193.20 15.70 o 9 3 1 19.77 23.36 9.85 o 10 3 1 134.48 128.31 14.63 o 11 3 1 95.06 122.05 16.85 o 12 3 1 14.85 10.55 12.64 o -11 4 1 408.73 461.13 26.50 o -10 4 1 70.88 72.43 14.55 o -9 4 1 13.42 8.50 9.47 o -8 4 1 57.27 78.62 27.19 o -7 4 1 3.31 0.00 5.62 o -6 4 1 1101.41 1074.84 27.17 o -5 4 1 51.73 46.43 6.80 o -4 4 1 10.49 7.24 3.87 o -3 4 1 785.33 654.64 15.75 o -2 4 1 905.16 866.08 15.52 o -1 4 1 1159.47 1090.73 17.75 o 0 4 1 0.72 0.00 1.80 o 1 4 1 118.37 112.05 8.28 o 2 4 1 234.96 220.85 13.16 o 3 4 1 4597.38 4579.22 83.96 o 4 4 1 875.34 905.10 19.41 o 5 4 1 99.21 88.98 10.91 o 6 4 1 473.02 493.91 22.79 o 7 4 1 636.71 589.65 25.35 o 8 4 1 221.25 222.29 17.57 o 9 4 1 300.50 315.98 20.87 o 10 4 1 521.76 526.64 34.09 o 11 4 1 3.44 17.22 12.42 o -11 5 1 73.34 117.31 20.30 o -10 5 1 593.40 672.87 32.36 o -9 5 1 204.90 220.36 19.32 o -8 5 1 472.43 450.90 29.30 o -7 5 1 1164.74 990.72 57.64 o -6 5 1 1.66 2.38 6.42 o -5 5 1 1.47 1.85 6.14 o -4 5 1 3381.53 3300.80 55.05 o -3 5 1 615.62 644.41 14.12 o -2 5 1 233.42 208.42 7.62 o -1 5 1 1527.73 1604.78 45.49 o 0 5 1 1099.98 1194.16 37.10 o 1 5 1 541.23 480.50 29.01 o 2 5 1 600.25 621.45 15.01 o 3 5 1 27.26 26.97 5.32 o 4 5 1 23.22 9.34 5.96 o 5 5 1 7.48 3.52 9.00 o 6 5 1 1399.34 1362.14 41.87 o 7 5 1 718.37 754.86 67.02 o 8 5 1 367.20 350.53 22.36 o 9 5 1 176.60 178.79 18.40 o 10 5 1 166.67 165.31 31.98 o 11 5 1 12.36 5.58 13.14 o -10 6 1 24.45 25.66 21.83 o -9 6 1 124.87 109.15 26.04 o -8 6 1 48.75 45.19 21.45 o -7 6 1 29.18 29.11 17.62 o -6 6 1 147.61 124.85 24.51 o -5 6 1 438.57 466.35 34.85 o -4 6 1 144.82 151.35 16.18 o -3 6 1 554.85 515.47 28.62 o -2 6 1 237.68 194.94 35.84 o -1 6 1 330.84 337.79 21.66 o 0 6 1 744.71 755.40 30.60 o 1 6 1 94.80 116.68 13.90 o 2 6 1 1525.16 1486.60 41.10 o 3 6 1 1094.35 1082.99 27.94 o 4 6 1 51.52 46.41 14.55 o 5 6 1 248.58 212.68 17.65 o 6 6 1 4.98 1.53 15.70 o 7 6 1 746.03 810.39 50.94 o 8 6 1 71.60 98.43 24.13 o 9 6 1 32.20 20.30 20.68 o 10 6 1 209.60 217.53 35.62 o -9 7 1 45.80 28.72 22.98 o -8 7 1 0.14 0.00 18.38 o -7 7 1 255.66 229.02 33.32 o -6 7 1 256.02 205.66 31.79 o -5 7 1 470.78 524.23 40.21 o -4 7 1 250.71 257.91 21.86 o -3 7 1 1088.20 1096.92 40.68 o -2 7 1 107.22 74.14 25.85 o -1 7 1 273.14 234.96 21.52 o 0 7 1 25.26 0.00 10.69 o 1 7 1 793.64 848.63 35.45 o 2 7 1 1951.95 1989.37 89.04 o 3 7 1 777.28 717.46 32.59 o 4 7 1 249.84 241.15 20.87 o 5 7 1 1.78 0.00 15.32 o 6 7 1 19.06 0.00 15.70 o 7 7 1 452.67 438.51 44.04 o 8 7 1 107.38 118.34 28.34 o 9 7 1 28.14 44.43 24.89 o -7 8 1 0.01 