#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:46:43 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181289 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/67/2236720.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236720_Fobs loop_ _publ_author_name 'Yu, Min' 'Huang, Xing' 'Gao, Feng' _publ_section_title ; Pyrrolidine-2,5-dione ; _journal_coeditor_code XU5605 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o2738 _journal_volume 68 _journal_year 2012 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.3661 _cell_length_b 9.5504 _cell_length_c 12.8501 _exptl_crystal_F_000 416.00 _reflns_d_resolution_high 0.8002 _cod_data_source_file xu5605Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 120417_s2_gf in Pbca ' _shelx_refln_list_code 4 _shelx_f_calc_maximum 128.27 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y, -z-1/2' '-x-1/2, y-1/2, z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 6627.20 5643.67 48.13 o 4 0 0 488.51 499.69 9.57 o 6 0 0 166.41 168.72 11.19 o 8 0 0 132.75 136.76 11.90 o 2 1 0 347.83 354.65 5.31 o 4 1 0 118.34 123.83 4.09 o 6 1 0 521.80 519.45 10.27 o 8 1 0 25.57 28.27 4.03 o 0 2 0 11353.04 9619.89 24.35 o 2 2 0 1472.56 1502.86 26.24 o 4 2 0 310.37 292.54 11.29 o 6 2 0 127.99 136.57 5.43 o 8 2 0 0.22 -2.95 3.02 o 2 3 0 1275.84 1251.76 23.36 o 4 3 0 13.73 14.20 3.29 o 6 3 0 491.15 517.51 14.01 o 8 3 0 1.50 4.87 2.76 o 0 4 0 16451.96 14789.84 69.52 o 2 4 0 0.43 -0.60 1.48 o 4 4 0 11.09 11.83 3.14 o 6 4 0 20.81 26.24 5.56 o 8 4 0 38.45 42.25 8.07 o 2 5 0 176.57 141.56 9.40 o 4 5 0 0.34 0.86 1.98 o 6 5 0 349.76 332.60 19.36 o 8 5 0 7.69 9.71 4.39 o 0 6 0 4448.51 4488.71 51.72 o 2 6 0 478.06 530.15 19.58 o 4 6 0 598.74 582.55 23.33 o 6 6 0 104.81 100.91 11.20 o 2 7 0 939.06 933.72 27.87 o 4 7 0 0.01 -1.44 2.10 o 6 7 0 118.26 124.21 12.95 o 0 8 0 89.84 74.73 8.25 o 2 8 0 555.22 523.86 22.45 o 4 8 0 134.36 163.63 13.98 o 6 8 0 151.35 143.87 14.59 o 2 9 0 1.22 19.83 5.19 o 4 9 0 4.85 7.98 3.94 o 6 9 0 56.23 52.35 9.38 o 0 10 0 45.73 36.49 6.86 o 2 10 0 86.34 75.60 9.86 o 4 10 0 111.41 114.93 12.99 o 2 11 0 247.01 273.44 19.28 o 1 1 1 1691.47 1640.43 10.35 o 2 1 1 3108.34 2932.14 13.95 o 3 1 1 11.90 11.72 0.82 o 4 1 1 41.36 42.52 1.82 o 5 1 1 29.66 29.14 1.61 o 6 1 1 84.93 91.71 3.08 o 7 1 1 0.50 1.86 1.03 o 8 1 1 49.43 51.60 3.73 o 9 1 1 21.79 19.37 4.50 o 0 2 1 1864.28 1802.80 13.79 o 1 2 1 202.47 230.22 3.52 o 2 2 1 1207.58 1293.14 10.69 o 3 2 1 82.55 82.18 3.48 o 4 2 1 0.19 1.13 0.77 o 5 2 1 636.87 628.03 9.15 o 6 2 1 16.44 18.62 1.41 o 7 2 1 0.16 1.28 0.92 o 8 2 1 140.71 154.28 7.67 o 9 2 1 13.52 11.77 2.86 o 1 3 1 1578.69 1550.97 7.79 o 2 3 1 3065.99 3077.19 26.10 o 3 3 1 275.91 287.22 8.85 o 4 3 1 31.85 25.46 3.05 o 5 3 1 107.55 111.35 6.67 o 6 3 1 26.46 29.39 2.85 o 7 3 1 3.81 6.65 1.37 o 8 3 1 245.23 254.82 12.12 o 0 4 1 712.92 759.86 7.57 o 1 4 1 389.46 380.49 5.48 o 2 4 1 209.05 246.62 8.09 o 3 4 1 367.04 345.73 11.12 o 4 4 1 332.06 371.08 12.75 o 5 4 1 12.12 8.88 2.31 o 6 4 1 149.23 149.55 6.34 o 7 4 1 86.48 89.48 7.37 o 8 4 1 0.25 -0.63 1.84 o 1 5 