#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:45:54 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181287 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/65/2236555.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236555_Fobs loop_ _publ_author_name 'Khan, Ashraf Y.' 'Fathima, Nikhath' 'Kalashetti, Mallikarjun B.' 'Begum, Noor Shahina' 'Khazi, I. M.' _publ_section_title ; 2-Amino-4-methyl-4,5,6,7-tetrahydro-1-benzothiophene-3-carbonitrile ; _journal_coeditor_code PV2585 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3025 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.221 _cell_angle_gamma 90.000 _cell_length_a 9.6771 _cell_length_b 7.6364 _cell_length_c 13.8156 _exptl_crystal_F_000 408.00 _reflns_d_resolution_high 0.7828 _cod_data_source_file pv2585Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' CHEM_AshrafK_2Megw_01_0m in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 120.09 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1637.50 1673.29 30.18 o 3 0 0 10.45 10.77 1.12 o 4 0 0 2.37 1.57 0.43 o 5 0 0 87.15 71.00 5.13 o 6 0 0 277.92 254.52 13.07 o 7 0 0 293.01 283.03 4.49 o 8 0 0 4.18 5.45 1.20 o 9 0 0 17.56 18.00 1.82 o 10 0 0 4.02 2.61 1.15 o 11 0 0 10.83 12.12 2.69 o 12 0 0 1.94 2.92 2.13 o 1 1 0 147.44 153.25 2.46 o 2 1 0 13461.88 10203.64 413.86 o 3 1 0 3141.61 3035.57 47.96 o 4 1 0 121.60 101.38 2.11 o 5 1 0 1.05 1.76 0.40 o 6 1 0 7.43 6.26 0.60 o 7 1 0 0.00 0.00 0.30 o 8 1 0 0.23 0.22 0.44 o 9 1 0 6.99 8.74 0.86 o 10 1 0 0.10 0.00 0.82 o 11 1 0 0.26 0.09 1.10 o 12 1 0 5.44 3.01 1.47 o 0 2 0 62.05 61.20 1.57 o 1 2 0 143.09 140.38 2.41 o 2 2 0 5483.41 5266.52 65.94 o 3 2 0 1179.79 1198.65 10.99 o 4 2 0 2650.18 2695.21 20.85 o 5 2 0 1465.57 1415.35 10.60 o 6 2 0 82.91 97.90 1.59 o 7 2 0 239.60 247.51 3.36 o 8 2 0 19.19 19.43 1.29 o 9 2 0 38.46 46.68 1.82 o 10 2 0 6.99 6.82 1.23 o 11 2 0 1.56 1.97 1.99 o 1 3 0 1.13 3.22 0.29 o 2 3 0 1329.34 1384.15 9.42 o 3 3 0 241.61 287.95 2.83 o 4 3 0 29.92 29.29 0.92 o 5 3 0 356.58 386.60 4.17 o 6 3 0 87.01 82.56 1.71 o 7 3 0 64.73 61.06 1.89 o 8 3 0 9.01 10.16 1.07 o 9 3 0 1.23 0.84 0.71 o 10 3 0 