#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:46:20 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181288 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/66/2236654.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236654_Fobs loop_ _publ_author_name 'Zai, De-Xin' _publ_section_title ; 1,4-Dibromobutane-2,3-dione ; _journal_coeditor_code SU2517 _journal_issue 11 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3245 _journal_volume 68 _journal_year 2012 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.9450 _cell_length_b 5.5420 _cell_length_c 17.2380 _exptl_crystal_F_000 456.00 _reflns_d_resolution_high 0.8288 _cod_data_source_file su2517Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' X in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 247.77 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 61387.73 58866.32 875.76 o 4 0 0 5451.20 5700.84 136.34 o 6 0 0 354.63 417.42 146.50 o 8 0 0 18.25 135.58 135.58 o 2 1 0 15262.20 13806.12 1798.04 o 4 1 0 6103.01 5905.68 505.11 o 6 1 0 1621.47 1775.27 103.87 o 8 1 0 300.06 423.78 217.66 o 0 2 0 17383.20 17598.44 197.98 o 2 2 0 4162.17 4956.10 1171.02 o 4 2 0 129.50 103.78 66.54 o 6 2 0 16.33 92.31 92.31 o 2 3 0 1124.52 1390.78 456.37 o 4 3 0 38.01 269.67 218.98 o 6 3 0 1.21 1.10 0.30 o 0 4 0 183.58 347.69 79.69 o 2 4 0 780.89 905.82 271.44 o 4 4 0 378.24 234.03 164.27 o 6 4 0 1.68 96.93 84.92 o 2 5 0 61.42 70.09 20.16 o 4 5 0 487.74 400.86 150.43 o 0 6 0 607.72 576.49 170.12 o 2 6 0 651.80 764.80 366.66 o 1 1 1 153.78 138.95 25.45 o 2 1 1 1429.60 1220.12 121.35 o 3 1 1 8.44 32.35 32.65 o 4 1 1 1243.71 1201.58 111.20 o 5 1 1 9.90 19.78 53.08 o 6 1 1 438.65 548.99 67.41 o 7 1 1 0.01 19.95 65.46 o 8 1 1 65.43 55.77 64.62 o 0 2 1 15617.38 16437.10 406.78 o 1 2 1 222.21 338.03 65.11 o 2 2 1 8787.50 8878.40 1385.32 o 3 2 1 657.81 793.89 100.71 o 4 2 1 1484.18 1336.21 111.20 o 5 2 1 207.74 168.24 65.21 o 6 2 1 38.61 64.27 64.27 o 7 2 1 22.30 50.32 116.01 o 1 3 1 4531.97 4939.36 1056.38 o 2 3 1 1938.57 2267.75 400.50 o 3 3 1 1158.71 1228.18 190.65 o 4 3 1 2473.65 2259.21 79.80 o 5 3 1 80.23 208.77 87.50 o 6 3 1 801.93 849.55 78.45 o 7 3 1 6.18 82.89 74.23 o 0 4 1 9572.79 9307.41 232.18 o 1 4 1 169.46 133.08 59.32 o 2 4 1 5624.62 6754.56 1348.77 o 3 4 1 708.40 