1 21.73 18.87 1.44 o 2 5 1 54.30 49.70 2.98 o 3 5 1 197.17 206.59 11.70 o 4 5 1 48.65 53.82 5.86 o 5 5 1 127.37 124.76 7.84 o 6 5 1 722.79 758.25 25.51 o 7 5 1 12.51 12.81 3.19 o 8 5 1 133.39 139.80 14.61 o 0 6 1 778.12 821.76 15.67 o 1 6 1 12.45 14.37 1.70 o 2 6 1 54.69 50.77 4.39 o 3 6 1 339.47 353.76 12.17 o 4 6 1 226.12 230.89 10.45 o 5 6 1 437.00 445.07 15.47 o 6 6 1 106.82 98.82 7.84 o 7 6 1 49.20 45.21 5.71 o 1 7 1 0.87 0.00 1.25 o 2 7 1 318.60 338.31 12.03 o 3 7 1 75.41 78.20 6.15 o 4 7 1 0.23 -0.26 1.63 o 5 7 1 16.95 26.28 4.19 o 6 7 1 21.80 24.04 4.31 o 7 7 1 99.68 129.47 13.71 o 0 8 1 393.72 384.17 12.73 o 1 8 1 16.11 13.15 1.95 o 2 8 1 52.50 54.95 7.28 o 3 8 1 8.76 5.44 2.26 o 4 8 1 37.67 35.47 4.60 o 5 8 1 61.66 64.51 11.23 o 6 8 1 4.50 9.20 2.96 o 1 9 1 88.29 78.41 4.49 o 2 9 1 13.11 19.37 4.07 o 3 9 1 272.34 291.78 18.43 o 4 9 1 49.93 51.25 5.96 o 5 9 1 6.19 3.81 3.62 o 6 9 1 365.37 393.87 36.50 o 0 10 1 435.84 427.64 15.32 o 1 10 1 3.80 0.77 1.79 o 2 10 1 18.10 18.64 3.81 o 3 10 1 12.36 14.71 2.97 o 4 10 1 151.65 185.33 16.28 o 1 11 1 1.76 4.12 2.27 o 2 11 1 6.95 10.09 3.27 o 3 11 1 2.88 3.81 2.79 o 0 0 2 219.38 203.82 3.33 o 1 0 2 141.28 149.55 3.27 o 2 0 2 862.58 851.81 7.66 o 3 0 2 655.16 671.99 9.80 o 4 0 2 902.07 946.52 26.46 o 5 0 2 16.85 18.07 2.30 o 6 0 2 118.33 126.57 5.51 o 7 0 2 69.01 71.06 5.71 o 8 0 2 2.32 2.56 1.50 o 9 0 2 203.02 218.48 17.17 o 1 1 2 9982.02 8303.37 24.70 o 2 1 2 10883.51 9903.85 39.57 o 3 1 2 1203.48 1239.18 7.07 o 4 1 2 11.69 16.85 1.05 o 5 1 2 139.95 157.27 5.29 o 6 1 2 9.00 10.69 1.34 o 7 1 2 205.59 213.48 6.82 o 8 1 2 21.01 18.07 3.90 o 9 1 2 1.50 1.75 3.09 o 0 2 2 107.56 109.17 3.55 o 1 2 2 4.15 3.00 0.64 o 2 2 2 149.46 173.48 4.01 o 3 2 2 55.99 53.20 2.42 o 4 2 2 166.71 165.93 4.04 o 5 2 2 86.99 95.96 3.43 o 6 2 2 16.41 14.36 1.36 o 7 2 2 1.42 1.80 0.98 o 8 2 2 30.63 31.34 3.63 o 9 2 2 19.19 13.34 3.25 o 1 3 2 392.57 376.92 3.98 o 2 3 2 90.14 97.59 4.75 o 3 3 2 222.39 227.72 7.94 o 4 3 2 1075.85 1098.76 19.20 o 5 3 2 2.92 4.33 1.50 o 6 3 2 7.76 7.14 1.44 o 7 3 2 1.80 1.77 1.62 o 8 3 2 4.98 4.61 1.72 o 0 4 2 508.75 466.79 6.38 o 1 4 2 30.86 33.36 2.11 o 2 4 2 377.14 408.85 6.10 o 3 4 2 311.41 312.93 10.05 o 4 4 2 155.70 142.12 7.38 o 5 4 2 86.36 83.31 11.25 o 6 4 2 1.86 0.67 1.12 o 7 4 2 73.77 70.78 6.63 o 8 4 2 39.27 41.57 4.23 o 1 5 2 792.54 843.44 11.39 o 2 5 2 2148.61 2120.41 18.14 o 3 5 2 218.77 231.43 9.22 o 4 5 2 43.65 53.30 4.91 o 5 5 2 50.14 51.57 5.08 o 6 5 2 9.32 9.08 2.73 o 7 5 2 67.53 66.67 6.70 o 8 5 2 3.66 4.26 2.27 o 0 6 2 91.92 81.08 4.00 o 1 6 2 5.80 5.99 1.42 o 2 6 2 304.39 276.54 8.43 o 3 6 2 11.70 11.62 2.26 o 4 6 2 247.16 233.81 10.59 o 5 6 2 101.97 139.21 8.75 o 6 6 2 0.39 0.62 1.76 o 7 6 2 1.43 2.25 2.52 o 1 7 2 83.95 80.00 4.00 o 2 7 2 457.61 451.81 19.17 o 3 7 2 6.78 9.00 2.34 o 4 7 2 792.90 740.25 19.80 o 5 7 2 68.14 63.56 6.46 o 6 7 2 41.09 52.37 6.99 o 7 7 2 18.33 15.80 3.76 o 0 8 2 83.00 94.76 6.45 o 1 8 2 0.18 1.25 1.26 o 2 8 2 265.78 260.76 15.50 o 3 8 2 67.13 61.02 7.99 o 4 8 2 10.36 13.74 3.62 o 5 8 2 103.39 116.66 8.82 o 6 8 2 