#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/66/2236678.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236678_Fobs loop_ _publ_author_name 'Apostolidis, Christos' 'Ahlmann, Martin' 'Walter, Olaf' _publ_section_title ; fac-Bromidotricarbonyl[2-(diisopropylphosphanyl)benzaldehyde-\k^2^O,P]rhenium(I) ; _journal_coeditor_code VN2046 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1201 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 125.293 _cell_angle_gamma 90.000 _cell_length_a 10.7504 _cell_length_b 15.1936 _cell_length_c 13.6992 _exptl_crystal_F_000 1088.00 _reflns_d_resolution_high 0.7496 _[local]_cod_data_source_file vn2046Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ca10b in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 350.64 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 122947.23 89854.73 471.98 o 2 0 0 2449.27 2654.27 38.76 o 3 0 0 37210.38 37775.63 143.12 o 4 0 0 37734.30 35630.97 233.62 o 5 0 0 61976.65 61513.02 497.07 o 6 0 0 44738.64 45026.48 372.59 o 7 0 0 7072.80 7274.70 204.84 o 8 0 0 8.49 0.11 21.26 o 9 0 0 11193.01 11118.22 158.77 o 10 0 0 18198.76 18499.38 552.36 o 11 0 0 14437.44 14647.27 810.65 o 1 1 0 11419.75 11964.96 103.41 o 2 1 0 99012.44 89588.80 408.43 o 3 1 0 115216.07 105901.80 762.00 o 4 1 0 50896.71 50567.81 484.07 o 5 1 0 479.38 435.92 16.55 o 6 1 0 11296.50 11753.20 97.23 o 7 1 0 28389.45 28644.69 175.67 o 8 1 0 28017.58 28151.63 297.39 o 9 1 0 7981.17 8283.48 177.92 o 10 1 0 133.11 114.12 41.09 o 11 1 0 1917.74 1955.44 95.61 o 0 2 0 31176.55 28741.04 292.33 o 1 2 0 24415.99 23771.04 183.59 o 2 2 0 115.42 157.95 10.87 o 3 2 0 11388.73 12318.85 56.32 o 4 2 0 13165.97 13633.81 168.13 o 5 2 0 5603.18 5510.91 56.41 o 6 2 0 6695.23 6971.61 67.96 o 7 2 0 2661.40 2785.18 48.43 o 8 2 0 804.15 804.03 37.55 o 9 2 0 212.87 239.82 24.74 o 10 2 0 2511.44 2694.95 92.93 o 11 2 0 2285.27 2393.08 150.47 o 1 3 0 29.74 95.25 19.01 o 2 3 0 45.85 117.62 6.90 o 3 3 0 4686.01 5393.33 39.57 o 4 3 0 5.58 21.54 7.99 o 5 3 0 167.59 225.51 15.78 o 6 3 0 657.90 670.36 23.09 o 7 3 0 145.29 162.40 15.76 o 8 3 0 283.25 310.91 24.25 o 9 3 0 331.02 333.29 26.82 o 10 3 0 187.26 211.11 29.93 o 11 3 0 254.67 265.86 45.66 o 0 4 0 51603.44 48689.41 610.13 o 1 4 0 4747.66 4839.70 68.36 o 2 4 0 899.34 907.86 14.27 o 3 4 0 6226.56 6604.51 75.65 o 4 4 0 8925.65 8947.42 114.48 o 5 4 0 15753.68 16213.43 157.38 o 6 4 0 