19.98 17.30 3.02 o 11 3 0 0.19 2.36 1.35 o 0 4 0 1430.63 1467.89 15.35 o 1 4 0 70.02 80.88 1.19 o 2 4 0 669.07 651.33 6.48 o 3 4 0 47.89 37.19 0.91 o 4 4 0 76.72 78.26 1.41 o 5 4 0 280.67 276.33 3.17 o 6 4 0 40.14 37.07 1.34 o 7 4 0 410.46 402.49 5.72 o 8 4 0 14.10 15.93 1.32 o 9 4 0 151.21 144.87 3.40 o 10 4 0 37.17 38.05 2.12 o 11 4 0 5.34 7.52 2.58 o 1 5 0 306.13 316.54 2.80 o 2 5 0 40.47 37.08 0.93 o 3 5 0 0.37 0.00 0.30 o 4 5 0 0.81 0.00 0.35 o 5 5 0 19.53 19.21 1.08 o 6 5 0 23.38 19.31 1.32 o 7 5 0 33.67 29.98 1.70 o 8 5 0 42.17 35.66 2.26 o 9 5 0 5.95 6.27 1.05 o 10 5 0 0.10 0.00 0.78 o 0 6 0 300.39 314.50 9.87 o 1 6 0 212.31 210.10 3.50 o 2 6 0 95.82 103.03 1.87 o 3 6 0 420.30 412.14 4.34 o 4 6 0 14.71 19.47 1.21 o 5 6 0 246.99 227.73 3.14 o 6 6 0 0.64 0.71 0.60 o 7 6 0 44.29 40.21 2.56 o 8 6 0 0.46 0.59 0.76 o 9 6 0 17.90 19.13 1.63 o 1 7 0 63.88 65.00 2.45 o 2 7 0 0.14 0.27 0.58 o 3 7 0 2.45 1.40 0.73 o 4 7 0 5.69 4.69 0.92 o 5 7 0 1.04 0.85 1.12 o 6 7 0 5.58 4.47 0.96 o 7 7 0 0.18 0.48 0.79 o 8 7 0 1.03 0.90 0.89 o 0 8 0 101.86 104.14 4.00 o 1 8 0 6.57 6.32 0.98 o 2 8 0 76.09 73.16 2.35 o 3 8 0 18.58 18.81 1.79 o 4 8 0 29.40 33.58 2.22 o 5 8 0 28.22 20.42 3.37 o 6 8 0 0.31 3.25 2.02 o 1 9 0 4.86 4.71 1.00 o 2 9 0 1.47 1.48 0.90 o 3 9 0 0.08 0.41 1.54 o 4 9 0 0.04 0.45 1.68 o -12 1 1 0.62 0.83 1.96 o -11 1 1 26.03 23.21 1.90 o -10 1 1 66.44 70.26 2.24 o -9 1 1 61.67 65.33 2.04 o -8 1 1 246.16 232.71 3.29 o -7 1 1 53.13 48.65 1.20 o -6 1 1 381.76 387.98 3.79 o -5 1 1 12.90 11.92 0.60 o -4 1 1 2460.97 2443.71 19.48 o -3 1 1 23.20 39.99 1.39 o -2 1 1 14421.45 10551.54 717.11 o -1 1 1 504.66 551.74 10.32 o 0 1 1 5756.72 4911.68 62.43 o 1 1 1 679.89 703.28 7.46 o 2 1 1 1235.20 1287.40 16.57 o 3 1 1 3182.42 3101.90 31.14 o 4 1 1 21.43 11.63 0.58 o 5 1 1 466.67 436.15 4.38 o 6 1 1 58.08 56.89 1.15 o 7 1 1 3.03 3.20 0.50 o 8 1 1 0.09 0.00 0.39 o 9 1 1 6.88 7.00 0.95 o 10 1 1 17.36 19.85 1.81 o 11 1 1 6.22 9.36 1.23 o -12 2 1 12.92 9.98 2.69 o -11 2 1 9.26 6.94 1.61 o -10 2 1 4.02 2.95 0.86 o -9 2 1 2.96 2.75 0.65 o -8 2 1 7.80 7.90 0.68 o -7 2 1 70.57 70.18 1.45 o -6 2 1 16.05 14.95 0.76 o -5 2 