#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:45:54 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181287 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/65/2236575.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236575_Fobs loop_ _publ_author_name 'Lu, Tao' 'Liao, Xiao-Jian' 'Liang, Yuan-Wei' 'Xu, Shi-Hai' _publ_section_title ; 2-Carbamoyl-3,4,5,6-tetrafluorobenzoic acid ; _journal_coeditor_code RK2367 _journal_issue 10 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2864 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.086 _cell_angle_gamma 90.000 _cell_length_a 14.5872 _cell_length_b 6.9193 _cell_length_c 8.6129 _exptl_crystal_F_000 472.00 _reflns_d_resolution_high 0.8676 _cod_data_source_file rk2367Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title 'LUTAO_0329 in P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 70.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 935.42 870.76 5.95 o 5 0 0 1981.20 1578.12 9.17 o 8 0 0 5013.94 4820.37 21.88 o 9 0 0 240.73 249.49 3.76 o 10 0 0 1364.54 1331.38 12.59 o 11 0 0 540.91 528.48 8.45 o 12 0 0 126.30 145.53 4.62 o 13 0 0 227.42 213.03 5.61 o 14 0 0 675.46 689.38 9.75 o 15 0 0 1.22 1.71 0.72 o 16 0 0 96.59 103.87 3.47 o 1 1 0 306.59 310.32 6.18 o 2 1 0 213.43 220.40 1.61 o 3 1 0 922.16 798.64 5.90 o 4 1 0 1115.37 968.77 12.05 o 5 1 0 1521.96 1307.84 7.28 o 6 1 0 196.58 157.94 2.82 o 7 1 0 324.27 304.90 10.63 o 8 1 0 0.57 4.54 3.02 o 9 1 0 537.52 556.93 7.27 o 10 1 0 34.21 43.11 1.20 o 11 1 0 5.26 7.09 1.40 o 12 1 0 30.81 35.77 2.48 o 13 1 0 3.88 4.61 1.10 o 14 1 0 600.61 572.40 9.32 o 15 1 0 128.74 121.65 4.02 o 16 1 0 54.78 63.36 1.87 o 2 2 0 901.04 844.89 28.45 o 3 2 0 72.69 81.50 8.53 o 4 2 0 0.02 4.99 1.63 o 5 2 0 196.14 183.48 3.84 o 6 2 0 437.87 325.57 5.62 o 7 2 0 182.40 178.26 20.17 o 8 2 0 0.06 0.56 0.39 o 9 2 0 358.98 361.12 3.19 o 10 2 0 6.94 9.13 0.83 o 11 2 0 197.47 219.98 5.93 o 12 2 0 725.61 757.17 11.14 o 13 2 0 96.85 100.92 4.12 o 14 2 0 4.76 7.26 1.04 o 15 2 0 4.62 4.69 0.55 o 1 3 0 1405.97 1368.12 9.34 o 2 3 0 1103.22 1205.90 35.26 o 3 3 0 257.64 272.45 8.18 o 4 3 0 1111.08 1198.39 9.87 o 5 3 0 34.16 57.12 2.39 o 6 3 0 160.72 149.45 4.21 o 7 3 0 1086.97 1044.15 15.35 o 8 3 0 743.27 718.59 5.53 o 9 3 0 