0.00 18.77 o -6 8 1 73.27 88.47 26.43 o -5 8 1 578.60 621.20 48.26 o -4 8 1 157.01 158.12 19.48 o -3 8 1 422.49 421.26 42.32 o -2 8 1 8.28 6.91 16.09 o -1 8 1 1032.59 1151.61 60.32 o 0 8 1 25.30 16.93 14.05 o 1 8 1 41.87 25.57 13.93 o 2 8 1 1453.67 1645.86 55.36 o 3 8 1 6.17 3.85 12.57 o 4 8 1 0.52 19.53 19.92 o 5 8 1 260.59 236.68 35.23 o 6 8 1 154.12 150.13 30.26 o 7 8 1 423.89 556.47 52.85 o -5 9 1 1.98 0.00 20.30 o -4 9 1 98.23 101.11 28.72 o -3 9 1 95.58 103.55 20.11 o -2 9 1 743.23 1005.28 44.95 o -1 9 1 0.24 0.00 18.00 o 0 9 1 122.37 161.19 22.07 o 1 9 1 26.08 17.12 15.87 o 2 9 1 935.17 1094.26 46.17 o 3 9 1 77.68 71.62 26.43 o 4 9 1 414.92 425.11 47.11 o 5 9 1 37.81 16.09 22.60 o -12 0 2 14.19 10.34 13.79 o -11 0 2 3263.95 3740.66 89.88 o -10 0 2 616.01 665.95 25.46 o -9 0 2 1095.66 1100.81 33.11 o -8 0 2 700.70 667.40 19.12 o -7 0 2 161.99 211.55 10.60 o -6 0 2 1613.65 1489.12 50.75 o -5 0 2 2584.70 2423.37 54.01 o -4 0 2 156.15 126.04 7.69 o -3 0 2 5292.43 5120.83 104.80 o -2 0 2 7718.24 7680.03 125.51 o -1 0 2 11534.54 12350.12 409.78 o 0 0 2 1204.96 1385.73 53.04 o 1 0 2 8918.80 10043.00 167.69 o 2 0 2 11151.99 10683.08 469.34 o 3 0 2 4976.39 4860.39 161.24 o 4 0 2 1159.40 1042.01 25.98 o 5 0 2 4065.07 3966.67 86.70 o 6 0 2 655.50 692.23 21.10 o 7 0 2 1358.93 1270.04 33.82 o 8 0 2 213.13 203.55 13.00 o 9 0 2 370.88 378.38 17.93 o 10 0 2 88.11 99.39 11.67 o 11 0 2 360.82 425.11 29.11 o 12 0 2 81.12 93.83 18.38 o -12 1 2 74.46 65.84 9.82 o -11 1 2 0.48 2.43 6.90 o -10 1 2 648.46 675.74 18.11 o -9 1 2 286.86 279.75 9.64 o -8 1 2 14.86 17.09 4.42 o -7 1 2 1988.25 1895.76 29.60 o -6 1 2 84.82 73.20 5.71 o -5 1 2 1573.79 1374.72 21.46 o -4 1 2 52.31 53.07 3.49 o -3 1 2 4090.71 4028.92 58.06 o -2 1 2 849.63 798.23 11.75 o -1 1 2 1215.23 1153.43 12.87 o 0 1 2 754.83 823.53 15.50 o 1 1 2 1990.98 2080.77 23.67 o 2 1 2 7707.16 7864.80 102.05 o 3 1 2 1037.39 1026.31 31.57 o 4 1 2 857.07 758.23 16.09 o 5 1 2 8.37 2.64 2.85 o 6 1 2 3730.25 3564.18 56.16 o 7 1 2 9.23 12.53 4.05 o 8 1 2 293.05 289.83 12.00 o 9 1 2 3810.77 4011.80 65.19 o 10 1 2 27.15 21.02 7.19 o 11 1 2 8.04 4.46 13.98 o 12 1 2 178.05 191.99 17.04 o -12 2 2 104.52 117.35 15.98 o -11 2 2 4.13 7.68 6.99 o -10 2 2 3.69 0.00 5.71 o -9 2 2 194.05 205.19 14.10 o -8 2 2 2370.90 2331.81 40.33 o -7 2 2 701.44 642.38 13.35 o -6 2 2 2505.44 2318.28 39.09 o -5 2 2 505.92 479.93 15.04 o -4 2 2 3001.07 3006.89 47.05 o -3 2 2 2.17 0.00 4.50 o -2 2 2 5245.07 5234.54 83.13 o -1 2 2 5883.03 5750.30 75.75 o 0 2 2 2282.70 2327.86 26.49 