11647.58 11926.97 133.42 o 7 4 0 829.65 873.88 41.95 o 8 4 0 9.82 44.96 23.15 o 9 4 0 2836.42 2906.08 56.12 o 10 4 0 7044.38 7024.61 107.40 o 11 4 0 3415.07 3816.20 96.39 o 1 5 0 6011.73 5961.30 40.81 o 2 5 0 24682.41 24655.54 177.89 o 3 5 0 27016.16 27371.61 235.75 o 4 5 0 21821.89 21515.01 192.64 o 5 5 0 1113.13 1179.08 25.64 o 6 5 0 6217.20 6323.40 91.59 o 7 5 0 21516.78 21873.47 332.41 o 8 5 0 24295.52 24220.44 325.79 o 9 5 0 3266.91 3465.22 61.96 o 10 5 0 118.25 155.78 26.87 o 11 5 0 1662.06 1712.31 185.94 o 0 6 0 82111.27 81435.81 914.28 o 1 6 0 29615.61 29214.52 298.75 o 2 6 0 402.89 415.31 18.60 o 3 6 0 4160.23 4120.86 53.21 o 4 6 0 12015.46 11950.98 96.74 o 5 6 0 11007.31 10892.90 111.50 o 6 6 0 9608.99 9899.54 98.39 o 7 6 0 4121.54 4184.10 88.83 o 8 6 0 55.71 86.44 19.39 o 9 6 0 3718.16 3893.23 95.47 o 10 6 0 7888.49 7970.82 104.32 o 11 6 0 5955.38 5898.49 177.40 o 1 7 0 733.24 1007.75 35.03 o 2 7 0 5793.63 5823.37 49.74 o 3 7 0 4897.30 4878.51 69.26 o 4 7 0 11359.83 11301.33 143.14 o 5 7 0 465.79 491.81 19.86 o 6 7 0 383.92 379.96 22.43 o 7 7 0 5518.79 5733.26 72.06 o 8 7 0 2900.10 3039.95 55.82 o 9 7 0 429.23 442.00 34.23 o 10 7 0 5.48 3.25 26.69 o 0 8 0 42.35 71.94 12.46 o 1 8 0 98.17 141.85 15.03 o 2 8 0 281.25 365.96 15.38 o 3 8 0 1634.70 1758.26 32.54 o 4 8 0 160.70 215.13 13.68 o 5 8 0 3176.93 3341.73 45.85 o 6 8 0 231.24 297.17 23.85 o 7 8 0 26.93 30.18 19.23 o 8 8 0 156.36 172.05 24.15 o 9 8 0 233.96 283.70 32.98 o 10 8 0 392.03 346.25 35.88 o 1 9 0 1623.86 1517.03 29.48 o 2 9 0 10885.95 10697.77 246.53 o 3 9 0 5745.42 5807.76 98.86 o 4 9 0 1164.32 1179.10 30.63 o 5 9 0 101.21 101.04 18.48 o 6 9 0 448.60 450.22 27.38 o 7 9 0 1614.69 1535.05 58.44 o 8 9 0 3128.60 3088.95 59.42 o 9 9 0 1618.19 1641.33 69.43 o 10 9 0 419.76 362.56 46.19 o 0 10 0 15400.29 15941.63 152.47 o 1 10 0 8085.69 8121.37 160.01 o 2 10 0 1659.75 1683.27 72.18 o 3 10 0 1475.82 1491.61 35.24 o 4 10 0 3946.07 3817.63 76.86 o 5 10 0 8745.14 8680.83 176.90 o 6 10 0 6184.90 6153.51 98.27 o 7 10 0 1313.38 1294.20 42.40 o 8 10 0 385.12 382.50 30.47 o 9 10 0 2322.05 2358.33 63.69 o 10 10 0 4722.36 4332.83 126.69 o 1 11 0 3620.02 3297.79 53.01 o 2 11 0 8094.28 7863.46 106.66 o 3 11 0 3789.71 3844.18 55.58 o 4 11 0 2809.31 2909.97 58.50 o 5 11 0 18.78 9.81 18.40 o 6 11 0 1191.26 1195.32 41.94 o 7 11 0 5851.81 5848.50 120.05 o 8 11 0 4798.27 4804.23 118.82 o 9 11 0 1115.53 