4.20 6.78 2.72 o 1 9 2 67.21 57.13 4.60 o 2 9 2 20.65 16.25 2.87 o 3 9 2 0.43 5.12 2.91 o 4 9 2 329.68 304.24 20.06 o 5 9 2 0.77 2.69 2.07 o 0 10 2 28.11 16.65 3.26 o 1 10 2 0.13 0.72 2.76 o 2 10 2 61.24 61.09 6.15 o 3 10 2 18.36 18.62 3.23 o 4 10 2 18.85 16.59 5.23 o 1 11 2 21.64 13.16 2.77 o 2 11 2 13.01 19.65 4.69 o 3 11 2 22.78 19.67 4.48 o 1 1 3 290.60 277.26 4.10 o 2 1 3 308.74 326.63 3.09 o 3 1 3 214.29 235.66 4.27 o 4 1 3 1145.64 1151.56 10.36 o 5 1 3 21.50 22.15 1.90 o 6 1 3 3.92 5.03 1.40 o 7 1 3 17.94 19.72 2.05 o 8 1 3 84.40 88.05 5.79 o 9 1 3 1.04 2.52 3.99 o 0 2 3 2144.69 2244.70 16.43 o 1 2 3 1520.54 1491.37 10.06 o 2 2 3 4852.66 4863.87 25.14 o 3 2 3 1452.75 1437.92 11.05 o 4 2 3 964.84 964.01 11.38 o 5 2 3 9.49 6.93 0.94 o 6 2 3 0.38 0.95 0.87 o 7 2 3 126.57 118.34 6.15 o 8 2 3 7.27 6.19 1.76 o 1 3 3 1494.87 1514.35 7.34 o 2 3 3 203.05 231.10 7.47 o 3 3 3 35.26 33.22 1.65 o 4 3 3 305.53 326.09 6.50 o 5 3 3 70.50 71.28 2.97 o 6 3 3 27.64 24.87 2.79 o 7 3 3 34.76 37.72 3.96 o 8 3 3 96.59 106.14 6.66 o 0 4 3 363.57 354.94 5.36 o 1 4 3 1099.10 1102.77 9.41 o 2 4 3 37.43 44.09 2.01 o 3 4 3 783.29 789.99 8.89 o 4 4 3 697.85 718.18 16.56 o 5 4 3 64.53 67.56 5.09 o 6 4 3 71.21 78.78 6.48 o 7 4 3 224.00 215.91 18.21 o 8 4 3 34.65 26.24 4.44 o 1 5 3 592.52 640.68 9.81 o 2 5 3 0.06 1.35 0.84 o 3 5 3 345.37 367.27 7.08 o 4 5 3 940.60 952.51 20.30 o 5 5 3 14.90 17.09 3.08 o 6 5 3 9.11 9.33 2.82 o 7 5 3 0.32 -0.05 1.97 o 8 5 3 11.69 8.88 2.72 o 0 6 3 540.75 503.31 9.50 o 1 6 3 12.40 12.28 2.78 o 2 6 3 406.60 379.56 26.05 o 3 6 3 12.70 12.84 1.57 o 4 6 3 0.18 2.01 2.25 o 5 6 3 0.00 0.79 1.44 o 6 6 3 12.04 7.57 2.49 o 7 6 3 28.88 29.33 7.49 o 1 7 3 6.80 4.36 1.50 o 2 7 3 199.14 218.06 13.36 o 3 7 3 105.92 90.89 9.26 o 4 7 3 278.25 287.70 14.67 o 5 7 3 3.79 5.27 2.18 o 6 7 3 1.11 -0.26 1.86 o 7 7 3 27.98 33.53 5.25 o 0 8 3 558.85 523.93 14.45 o 1 8 3 144.83 148.41 5.80 o 2 8 3 93.32 92.91 7.00 o 3 8 3 28.81 40.04 6.67 o 4 8 3 168.96 205.71 15.63 o 5 8 3 135.79 138.17 9.73 o 6 8 3 82.08 88.60 8.28 o 1 9 3 137.88 161.12 6.37 o 2 9 3 151.09 148.42 13.00 o 3 9 3 37.88 40.55 7.06 o 4 9 3 88.33 92.99 11.30 o 5 9 3 20.05 15.51 5.31 o 0 10 3 48.75 41.34 5.27 o 1 10 3 73.72 84.03 5.75 o 2 10 3 134.81 118.56 10.98 o 3 10 3 41.74 52.20 4.93 o 4 10 3 141.84 141.11 14.30 o 1 11 3 17.45 15.38 3.58 o 2 11 3 0.00 -0.08 3.30 o 3 11 3 59.08 75.49 7.76 o 0 0 4 1984.69 2083.88 14.98 o 1 0 4 10.66 5.84 0.80 o 2 0 4 2201.08 2322.36 18.99 o 3 0 4 1460.97 1506.83 12.71 o 4 0 4 82.61 92.63 3.65 o 5 0 4 743.84 732.74 18.37 o 6 0 4 221.44 213.85 7.57 o 7 0 4 63.83 65.69 4.49 o 8 0 4 1.70 5.93 3.84 o 1 1 4 150.50 156.58 3.44 o 2 1 4 0.07 0.15 0.29 o 3 1 4 190.31 176.22 3.09 o 4 1 4 336.05 316.20 5.51 o 5 1 4 5.91 4.58 1.17 o 6 1 4 15.03 14.99 2.17 o 7 1 4 382.22 398.21 9.82 o 8 1 4 126.03 131.87 7.23 o 0 2 4 505.86 487.43 9.10 o 1 2 4 218.98 221.84 3.72 o 2 2 4 155.30 171.49 8.82 o 3 2 4 836.01 936.43 15.59 o 4 2 4 3.12 1.75 0.65 o 5 2 4 376.70 390.18 5.69 o 6 2 4 1.49 0.89 0.84 o 7 2 4 1.27 -1.03 1.54 o 8 2 4 0.24 -1.70 1.70 o 1 3 4 177.86 