467.13 468.37 5.51 o 10 3 0 405.77 415.11 5.37 o 11 3 0 698.91 690.58 10.38 o 12 3 0 3.36 2.16 1.00 o 13 3 0 78.13 87.10 2.12 o 14 3 0 6.94 7.49 0.83 o 15 3 0 27.37 27.34 1.21 o 0 4 0 20.61 21.24 1.49 o 1 4 0 142.34 119.63 3.28 o 2 4 0 188.46 215.87 4.23 o 3 4 0 764.44 821.97 8.04 o 4 4 0 157.58 164.00 4.18 o 5 4 0 98.08 84.12 2.05 o 6 4 0 123.83 107.28 3.71 o 7 4 0 18.13 18.88 1.72 o 8 4 0 117.85 118.16 4.19 o 9 4 0 0.46 2.29 1.00 o 10 4 0 728.18 772.95 10.20 o 11 4 0 27.08 33.24 1.73 o 12 4 0 163.03 170.08 3.59 o 13 4 0 20.10 22.89 1.28 o 14 4 0 4.44 6.92 1.05 o 1 5 0 173.03 190.55 8.67 o 2 5 0 4.45 7.29 0.89 o 3 5 0 33.90 32.41 1.28 o 4 5 0 22.65 25.54 1.30 o 5 5 0 155.74 164.08 5.71 o 6 5 0 680.97 737.32 7.70 o 7 5 0 151.16 159.55 3.74 o 8 5 0 118.17 117.54 4.75 o 9 5 0 106.17 105.09 4.52 o 10 5 0 33.68 38.51 2.75 o 11 5 0 12.53 9.87 1.45 o 12 5 0 57.13 72.10 3.25 o 0 6 0 1772.35 1931.65 18.13 o 1 6 0 727.49 775.42 8.09 o 2 6 0 236.70 251.86 4.61 o 3 6 0 0.44 1.88 1.59 o 4 6 0 11.80 12.16 1.12 o 5 6 0 318.44 299.94 8.38 o 6 6 0 0.22 0.31 1.30 o 7 6 0 235.32 201.68 7.00 o 8 6 0 313.08 289.73 8.12 o 9 6 0 6.20 9.37 1.01 o 10 6 0 45.01 42.71 1.80 o 1 7 0 17.09 20.23 1.32 o 2 7 0 190.95 195.77 3.69 o 3 7 0 0.03 0.99 1.04 o 4 7 0 23.23 29.50 2.40 o 5 7 0 5.70 5.78 1.29 o 6 7 0 19.71 21.81 2.06 o 7 7 0 6.90 8.10 1.33 o -16 1 1 143.67 146.97 2.86 o -15 1 1 160.93 156.15 5.10 o -14 1 1 42.66 42.31 2.65 o -13 1 1 0.03 4.23 1.10 o -12 1 1 500.90 507.00 8.81 o -11 1 1 9.50 9.11 0.86 o -10 1 1 294.52 311.66 3.11 o -9 1 1 40.35 47.71 2.08 o -8 1 1 233.89 247.06 9.58 o -7 1 1 228.22 241.23 7.17 o -5 1 1 5.23 3.32 1.01 o -4 1 1 136.69 132.75 11.81 o -3 1 1 366.59 372.23 5.48 o -1 1 1 4.52 4.87 0.42 o 0 1 1 545.91 519.16 3.63 o 1 1 1 678.35 632.46 3.94 o 3 1 1 380.49 347.99 15.13 o 4 1 1 1194.53 1094.45 20.11 o 5 1 1 857.67 697.20 4.39 o 6 1 1 0.01 5.30 3.32 o 7 1 1 405.83 443.49 8.21 o 8 1 1 3.24 9.47 2.88 o 9 1 1 329.40 328.16 3.16 o 10 1 1 0.76 1.34 0.49 o 11 1 1 140.63 148.72 2.67 o 12 1 1 459.12 438.99 8.53 o 13 1 1 38.02 32.31 2.40 o 14 1 1 58.13 55.25 2.90 o 15 1 1 3.21 5.83 1.01 o 16 1 1 19.21 20.92 1.53 o -16 2 1 57.32 62.36 2.62 o -15 2 1 151.91 159.59 3.14 o -14 2 1 121.03 129.18 2.56 o -13 2 1 107.17 110.51 2.47 o -12 2 