#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/67/2236726.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236726_Fobs loop_ _publ_author_name 'Kunnath, Roji J.' 'Prathapachandra Kurup, M. R.' 'Ng, Seik Weng' _publ_section_title ; Di-\m-azido-\k^4^N^1^:N^1'^-bis({1-[(E)-phenyl(pyridin-2-yl-\kN)methylidene]thiosemicarbazidato-\k^2^N^1^,S}copper(II)) ; _journal_coeditor_code XU5611 _journal_issue 9 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1195 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 96.653 _cell_angle_gamma 90.000 _cell_length_a 11.2462 _cell_length_b 7.2344 _cell_length_c 18.5187 _exptl_crystal_F_000 732.00 _reflns_d_resolution_high 0.7472 _[local]_cod_data_source_file xu5611Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P21/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 172.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 8446.99 9346.25 669.84 o 3 0 0 2475.91 2876.54 168.36 o 4 0 0 16203.69 20770.55 1477.76 o 5 0 0 2279.91 2267.19 145.05 o 6 0 0 7177.90 7466.38 547.26 o 7 0 0 1887.27 1926.94 123.35 o 8 0 0 777.08 746.00 49.35 o 9 0 0 118.59 113.29 10.81 o 10 0 0 328.00 396.63 27.12 o 11 0 0 1069.26 1032.60 68.21 o 12 0 0 694.43 718.95 53.27 o 13 0 0 0.41 2.31 6.53 o 14 0 0 98.13 131.46 18.07 o 1 1 0 19230.07 17726.04 926.78 o 2 1 0 1377.36 1548.02 69.91 o 3 1 0 1324.02 1374.60 74.08 o 4 1 0 1851.14 1817.82 77.19 o 5 1 0 33.48 33.52 2.22 o 6 1 0 3.98 2.43 2.41 o 7 1 0 1931.28 2154.32 117.11 o 8 1 0 885.65 860.50 42.05 o 9 1 0 607.29 604.68 28.53 o 10 1 0 367.77 369.14 17.92 o 11 1 0 76.94 76.27 6.26 o 12 1 0 467.42 485.78 28.27 o 13 1 0 342.32 378.67 24.18 o 14 1 0 103.68 105.67 8.94 o 0 2 0 4586.65 4539.18 293.76 o 1 2 0 51.31 62.81 3.85 o 2 2 0 8.24 11.63 2.64 o 3 2 0 1813.11 2071.93 108.73 o 4 2 0 493.46 632.58 26.93 o 5 2 0 3524.85 3897.64 195.93 o 6 2 0 3116.45 3168.44 204.38 o 7 2 0 729.09 674.52 44.14 o 8 2 0 661.88 644.55 35.92 o 9 2 0 31.67 24.76 4.77 o 10 2 0 26.09 27.40 5.22 o 11 2 0 200.95 231.61 14.61 o 12 2 0 92.94 83.51 7.17 o 13 2 0 16.82 -4.31 6.35 o 14 2 0 0.28 -6.07 6.07 o 1 3 0 2.23 -1.78 2.84 o 2 3 0 11.92 10.87 3.41 o 3 3 0 1513.84 1449.10 81.12 o 4 3 0 1486.52 1755.14 92.29 o 5 3 0 1871.89 