186.60 3.55 o 2 3 4 23.81 16.23 2.93 o 3 3 4 27.43 28.23 3.70 o 4 3 4 589.63 579.61 9.44 o 5 3 4 41.05 38.77 2.43 o 6 3 4 1.05 1.49 1.48 o 7 3 4 0.11 -1.64 1.64 o 8 3 4 74.20 74.11 4.92 o 0 4 4 211.28 198.60 3.84 o 1 4 4 173.71 184.85 3.20 o 2 4 4 1588.90 1568.78 25.31 o 3 4 4 0.07 2.18 3.22 o 4 4 4 31.41 35.69 3.91 o 5 4 4 6.94 8.12 5.70 o 6 4 4 149.64 162.09 9.85 o 7 4 4 75.68 81.32 12.19 o 8 4 4 2.72 2.66 1.90 o 1 5 4 321.83 295.38 6.05 o 2 5 4 10.90 10.83 1.15 o 3 5 4 38.99 40.74 2.74 o 4 5 4 10.84 10.22 2.62 o 5 5 4 8.81 13.00 2.82 o 6 5 4 27.30 32.13 6.67 o 7 5 4 121.12 109.14 8.52 o 8 5 4 84.71 81.89 7.88 o 0 6 4 155.59 145.46 7.47 o 1 6 4 26.92 23.05 1.76 o 2 6 4 73.04 67.40 3.74 o 3 6 4 358.16 320.36 16.46 o 4 6 4 0.84 0.80 1.51 o 5 6 4 324.15 321.74 13.41 o 6 6 4 38.94 38.89 4.96 o 7 6 4 0.00 0.25 2.20 o 1 7 4 519.55 533.05 10.02 o 2 7 4 2.48 4.81 2.50 o 3 7 4 0.11 -1.97 2.31 o 4 7 4 533.83 507.56 23.37 o 5 7 4 19.32 19.25 3.66 o 6 7 4 7.73 6.27 2.62 o 7 7 4 72.89 72.81 7.65 o 0 8 4 15.50 17.73 2.83 o 1 8 4 198.06 187.40 7.61 o 2 8 4 493.16 510.42 16.20 o 3 8 4 427.65 406.23 20.74 o 4 8 4 2.72 2.87 2.91 o 5 8 4 196.35 187.08 15.88 o 6 8 4 19.32 22.91 6.32 o 1 9 4 5.24 3.14 1.22 o 2 9 4 2.10 3.34 2.32 o 3 9 4 5.55 7.65 3.67 o 4 9 4 2.62 -2.40 2.52 o 5 9 4 3.23 3.36 3.21 o 0 10 4 2.64 2.16 3.39 o 1 10 4 22.39 22.52 4.26 o 2 10 4 1.58 2.90 4.19 o 3 10 4 32.54 31.98 4.93 o 4 10 4 0.21 -1.34 2.55 o 1 11 4 196.90 209.83 12.93 o 2 11 4 7.86 7.51 3.97 o 1 1 5 214.85 226.64 5.11 o 2 1 5 629.13 651.21 8.11 o 3 1 5 447.40 480.42 7.37 o 4 1 5 477.01 509.46 7.54 o 5 1 5 383.42 379.90 6.78 o 6 1 5 1.47 1.14 1.00 o 7 1 5 0.61 -0.79 1.06 o 8 1 5 0.41 -1.15 1.62 o 0 2 5 68.15 56.93 3.49 o 1 2 5 1562.83 1639.88 17.75 o 2 2 5 429.27 461.36 11.06 o 3 2 5 790.93 799.30 10.87 o 4 2 5 367.32 376.70 11.09 o 5 2 5 289.75 282.66 7.41 o 6 2 5 8.73 8.56 1.73 o 7 2 5 394.19 404.85 11.85 o 8 2 5 165.79 168.12 9.21 o 1 3 5 101.39 93.81 3.94 o 2 3 5 474.23 461.83 15.67 o 3 3 5 992.40 1011.07 25.84 o 4 3 5 717.05 727.00 16.40 o 5 3 5 1216.15 1201.28 25.84 o 6 3 5 42.23 38.58 6.31 o 7 3 5 52.22 41.66 4.05 o 8 3 5 4.09 1.99 1.48 o 0 4 5 59.65 51.19 3.48 o 1 4 5 25.00 36.95 2.13 o 2 4 5 200.55 210.16 6.20 o 3 4 5 18.12 19.18 3.90 o 4 4 5 133.32 139.55 11.04 o 5 4 5 16.28 13.32 3.23 o 6 4 5 63.98 69.30 11.07 o 7 4 5 52.79 43.89 5.27 o 8 4 5 81.20 81.78 6.09 o 1 5 5 682.58 717.41 10.48 o 2 5 5 174.29 178.98 6.31 o 3 5 5 82.38 82.41 8.06 o 4 5 5 3.12 4.40 2.75 o 5 5 5 187.98 181.22 9.77 o 6 5 5 173.77 162.48 9.84 o 7 5 5 99.91 102.31 9.51 o 0 6 5 0.48 0.13 0.80 o 1 6 5 230.99 229.45 6.82 o 2 6 5 447.44 441.97 7.40 o 3 6 5 99.27 101.76 9.57 o 4 6 5 25.97 23.71 5.26 o 5 6 5 17.20 11.67 4.17 o 6 6 5 45.49 37.69 4.96 o 7 6 5 20.29 14.35 3.68 o 1 7 5 10.16 5.04 1.84 o 2 7 5 339.65 323.12 12.42 o 3 7 5 41.89 53.19 7.24 o 4 7 5 3.18 12.78 4.41 o 5 7 5 43.72 48.34 8.27 o 6 7 5 9.15 10.56 4.90 o 0 8 5 318.94 296.65 11.24 o 1 8 5 19.79 18.25 2.12 o 2 8 5 4.52 7.42 2.65 o 3 8 5 15.82 23.16 5.32 o 4 8 5 63.98 52.17 8.05 o 5 8 5 1.03 7.02 4.19 o 6 8 5 0.12 