1 1572.50 1603.53 15.99 o -11 2 1 427.53 442.17 8.14 o -10 2 1 227.01 221.36 5.55 o -9 2 1 45.59 52.54 2.39 o -8 2 1 65.38 62.43 2.95 o -7 2 1 1437.45 1286.66 33.66 o -6 2 1 10.35 4.60 0.90 o -5 2 1 473.69 504.16 11.11 o -3 2 1 126.62 147.90 3.02 o -2 2 1 327.50 291.22 2.62 o -1 2 1 15.44 17.80 1.27 o 0 2 1 2.74 5.19 1.59 o 2 2 1 42.26 48.14 0.92 o 4 2 1 1160.52 1020.55 14.94 o 5 2 1 685.80 599.51 4.32 o 6 2 1 152.39 160.76 4.03 o 7 2 1 240.88 228.76 5.20 o 8 2 1 114.18 114.91 1.97 o 9 2 1 0.05 1.34 0.42 o 10 2 1 35.97 40.57 1.34 o 11 2 1 0.21 -0.22 1.00 o 12 2 1 116.24 120.33 4.59 o 13 2 1 0.94 2.94 1.04 o 14 2 1 42.11 39.87 2.46 o 15 2 1 168.96 188.11 3.22 o -15 3 1 13.70 11.02 0.84 o -14 3 1 363.76 360.35 4.95 o -13 3 1 209.91 216.97 3.34 o -12 3 1 301.70 307.50 4.09 o -11 3 1 98.80 103.27 2.40 o -10 3 1 144.52 148.16 3.28 o -9 3 1 204.14 204.06 3.66 o -8 3 1 658.95 635.12 5.15 o -7 3 1 109.39 116.05 6.15 o -6 3 1 347.86 330.62 6.40 o -5 3 1 232.81 287.41 5.52 o -4 3 1 918.71 942.40 9.22 o -3 3 1 206.91 244.86 4.07 o -2 3 1 1.18 5.16 0.55 o -1 3 1 2082.60 1984.19 11.55 o 1 3 1 68.66 87.34 2.12 o 3 3 1 2449.11 2536.48 8.32 o 4 3 1 1572.89 1590.41 9.70 o 5 3 1 822.81 844.03 5.59 o 6 3 1 6.29 9.01 1.43 o 7 3 1 27.12 28.92 1.05 o 8 3 1 256.43 249.72 4.10 o 9 3 1 1339.11 1318.45 9.44 o 11 3 1 65.17 67.57 2.26 o 12 3 1 72.43 75.39 3.51 o 13 3 1 20.74 21.95 1.88 o 14 3 1 224.38 230.02 3.03 o -14 4 1 2.11 1.66 0.69 o -13 4 1 213.68 237.55 6.07 o -12 4 1 950.67 966.55 13.08 o -11 4 1 78.54 98.31 14.19 o -10 4 1 283.75 292.75 4.85 o -9 4 1 53.92 58.49 3.42 o -8 4 1 111.22 101.27 4.30 o -7 4 1 51.49 51.73 2.06 o -6 4 1 0.06 1.27 0.47 o -5 4 1 3505.20 3334.43 14.04 o -4 4 1 276.06 294.89 3.91 o -3 4 1 23.68 25.74 1.52 o -2 4 1 105.59 106.87 3.19 o -1 4 1 1.90 22.18 1.47 o 0 4 1 18.12 19.79 1.46 o 1 4 1 135.48 122.96 4.97 o 2 4 1 26.04 26.86 1.46 o 3 4 1 241.36 213.55 4.17 o 4 4 1 235.24 240.72 2.78 o 5 4 1 1.47 1.89 0.48 o 6 4 1 52.85 52.58 1.80 o 7 4 1 11.08 12.68 0.96 o 8 4 1 13.85 16.22 1.11 o 9 4 1 18.48 15.77 1.76 o 10 4 1 506.52 514.02 6.07 o 11 4 1 144.34 147.56 4.47 o 12 4 1 310.57 308.05 4.69 o 13 4 1 6.45 9.84 0.87 o -13 5 1 29.77 28.60 1.87 o -12 5 1 30.08 36.89 1.73 o -11 5 1 83.67 99.62 5.26 o -10 5 1 5.97 7.30 1.40 