863.73 149.62 o 4 4 1 1100.51 1181.65 211.93 o 5 4 1 287.20 350.66 68.61 o 6 4 1 40.02 30.97 59.02 o 1 5 1 1200.77 1753.90 297.54 o 2 5 1 381.17 528.38 86.79 o 3 5 1 283.09 339.03 162.87 o 4 5 1 491.24 673.04 192.96 o 5 5 1 1.80 115.72 58.97 o 0 6 1 257.46 268.13 98.24 o 1 6 1 28.29 32.43 116.05 o 2 6 1 144.61 96.43 141.27 o 3 6 1 110.47 86.67 136.08 o 0 0 2 2969.28 2916.11 244.74 o 1 0 2 1527.89 1894.40 309.65 o 2 0 2 8308.91 7638.58 1740.89 o 3 0 2 5517.71 5790.31 1865.77 o 4 0 2 3022.42 2659.85 470.69 o 5 0 2 2762.74 2772.55 665.44 o 6 0 2 20.54 36.27 83.69 o 7 0 2 496.11 578.08 133.19 o 8 0 2 2.18 155.51 91.25 o 1 1 2 30813.94 32261.85 5194.24 o 2 1 2 20.66 38.64 25.98 o 3 1 2 7529.54 6460.16 771.90 o 4 1 2 2009.94 1978.82 249.86 o 5 1 2 650.25 535.29 53.79 o 6 1 2 793.35 915.84 63.33 o 7 1 2 0.11 22.60 60.90 o 8 1 2 39.52 93.84 113.27 o 0 2 2 2331.90 2428.29 55.71 o 1 2 2 780.31 828.35 122.00 o 2 2 2 4842.16 4180.88 596.40 o 3 2 2 1901.12 2056.65 201.63 o 4 2 2 1740.46 1705.99 162.62 o 5 2 2 978.68 926.70 60.98 o 6 2 2 5.01 72.88 65.25 o 7 2 2 231.80 291.50 69.25 o 1 3 2 46.56 94.37 58.97 o 2 3 2 31.23 117.67 39.73 o 3 3 2 1.73 83.74 45.75 o 4 3 2 494.80 584.11 99.64 o 5 3 2 5.85 6.88 63.54 o 6 3 2 261.15 402.28 77.43 o 7 3 2 3.55 2.12 68.39 o 0 4 2 419.26 421.18 34.51 o 1 4 2 14.49 22.14 41.17 o 2 4 2 1.46 13.80 50.42 o 3 4 2 87.48 114.14 63.62 o 4 4 2 20.20 17.87 111.77 o 5 4 2 75.40 55.70 93.14 o 6 4 2 32.47 58.78 71.92 o 1 5 2 732.45 792.23 131.30 o 2 5 2 271.85 300.21 93.62 o 3 5 2 286.59 280.55 137.53 o 4 5 2 44.19 187.55 105.16 o 5 5 2 18.50 80.03 92.59 o 0 6 2 1199.18 1164.20 77.70 o 1 6 2 32.94 88.20 88.20 o 2 6 2 435.90 251.87 108.34 o 3 6 2 165.56 219.93 121.81 o 1 1 3 8041.26 9218.17 2193.23 o 2 1 3 1.40 19.32 31.87 o 3 1 3 2635.85 2754.17 348.79 o 4 1 3 27.95 27.01 8.41 o 5 1 3 209.47 234.49 49.12 o 6 1 3 6.24 117.65 57.02 o 7 1 3 3.40 5.35 66.76 o 8 1 3 0.40 75.57 89.89 o 0 2 3 2494.93 2594.39 108.78 o 1 2 3 1206.12 1134.60 125.37 o 2 2 3 1278.80 1357.33 225.21 o 3 2 3 4422.30 4876.02 303.50 o 4 2 3 281.93 339.63 49.18 o 5 2 3 3005.42 2778.19 323.30 o 6 2 3 21.06 63.89 61.20 o 7 2 3 745.17 717.83 66.31 o 1 3 3 15616.29 17047.56 2362.44 o 2 3 3 142.94 151.97 41.81 o 3 3 3 5622.77 5158.14 911.29 o 4 3 3 158.03 201.70 