1202.66 56.64 o 0 12 0 312.98 315.24 35.24 o 1 12 0 196.85 225.51 23.39 o 2 12 0 0.62 -9.58 21.02 o 3 12 0 1201.08 1273.75 42.20 o 4 12 0 2119.91 2063.94 44.63 o 5 12 0 61.91 83.10 21.51 o 6 12 0 51.19 68.01 22.75 o 7 12 0 39.23 63.66 24.29 o 8 12 0 259.03 305.36 43.11 o 9 12 0 341.32 345.63 38.92 o 1 13 0 1473.16 1580.17 53.92 o 2 13 0 5950.67 5744.11 87.29 o 3 13 0 6726.90 6533.13 83.96 o 4 13 0 1276.15 1208.35 70.38 o 5 13 0 194.50 164.89 27.40 o 6 13 0 282.40 293.72 31.51 o 7 13 0 549.73 565.23 44.12 o 8 13 0 1298.32 1363.32 50.97 o 0 14 0 13249.76 12889.95 417.37 o 1 14 0 10548.36 10535.82 208.10 o 2 14 0 2790.71 2861.40 107.91 o 3 14 0 312.61 267.07 32.83 o 4 14 0 7787.48 7628.85 160.25 o 5 14 0 17096.77 16803.96 554.66 o 6 14 0 10282.36 9922.29 171.03 o 7 14 0 2145.04 2050.15 64.85 o 8 14 0 431.04 420.74 45.10 o 1 15 0 7905.26 7493.91 171.53 o 2 15 0 21638.17 21164.73 419.26 o 3 15 0 17901.26 16736.85 164.74 o 4 15 0 4616.92 4514.10 165.78 o 5 15 0 240.70 218.35 31.72 o 6 15 0 2196.94 2246.11 92.87 o 7 15 0 6334.39 6450.55 126.06 o 0 16 0 10854.67 11064.68 554.27 o 1 16 0 8802.33 8496.48 257.54 o 2 16 0 3428.90 3448.73 121.44 o 3 16 0 112.38 153.98 34.38 o 4 16 0 5454.44 5442.66 150.66 o 5 16 0 6989.52 7027.59 208.19 o 6 16 0 7338.90 7334.61 239.79 o 7 16 0 1225.01 1297.17 116.39 o 1 17 0 2245.91 2370.52 73.70 o 2 17 0 2939.94 3091.44 81.71 o 3 17 0 1717.85 1686.88 67.01 o 4 17 0 1368.77 1378.23 64.51 o 5 17 0 4.66 14.60 36.27 o 6 17 0 216.77 142.57 69.43 o 0 18 0 276.51 455.23 74.15 o 1 18 0 307.14 268.10 56.24 o 2 18 0 5.87 3.59 35.49 o 3 18 0 1.88 -35.26 35.26 o 4 18 0 43.46 18.07 44.64 o 5 18 0 63.74 86.28 65.27 o 1 19 0 1261.06 1311.62 78.33 o 2 19 0 3473.09 3654.47 194.42 o 3 19 0 5055.70 4974.10 140.25 o -12 1 1 528.74 761.94 116.28 o -11 1 1 24.10 55.09 34.24 o -10 1 1 1772.99 1998.63 90.55 o -9 1 1 6956.53 6981.18 69.44 o -8 1 1 5067.23 5119.60 102.31 o -7 1 1 3820.59 3959.21 52.76 o -6 1 1 23.02 29.58 9.13 o -5 1 1 5495.26 5298.18 72.79 o -4 1 1 22198.20 22013.54 141.31 o -3 1 1 23475.15 24765.00 243.88 o -2 1 1 8081.48 8539.21 79.94 o -1 1 1 2223.13 2201.98 29.09 o 0 1 1 12527.60 12758.64 198.49 o 1 1 1 13002.76 13023.33 244.18 o 2 1 1 48638.23 49055.07 292.74 o 3 1 1 25631.48 26745.69 203.77 o 4 1 1 738.74 775.13 18.44 o 5 1 1 2434.84 2565.88 30.62 o 6 1 1 7614.46 7756.04 71.45 o 7 1 1 9383.29 9644.64 102.41 o 8 1 1 4836.65 4758.79 