1.94 3.38 o 1 9 5 421.08 411.91 12.49 o 2 9 5 17.59 16.20 3.32 o 3 9 5 79.43 97.34 8.08 o 4 9 5 57.88 61.73 9.29 o 5 9 5 199.02 230.43 18.66 o 0 10 5 144.49 127.51 13.75 o 1 10 5 12.98 12.50 3.64 o 2 10 5 48.74 45.11 5.60 o 3 10 5 1.43 2.40 2.13 o 4 10 5 7.50 8.73 5.20 o 1 11 5 4.02 1.67 2.33 o 2 11 5 14.62 13.86 4.86 o 0 0 6 3519.64 3637.92 24.55 o 1 0 6 622.05 659.26 8.99 o 2 0 6 0.02 0.80 0.64 o 3 0 6 360.25 383.87 9.04 o 4 0 6 101.10 94.18 4.87 o 5 0 6 447.05 445.13 19.66 o 6 0 6 44.95 45.29 4.07 o 7 0 6 332.58 303.70 13.39 o 8 0 6 213.79 225.20 12.77 o 1 1 6 50.17 50.27 2.20 o 2 1 6 3.98 6.18 1.15 o 3 1 6 918.72 879.10 8.30 o 4 1 6 515.95 541.85 13.28 o 5 1 6 9.83 6.31 5.06 o 6 1 6 103.30 109.29 5.00 o 7 1 6 31.87 38.90 5.01 o 8 1 6 37.40 44.85 7.28 o 0 2 6 45.50 46.71 4.95 o 1 2 6 279.27 297.58 5.45 o 2 2 6 0.11 0.17 0.49 o 3 2 6 144.37 149.40 5.74 o 4 2 6 1.80 0.88 2.02 o 5 2 6 27.00 24.95 3.64 o 6 2 6 14.15 10.81 2.08 o 7 2 6 10.32 11.79 2.30 o 8 2 6 5.22 3.47 1.80 o 1 3 6 932.81 1031.68 9.86 o 2 3 6 416.27 469.24 16.61 o 3 3 6 7.36 16.06 2.19 o 4 3 6 6.64 5.62 1.36 o 5 3 6 8.94 14.31 4.62 o 6 3 6 181.71 168.46 8.57 o 7 3 6 39.28 32.93 3.71 o 8 3 6 0.76 2.80 2.19 o 0 4 6 1305.08 1305.10 17.58 o 1 4 6 75.79 70.55 2.80 o 2 4 6 12.77 14.30 2.06 o 3 4 6 105.14 107.52 9.06 o 4 4 6 70.98 70.27 8.21 o 5 4 6 77.19 69.08 8.54 o 6 4 6 2.84 7.27 2.50 o 7 4 6 113.99 100.79 6.48 o 1 5 6 107.56 117.75 3.13 o 2 5 6 2.40 1.76 1.01 o 3 5 6 327.86 309.43 15.75 o 4 5 6 227.46 231.25 14.91 o 5 5 6 6.32 11.01 4.05 o 6 5 6 48.30 39.76 7.44 o 7 5 6 0.00 -0.19 2.25 o 0 6 6 54.22 72.53 4.96 o 1 6 6 606.38 595.43 7.74 o 2 6 6 0.40 -0.36 1.58 o 3 6 6 569.36 566.43 22.71 o 4 6 6 14.10 11.54 3.91 o 5 6 6 1.66 3.61 2.67 o 6 6 6 48.01 45.76 8.28 o 7 6 6 5.86 -1.24 3.27 o 1 7 6 525.70 518.22 9.34 o 2 7 6 430.20 416.66 14.23 o 3 7 6 242.46 226.72 14.88 o 4 7 6 57.58 59.52 8.24 o 5 7 6 39.02 37.42 7.20 o 6 7 6 115.83 126.25 13.76 o 0 8 6 353.23 377.43 12.71 o 1 8 6 107.51 105.95 6.15 o 2 8 6 2.15 4.42 2.24 o 3 8 6 97.89 84.08 9.55 o 4 8 6 29.68 35.44 6.86 o 5 8 6 5.58 -2.20 2.61 o 1 9 6 412.42 431.82 12.99 o 2 9 6 55.25 49.92 5.81 o 3 9 6 2.16 2.57 2.47 o 4 9 6 0.01 -0.89 2.56 o 0 10 6 23.34 23.05 6.33 o 1 10 6 120.50 136.34 7.80 o 2 10 6 0.41 3.03 2.23 o 3 10 6 146.74 169.06 14.39 o 1 1 7 15.93 18.21 1.25 o 2 1 7 194.75 187.47 5.59 o 3 1 7 8.65 9.29 1.01 o 4 1 7 109.25 97.95 3.99 o 5 1 7 108.82 96.13 6.99 o 6 1 7 558.58 571.12 14.55 o 7 1 7 5.00 4.19 2.36 o 8 1 7 0.30 0.88 1.55 o 0 2 7 2058.72 2229.39 34.37 o 1 2 7 41.83 32.05 1.43 o 2 2 7 88.09 72.74 4.22 o 3 2 7 51.29 45.49 6.65 o 4 2 7 157.80 143.56 11.14 o 5 2 7 4.70 3.19 1.93 o 6 2 7 532.14 502.31 16.96 o 7 2 7 137.93 126.40 9.10 o 8 2 7 0.49 -0.72 6.09 o 1 3 7 14.46 12.40 1.44 o 2 3 7 27.13 39.33 5.03 o 3 3 7 13.25 8.62 1.65 o 4 3 7 335.01 303.99 16.77 o 5 3 7 251.35 225.63 15.55 o 6 3 7 847.91 838.35 22.17 o 7 3 7 29.73 26.46 4.49 o 0 4 7 382.12 418.23 10.45 o 1 4 7 13.90 13.48 1.44 o 2 4 7 157.70 147.20 4.40 o 3 4 7 0.27 0.65 2.24 o 4 4 7 16.95 10.23 3.49 o 5 4 7 86.62 71.35 9.03 o 