55.65 o 5 3 3 607.11 623.66 119.13 o 6 3 3 74.27 103.27 73.95 o 7 3 3 2.29 8.65 69.15 o 0 4 3 91.57 46.74 32.01 o 1 4 3 220.27 341.09 116.63 o 2 4 3 54.41 36.55 69.84 o 3 4 3 987.63 1118.93 199.16 o 4 4 3 6.50 75.27 107.10 o 5 4 3 760.04 722.62 56.64 o 6 4 3 0.70 74.01 74.01 o 1 5 3 1386.57 1712.71 287.23 o 2 5 3 7.65 36.30 99.47 o 3 5 3 619.92 626.89 155.91 o 4 5 3 8.73 66.27 84.25 o 5 5 3 106.17 73.43 76.47 o 0 6 3 52.63 74.80 147.88 o 1 6 3 2.83 81.10 77.10 o 2 6 3 32.21 166.63 89.35 o 3 6 3 13.72 64.35 94.03 o 0 0 4 665.95 645.32 196.01 o 1 0 4 1572.60 1594.93 66.40 o 2 0 4 2908.29 2909.33 611.25 o 3 0 4 6629.37 6858.49 2096.06 o 4 0 4 1409.65 1393.90 388.47 o 5 0 4 3766.37 3809.33 1309.92 o 6 0 4 13.59 73.36 73.36 o 7 0 4 623.61 748.38 215.12 o 8 0 4 0.07 33.92 71.59 o 1 1 4 25237.95 23884.59 4394.51 o 2 1 4 732.70 848.30 90.85 o 3 1 4 8429.14 8678.01 1292.84 o 4 1 4 197.85 316.54 94.10 o 5 1 4 588.75 597.80 66.82 o 6 1 4 99.74 183.70 55.06 o 7 1 4 0.31 24.88 66.99 o 8 1 4 0.50 18.78 50.06 o 0 2 4 640.67 753.69 68.00 o 1 2 4 353.91 340.39 32.33 o 2 2 4 209.41 107.61 82.57 o 3 2 4 2093.51 2350.24 233.09 o 4 2 4 262.90 424.26 129.52 o 5 2 4 1341.38 1265.94 236.89 o 6 2 4 16.38 40.77 52.49 o 7 2 4 233.80 196.40 70.98 o 1 3 4 1522.19 1947.23 200.77 o 2 3 4 60.20 0.59 36.70 o 3 3 4 636.81 722.45 173.82 o 4 3 4 251.29 91.24 77.03 o 5 3 4 37.81 12.10 46.68 o 6 3 4 175.86 124.81 103.22 o 7 3 4 1.17 35.35 65.31 o 0 4 4 353.21 369.22 34.33 o 1 4 4 11.75 15.81 41.03 o 2 4 4 2.23 2.26 0.65 o 3 4 4 11.60 38.83 49.83 o 4 4 4 21.54 74.83 61.54 o 5 4 4 1.97 31.19 51.74 o 6 4 4 18.91 32.56 51.00 o 1 5 4 1500.72 1747.25 229.19 o 2 5 4 213.32 321.85 80.17 o 3 5 4 527.09 587.90 87.92 o 4 5 4 28.48 21.22 60.31 o 5 5 4 97.46 64.41 112.12 o 0 6 4 368.59 331.08 70.17 o 1 6 4 73.98 77.41 71.47 o 2 6 4 77.43 73.80 73.80 o 3 6 4 278.38 136.78 83.32 o 1 1 5 5411.41 5222.30 310.80 o 2 1 5 921.81 1071.56 128.24 o 3 1 5 1409.21 1492.04 133.43 o 4 1 5 956.14 882.67 119.16 o 5 1 5 193.02 168.32 46.76 o 6 1 5 392.72 325.00 61.23 o 7 1 5 17.95 82.27 73.18 o 8 1 5 75.62 170.34 48.96 o 0 2 5 9516.20 10442.14 1349.37 o 1 2 5 234.62 176.01 38.81 o 2 2 5 5298.16 5792.53 1423.97 o 3 2 5 982.49 1073.03 128.09 o 4 2 5 915.03 928.19 59.02 o 5 2 5 412.15 390.23 83.20 o 6 2 