1 938.56 1016.16 7.95 o -4 2 1 288.81 313.18 5.18 o -3 2 1 1.71 2.22 0.38 o -2 2 1 129.85 118.76 2.38 o -1 2 1 450.85 493.60 6.78 o 0 2 1 4.91 1.24 0.13 o 1 2 1 94.35 100.39 1.56 o 2 2 1 2.49 4.84 0.43 o 3 2 1 435.83 468.35 4.44 o 4 2 1 785.82 814.06 8.05 o 5 2 1 686.46 755.13 6.15 o 6 2 1 30.14 29.39 0.89 o 7 2 1 1.81 2.14 0.50 o 8 2 1 2.15 2.33 0.57 o 9 2 1 1.32 1.70 0.86 o 10 2 1 29.92 25.55 2.02 o 11 2 1 1.64 0.93 0.99 o -11 3 1 21.12 21.26 2.30 o -10 3 1 3.30 3.26 0.88 o -9 3 1 204.56 192.81 5.31 o -8 3 1 61.59 66.53 2.08 o -7 3 1 444.84 439.79 4.98 o -6 3 1 895.12 958.29 17.39 o -5 3 1 10.96 11.17 0.72 o -4 3 1 1097.90 1161.03 9.82 o -3 3 1 1101.20 1152.40 9.57 o -2 3 1 686.03 677.60 6.51 o -1 3 1 196.27 195.44 1.85 o 0 3 1 2302.94 2347.08 15.23 o 1 3 1 378.12 355.27 4.43 o 2 3 1 10.68 4.85 0.62 o 3 3 1 27.04 15.18 0.54 o 4 3 1 55.86 66.41 1.35 o 5 3 1 476.09 463.22 4.39 o 6 3 1 1.19 1.47 0.54 o 7 3 1 219.11 223.76 3.71 o 8 3 1 254.48 263.05 4.32 o 9 3 1 0.41 0.00 0.73 o 10 3 1 34.23 30.87 2.27 o 11 3 1 0.82 0.70 0.92 o -11 4 1 2.39 0.75 1.46 o -10 4 1 0.04 0.00 0.82 o -9 4 1 6.33 3.28 1.01 o -8 4 1 63.13 58.25 2.42 o -7 4 1 0.73 0.00 0.62 o -6 4 1 0.86 0.42 0.47 o -5 4 1 9.69 8.61 0.71 o -4 4 1 261.92 271.90 3.01 o -3 4 1 153.78 175.52 2.15 o -2 4 1 2.40 2.68 0.29 o -1 4 1 316.38 385.32 3.30 o 0 4 1 0.24 0.16 0.21 o 1 4 1 691.18 769.95 5.67 o 2 4 1 60.05 58.63 0.93 o 3 4 1 87.35 93.61 1.27 o 4 4 1 8.24 8.62 0.56 o 5 4 1 72.16 75.70 1.67 o 6 4 1 290.45 269.24 4.23 o 7 4 1 8.71 9.36 1.17 o 8 4 1 21.67 18.33 1.39 o 9 4 1 4.82 2.62 0.95 o 10 4 1 0.23 0.00 0.65 o -10 5 1 10.41 10.10 1.32 o -9 5 1 40.82 41.61 2.29 o -8 5 1 27.46 29.65 1.79 o -7 5 1 53.32 49.78 1.92 o -6 5 1 28.90 31.37 1.48 o -5 5 1 132.84 122.78 4.16 o -4 5 1 538.66 532.30 5.60 o -3 5 1 3.02 2.56 0.37 o -2 5 1 237.18 236.04 2.34 o -1 5 1 115.41 117.58 1.97 o 0 5 1 0.04 0.00 0.24 o 1 5 1 548.63 544.77 4.55 o 2 5 1 10.28 9.09 0.72 o 3 5 1 826.99 840.68 6.62 o 4 5 1 104.69 99.50 1.78 o 5 5 1 118.66 110.56 2.66 o 6 5 1 81.01 84.61 2.32 o 7 5 1 41.81 42.13 2.11 o 8 5 1 12.21 14.07 1.34 o 9 5 1 11.11 10.35 1.68 o 10 5 1 14.42 17.19 