6 4 7 445.74 411.32 22.95 o 7 4 7 110.71 100.66 8.36 o 1 5 7 35.03 34.16 1.53 o 2 5 7 140.08 153.56 10.51 o 3 5 7 144.32 148.20 11.39 o 4 5 7 112.46 111.65 10.69 o 5 5 7 48.26 55.57 8.37 o 6 5 7 5.15 4.21 2.75 o 7 5 7 42.50 33.00 7.73 o 0 6 7 1502.01 1520.48 22.54 o 1 6 7 25.44 23.00 2.06 o 2 6 7 8.78 9.08 2.43 o 3 6 7 29.39 22.19 4.95 o 4 6 7 1.17 1.56 3.14 o 5 6 7 49.69 42.63 7.54 o 6 6 7 12.01 21.56 6.27 o 1 7 7 23.71 23.49 2.97 o 2 7 7 6.11 6.15 2.70 o 3 7 7 3.34 4.57 2.40 o 4 7 7 0.28 -1.24 1.84 o 5 7 7 0.45 3.38 3.44 o 6 7 7 51.01 36.84 7.62 o 0 8 7 10.91 10.52 2.62 o 1 8 7 27.89 26.03 3.18 o 2 8 7 12.16 9.91 2.89 o 3 8 7 24.50 17.57 3.66 o 4 8 7 4.33 0.93 2.18 o 5 8 7 1.15 1.82 2.23 o 1 9 7 8.27 3.52 1.87 o 2 9 7 193.51 211.06 12.76 o 3 9 7 96.98 106.46 11.49 o 4 9 7 15.90 15.97 4.94 o 0 10 7 273.72 262.93 20.57 o 1 10 7 28.33 41.00 6.58 o 2 10 7 1.03 0.89 1.67 o 3 10 7 2.05 5.52 2.74 o 0 0 8 68.08 77.59 4.24 o 1 0 8 464.60 444.87 7.23 o 2 0 8 872.59 892.34 28.71 o 3 0 8 159.61 164.14 11.78 o 4 0 8 139.53 151.98 12.00 o 5 0 8 900.91 904.31 30.63 o 6 0 8 43.43 50.81 8.17 o 7 0 8 75.03 78.06 7.42 o 1 1 8 1210.38 1245.55 8.85 o 2 1 8 11.40 11.90 1.34 o 3 1 8 1.05 1.89 0.73 o 4 1 8 59.99 66.00 14.68 o 5 1 8 106.40 104.19 7.60 o 6 1 8 107.92 103.06 6.53 o 7 1 8 42.77 44.77 5.72 o 0 2 8 623.56 688.26 20.22 o 1 2 8 25.88 25.48 1.59 o 2 2 8 157.39 170.19 7.96 o 3 2 8 0.17 0.22 0.49 o 4 2 8 1.32 -0.31 1.03 o 5 2 8 61.24 58.42 5.68 o 6 2 8 13.64 10.48 3.10 o 7 2 8 11.27 10.21 3.08 o 1 3 8 192.25 181.46 5.34 o 2 3 8 79.23 87.17 3.09 o 3 3 8 107.02 112.27 9.81 o 4 3 8 26.92 21.32 4.92 o 5 3 8 25.62 30.24 6.35 o 6 3 8 73.85 69.87 6.76 o 7 3 8 9.64 7.59 2.94 o 0 4 8 449.45 493.54 11.96 o 1 4 8 296.24 284.62 6.16 o 2 4 8 47.65 40.01 5.57 o 3 4 8 2.63 1.38 2.08 o 4 4 8 53.98 43.00 6.82 o 5 4 8 190.00 178.45 14.42 o 6 4 8 0.32 2.76 3.30 o 7 4 8 12.95 3.89 3.36 o 1 5 8 725.23 696.36 10.81 o 2 5 8 4.36 4.75 2.54 o 3 5 8 8.36 11.68 3.70 o 4 5 8 96.65 107.05 10.69 o 5 5 8 107.72 96.86 10.92 o 6 5 8 16.81 20.22 5.69 o 0 6 8 538.31 528.35 24.41 o 1 6 8 112.55 110.61 4.29 o 2 6 8 105.17 103.09 7.18 o 3 6 8 75.52 61.10 7.80 o 4 6 8 0.28 -2.66 2.66 o 5 6 8 32.77 35.89 7.36 o 6 6 8 0.77 -1.11 2.29 o 1 7 8 90.04 86.52 5.49 o 2 7 8 191.50 215.93 10.71 o 3 7 8 165.12 166.63 13.36 o 4 7 8 11.87 13.12 4.31 o 5 7 8 13.47 7.84 4.47 o 0 8 8 982.37 1018.65 37.16 o 1 8 8 18.39 19.09 3.32 o 2 8 8 60.14 53.53 5.78 o 3 8 8 3.78 6.88 2.66 o 4 8 8 5.91 0.14 2.33 o 5 8 8 1.27 1.50 2.73 o 1 9 8 19.51 28.75 5.07 o 2 9 8 3.58 1.47 7.49 o 3 9 8 0.50 3.96 2.55 o 0 10 8 5.82 8.15 4.34 o 1 10 8 77.61 88.75 8.83 o 2 10 8 16.60 11.88 6.06 o 1 1 9 10.42 8.82 1.26 o 2 1 9 20.76 21.61 2.31 o 3 1 9 211.90 201.45 6.41 o 4 1 9 307.67 286.51 12.34 o 5 1 9 2.91 3.07 2.39 o 6 1 9 15.17 18.71 3.17 o 7 1 9 1.22 2.67 3.72 o 0 2 9 9.02 10.86 3.19 o 1 2 9 72.79 77.89 7.45 o 2 2 9 6.40 14.58 4.02 o 3 2 9 801.36 768.76 19.20 o 4 2 9 420.12 381.57 19.97 o 5 2 9 189.94 168.00 9.91 o 6 2 9 4.10 1.22 2.79 o 7 2 9 9.52 5.23 2.66 o 1 3 9 387.96 369.48 8.89 o 2 3 9 4.43 5.02 0.72 o 