5 16.76 52.68 86.30 o 7 2 5 50.50 136.97 75.79 o 1 3 5 6954.45 7320.55 623.55 o 2 3 5 955.99 1202.24 227.97 o 3 3 5 2154.26 2028.94 417.04 o 4 3 5 1225.08 1211.15 100.27 o 5 3 5 149.90 14.27 75.80 o 6 3 5 423.09 322.73 63.96 o 7 3 5 2.92 34.51 61.46 o 0 4 5 2817.17 2736.77 77.65 o 1 4 5 384.96 561.57 112.68 o 2 4 5 1569.67 1637.23 216.78 o 3 4 5 1525.82 1663.63 309.55 o 4 4 5 264.07 355.87 84.61 o 5 4 5 800.53 692.53 79.65 o 6 4 5 1.65 54.99 41.52 o 1 5 5 1926.33 1736.30 159.35 o 2 5 5 72.08 53.87 85.47 o 3 5 5 498.97 563.35 134.97 o 4 5 5 73.74 65.69 20.39 o 5 5 5 10.50 52.16 52.16 o 0 6 5 30.03 46.62 104.30 o 1 6 5 32.64 38.34 78.24 o 2 6 5 15.50 35.06 104.91 o 3 6 5 129.62 134.62 117.51 o 0 0 6 49894.44 44283.39 7831.50 o 1 0 6 1136.48 1122.82 67.91 o 2 0 6 17010.52 16593.26 2094.70 o 3 0 6 2060.16 2190.90 384.07 o 4 0 6 1346.45 1495.79 491.88 o 5 0 6 1085.11 1156.08 307.65 o 6 0 6 37.29 7.64 71.87 o 7 0 6 414.50 327.14 155.15 o 8 0 6 25.78 37.60 86.92 o 1 1 6 5005.37 5019.22 777.17 o 2 1 6 7611.07 8303.70 756.61 o 3 1 6 1098.40 1192.45 114.45 o 4 1 6 3553.06 3595.85 628.39 o 5 1 6 147.58 160.12 82.54 o 6 1 6 955.78 860.54 89.58 o 7 1 6 0.78 16.93 46.72 o 0 2 6 13817.71 14797.27 1495.46 o 1 2 6 85.83 31.79 55.18 o 2 2 6 3936.34 4073.78 705.96 o 3 2 6 141.84 164.14 49.61 o 4 2 6 258.10 186.45 60.57 o 5 2 6 36.87 25.67 66.06 o 6 2 6 43.51 85.85 57.37 o 7 2 6 6.09 64.07 64.07 o 1 3 6 261.92 233.63 74.72 o 2 3 6 413.76 721.09 210.19 o 3 3 6 20.17 46.83 46.83 o 4 3 6 3.59 38.08 76.65 o 5 3 6 10.20 59.88 65.73 o 6 3 6 7.36 36.19 60.59 o 7 3 6 2.21 115.48 56.47 o 0 4 6 186.78 130.30 51.72 o 1 4 6 3.21 134.96 90.25 o 2 4 6 510.07 729.29 173.11 o 3 4 6 5.65 30.24 88.15 o 4 4 6 245.66 231.32 64.37 o 5 4 6 20.65 8.94 79.28 o 6 4 6 0.48 7.55 59.94 o 1 5 6 92.81 178.99 61.32 o 2 5 6 26.56 42.11 62.52 o 3 5 6 66.01 14.93 109.18 o 4 5 6 251.48 226.35 96.52 o 5 5 6 3.86 52.62 70.82 o 0 6 6 533.72 498.79 66.73 o 1 6 6 0.25 23.75 92.78 o 2 6 6 541.03 463.52 148.48 o 1 1 7 15.06 15.24 15.24 o 2 1 7 162.55 86.09 67.21 o 3 1 7 5.01 152.79 75.06 o 4 1 7 250.39 235.36 62.07 o 5 1 7 1.19 67.95 56.50 o 6 1 7 36.65 140.03 59.22 o 7 1 7 2.24 3.95 51.55 o 0 2 7 11056.87 10269.82 974.11 o 1 2 7 19.78 127.83 56.64 o 2 2 7 6363.96 6350.08 329.39 o 3 2 7 51.90 136.73 