99.29 o 9 1 1 66.76 73.15 27.34 o 10 1 1 890.72 926.47 73.39 o 11 1 1 2269.51 2211.01 189.55 o -12 2 1 7320.38 8343.29 269.64 o -11 2 1 9025.83 9639.49 323.05 o -10 2 1 7762.72 7968.45 96.02 o -9 2 1 20.34 98.17 31.22 o -8 2 1 1562.13 1586.34 35.36 o -7 2 1 13103.87 13342.97 160.10 o -6 2 1 37056.47 37451.87 328.72 o -5 2 1 30121.77 30134.99 163.51 o -4 2 1 5669.19 5844.52 52.48 o -3 2 1 11227.43 11565.71 110.89 o -2 2 1 42313.68 40152.51 578.34 o -1 2 1 97256.66 82500.73 546.49 o 0 2 1 114960.26 100607.48 2465.54 o 1 2 1 1918.05 2039.38 39.84 o 2 2 1 391.51 545.98 13.91 o 3 2 1 42230.13 41854.61 204.23 o 4 2 1 46014.23 45245.07 427.63 o 5 2 1 51672.41 51479.20 162.12 o 6 2 1 3223.28 3394.71 41.59 o 7 2 1 543.82 587.38 29.40 o 8 2 1 5084.23 5180.53 68.09 o 9 2 1 12544.28 12563.64 124.76 o 10 2 1 9913.57 10037.96 131.01 o 11 2 1 4869.21 4877.57 219.02 o -12 3 1 932.15 1338.06 142.57 o -11 3 1 52.24 108.29 53.51 o -10 3 1 4853.96 5094.66 160.91 o -9 3 1 12819.76 13176.96 353.31 o -8 3 1 28776.65 28418.57 317.55 o -7 3 1 9128.54 8979.06 135.86 o -6 3 1 515.42 552.07 21.22 o -5 3 1 32253.27 31737.08 254.12 o -4 3 1 76143.70 74574.65 331.31 o -3 3 1 63969.80 61405.50 290.16 o -2 3 1 26249.84 25998.25 244.34 o -1 3 1 1007.53 1216.97 18.74 o 0 3 1 22141.76 21566.01 135.63 o 1 3 1 85957.75 79029.82 956.54 o 2 3 1 46407.86 45464.42 379.99 o 3 3 1 32618.77 32518.21 509.69 o 4 3 1 2117.27 2211.58 28.82 o 5 3 1 11579.53 11753.32 109.31 o 6 3 1 35017.82 35101.77 372.56 o 7 3 1 34912.20 35014.63 213.96 o 8 3 1 15706.45 15841.21 168.90 o 9 3 1 201.83 216.26 28.66 o 10 3 1 1643.18 1836.68 60.83 o 11 3 1 4163.82 4346.39 225.66 o -11 4 1 5354.95 5862.47 118.67 o -10 4 1 1475.31 1524.56 46.53 o -9 4 1 899.11 861.24 42.10 o -8 4 1 8382.62 8671.99 142.93 o -7 4 1 9092.15 9232.95 145.58 o -6 4 1 14279.53 14758.07 231.85 o -5 4 1 9767.93 10080.29 80.97 o -4 4 1 1353.16 1553.14 20.03 o -3 4 1 19252.48 19454.54 137.31 o -2 4 1 51935.44 49982.45 324.69 o -1 4 1 32332.71 31471.09 271.83 o 0 4 1 4146.96 4210.29 56.20 o 1 4 1 54.33 102.83 21.85 o 2 4 1 10943.90 10751.19 77.10 o 3 4 1 34902.36 34459.89 348.28 o 4 4 1 36306.56 37240.90 286.33 o 5 4 1 7836.70 8027.03 65.62 o 6 4 1 259.98 282.61 21.25 o 7 4 1 1413.78 1449.53 36.26 o 8 4 1 1886.88 1907.91 46.58 o 9 4 1 4065.44 4413.53 104.71 o 10 4 1 5222.86 5584.51 91.94 o -11 5 1 326.43 341.82 40.87 o -10 5 1 248.21 291.99 28.06 o -9 5 