3 3 9 90.01 89.13 8.93 o 4 3 9 386.69 368.85 19.59 o 5 3 9 39.31 39.99 5.18 o 6 3 9 33.67 31.66 5.71 o 7 3 9 18.58 15.61 3.66 o 0 4 9 4.36 5.43 2.96 o 1 4 9 176.13 184.38 5.25 o 2 4 9 243.11 247.70 10.39 o 3 4 9 241.30 226.03 14.46 o 4 4 9 327.35 307.66 18.30 o 5 4 9 2.59 3.31 3.07 o 6 4 9 2.88 -2.65 2.65 o 1 5 9 560.58 577.92 9.96 o 2 5 9 127.99 123.59 13.77 o 3 5 9 221.91 230.63 14.83 o 4 5 9 6.18 9.73 3.85 o 5 5 9 50.01 52.14 8.49 o 6 5 9 1.23 1.64 2.67 o 0 6 9 0.00 1.09 1.24 o 1 6 9 29.40 32.82 3.48 o 2 6 9 173.22 179.45 9.57 o 3 6 9 5.84 4.20 2.73 o 4 6 9 2.51 -3.33 3.33 o 5 6 9 18.63 10.81 3.99 o 6 6 9 3.07 7.65 3.45 o 1 7 9 1.73 0.19 1.28 o 2 7 9 52.60 55.96 5.74 o 3 7 9 65.22 59.88 6.26 o 4 7 9 37.53 40.23 7.42 o 5 7 9 0.15 -2.75 3.00 o 0 8 9 53.97 56.25 9.26 o 1 8 9 27.34 29.00 4.95 o 2 8 9 54.45 56.21 5.94 o 3 8 9 2.56 1.24 1.73 o 4 8 9 98.59 94.27 8.49 o 1 9 9 179.11 217.68 13.31 o 2 9 9 11.89 16.04 5.96 o 3 9 9 40.56 48.08 6.81 o 0 0 10 179.47 188.57 11.72 o 1 0 10 0.26 0.38 1.08 o 2 0 10 995.10 958.47 17.50 o 3 0 10 54.16 48.85 7.30 o 4 0 10 11.17 12.90 4.54 o 5 0 10 8.52 10.15 5.35 o 6 0 10 24.40 20.91 6.73 o 7 0 10 0.44 7.08 5.55 o 1 1 10 62.19 66.67 2.64 o 2 1 10 464.29 472.47 7.79 o 3 1 10 237.78 219.84 9.42 o 4 1 10 582.00 634.17 19.01 o 5 1 10 0.87 2.23 2.22 o 6 1 10 6.91 7.72 5.29 o 7 1 10 17.62 15.52 4.05 o 0 2 10 10.21 7.80 2.94 o 1 2 10 9.36 9.24 3.43 o 2 2 10 5.06 2.73 1.59 o 3 2 10 0.15 -0.33 1.32 o 4 2 10 2.72 -2.63 3.73 o 5 2 10 15.94 10.91 3.21 o 6 2 10 0.87 -1.50 2.10 o 7 2 10 0.19 -1.32 4.95 o 1 3 10 2.78 -0.57 2.54 o 2 3 10 20.82 38.19 6.42 o 3 3 10 66.50 64.54 8.10 o 4 3 10 38.72 35.98 5.84 o 5 3 10 13.73 9.81 2.85 o 6 3 10 2.05 1.14 3.15 o 0 4 10 89.24 71.95 5.13 o 1 4 10 0.75 1.27 1.05 o 2 4 10 567.53 547.01 15.92 o 3 4 10 60.28 53.31 7.40 o 4 4 10 1.47 1.40 2.50 o 5 4 10 0.59 0.66 2.47 o 6 4 10 52.47 54.36 6.40 o 1 5 10 51.51 54.23 4.82 o 2 5 10 52.56 42.44 4.82 o 3 5 10 126.78 101.63 10.23 o 4 5 10 52.78 62.35 8.66 o 5 5 10 0.18 0.82 1.87 o 6 5 10 5.97 9.21 4.51 o 0 6 10 149.97 143.33 13.48 o 1 6 10 29.12 31.46 3.49 o 2 6 10 49.42 39.20 4.93 o 3 6 10 0.06 4.38 3.16 o 4 6 10 0.37 -0.27 3.16 o 5 6 10 44.68 29.35 6.44 o 1 7 10 22.75 19.97 4.09 o 2 7 10 126.12 132.23 8.87 o 3 7 10 2.30 0.06 2.53 o 4 7 10 6.90 9.06 3.99 o 0 8 10 29.33 32.06 7.47 o 1 8 10 8.00 5.11 2.63 o 2 8 10 36.31 22.05 6.55 o 3 8 10 19.39 20.40 4.17 o 1 9 10 7.84 11.78 4.09 o 1 1 11 4.80 2.54 0.91 o 2 1 11 86.10 84.08 4.01 o 3 1 11 0.19 -2.08 2.08 o 4 1 11 100.79 105.57 8.23 o 5 1 11 57.51 70.28 7.16 o 6 1 11 22.36 23.61 4.71 o 0 2 11 237.48 238.81 9.83 o 1 2 11 680.61 686.59 13.60 o 2 2 11 124.01 116.39 5.67 o 3 2 11 471.08 436.90 22.19 o 4 2 11 3.25 -0.20 3.88 o 5 2 11 5.72 5.17 3.27 o 6 2 11 59.94 60.27 6.98 o 1 3 11 258.41 260.71 15.43 o 2 3 11 304.84 289.79 16.94 o 3 3 11 1.03 1.81 2.17 o 4 3 11 74.41 64.88 11.41 o 5 3 11 98.03 110.60 8.82 o 6 3 11 115.84 132.72 10.20 o 0 4 11 170.80 180.45 8.27 o 1 4 11 199.50 198.18 9.34 o 2 4 11 90.53 99.32 7.17 o 3 4 11 426.43 409.91 15.17 o 4 4 11 39.87 42.30 7.52 o 5 4 