o -9 5 1 79.36 66.20 3.65 o -8 5 1 17.36 16.71 1.92 o -7 5 1 45.49 36.09 2.66 o -6 5 1 17.11 15.26 1.36 o -5 5 1 403.33 403.66 8.78 o -4 5 1 145.22 132.39 5.23 o -3 5 1 31.53 30.78 2.56 o -2 5 1 0.04 0.71 0.86 o -1 5 1 693.20 725.45 12.68 o 0 5 1 80.71 85.71 2.55 o 1 5 1 29.96 56.02 17.20 o 2 5 1 219.78 238.12 4.29 o 3 5 1 129.57 132.38 2.96 o 4 5 1 169.65 178.04 3.47 o 5 5 1 171.01 168.44 3.41 o 6 5 1 80.78 84.22 2.45 o 7 5 1 66.94 66.27 1.84 o 8 5 1 0.01 2.04 0.81 o 9 5 1 13.36 13.25 1.19 o 10 5 1 69.58 70.22 3.57 o 11 5 1 52.58 56.68 3.01 o 12 5 1 1.16 1.09 0.68 o -10 6 1 21.46 25.03 1.42 o -9 6 1 154.27 143.41 3.55 o -8 6 1 31.70 28.56 2.14 o -7 6 1 322.57 275.03 7.96 o -6 6 1 135.18 134.64 5.65 o -5 6 1 59.18 48.40 3.46 o -4 6 1 25.35 25.45 2.57 o -3 6 1 33.96 38.67 3.03 o -2 6 1 509.04 527.77 10.27 o -1 6 1 1225.98 1323.53 10.30 o 0 6 1 605.19 633.88 7.27 o 1 6 1 619.71 652.93 8.53 o 2 6 1 253.84 258.56 6.71 o 3 6 1 145.80 155.88 5.43 o 4 6 1 95.81 88.33 2.74 o 5 6 1 30.03 35.98 1.76 o 6 6 1 303.58 283.25 4.58 o 7 6 1 76.22 61.36 3.90 o 8 6 1 175.76 158.90 5.97 o 9 6 1 195.29 204.49 6.39 o 10 6 1 20.36 25.65 2.20 o -7 7 1 45.55 43.35 2.69 o -6 7 1 1.97 5.33 1.27 o -5 7 1 1.81 1.75 1.03 o -4 7 1 30.03 29.57 2.54 o -3 7 1 237.45 229.79 6.41 o -2 7 1 90.33 94.50 4.14 o -1 7 1 113.63 119.18 4.50 o 0 7 1 295.12 296.91 6.72 o 1 7 1 76.39 87.40 2.49 o 2 7 1 2.28 3.02 0.69 o 3 7 1 107.93 112.55 2.76 o 4 7 1 2.76 2.29 0.59 o 5 7 1 14.84 8.88 1.45 o 6 7 1 20.49 18.61 1.82 o 7 7 1 61.34 49.35 2.73 o -16 0 2 1.35 1.11 0.66 o -15 0 2 436.66 441.38 7.97 o -14 0 2 15.15 17.50 1.82 o -13 0 2 24.13 19.92 1.89 o -12 0 2 1.54 1.32 0.72 o -11 0 2 777.44 791.43 10.23 o -10 0 2 441.06 467.79 5.41 o -9 0 2 98.71 102.35 3.50 o -8 0 2 368.46 349.05 5.91 o -7 0 2 5.94 10.99 1.04 o -6 0 2 38.51 53.55 2.03 o -5 0 2 11.49 11.75 1.65 o 1 0 2 1631.08 1372.06 7.98 o 2 0 2 752.27 731.81 6.25 o 3 0 2 163.59 167.38 3.25 o 4 0 2 38.95 43.29 1.76 o 6 0 2 17.08 13.21 2.18 o 7 0 2 94.69 136.83 3.64 o 8 0 2 382.50 407.75 5.06 o 9 0 2 512.51 530.21 5.89 o 10 0 2 825.66 860.46 11.26 o 11 0 2 240.24 278.64 6.76 o 12 0 2 1323.67 1201.56 13.60 o 13 0 2 479.00 443.00 8.00 o 14 0 2 259.09 233.72 5.38 o 15 0 2 14.52 14.13 1.22 o -16 1 2 64.42 66.97 1.94 o -15 