59.01 o 4 2 7 1229.99 1213.47 223.41 o 5 2 7 5.61 48.87 48.87 o 6 2 7 66.82 5.13 80.57 o 7 2 7 0.09 29.19 52.24 o 1 3 7 83.45 40.71 44.73 o 2 3 7 1569.53 2122.79 436.60 o 3 3 7 1.11 29.36 63.72 o 4 3 7 1924.82 2206.87 255.58 o 5 3 7 7.46 5.98 58.92 o 6 3 7 665.68 642.17 131.43 o 0 4 7 5964.00 6053.55 456.63 o 1 4 7 12.26 35.39 67.20 o 2 4 7 3623.18 3928.41 543.82 o 3 4 7 39.96 131.56 63.71 o 4 4 7 655.23 579.14 152.77 o 5 4 7 2.28 0.32 99.56 o 6 4 7 16.28 34.36 66.57 o 1 5 7 18.11 83.69 87.75 o 2 5 7 389.52 272.32 83.58 o 3 5 7 1.28 70.99 102.69 o 4 5 7 555.48 593.16 144.22 o 0 6 7 352.63 384.74 69.23 o 1 6 7 2.09 21.26 89.19 o 2 6 7 201.81 160.52 91.31 o 0 0 8 7154.23 7328.06 2067.77 o 1 0 8 1016.63 854.92 139.05 o 2 0 8 8421.77 8335.56 112.57 o 3 0 8 2222.34 2793.44 274.17 o 4 0 8 2600.79 3003.35 346.72 o 5 0 8 1127.76 1152.26 100.77 o 6 0 8 48.49 212.44 89.20 o 7 0 8 364.69 349.80 83.25 o 1 1 8 4684.78 4816.55 1356.02 o 2 1 8 500.86 526.31 90.76 o 3 1 8 881.66 1048.78 85.26 o 4 1 8 2454.18 2404.85 172.12 o 5 1 8 69.93 79.16 111.17 o 6 1 8 1043.18 1044.24 117.52 o 7 1 8 3.19 46.11 46.11 o 0 2 8 3943.60 3377.56 255.34 o 1 2 8 109.78 25.57 61.60 o 2 2 8 4127.19 4472.23 591.93 o 3 2 8 144.10 206.09 61.86 o 4 2 8 1266.85 1236.93 70.55 o 5 2 8 27.76 52.71 63.78 o 6 2 8 8.63 66.48 98.57 o 7 2 8 4.22 34.85 65.92 o 1 3 8 1.71 23.98 95.42 o 2 3 8 12.33 41.54 44.20 o 3 3 8 41.71 101.85 75.10 o 4 3 8 153.46 123.52 32.44 o 5 3 8 0.46 14.55 47.93 o 6 3 8 63.29 160.99 80.97 o 0 4 8 318.51 603.82 174.31 o 1 4 8 3.38 4.30 1.38 o 2 4 8 26.47 171.38 163.98 o 3 4 8 94.72 93.20 28.19 o 4 4 8 0.50 81.35 84.44 o 5 4 8 106.93 233.90 153.30 o 1 5 8 350.03 397.70 84.73 o 2 5 8 147.31 227.78 89.23 o 3 5 8 171.44 389.95 106.42 o 4 5 8 37.78 26.88 108.91 o 0 6 8 881.27 815.76 92.75 o 1 6 8 1.92 58.44 65.36 o 1 1 9 3646.60 3914.30 1263.72 o 2 1 9 197.82 213.41 53.47 o 3 1 9 1152.51 1188.13 74.25 o 4 1 9 281.80 402.96 68.63 o 5 1 9 123.12 88.50 60.45 o 6 1 9 133.74 118.85 68.36 o 7 1 9 0.47 6.04 59.75 o 0 2 9 3627.90 3534.93 339.72 o 1 2 9 199.56 241.12 104.79 o 2 2 9 2165.82 2267.55 396.25 o 3 2 9 902.64 1023.78 179.15 o 4 2 9 482.07 384.69 69.86 o 5 2 9 603.51 713.80 139.00 o 6 2 9 15.60 176.40 127.20 o 7 2 9 105.57 103.86 69.93 o 1 3 9 3932.15 4895.48 627.32 