11 4.40 1.14 7.67 o 1 5 11 381.73 387.79 17.27 o 2 5 11 43.97 50.10 5.35 o 3 5 11 2.42 2.21 1.93 o 4 5 11 64.03 62.59 8.87 o 5 5 11 0.86 1.95 2.26 o 0 6 11 2.44 1.65 3.06 o 1 6 11 15.74 10.87 3.15 o 2 6 11 202.33 202.61 10.71 o 3 6 11 35.82 41.09 6.43 o 4 6 11 31.20 26.94 6.19 o 1 7 11 2.07 -2.63 2.63 o 2 7 11 39.48 55.52 9.42 o 3 7 11 8.55 12.02 3.59 o 0 8 11 107.22 137.84 15.04 o 1 8 11 27.56 25.75 5.17 o 2 8 11 38.60 47.76 9.46 o 0 0 12 607.05 578.24 22.80 o 1 0 12 282.56 287.99 8.40 o 2 0 12 326.00 338.62 9.20 o 3 0 12 99.85 105.04 11.37 o 4 0 12 88.77 86.29 11.20 o 5 0 12 19.93 28.55 7.06 o 6 0 12 4.14 7.26 5.50 o 1 1 12 393.44 373.25 8.95 o 2 1 12 81.30 70.66 4.04 o 3 1 12 13.02 11.34 2.45 o 4 1 12 30.65 29.75 4.89 o 5 1 12 3.85 3.13 3.00 o 6 1 12 1.01 6.50 4.23 o 0 2 12 372.80 399.95 13.18 o 1 2 12 5.44 4.97 1.55 o 2 2 12 64.12 68.31 7.06 o 3 2 12 10.27 10.17 4.98 o 4 2 12 7.97 6.28 4.48 o 5 2 12 0.01 -2.28 5.34 o 1 3 12 95.77 101.22 10.10 o 2 3 12 1.61 2.55 1.93 o 3 3 12 1.79 -1.45 2.28 o 4 3 12 54.21 42.99 5.51 o 5 3 12 17.67 26.59 4.78 o 0 4 12 0.33 -0.17 3.10 o 1 4 12 102.55 92.62 6.64 o 2 4 12 22.59 22.00 3.80 o 3 4 12 5.44 2.56 2.09 o 4 4 12 34.35 41.52 5.39 o 5 4 12 1.09 4.91 2.60 o 1 5 12 231.93 239.75 17.34 o 2 5 12 14.61 14.42 3.20 o 3 5 12 13.88 13.25 3.16 o 4 5 12 71.96 74.49 7.39 o 0 6 12 350.41 389.82 23.03 o 1 6 12 1.26 3.42 3.47 o 2 6 12 21.40 24.59 4.08 o 3 6 12 0.04 -0.79 2.19 o 4 6 12 16.62 20.72 9.73 o 1 7 12 2.84 2.06 3.13 o 2 7 12 0.00 5.88 4.31 o 1 1 13 110.56 111.93 6.37 o 2 1 13 113.61 118.27 6.46 o 3 1 13 66.26 65.59 6.84 o 4 1 13 18.89 22.55 4.52 o 5 1 13 3.78 4.05 3.05 o 0 2 13 5.44 2.13 3.13 o 1 2 13 11.64 13.81 2.60 o 2 2 13 0.18 0.64 1.66 o 3 2 13 1.71 3.18 2.02 o 4 2 13 181.11 194.12 16.93 o 5 2 13 9.80 3.07 2.98 o 1 3 13 194.72 206.03 8.46 o 2 3 13 195.13 199.17 8.32 o 3 3 13 194.91 207.10 9.26 o 4 3 13 64.61 62.23 5.41 o 0 4 13 181.27 194.39 14.94 o 1 4 13 21.27 27.29 6.13 o 2 4 13 9.54 13.15 3.11 o 3 4 13 18.21 13.67 3.13 o 4 4 13 54.94 61.23 5.53 o 1 5 13 0.15 -0.56 3.34 o 2 5 13 0.25 1.59 2.83 o 3 5 13 17.96 12.20 5.37 o 0 6 13 120.17 122.04 13.30 o 1 6 13 35.41 33.79 7.85 o 2 6 13 4.95 7.65 4.94 o 0 0 14 1026.82 1064.59 34.08 o 1 0 14 96.10 100.09 7.55 o 2 0 14 22.06 15.14 5.28 o 3 0 14 22.97 25.87 6.92 o 4 0 14 42.90 44.40 8.90 o 1 1 14 208.70 205.79 8.80 o 2 1 14 140.32 167.39 21.06 o 3 1 14 0.29 -0.08 2.63 o 4 1 14 20.59 21.09 7.24 o 0 2 14 64.02 49.86 7.79 o 1 2 14 4.23 2.73 1.91 o 2 2 14 1.40 -3.36 4.50 o 3 2 14 14.93 15.00 5.71 o 4 2 14 40.79 42.77 8.99 o 1 3 14 18.88 26.90 3.33 o 2 3 14 28.00 27.08 3.45 o 3 3 14 45.73 37.53 4.91 o 0 4 14 360.50 367.81 14.93 o 1 4 14 50.11 52.09 6.29 o 2 4 14 3.71 2.97 2.13 o 3 4 14 8.94 10.59 2.64 o 1 5 14 28.60 26.22 6.25 o 2 5 14 84.03 105.02 12.54 o 1 1 15 22.64 30.51 4.50 o 2 1 15 6.51 8.77 3.33 o 3 1 15 44.65 54.87 6.84 o 0 2 15 112.09 119.16 12.26 o 1 2 15 70.60 70.44 6.68 o 2 2 15 4.14 11.72 4.68 o 1 3 15 21.48 13.79 3.25 o 2 3 15 3.03 9.34 5.03 o 0 4 15 27.31 25.62 6.02 o 1 4 15 21.63 14.82 4.65 o 0 0 16 39.38 62.01 9.49 o