1.59 o -9 6 1 5.16 4.65 1.05 o -8 6 1 14.55 14.25 1.40 o -7 6 1 2.99 2.04 0.79 o -6 6 1 0.08 0.14 0.46 o -5 6 1 0.22 0.00 0.40 o -4 6 1 32.68 32.22 1.33 o -3 6 1 1.56 0.54 0.45 o -2 6 1 275.81 272.57 4.49 o -1 6 1 3.39 2.94 0.66 o 0 6 1 4.31 6.83 0.79 o 1 6 1 16.97 15.13 0.95 o 2 6 1 1.16 1.13 0.42 o 3 6 1 3.75 7.49 0.72 o 4 6 1 6.90 6.43 0.67 o 5 6 1 6.90 5.13 0.83 o 6 6 1 3.73 3.37 0.79 o 7 6 1 2.92 2.07 0.78 o 8 6 1 10.26 7.62 1.34 o 9 6 1 2.51 1.61 0.92 o -8 7 1 5.51 4.13 1.21 o -7 7 1 20.94 20.02 2.21 o -6 7 1 52.10 65.04 3.17 o -5 7 1 1.83 0.58 1.00 o -4 7 1 1.53 2.50 0.81 o -3 7 1 11.06 10.49 1.21 o -2 7 1 156.94 150.39 3.18 o -1 7 1 111.24 118.45 2.75 o 0 7 1 182.30 171.98 3.38 o 1 7 1 236.90 228.44 3.95 o 2 7 1 1.78 0.76 0.59 o 3 7 1 159.47 150.97 3.16 o 4 7 1 22.43 23.80 1.79 o 5 7 1 62.35 56.38 2.23 o 6 7 1 53.91 60.50 2.47 o 7 7 1 2.13 1.87 0.83 o 8 7 1 12.07 13.64 1.68 o -7 8 1 2.89 0.45 1.80 o -6 8 1 23.60 21.09 3.48 o -5 8 1 1.05 1.76 1.13 o -4 8 1 4.04 3.78 1.03 o -3 8 1 0.03 0.63 0.84 o -2 8 1 22.78 20.02 1.77 o -1 8 1 30.98 28.91 1.75 o 0 8 1 14.81 16.82 1.38 o 1 8 1 2.05 1.75 0.72 o 2 8 1 28.15 31.14 2.74 o 3 8 1 0.55 1.30 0.71 o 4 8 1 8.15 7.97 2.36 o 5 8 1 0.74 2.24 1.80 o 6 8 1 0.93 2.58 1.80 o -4 9 1 75.36 77.32 3.12 o -3 9 1 12.18 9.36 1.42 o -2 9 1 20.27 20.86 1.89 o -1 9 1 26.03 30.88 1.96 o 0 9 1 0.01 0.05 0.65 o 1 9 1 20.47 21.86 1.66 o 2 9 1 6.44 5.89 1.06 o 3 9 1 24.89 24.46 3.81 o 4 9 1 7.85 7.52 2.47 o -12 0 2 38.56 38.66 5.33 o -11 0 2 9.09 9.58 2.02 o -10 0 2 114.03 110.52 3.10 o -9 0 2 0.57 0.00 0.67 o -8 0 2 241.33 259.36 5.54 o -7 0 2 170.81 161.68 3.93 o -6 0 2 153.75 152.80 3.58 o -5 0 2 118.23 118.00 2.80 o -4 0 2 694.17 682.85 9.53 o -3 0 2 504.91 498.34 10.43 o -2 0 2 5768.15 5418.92 94.46 o -1 0 2 151.24 157.06 3.70 o 0 0 2 2707.26 2422.03 42.29 o 1 0 2 297.87 330.45 9.48 o 2 0 2 2265.75 2068.33 26.10 o 3 0 2 777.32 834.12 16.38 o 4 0 2 1068.43 1156.55 22.16 o 5 0 2 325.62 351.73 6.13 o 6 0 2 29.91 24.16 1.17 o 7 0 2 248.95 246.07 5.38 o 8 0 2 10.24 8.95 2.08 o 9 0 2 14.74 16.03 1.85 o 10 0 2 0.00 0.50 1.03 o 11 0 2 2.84 1.12 1.19 o -12 1 2 1.31 0.00 