2427.24 147.30 o 6 3 0 0.21 1.11 3.58 o 7 3 0 1629.02 1834.34 115.37 o 8 3 0 223.58 257.41 26.21 o 9 3 0 6.35 6.01 6.32 o 10 3 0 35.29 24.17 5.45 o 11 3 0 16.55 7.67 6.05 o 12 3 0 52.12 46.58 11.85 o 13 3 0 0.26 -3.53 5.89 o 14 3 0 5.81 3.57 6.46 o 0 4 0 743.70 855.94 61.64 o 1 4 0 2221.75 2303.19 116.04 o 2 4 0 116.94 97.67 7.88 o 3 4 0 266.94 293.76 21.16 o 4 4 0 1652.03 1679.30 106.49 o 5 4 0 1305.41 1417.50 85.90 o 6 4 0 249.52 253.80 18.18 o 7 4 0 1361.84 1501.81 87.07 o 8 4 0 21.01 16.25 7.49 o 9 4 0 0.62 -4.54 4.54 o 10 4 0 115.91 105.20 15.43 o 11 4 0 201.43 204.98 35.56 o 12 4 0 5.59 1.15 5.52 o 13 4 0 59.76 45.50 20.36 o 1 5 0 379.84 324.50 22.63 o 2 5 0 697.90 675.84 53.48 o 3 5 0 3674.14 3593.16 263.68 o 4 5 0 2110.02 1991.61 149.30 o 5 5 0 22.78 32.01 5.51 o 6 5 0 22.49 22.15 6.47 o 7 5 0 1728.23 1797.43 121.34 o 8 5 0 265.74 328.68 34.73 o 9 5 0 69.25 58.43 9.82 o 10 5 0 40.71 47.89 7.33 o 11 5 0 1.59 -0.20 4.54 o 12 5 0 14.31 9.51 6.08 o 0 6 0 1946.34 2150.89 209.29 o 1 6 0 754.70 758.26 46.05 o 2 6 0 841.24 855.97 67.41 o 3 6 0 6.79 0.01 7.31 o 4 6 0 244.30 270.38 24.90 o 5 6 0 919.30 1076.77 75.90 o 6 6 0 963.07 1129.86 87.20 o 7 6 0 154.58 183.51 18.02 o 8 6 0 0.69 7.04 4.77 o 9 6 0 17.59 16.23 5.52 o 10 6 0 11.37 6.73 8.27 o 11 6 0 125.05 111.20 13.17 o 1 7 0 436.26 446.07 34.62 o 2 7 0 583.14 543.29 55.80 o 3 7 0 317.99 319.59 29.57 o 4 7 0 255.23 260.98 25.30 o 5 7 0 59.71 76.99 18.77 o 6 7 0 11.25 6.52 9.88 o 7 7 0 69.87 80.46 12.53 o 8 7 0 190.57 226.87 23.06 o 9 7 0 116.90 163.00 27.73 o 10 7 0 84.72 124.15 76.30 o 0 8 0 169.56 135.96 64.77 o 1 8 0 41.62 38.46 11.45 o 2 8 0 24.42 27.59 8.85 o 3 8 0 24.75 24.66 9.04 o 4 8 0 4.31 -5.32 12.87 o 5 8 0 48.67 40.59 17.12 o 6 8 0 15.24 5.15 13.93 o 7 8 0 34.06 43.84 11.55 o 8 8 0 6.25 7.46 22.10 o 1 9 0 1.24 -2.49 8.45 o 2 9 0 3.19 12.76 33.06 o 3 9 0 19.98 33.66 25.37 o 4 9 0 30.85 46.84 18.66 o 5 9 0 85.68 56.16 38.05 o -14 1 1 36.73 35.66 5.45 o -13 1 1 103.42 107.53 8.94 o -12 1 1 132.81 120.27 8.94 o -11 1 1 528.81 520.61 29.91 o -10 1 1 1205.15 1242.49 57.31 o -9 1 1 550.79 524.82 24.67 o -8 1 1 361.01 352.98 17.07 o -7 1 1 3084.96 3099.87 154.68 o -6 1 1 709.95 634.12 30.77 o -5 1 1 644.98 587.84 