1 86.01 98.06 21.61 o -8 5 1 417.98 489.22 25.99 o -7 5 1 331.81 370.78 18.55 o -6 5 1 3780.89 3786.41 64.88 o -5 5 1 15290.39 15616.72 265.52 o -4 5 1 8285.75 8366.75 75.92 o -3 5 1 460.37 617.41 16.12 o -2 5 1 8140.78 8460.14 78.47 o -1 5 1 39099.95 37712.21 348.05 o 0 5 1 9653.24 9468.03 97.92 o 1 5 1 4686.69 4651.24 77.54 o 2 5 1 72.95 139.93 12.03 o 3 5 1 399.90 478.50 33.25 o 4 5 1 490.22 508.40 19.32 o 5 5 1 2527.51 2550.91 39.67 o 6 5 1 2528.99 2623.49 42.62 o 7 5 1 2858.14 2967.49 47.89 o 8 5 1 548.51 589.70 31.87 o 9 5 1 804.56 731.45 38.01 o 10 5 1 558.75 551.08 40.65 o -11 6 1 1298.02 1254.00 61.91 o -10 6 1 4033.57 4056.89 89.06 o -9 6 1 1899.26 1974.21 44.63 o -8 6 1 420.33 466.88 25.66 o -7 6 1 1307.38 1329.75 34.36 o -6 6 1 11644.32 11658.11 84.17 o -5 6 1 16122.22 16497.21 247.88 o -4 6 1 9024.35 8867.30 46.59 o -3 6 1 2625.80 2712.75 29.47 o -2 6 1 1411.95 1610.44 33.61 o -1 6 1 5694.92 6030.39 73.92 o 0 6 1 7027.39 7000.73 67.31 o 1 6 1 5268.24 4879.36 52.03 o 2 6 1 6168.78 6192.44 54.96 o 3 6 1 574.10 589.83 29.34 o 4 6 1 3208.02 3136.54 49.99 o 5 6 1 12965.72 12895.96 159.12 o 6 6 1 4660.39 4700.70 66.66 o 7 6 1 444.45 465.10 26.66 o 8 6 1 283.15 268.87 24.42 o 9 6 1 1158.96 1179.62 57.00 o 10 6 1 1550.27 1401.43 64.08 o -11 7 1 45.70 60.05 34.35 o -10 7 1 3624.88 3719.41 86.59 o -9 7 1 7475.37 7599.50 171.20 o -8 7 1 12721.08 12777.97 282.83 o -7 7 1 6957.97 6968.22 87.24 o -6 7 1 4254.74 4249.29 81.94 o -5 7 1 1868.72 2047.13 30.69 o -4 7 1 12631.12 12343.08 132.13 o -3 7 1 30505.30 29899.16 319.58 o -2 7 1 28290.25 27666.69 220.57 o -1 7 1 3317.51 3075.05 67.63 o 0 7 1 166.95 246.54 17.56 o 1 7 1 16330.27 16116.54 74.35 o 2 7 1 28509.25 28523.34 427.29 o 3 7 1 21089.54 20071.80 159.01 o 4 7 1 1052.43 1061.57 31.44 o 5 7 1 77.77 95.48 16.33 o 6 7 1 2052.29 2178.51 42.11 o 7 7 1 7720.80 7753.89 127.12 o 8 7 1 7505.35 7567.11 140.64 o 9 7 1 1596.07 1648.44 54.24 o 10 7 1 26.23 51.28 29.88 o -11 8 1 6874.83 6392.25 137.28 o -10 8 1 5459.65 5293.65 101.67 o -9 8 1 3137.30 3260.33 80.11 o -8 8 1 8.04 -5.74 19.83 o -7 8 1 6214.16 6114.11 71.36 o -6 8 1 16361.40 16138.18 277.63 o -5 8 1 19551.39 19224.14 125.66 o -4 8 1 7505.46 7181.96 94.63 o -3 8 1 132.68 157.52 19.02 o -2 8 1 11590.00 11537.27 75.64 o -1 8 1 24462.90 24365.98 258.85 o 0 8 1 40541.32 40949.73 480.36 o 1 8 1 12674.29 12117.69 70.68 o 2 8 1 1601.71 1612.22 27.99 o 3 8 1 