0.78 o -11 1 2 7.11 6.72 1.06 o -10 1 2 0.92 1.67 0.70 o -9 1 2 0.52 1.31 0.55 o -8 1 2 7.39 7.94 0.73 o -7 1 2 70.95 70.32 1.47 o -6 1 2 40.56 40.31 1.22 o -5 1 2 141.89 147.96 1.89 o -4 1 2 283.43 298.81 2.84 o -3 1 2 119.62 108.16 1.96 o -2 1 2 1557.14 1597.80 28.78 o -1 1 2 407.69 416.22 8.41 o 0 1 2 998.24 974.82 12.36 o 1 1 2 193.69 170.42 1.90 o 2 1 2 2937.75 2985.56 39.53 o 3 1 2 249.23 291.06 3.46 o 4 1 2 4.81 7.78 0.58 o 5 1 2 20.86 19.15 0.84 o 6 1 2 32.66 43.11 1.21 o 7 1 2 37.33 44.07 1.96 o 8 1 2 1.13 0.74 0.55 o 9 1 2 0.40 0.35 0.65 o 10 1 2 0.10 0.00 0.68 o 11 1 2 11.54 10.76 1.52 o -12 2 2 1.24 1.23 1.19 o -11 2 2 41.14 41.16 2.48 o -10 2 2 68.13 72.73 2.74 o -9 2 2 35.78 34.85 1.43 o -8 2 2 136.56 138.56 2.25 o -7 2 2 7.05 8.91 0.65 o -6 2 2 382.22 392.00 3.91 o -5 2 2 349.60 310.47 3.16 o -4 2 2 1388.59 1436.92 11.73 o -3 2 2 820.71 845.37 7.16 o -2 2 2 4.65 3.60 0.71 o -1 2 2 244.31 260.51 4.02 o 0 2 2 1951.45 1895.50 19.32 o 1 2 2 1085.41 1076.72 14.48 o 2 2 2 122.83 121.43 2.30 o 3 2 2 218.11 183.60 2.04 o 4 2 2 0.15 2.20 0.57 o 5 2 2 0.06 1.25 0.72 o 6 2 2 54.41 51.77 1.32 o 7 2 2 74.38 72.34 1.70 o 8 2 2 43.61 45.49 1.67 o 9 2 2 146.14 155.42 3.94 o 10 2 2 1.27 0.17 0.74 o 11 2 2 12.35 13.12 1.68 o -11 3 2 0.25 0.00 1.17 o -10 3 2 1.19 1.46 0.89 o -9 3 2 7.15 7.39 1.75 o -8 3 2 43.97 46.08 1.51 o -7 3 2 66.69 69.49 2.17 o -6 3 2 1.17 0.67 0.41 o -5 3 2 43.90 52.59 1.47 o -4 3 2 1.40 1.88 0.38 o -3 3 2 0.88 0.00 0.28 o -2 3 2 67.04 67.44 1.32 o -1 3 2 20.62 36.34 0.71 o 0 3 2 179.32 166.74 1.57 o 1 3 2 182.16 185.20 2.59 o 2 3 2 40.26 40.36 1.23 o 3 3 2 266.04 295.53 2.98 o 4 3 2 54.07 50.45 1.42 o 5 3 2 12.98 10.28 0.73 o 6 3 2 36.82 38.66 1.49 o 7 3 2 58.46 54.95 1.85 o 8 3 2 3.59 3.02 0.77 o 9 3 2 13.10 12.24 1.45 o 10 3 2 1.64 2.11 1.01 o 11 3 2 2.96 1.29 1.04 o -11 4 2 2.56 1.63 2.24 o -10 4 2 5.85 5.39 1.43 o -9 4 2 43.86 36.75 2.82 o -8 4 2 101.08 98.36 2.22 o -7 4 2 70.52 68.60 1.83 o -6 4 2 659.72 657.30 6.69 o -5 4 2 267.43 282.79 3.54 o -4 4 2 18.84 15.77 0.91 o -3 4 2 328.14 343.82 3.73 o -2 4 2 1.61 1.49 0.30 o -1 4 2 340.23 330.67 3.33 o 0 4 2 150.42 164.21 