25.81 o -4 1 1 625.60 613.37 33.30 o -3 1 1 24.79 26.18 1.68 o -2 1 1 2909.51 4179.04 175.82 o -1 1 1 240.11 302.89 19.43 o 0 1 1 5334.42 4212.30 296.99 o 1 1 1 6150.56 6530.61 325.22 o 2 1 1 1354.13 1627.41 60.92 o 3 1 1 2247.70 2397.21 102.61 o 4 1 1 7156.79 7574.18 320.93 o 5 1 1 1541.67 1796.39 86.05 o 6 1 1 3.07 3.63 1.40 o 7 1 1 57.54 68.86 4.41 o 8 1 1 60.50 47.70 5.57 o 9 1 1 378.15 366.65 18.66 o 10 1 1 823.71 851.49 39.87 o 11 1 1 882.27 929.18 43.38 o 12 1 1 708.89 771.23 43.40 o 13 1 1 2.03 -2.49 4.84 o 14 1 1 25.30 18.76 4.91 o -14 2 1 25.82 21.76 7.00 o -13 2 1 430.86 474.49 37.09 o -12 2 1 475.70 523.40 30.46 o -11 2 1 29.92 38.24 6.27 o -10 2 1 42.33 43.17 5.10 o -9 2 1 2250.94 2181.17 118.47 o -8 2 1 3244.30 3303.61 180.38 o -7 2 1 602.99 523.29 27.45 o -6 2 1 5.57 2.79 1.97 o -5 2 1 14.24 12.94 1.65 o -4 2 1 139.29 169.39 11.43 o -3 2 1 33.66 33.67 2.93 o -2 2 1 2475.17 2582.91 153.17 o -1 2 1 5089.95 4965.04 226.38 o 0 2 1 19021.18 22244.41 1102.41 o 1 2 1 943.71 794.97 33.69 o 2 2 1 1232.39 1185.86 61.57 o 3 2 1 4421.12 4967.67 277.67 o 4 2 1 6654.13 7150.86 347.68 o 5 2 1 18.19 21.13 2.43 o 6 2 1 74.08 81.55 5.05 o 7 2 1 61.03 54.58 8.65 o 8 2 1 1992.98 1910.31 122.84 o 9 2 1 505.55 449.78 25.93 o 10 2 1 301.82 289.24 19.47 o 11 2 1 15.05 13.18 6.46 o 12 2 1 401.60 475.47 27.85 o 13 2 1 255.06 273.57 21.05 o 14 2 1 168.32 182.10 16.97 o -14 3 1 1.52 -4.04 9.42 o -13 3 1 89.47 99.16 13.32 o -12 3 1 372.90 414.89 44.99 o -11 3 1 1202.16 1250.14 110.20 o -10 3 1 487.98 442.18 31.03 o -9 3 1 1542.55 1602.88 104.90 o -8 3 1 2.56 3.24 3.33 o -7 3 1 111.86 109.10 8.50 o -6 3 1 2838.60 3191.56 168.34 o -5 3 1 4726.44 5215.89 313.99 o -4 3 1 3223.21 3694.61 191.70 o -3 3 1 365.83 426.43 26.17 o -2 3 1 1412.18 1344.40 81.17 o -1 3 1 2011.95 2028.78 94.67 o 0 3 1 3675.03 3838.08 180.06 o 1 3 1 3405.89 3276.90 161.34 o 2 3 1 1515.65 1402.39 70.97 o 3 3 1 120.25 118.14 8.83 o 4 3 1 664.04 732.90 39.99 o 5 3 1 5506.64 5818.86 328.48 o 6 3 1 3044.43 3056.08 174.77 o 7 3 1 3434.29 3656.86 209.91 o 8 3 1 61.49 66.35 7.88 o 9 3 1 567.01 596.89 52.36 o 10 3 1 427.33 387.29 27.42 o 11 3 1 573.49 639.27 59.60 o 12 3 1 367.95 379.34 36.97 o 13 3 1 59.26 64.53 11.04 