1223.49 1237.42 28.88 o 4 8 1 12615.97 12755.13 147.04 o 5 8 1 17103.47 16524.59 230.23 o 6 8 1 6706.63 6595.41 96.70 o 7 8 1 27.99 37.69 19.86 o 8 8 1 1434.27 1435.00 45.44 o 9 8 1 3919.14 4071.96 88.82 o 10 8 1 4417.76 4564.25 139.14 o -10 9 1 498.04 526.76 39.84 o -9 9 1 2699.05 2806.33 58.40 o -8 9 1 6845.50 6912.19 97.13 o -7 9 1 4473.93 4458.89 63.59 o -6 9 1 1622.86 1686.47 41.37 o -5 9 1 83.99 98.61 15.02 o -4 9 1 8104.65 7932.41 80.05 o -3 9 1 14091.56 14190.82 109.30 o -2 9 1 10059.34 9810.11 87.43 o -1 9 1 908.63 868.10 23.57 o 0 9 1 497.65 552.76 22.56 o 1 9 1 2509.97 2486.63 62.81 o 2 9 1 8784.41 8699.16 159.00 o 3 9 1 10686.40 10160.81 101.57 o 4 9 1 7087.33 6855.41 123.04 o 5 9 1 202.75 264.84 40.58 o 6 9 1 1994.90 1929.63 46.26 o 7 9 1 5375.17 5288.04 140.62 o 8 9 1 1627.98 1706.21 49.63 o 9 9 1 1084.02 1106.59 50.82 o 10 9 1 20.49 62.84 45.12 o -10 10 1 3.76 -14.04 30.91 o -9 10 1 151.74 164.90 30.59 o -8 10 1 30.50 41.99 21.78 o -7 10 1 435.15 502.65 54.30 o -6 10 1 34.66 42.90 23.09 o -5 10 1 193.83 227.60 21.80 o -4 10 1 4690.90 4634.51 51.62 o -3 10 1 2004.64 2042.81 34.95 o -2 10 1 865.29 836.96 25.94 o -1 10 1 174.47 237.87 27.45 o 0 10 1 82.34 68.67 16.79 o 1 10 1 2007.02 2060.84 37.88 o 2 10 1 496.20 509.33 25.88 o 3 10 1 822.01 886.00 31.63 o 4 10 1 0.69 12.32 16.05 o 5 10 1 477.89 522.16 40.28 o 6 10 1 52.94 45.05 20.88 o 7 10 1 232.35 260.56 27.03 o 8 10 1 437.82 483.48 33.13 o 9 10 1 73.79 51.19 26.82 o -10 11 1 1409.68 1288.05 71.88 o -9 11 1 3220.52 3224.93 139.21 o -8 11 1 2162.14 2195.82 72.79 o -7 11 1 59.96 77.17 27.74 o -6 11 1 47.74 27.26 19.08 o -5 11 1 720.51 728.89 33.21 o -4 11 1 3016.54 3030.64 41.92 o -3 11 1 8793.96 8846.25 75.01 o -2 11 1 5014.98 5120.35 108.72 o -1 11 1 0.76 9.53 24.72 o 0 11 1 2728.57 2831.70 50.36 o 1 11 1 14349.41 13932.74 182.39 o 2 11 1 10210.03 10366.62 256.58 o 3 11 1 3156.16 3235.09 84.11 o 4 11 1 318.81 354.36 34.41 o 5 11 1 1491.90 1413.99 45.89 o 6 11 1 886.20 930.93 42.51 o 7 11 1 1955.68 1928.49 88.96 o 8 11 1 1820.09 1911.51 54.07 o 9 11 1 687.30 677.04 45.59 o -9 12 1 1002.88 1024.79 52.85 o -8 12 1 208.38 216.03 28.55 o -7 12 1 8967.43 8996.70 159.53 o -6 12 1 18307.50 17957.85 294.49 o -5 12 1 14483.00 14216.01 260.54 o -4 12 1 316.36 293.22 19.55 o -3 12 1 2137.68 2153.75 49.71 o -2 12 1 9960.16 9779.90 226.73 o -1 12 1 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