1.94 o 1 4 2 8.62 2.31 0.27 o 2 4 2 422.43 416.11 3.62 o 3 4 2 1.15 1.12 0.27 o 4 4 2 289.58 305.14 3.25 o 5 4 2 0.00 0.00 0.39 o 6 4 2 232.77 223.25 3.84 o 7 4 2 19.17 20.94 1.44 o 8 4 2 17.43 22.89 3.82 o 9 4 2 2.22 1.65 0.80 o 10 4 2 5.15 5.07 1.27 o -10 5 2 5.02 4.98 1.24 o -9 5 2 37.79 40.90 2.52 o -8 5 2 21.20 22.08 1.83 o -7 5 2 4.72 4.45 0.92 o -6 5 2 53.00 50.00 2.30 o -5 5 2 16.62 16.04 0.89 o -4 5 2 432.14 417.09 4.63 o -3 5 2 102.89 108.04 2.67 o -2 5 2 0.03 0.00 0.25 o -1 5 2 84.54 93.94 1.41 o 0 5 2 6.81 4.71 0.51 o 1 5 2 63.07 64.82 1.65 o 2 5 2 25.69 26.81 0.89 o 3 5 2 62.71 70.76 1.36 o 4 5 2 147.08 135.21 2.47 o 5 5 2 6.36 5.55 0.81 o 6 5 2 3.43 1.43 0.64 o 7 5 2 8.12 8.28 1.03 o 8 5 2 0.66 0.57 0.81 o 9 5 2 7.75 7.31 1.15 o 10 5 2 0.48 0.00 1.57 o -9 6 2 0.48 1.02 0.97 o -8 6 2 50.62 57.44 2.61 o -7 6 2 33.57 35.28 2.24 o -6 6 2 8.14 7.58 1.25 o -5 6 2 5.28 4.23 0.73 o -4 6 2 39.30 36.02 1.73 o -3 6 2 35.07 35.28 1.90 o -2 6 2 65.43 68.33 2.46 o -1 6 2 390.35 397.46 4.66 o 0 6 2 40.89 41.71 1.36 o 1 6 2 332.50 325.50 4.08 o 2 6 2 217.33 214.24 2.91 o 3 6 2 28.43 21.31 0.97 o 4 6 2 98.34 93.20 2.54 o 5 6 2 0.02 0.22 0.57 o 6 6 2 16.90 18.44 1.40 o 7 6 2 7.01 8.10 1.10 o 8 6 2 8.44 7.41 1.13 o 9 6 2 15.40 18.58 1.65 o -8 7 2 42.52 44.09 4.82 o -7 7 2 6.89 7.74 2.47 o -6 7 2 40.08 46.80 2.52 o -5 7 2 28.85 28.17 1.91 o -4 7 2 8.32 8.70 1.20 o -3 7 2 35.14 34.94 2.09 o -2 7 2 21.99 19.98 1.59 o -1 7 2 13.95 12.58 1.16 o 0 7 2 75.12 78.59 2.46 o 1 7 2 12.78 13.24 1.26 o 2 7 2 0.35 0.03 0.65 o 3 7 2 0.01 0.04 0.49 o 4 7 2 1.04 0.76 0.73 o 5 7 2 0.59 1.04 0.69 o 6 7 2 10.67 10.55 1.28 o 7 7 2 4.97 5.73 1.06 o 8 7 2 0.72 0.20 0.83 o -7 8 2 0.00 0.00 1.57 o -6 8 2 47.64 53.96 5.27 o -5 8 2 32.56 35.05 2.32 o -4 8 2 24.00 30.04 2.16 o -3 8 2 96.36 111.72 3.43 o -2 8 2 12.54 13.43 1.53 o -1 8 2 15.01 15.77 1.34 o 0 8 2 5.82 6.66 1.00 o 1 8 2 46.12 41.23 2.48 o 2 8 2 0.47 0.00 0.64 o 3 8 2 35.30 30.80 2.74 o 4 8 2 62.91 67.20 5.05 o 5 8 2 1.15 1.46 1.80 o 6 8 2 12.61 11.33 2.80 o -4 9 2 10.22 12.68 1.64 o -3 9 2 9.61 10.47 1.49 o -2 9 2 0.33 2.71 1.08 o -1 9 2 0.41 1.60 0.99 o 0 9 2 