1 2 273.99 273.75 4.35 o -14 1 2 128.01 138.60 3.33 o -13 1 2 29.25 28.09 1.30 o -12 1 2 679.31 698.36 7.44 o -11 1 2 376.73 366.62 4.98 o -10 1 2 1141.02 1190.27 5.50 o -9 1 2 6.16 4.96 0.45 o -8 1 2 67.78 66.20 1.55 o -7 1 2 467.83 491.34 3.86 o -6 1 2 176.26 158.83 2.03 o -4 1 2 643.35 700.48 3.48 o -1 1 2 160.70 172.86 1.84 o 1 1 2 1197.05 925.60 6.20 o 2 1 2 163.13 138.76 5.48 o 3 1 2 1273.03 1275.30 8.45 o 4 1 2 296.46 317.14 3.11 o 6 1 2 1157.88 1218.16 39.07 o 7 1 2 332.53 329.76 3.81 o 8 1 2 418.08 441.83 4.36 o 9 1 2 247.88 265.63 2.97 o 10 1 2 56.57 54.28 4.99 o 11 1 2 11.93 12.75 0.87 o 12 1 2 48.35 46.76 2.88 o 13 1 2 91.28 109.89 4.24 o 14 1 2 46.70 43.75 2.50 o 15 1 2 51.52 54.09 2.41 o -16 2 2 30.61 35.38 2.01 o -15 2 2 0.06 0.30 0.66 o -14 2 2 368.21 381.16 5.27 o -13 2 2 32.38 36.15 4.23 o -12 2 2 2020.07 2058.05 10.51 o -11 2 2 361.41 373.85 4.40 o -10 2 2 76.51 77.98 1.96 o -9 2 2 149.39 138.59 2.17 o -8 2 2 0.22 3.80 0.84 o -7 2 2 1016.93 1021.44 11.19 o -6 2 2 1176.27 1223.91 11.54 o -5 2 2 144.43 159.73 3.94 o -1 2 2 465.25 455.49 7.49 o 0 2 2 28.76 25.75 1.08 o 1 2 2 368.75 385.25 3.26 o 2 2 2 402.77 439.52 2.74 o 3 2 2 4.05 4.22 1.76 o 5 2 2 188.94 176.59 2.90 o 6 2 2 346.80 321.41 3.86 o 7 2 2 50.20 51.85 2.53 o 8 2 2 0.28 2.55 1.11 o 9 2 2 172.64 163.39 2.77 o 10 2 2 94.57 92.23 2.40 o 11 2 2 4.78 5.21 1.06 o 12 2 2 334.13 318.97 7.42 o 13 2 2 0.08 0.74 0.79 o 14 2 2 60.86 64.37 2.93 o 15 2 2 293.73 306.04 5.45 o -15 3 2 3.35 3.83 0.56 o -14 3 2 7.02 6.20 0.77 o -13 3 2 61.54 69.58 2.91 o -12 3 2 3.43 5.99 1.87 o -11 3 2 1.71 0.94 0.53 o -10 3 2 9.96 8.61 0.97 o -9 3 2 5.54 8.31 0.71 o -8 3 2 278.00 296.43 3.20 o -7 3 2 149.39 150.38 2.15 o -6 3 2 37.47 41.41 2.37 o -5 3 2 333.44 345.31 6.33 o -4 3 2 254.33 260.55 5.13 o -3 3 2 95.99 117.92 3.32 o -2 3 2 617.28 573.22 8.10 o -1 3 2 647.64 649.46 4.92 o 0 3 2 165.45 186.98 5.70 o 1 3 2 22.54 16.38 0.89 o 2 3 2 124.97 109.33 2.08 o 3 3 2 773.56 817.77 7.85 o 4 3 2 2.39 3.13 0.63 o 5 3 2 380.65 366.48 4.15 o 6 3 2 4.17 4.82 0.50 o 7 3 2 18.50 18.23 1.41 o 8 3 2 352.84 341.74 6.86 o 9 3 2 530.55 543.07 8.61 o 10 3 2 132.55 127.02 3.10 o 11 3 2 46.51 49.07 1.92 o 12 3 2 5.08 6.16 1.19 o 13 3 2 19.52 23.57 1.85 o 14 3 2 95.02 115.43 3.49 o -14 4 