o 14 3 1 11.48 -3.25 12.88 o -13 4 1 122.33 139.66 13.65 o -12 4 1 49.75 49.00 8.05 o -11 4 1 1.03 -7.66 7.66 o -10 4 1 54.71 46.87 13.32 o -9 4 1 46.56 42.36 11.67 o -8 4 1 858.51 1032.72 73.02 o -7 4 1 1970.62 2189.82 125.98 o -6 4 1 2534.47 2778.22 192.87 o -5 4 1 0.15 -1.12 4.48 o -4 4 1 2249.21 2221.21 113.04 o -3 4 1 5853.69 5385.31 395.00 o -2 4 1 4641.96 4398.40 249.10 o -1 4 1 3.94 7.75 4.93 o 0 4 1 193.38 172.53 9.98 o 1 4 1 686.22 606.09 29.95 o 2 4 1 231.66 258.27 16.52 o 3 4 1 1155.34 1116.77 70.84 o 4 4 1 283.68 260.47 19.36 o 5 4 1 410.06 434.94 25.54 o 6 4 1 230.20 256.03 17.37 o 7 4 1 1819.44 1901.16 107.28 o 8 4 1 1826.28 1997.68 130.75 o 9 4 1 84.20 75.86 14.70 o 10 4 1 3.93 5.46 6.10 o 11 4 1 6.78 2.72 4.99 o 12 4 1 43.26 32.26 9.27 o 13 4 1 106.47 109.58 20.19 o -12 5 1 35.58 22.57 6.55 o -11 5 1 16.91 15.49 5.70 o -10 5 1 31.35 22.07 5.17 o -9 5 1 16.32 13.98 5.23 o -8 5 1 3.49 -3.24 4.08 o -7 5 1 20.58 19.18 7.36 o -6 5 1 258.63 266.39 27.30 o -5 5 1 254.81 274.55 29.02 o -4 5 1 367.56 294.40 33.56 o -3 5 1 311.28 364.27 30.69 o -2 5 1 3.97 -1.79 8.27 o -1 5 1 12.40 6.89 5.97 o 0 5 1 6.13 2.17 4.99 o 1 5 1 304.71 340.02 24.77 o 2 5 1 4.10 -5.68 5.68 o 3 5 1 76.52 93.63 11.96 o 4 5 1 3.53 0.11 5.89 o 5 5 1 24.41 24.43 5.07 o 6 5 1 129.37 128.70 12.82 o 7 5 1 166.57 172.48 12.73 o 8 5 1 137.75 120.72 10.59 o 9 5 1 4.37 5.31 5.24 o 10 5 1 82.13 75.29 24.41 o 11 5 1 49.13 44.58 7.52 o 12 5 1 48.47 43.26 10.86 o -11 6 1 0.66 -5.09 5.09 o -10 6 1 0.92 -4.53 5.37 o -9 6 1 23.99 27.05 5.98 o -8 6 1 11.66 7.09 4.16 o -7 6 1 15.08 21.18 9.08 o -6 6 1 79.16 97.13 12.14 o -5 6 1 17.39 18.24 5.97 o -4 6 1 37.62 47.27 9.44 o -3 6 1 497.93 465.00 38.92 o -2 6 1 24.36 18.95 7.23 o -1 6 1 53.24 63.71 11.77 o 0 6 1 188.64 171.22 18.97 o 1 6 1 165.50 182.28 14.03 o 2 6 1 184.73 155.44 29.57 o 3 6 1 18.01 16.80 8.25 o 4 6 1 33.06 30.25 8.79 o 5 6 1 26.01 24.99 5.71 o 6 6 1 1.99 -3.35 15.70 o 7 6 1 0.51 -4.14 8.15 o 8 6 1 54.94 64.89 7.52 o 9 6 1 23.91 31.04 6.11 o 10 6 1 35.15 44.01 8.71 o 11 6 1 9.59 14.71 6.86 o -10 7 1 56.31 67.20 55.93 o -9 7 1 0.21 -2.38 11.22 o -8 7 1 3.07 -2.00 10.59 o -7 7 1 0.47 -3.18 9.53 o -6 7 1 82.36 90.25 11.61 o -5 7 1 126.60 153.86 