o 2 3 9 315.44 346.74 78.47 o 3 3 9 1485.88 1486.52 128.60 o 4 3 9 427.32 324.74 115.97 o 5 3 9 137.29 45.89 59.88 o 6 3 9 175.53 189.89 64.77 o 0 4 9 1071.51 1159.49 107.18 o 1 4 9 117.35 125.11 95.83 o 2 4 9 637.82 684.94 180.04 o 3 4 9 520.89 643.09 187.81 o 4 4 9 143.65 136.65 108.94 o 5 4 9 441.20 444.64 111.85 o 1 5 9 443.47 442.26 98.61 o 2 5 9 35.94 52.97 117.80 o 3 5 9 205.90 223.04 118.51 o 4 5 9 40.84 11.90 64.02 o 0 6 9 92.18 45.02 76.99 o 0 0 10 2226.57 1542.83 344.58 o 1 0 10 401.52 256.26 73.69 o 2 0 10 367.90 303.91 74.76 o 3 0 10 2416.71 2390.44 273.19 o 4 0 10 5.20 87.53 87.53 o 5 0 10 1619.42 1582.80 334.03 o 6 0 10 17.22 74.19 74.19 o 7 0 10 253.18 501.10 321.70 o 1 1 10 7255.16 7345.42 1918.52 o 2 1 10 370.13 289.67 93.57 o 3 1 10 3086.77 3026.33 136.13 o 4 1 10 15.73 3.02 87.51 o 5 1 10 201.84 231.22 69.18 o 6 1 10 0.52 11.57 71.15 o 7 1 10 0.20 28.25 54.49 o 0 2 10 660.14 505.68 182.89 o 1 2 10 75.08 0.60 43.27 o 2 2 10 67.80 55.88 55.88 o 3 2 10 764.20 742.83 112.09 o 4 2 10 4.96 76.67 67.44 o 5 2 10 586.33 624.90 77.00 o 6 2 10 6.61 14.21 55.94 o 1 3 10 697.84 613.33 133.78 o 2 3 10 194.08 97.96 109.71 o 3 3 10 380.01 507.78 135.55 o 4 3 10 19.52 223.51 112.94 o 5 3 10 14.33 22.24 85.06 o 6 3 10 4.98 51.02 71.30 o 0 4 10 268.07 85.78 88.27 o 1 4 10 10.50 75.79 87.87 o 2 4 10 33.75 67.94 67.94 o 3 4 10 3.59 122.41 118.67 o 4 4 10 0.31 35.45 85.03 o 5 4 10 0.88 15.91 101.84 o 1 5 10 838.59 1122.66 117.16 o 2 5 10 27.04 18.46 127.59 o 3 5 10 260.66 108.07 100.47 o 1 1 11 1920.37 1941.02 781.74 o 2 1 11 56.07 41.53 59.83 o 3 1 11 664.81 576.10 133.81 o 4 1 11 93.65 26.55 42.98 o 5 1 11 76.39 54.30 141.67 o 6 1 11 31.62 74.15 97.64 o 7 1 11 2.23 104.89 97.23 o 0 2 11 1684.05 1097.47 289.27 o 1 2 11 202.60 76.75 113.97 o 2 2 11 934.21 1149.83 367.13 o 3 2 11 838.29 1261.43 377.39 o 4 2 11 165.70 119.15 73.43 o 5 2 11 495.67 507.94 92.49 o 6 2 11 0.25 17.29 72.89 o 1 3 11 4396.32 4898.45 1013.22 o 2 3 11 157.03 35.04 80.23 o 3 3 11 1465.12 1980.43 449.32 o 4 3 11 193.78 237.70 92.18 o 5 3 11 132.10 251.73 73.47 o 6 3 11 77.59 57.71 104.43 o 0 4 11 21.24 220.73 120.42 o 1 4 11 151.38 104.27 166.87 o 2 4 11 6.09 149.77 103.68 o 3 4 11 609.96 590.75 114.12 o 4 4 11 0.87 9.33 53.38 o 5 4 11 305.23 422.27 87.44 o 1 5 11 