2 44.85 54.66 2.57 o -13 4 2 384.32 396.14 7.63 o -12 4 2 416.56 430.35 8.64 o -11 4 2 32.85 32.34 2.64 o -10 4 2 77.41 79.35 4.01 o -9 4 2 25.80 30.45 2.55 o -8 4 2 0.66 2.04 0.96 o -7 4 2 547.56 529.48 9.39 o -6 4 2 138.92 127.20 3.11 o -5 4 2 671.49 683.62 8.20 o -4 4 2 354.17 384.23 4.11 o -3 4 2 434.15 436.46 8.56 o -2 4 2 11.30 15.72 1.05 o -1 4 2 643.55 666.07 4.90 o 0 4 2 276.38 297.54 7.17 o 1 4 2 249.97 231.94 3.37 o 2 4 2 46.60 66.39 1.37 o 3 4 2 718.11 723.62 3.84 o 4 4 2 393.14 363.91 2.61 o 5 4 2 48.02 44.40 1.41 o 6 4 2 2.26 3.51 0.65 o 7 4 2 98.64 93.35 5.67 o 8 4 2 319.55 328.40 7.23 o 9 4 2 208.30 219.50 4.84 o 10 4 2 71.56 71.61 2.43 o 11 4 2 202.76 209.93 3.69 o 12 4 2 48.63 47.65 2.36 o 13 4 2 1.87 0.99 0.66 o -13 5 2 3.08 5.28 0.97 o -12 5 2 263.74 251.20 5.97 o -11 5 2 41.92 51.91 2.12 o -10 5 2 42.19 45.13 2.12 o -9 5 2 479.29 417.87 7.41 o -8 5 2 0.71 4.04 0.87 o -7 5 2 0.66 2.12 0.77 o -6 5 2 32.97 29.92 2.10 o -5 5 2 135.14 137.52 4.61 o -4 5 2 247.57 244.72 4.46 o -3 5 2 145.14 138.35 5.12 o -2 5 2 466.18 472.81 9.08 o -1 5 2 467.74 469.77 7.29 o 0 5 2 0.05 2.52 1.31 o 1 5 2 4.41 5.06 0.61 o 2 5 2 162.10 159.08 3.46 o 3 5 2 195.41 192.58 3.74 o 4 5 2 481.70 508.34 6.10 o 5 5 2 3.79 5.36 0.80 o 6 5 2 383.98 358.41 5.41 o 7 5 2 1.44 1.96 0.66 o 8 5 2 190.01 195.45 5.75 o 9 5 2 3.82 3.90 1.10 o 10 5 2 73.83 80.08 5.32 o 11 5 2 214.96 246.19 5.76 o -10 6 2 38.56 35.16 1.58 o -9 6 2 33.28 32.24 1.97 o -8 6 2 30.48 31.53 2.16 o -7 6 2 0.03 2.00 0.68 o -6 6 2 164.71 153.97 5.75 o -5 6 2 181.33 160.46 5.90 o -4 6 2 49.08 51.07 2.30 o -3 6 2 70.97 80.71 3.76 o -2 6 2 528.56 543.43 6.79 o -1 6 2 21.26 45.09 3.16 o 0 6 2 571.94 593.55 10.39 o 1 6 2 29.69 33.35 2.57 o 2 6 2 104.57 106.02 7.33 o 3 6 2 4.42 4.08 0.85 o 4 6 2 5.38 12.17 1.19 o 5 6 2 20.24 16.00 1.03 o 6 6 2 253.64 260.18 4.39 o 7 6 2 324.17 323.53 4.79 o 8 6 2 1.50 3.12 1.16 o 9 6 2 87.83 86.54 3.89 o -7 7 2 15.40 15.82 1.66 o -6 7 2 99.92 84.99 3.69 o -5 7 2 21.35 23.20 2.16 o -4 7 2 8.17 8.73 1.56 o -3 7 2 358.61 373.97 7.97 o -2 7 2 711.55 756.68 11.14 o -1 7 2 244.70 252.88 6.35 o 0 7 2 242.08 242.40 5.95 o 1 7 2 16.40 15.62 1.68 o 2 7 2 4.21 7.41 1.21 o 3 7 2 192.53 188.77 4.69 o 4 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