31.71 o -4 7 1 153.09 169.10 30.53 o -3 7 1 1.01 3.48 7.10 o -2 7 1 115.12 89.97 25.67 o -1 7 1 22.05 14.58 8.07 o 0 7 1 5.54 -6.16 6.69 o 1 7 1 24.19 9.90 7.83 o 2 7 1 152.59 144.31 18.75 o 3 7 1 109.09 93.95 13.72 o 4 7 1 29.70 25.25 12.47 o 5 7 1 315.27 353.47 88.98 o 6 7 1 228.25 271.05 23.40 o 7 7 1 179.14 170.78 17.67 o 8 7 1 2.03 -2.57 9.82 o 9 7 1 144.26 158.90 21.16 o 10 7 1 32.23 31.74 14.54 o -8 8 1 139.32 191.61 46.51 o -7 8 1 72.31 106.84 18.45 o -6 8 1 2.86 -1.48 14.85 o -5 8 1 13.34 8.09 14.66 o -4 8 1 118.36 122.64 14.87 o -3 8 1 188.37 208.88 25.69 o -2 8 1 240.75 239.17 36.55 o -1 8 1 126.12 127.67 27.18 o 0 8 1 19.93 10.11 8.06 o 1 8 1 12.92 20.09 8.78 o 2 8 1 328.61 372.06 36.01 o 3 8 1 415.82 425.95 44.94 o 4 8 1 220.62 278.06 28.05 o 5 8 1 11.52 9.21 14.78 o 6 8 1 9.20 2.13 14.85 o 7 8 1 17.29 16.69 16.54 o 8 8 1 120.70 133.53 21.54 o -5 9 1 55.81 26.91 50.35 o -4 9 1 171.46 159.70 57.46 o -3 9 1 23.64 21.35 15.60 o -2 9 1 0.62 -6.47 13.27 o -1 9 1 44.55 57.40 18.03 o 0 9 1 198.18 41.45 35.53 o 1 9 1 171.85 188.70 39.96 o 2 9 1 26.15 24.75 10.26 o 3 9 1 32.53 20.62 25.75 o 4 9 1 91.60 51.12 46.89 o 5 9 1 25.78 34.47 18.91 o -15 0 2 29.95 22.29 8.84 o -14 0 2 0.65 -5.00 7.30 o -13 0 2 62.87 81.49 13.07 o -12 0 2 166.84 177.25 19.03 o -11 0 2 1420.39 1522.65 98.62 o -10 0 2 470.77 520.95 34.23 o -9 0 2 5395.24 5483.28 349.68 o -8 0 2 38.95 37.56 4.61 o -7 0 2 6407.61 6212.10 395.32 o -6 0 2 13447.60 14657.03 900.27 o -5 0 2 11000.31 10966.24 692.04 o -4 0 2 602.89 601.37 38.98 o -3 0 2 481.01 562.45 39.56 o -2 0 2 861.32 846.28 40.17 o -1 0 2 13014.85 6908.94 493.31 o 0 0 2 25095.91 21000.53 1633.98 o 1 0 2 13096.21 13833.15 697.46 o 2 0 2 1153.47 1265.31 73.53 o 3 0 2 1105.61 1521.57 89.14 o 4 0 2 4352.93 4667.09 333.63 o 5 0 2 8712.88 8422.83 602.17 o 6 0 2 2026.16 1798.73 106.59 o 7 0 2 1729.23 1821.41 131.41 o 8 0 2 1127.60 1044.37 67.71 o 9 0 2 1027.30 945.54 61.78 o 10 0 2 93.09 95.45 8.59 o 11 0 2 1521.00 1558.33 101.95 o 12 0 2 1516.24 1610.17 105.39 o 13 0 2 107.45 133.76 17.68 o 14 0 2 34.49 68.80 11.92 o -14 1 2 78.98 89.18 8.05 o -13 1 2 283.72 307.61 20.04 o -12 1 2 420.25 451.13 28.26 o -11 1 2 189.94 188.25 13.81 o -10 1 2 5.72 1.40 