o 1 2 2 13554.96 13557.06 167.62 o 2 2 2 155.77 147.37 8.39 o 3 2 2 867.00 958.83 25.75 o 4 2 2 5.26 3.78 4.96 o 5 2 2 1.74 7.15 3.15 o 6 2 2 101.00 91.29 5.03 o 7 2 2 0.15 0.00 3.20 o 8 2 2 0.71 0.00 5.08 o 9 2 2 2.04 0.00 5.22 o 10 2 2 61.76 71.28 12.00 o 11 2 2 68.94 82.32 9.18 o 12 2 2 60.32 75.52 10.32 o -12 3 2 0.28 9.32 11.96 o -11 3 2 14.52 18.93 11.94 o -10 3 2 259.00 264.71 19.60 o -9 3 2 1.16 6.10 7.00 o -8 3 2 17.80 22.39 7.21 o -7 3 2 58.80 49.13 7.38 o -6 3 2 435.59 405.81 14.90 o -5 3 2 247.27 208.34 8.32 o -4 3 2 1583.62 1510.28 22.98 o -3 3 2 604.29 645.65 9.88 o -2 3 2 5232.37 5257.75 79.92 o -1 3 2 502.40 457.61 8.30 o 0 3 2 13.00 11.68 1.77 o 1 3 2 1302.76 1270.07 19.50 o 2 3 2 3387.21 3540.61 64.65 o 3 3 2 41.25 116.15 5.64 o 4 3 2 786.91 741.73 19.33 o 5 3 2 58.31 31.78 7.18 o 6 3 2 695.33 693.60 24.70 o 7 3 2 2.96 3.78 7.08 o 8 3 2 35.97 26.92 9.34 o 9 3 2 482.07 483.96 23.50 o 10 3 2 6.67 13.63 10.03 o 11 3 2 94.77 93.37 15.08 o 12 3 2 463.19 591.64 44.62 o -11 4 2 279.09 369.94 38.49 o -10 4 2 7.72 15.62 11.87 o -9 4 2 248.12 220.37 18.54 o -8 4 2 420.83 394.68 21.26 o -7 4 2 465.84 442.07 17.39 o -6 4 2 17.39 14.59 6.37 o -5 4 2 444.51 418.04 15.24 o -4 4 2 893.14 842.29 18.70 o -3 4 2 75.94 88.02 6.98 o -2 4 2 224.26 223.89 7.47 o -1 4 2 862.11 846.72 16.17 o 0 4 2 477.04 522.62 8.85 o 1 4 2 4129.69 4479.04 69.48 o 2 4 2 676.37 610.33 15.98 o 3 4 2 1678.24 1579.28 33.48 o 4 4 2 1424.11 1426.93 26.93 o 5 4 2 173.48 154.77 21.64 o 6 4 2 148.90 157.53 13.80 o 7 4 2 1293.60 1225.26 49.02 o 8 4 2 114.11 90.98 13.34 o 9 4 2 22.91 21.22 10.67 o 10 4 2 17.72 0.00 16.47 o 11 4 2 40.97 73.87 14.67 o -11 5 2 50.05 41.48 14.45 o -10 5 2 308.43 372.42 24.66 o -9 5 2 102.65 137.24 22.21 o -8 5 2 292.10 274.67 21.64 o -7 5 2 28.44 6.55 10.39 o -6 5 2 5.93 0.00 6.00 o -5 5 2 555.02 490.82 18.56 o -4 5 2 680.47 643.83 18.02 o -3 5 2 0.82 2.10 7.91 o -2 5 2 286.25 292.07 9.01 o -1 5 2 45.01 35.57 4.53 o 0 5 2 75.37 66.28 3.87 o 1 5 2 1926.26 2028.94 54.54 o 2 5 2 87.42 112.72 11.46 o 3 5 2 83.01 59.82 8.68 o 4 5 2 155.39 159.00 17.59 o 5 5 2 78.15 67.89 10.70 o 6 5 2 550.69 512.67 24.11 o 7 5 2 136.27 329.75 28.72 o 8 5 2 230.50 204.94 18.59 o 9 5 2 10.88 11.03 24.51 o 10 5 2 6.65 20.31 14.17 o -10 6 2 187.75 198.38 33.32 o -9 6 2 9.85 14.55 20.30 o -8 6 2 66.45 64.72 22.60 o -7 6 2 95.81 79.28 21.83 o -6 6 2 180.47 162.77 26.81 o -5 6 2 646.10 655.41 22.35 o -4 6 2 1630.83 1542.33 36.71 o -3 6 2 416.07 387.08 15.50 o -2 6 2 652.12 618.22 58.56 o -1 6 2 8.09 11.45 9.59 o 