716.01 943.00 128.34 o 2 5 11 0.31 113.78 113.78 o 3 5 11 173.80 75.97 75.97 o 0 0 12 4330.16 4912.16 1131.56 o 1 0 12 373.94 500.37 80.34 o 2 0 12 1529.16 1590.25 196.76 o 3 0 12 1034.81 852.57 159.99 o 4 0 12 62.37 8.71 77.28 o 5 0 12 554.39 540.19 120.93 o 6 0 12 0.38 0.35 118.65 o 1 1 12 4520.07 4860.75 1258.75 o 2 1 12 1067.96 920.88 139.10 o 3 1 12 1202.26 1077.79 96.38 o 4 1 12 581.89 764.25 97.97 o 5 1 12 168.32 135.50 154.23 o 6 1 12 124.30 208.42 124.97 o 0 2 12 2075.84 1727.61 464.17 o 1 2 12 160.68 125.51 111.65 o 2 2 12 670.12 548.63 116.09 o 3 2 12 322.74 214.96 163.35 o 4 2 12 38.35 206.07 163.25 o 5 2 12 141.25 206.79 76.19 o 6 2 12 5.70 34.64 56.59 o 1 3 12 57.38 6.30 53.38 o 2 3 12 57.35 108.69 91.52 o 3 3 12 1.42 37.26 58.71 o 4 3 12 0.32 17.13 83.07 o 5 3 12 0.49 46.08 50.92 o 0 4 12 40.55 75.21 128.85 o 1 4 12 0.73 41.16 147.59 o 2 4 12 90.07 63.28 63.28 o 3 4 12 9.01 44.50 84.12 o 4 4 12 43.70 10.37 104.44 o 1 5 12 41.73 101.05 112.26 o 2 5 12 10.12 17.28 133.66 o 1 1 13 21.29 0.39 56.82 o 2 1 13 90.68 11.36 49.76 o 3 1 13 6.54 21.39 45.34 o 4 1 13 103.52 31.67 51.48 o 5 1 13 3.85 47.54 47.54 o 6 1 13 27.62 51.58 51.58 o 0 2 13 2136.37 1689.96 547.76 o 1 2 13 3.20 39.46 51.09 o 2 2 13 1291.31 1223.56 239.71 o 3 2 13 15.45 40.31 40.31 o 4 2 13 252.86 345.54 135.41 o 5 2 13 16.95 29.95 38.12 o 6 2 13 15.93 172.35 113.50 o 1 3 13 288.85 285.77 80.82 o 2 3 13 341.39 424.74 104.13 o 3 3 13 159.21 133.70 99.21 o 4 3 13 437.07 493.83 162.27 o 5 3 13 43.37 36.99 36.99 o 0 4 13 1663.80 1620.30 221.51 o 1 4 13 1.57 75.05 102.82 o 2 4 13 1001.96 1189.36 270.43 o 3 4 13 13.33 262.48 231.34 o 4 4 13 176.08 587.55 228.10 o 1 5 13 170.93 432.41 146.22 o 0 0 14 5528.03 6966.30 1578.89 o 1 0 14 86.17 105.68 86.58 o 2 0 14 4174.45 3635.40 1040.16 o 3 0 14 140.25 116.85 34.74 o 4 0 14 1228.63 1397.47 118.96 o 5 0 14 56.07 36.83 116.60 o 6 0 14 55.84 62.55 136.44 o 1 1 14 48.36 8.22 50.59 o 2 1 14 278.54 264.38 131.99 o 3 1 14 4.74 15.70 44.32 o 4 1 14 742.46 700.34 127.96 o 5 1 14 3.78 44.77 44.77 o 6 1 14 341.90 322.07 75.54 o 0 2 14 605.33 666.48 162.10 o 1 2 14 5.04 29.26 125.27 o 2 2 14 567.51 819.80 252.06 o 3 2 14 1.64 18.21 34.40 o 4 2 14 147.01 59.07 52.37 o 5 2 14 15.50 12.52 54.25 o 1 3 14 34.83 139.17 124.14 o 2 3 14 0.57 