4.31 5.03 1.02 o 1 9 2 17.70 19.89 1.65 o 2 9 2 29.71 31.90 2.42 o 3 9 2 3.23 4.80 1.47 o 4 9 2 2.82 3.81 2.02 o -12 1 3 18.14 18.37 1.62 o -11 1 3 0.02 0.00 0.59 o -10 1 3 29.82 28.94 1.36 o -9 1 3 65.01 66.65 1.65 o -8 1 3 2.44 2.11 0.64 o -7 1 3 171.19 161.31 2.93 o -6 1 3 3.05 2.96 0.42 o -5 1 3 405.06 383.58 3.67 o -4 1 3 145.46 138.63 2.05 o -3 1 3 137.12 150.84 1.88 o -2 1 3 1147.26 1042.78 13.84 o -1 1 3 25.80 11.74 3.03 o 0 1 3 2145.03 2009.23 25.14 o 1 1 3 945.78 1052.36 12.88 o 2 1 3 1280.33 1252.33 10.30 o 3 1 3 920.95 971.20 9.40 o 4 1 3 1.01 1.46 0.30 o 5 1 3 562.06 566.23 5.05 o 6 1 3 2.61 4.21 0.49 o 7 1 3 199.99 213.48 3.57 o 8 1 3 26.33 26.97 1.54 o 9 1 3 22.01 20.50 1.30 o 10 1 3 37.26 35.02 1.75 o 11 1 3 0.01 0.00 0.79 o -12 2 3 1.78 2.45 1.05 o -11 2 3 13.99 14.56 1.57 o -10 2 3 26.56 26.61 1.45 o -9 2 3 7.88 7.35 0.87 o -8 2 3 20.79 22.71 1.26 o -7 2 3 23.36 25.75 1.50 o -6 2 3 32.12 34.09 1.55 o -5 2 3 7.35 9.29 0.79 o -4 2 3 42.38 53.43 1.36 o -3 2 3 134.34 135.61 1.82 o -2 2 3 1009.31 1073.44 11.31 o -1 2 3 1302.54 1447.69 19.67 o 0 2 3 808.08 835.61 10.94 o 1 2 3 309.44 340.18 8.13 o 2 2 3 71.11 87.11 1.26 o 3 2 3 115.62 135.72 1.70 o 4 2 3 98.60 102.49 1.52 o 5 2 3 23.70 24.33 1.03 o 6 2 3 9.43 10.87 0.72 o 7 2 3 39.13 38.99 1.25 o 8 2 3 7.04 6.35 0.92 o 9 2 3 3.93 4.63 1.07 o 10 2 3 0.56 1.50 1.52 o 11 2 3 0.13 0.00 0.90 o -11 3 3 1.96 1.74 0.92 o -10 3 3 1.22 0.43 0.84 o -9 3 3 8.22 7.93 0.99 o -8 3 3 121.38 119.62 2.69 o -7 3 3 102.89 103.48 3.14 o -6 3 3 0.31 0.95 0.73 o -5 3 3 78.73 72.13 1.47 o -4 3 3 68.61 71.13 1.60 o -3 3 3 659.32 685.53 6.91 o -2 3 3 1358.91 1367.34 11.08 o -1 3 3 0.10 1.50 0.38 o 0 3 3 2007.05 2081.17 20.94 o 1 3 3 2036.19 2196.14 17.29 o 2 3 3 4.65 9.23 0.41 o 3 3 3 77.70 85.85 1.77 o 4 3 3 102.85 98.81 2.52 o 5 3 3 371.15 354.26 4.64 o 6 3 3 1.79 2.01 0.57 o 7 3 3 166.95 159.57 3.22 o 8 3 3 6.02 6.88 1.10 o 9 3 3 4.20 4.15 1.10 o 10 3 3 15.11 15.63 1.69 o 11 3 3 0.06 0.00 1.68 o -11 4 3 8.11 9.05 1.47 o -10 4 3 1.93 1.49 0.95 o -9 4 3 1.97 2.16 0.90 o -8 4 3 2.46 2.13 0.67 o -7 4 3 0.70 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