0 6 2 436.02 451.94 26.43 o 1 6 2 57.28 55.31 17.43 o 2 6 2 744.75 782.86 31.40 o 3 6 2 141.34 118.76 10.33 o 4 6 2 14.29 6.00 9.00 o 5 6 2 1829.59 1603.54 73.92 o 6 6 2 1095.79 1105.67 60.13 o 7 6 2 93.92 92.68 23.74 o 8 6 2 144.74 102.26 24.51 o 9 6 2 38.78 62.43 23.36 o 10 6 2 288.56 333.19 41.36 o -9 7 2 158.21 237.45 36.77 o -8 7 2 48.32 73.15 24.89 o -7 7 2 34.52 35.62 21.45 o -6 7 2 44.34 19.92 19.92 o -5 7 2 185.77 153.07 17.78 o -4 7 2 93.99 77.20 15.26 o -3 7 2 1186.24 1279.02 45.04 o -2 7 2 8.01 18.43 11.24 o -1 7 2 398.27 389.61 80.43 o 0 7 2 571.34 512.30 41.36 o 1 7 2 0.02 6.11 11.22 o 2 7 2 5.77 0.00 10.67 o 3 7 2 213.65 186.71 19.32 o 4 7 2 105.09 111.15 15.26 o 5 7 2 56.11 28.34 19.15 o 6 7 2 289.99 298.34 37.15 o 7 7 2 140.76 119.87 27.96 o 8 7 2 9.44 48.64 23.74 o 9 7 2 209.77 221.75 36.00 o -7 8 2 24.65 34.47 23.74 o -6 8 2 53.10 31.02 22.60 o -5 8 2 2.64 0.00 14.55 o -4 8 2 11.10 14.17 13.54 o -3 8 2 26.55 8.68 13.26 o -2 8 2 130.59 143.98 19.49 o -1 8 2 274.33 301.26 30.64 o 0 8 2 24.48 13.57 20.87 o 1 8 2 259.32 231.33 23.94 o 2 8 2 3.72 0.00 12.84 o 3 8 2 206.22 189.01 20.65 o 4 8 2 165.22 180.38 31.02 o 5 8 2 0.61 3.83 18.38 o 6 8 2 6.48 11.87 21.06 o 7 8 2 7.91 21.06 22.98 o -5 9 2 39.23 33.70 23.36 o -4 9 2 11.54 25.28 21.83 o -3 9 2 72.85 71.84 18.54 o -2 9 2 317.67 347.58 29.36 o -1 9 2 427.43 417.35 32.34 o 0 9 2 133.36 160.30 22.94 o 1 9 2 14.51 0.00 14.35 o 2 9 2 263.54 309.69 28.35 o 3 9 2 14.48 22.21 22.60 o 4 9 2 4.37 17.23 22.60 o 5 9 2 14.36 4.21 21.45 o -12 1 3 1.88 0.00 7.82 o -11 1 3 103.70 126.32 15.24 o -10 1 3 8.88 1.60 6.17 o -9 1 3 43.03 23.94 5.03 o -8 1 3 9.19 6.26 4.20 o -7 1 3 134.58 110.20 6.46 o -6 1 3 36.70 39.86 4.18 o -5 1 3 117.75 78.04 5.83 o -4 1 3 103.49 98.11 4.83 o -3 1 3 5791.32 5445.57 80.54 o -2 1 3 13585.28 13710.18 169.17 o -1 1 3 20.59 40.10 2.26 o 0 1 3 8667.66 8996.70 128.95 o 1 1 3 7115.22 7228.23 93.95 o 2 1 3 5562.20 5646.14 83.22 o 3 1 3 3553.04 3787.11 66.17 o 4 1 3 239.03 260.14 7.26 o 5 1 3 708.29 720.28 14.45 o 6 1 3 34.66 21.80 4.08 o 7 1 3 272.85 271.03 9.51 o 8 1 3 96.97 113.95 7.63 o 9 1 3 260.18 267.67 13.21 o 10 1 3 538.67 562.56 18.88 o 11 1 3 126.29 120.48 19.53 o 12 1 3 176.19 202.49 26.04 o -12 2 3 35.52 11.52 11.47 o -11 2 3 1.19 0.00 12.13 o -10 2 3 98.74 91.78 7.88 o -9 2 3 77.67 72.77 6.39 o -8 2 3 76.52 75.77 5.99 o -7 2 3 24.91 31.85 4.29 o -6 2 3 49.31 43.08 5.20 o -5 2 3 94.01 94.07 9.29 o -4 2 3 1336.63 1367.68 24.13 o -3 2 3 1881.44 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