42.49 75.35 o 3 3 14 42.04 17.82 47.08 o 4 3 14 27.47 40.48 40.48 o 0 4 14 137.99 35.66 100.85 o 1 4 14 1.29 95.46 265.30 o 2 4 14 42.84 21.99 84.96 o 3 4 14 39.29 2.30 71.12 o 1 1 15 73.65 30.46 30.46 o 2 1 15 115.89 20.93 75.47 o 3 1 15 15.43 92.15 56.30 o 4 1 15 167.89 59.01 101.91 o 5 1 15 0.52 3.12 98.56 o 0 2 15 967.86 1268.29 340.53 o 1 2 15 17.67 33.56 42.98 o 2 2 15 578.71 611.59 78.86 o 3 2 15 71.88 62.28 88.19 o 4 2 15 106.14 35.14 53.01 o 5 2 15 38.74 44.84 74.21 o 1 3 15 448.08 369.70 120.05 o 2 3 15 131.41 241.10 156.45 o 3 3 15 169.95 97.36 95.87 o 4 3 15 185.22 321.56 150.70 o 0 4 15 806.36 958.04 238.37 o 1 4 15 11.30 67.99 103.31 o 2 4 15 503.52 234.10 215.63 o 0 0 16 890.48 1250.94 224.27 o 1 0 16 25.08 30.01 30.01 o 2 0 16 372.98 461.04 92.26 o 3 0 16 231.41 383.31 87.25 o 4 0 16 38.63 42.51 42.51 o 5 0 16 169.07 130.99 251.94 o 1 1 16 1084.45 1440.42 259.67 o 2 1 16 109.25 24.60 72.92 o 3 1 16 519.48 608.94 79.67 o 4 1 16 48.83 43.52 69.39 o 5 1 16 42.10 8.55 42.86 o 0 2 16 520.65 489.65 124.44 o 1 2 16 13.87 94.85 99.30 o 2 2 16 226.95 318.64 76.74 o 3 2 16 138.38 164.04 71.38 o 4 2 16 29.28 34.40 34.40 o 1 3 16 0.25 92.38 95.66 o 2 3 16 79.77 34.14 75.86 o 3 3 16 1.14 45.10 45.10 o 0 4 16 36.63 88.12 268.22 o 1 4 16 6.32 83.02 87.65 o 1 1 17 278.56 285.76 88.21 o 2 1 17 5.96 32.28 45.77 o 3 1 17 100.48 107.03 103.13 o 4 1 17 7.91 37.93 56.34 o 0 2 17 0.22 87.36 87.36 o 1 2 17 60.04 65.71 65.71 o 2 2 17 0.44 46.49 50.09 o 3 2 17 267.68 248.61 101.48 o 4 2 17 5.63 5.31 1.44 o 1 3 17 856.20 1252.03 163.92 o 2 3 17 0.16 211.89 101.02 o 3 3 17 281.35 73.53 218.26 o 0 0 18 235.84 221.63 52.06 o 1 0 18 76.94 184.23 108.13 o 2 0 18 81.34 4.01 132.09 o 3 0 18 221.06 70.86 96.84 o 4 0 18 2.17 30.84 39.34 o 1 1 18 860.59 841.85 122.80 o 2 1 18 34.31 28.00 28.00 o 3 1 18 223.81 184.23 65.60 o 4 1 18 9.78 56.43 56.43 o 0 2 18 18.36 61.39 61.39 o 1 2 18 32.23 136.90 131.94 o 2 2 18 1.08 5.49 52.22 o 3 2 18 77.27 73.81 75.65 o 1 3 18 37.47 62.45 62.45 o 1 1 19 33.13 97.79 83.92 o 2 1 19 20.79 74.75 76.54 o 3 1 19 17.70 35.97 35.97 o 0 2 19 181.41 467.10 209.13 o 1 2 19 1.08 230.18 168.48 o 2 2 19 111.81 80.51 101.83 o 0 0 20 556.84 491.74 174.68 o 1 0 20 0.03 30.75 63.02 o 2 0 20 378.25 367.96 98.38 o 1 1 20 25.89 136.13 111.89 o