2.59 o -9 1 2 140.95 147.04 8.34 o -8 1 2 3418.06 3689.57 198.45 o -7 1 2 2370.84 2311.15 99.37 o -6 1 2 94.63 59.27 3.40 o -5 1 2 0.26 5.76 2.76 o -4 1 2 1792.37 2195.26 94.40 o -3 1 2 589.56 590.61 24.45 o -2 1 2 1968.08 1949.80 87.79 o -1 1 2 22737.07 23706.05 1712.60 o 0 1 2 1872.72 1655.96 89.72 o 1 1 2 2720.81 2748.53 127.05 o 2 1 2 4136.23 4084.94 168.91 o 3 1 2 6894.51 7170.74 263.26 o 4 1 2 5874.47 6283.05 229.96 o 5 1 2 2377.76 2934.47 124.79 o 6 1 2 671.88 672.68 36.68 o 7 1 2 324.92 309.74 17.45 o 8 1 2 1116.54 1136.26 55.10 o 9 1 2 1189.74 1149.12 55.78 o 10 1 2 1675.25 1710.50 82.74 o 11 1 2 238.65 246.70 16.96 o 12 1 2 76.56 99.43 7.95 o 13 1 2 409.12 474.50 29.80 o 14 1 2 142.02 143.17 10.99 o -14 2 2 126.85 141.45 14.25 o -13 2 2 14.35 5.38 6.46 o -12 2 2 149.34 145.10 14.48 o -11 2 2 9.19 12.01 5.77 o -10 2 2 8.94 5.12 3.30 o -9 2 2 673.97 669.91 37.24 o -8 2 2 872.96 876.10 48.79 o -7 2 2 61.06 44.90 4.35 o -6 2 2 4.78 0.01 1.83 o -5 2 2 266.21 199.59 12.52 o -4 2 2 1999.32 2215.88 177.56 o -3 2 2 27.88 34.10 3.00 o -2 2 2 4218.97 4261.57 253.45 o -1 2 2 22701.98 25405.81 1346.20 o 0 2 2 4728.83 5022.38 224.29 o 1 2 2 2486.60 2416.84 106.64 o 2 2 2 1959.59 2116.60 100.60 o 3 2 2 171.74 167.10 8.63 o 4 2 2 100.59 109.63 5.68 o 5 2 2 2341.10 2544.79 127.94 o 6 2 2 4710.96 4908.10 262.81 o 7 2 2 430.01 399.70 22.62 o 8 2 2 55.01 59.03 11.37 o 9 2 2 510.50 490.51 32.95 o 10 2 2 47.92 43.25 7.48 o 11 2 2 406.31 403.11 23.88 o 12 2 2 10.94 12.48 4.99 o 13 2 2 0.88 -6.42 6.42 o 14 2 2 66.82 93.11 16.34 o -14 3 2 16.30 7.92 6.93 o -13 3 2 100.27 110.67 18.83 o -12 3 2 19.77 18.95 5.96 o -11 3 2 205.01 206.62 16.75 o -10 3 2 181.30 168.38 26.90 o -9 3 2 3.59 -4.67 4.67 o -8 3 2 186.12 172.38 15.10 o -7 3 2 6.55 4.33 2.90 o -6 3 2 328.90 330.96 17.92 o -5 3 2 544.85 592.32 48.37 o -4 3 2 12.02 3.04 2.57 o -3 3 2 45.80 39.40 5.38 o -2 3 2 3040.02 3386.30 200.46 o -1 3 2 1721.42 1697.47 98.12 o 0 3 2 1535.01 1590.76 75.88 o 1 3 2 307.97 305.16 16.79 o 2 3 2 115.37 131.10 8.41 o 3 3 2 1239.66 1281.14 71.29 o 4 3 2 109.08 156.39 8.56 o 5 3 2 777.72 802.62 38.22 o 6 3 2 10.58 10.07 3.34 o 7 3 2 128.73 143.66 16.67 o 8 3 2 236.40 210.34 16.93 o 9 3 2 138.09 138.93 22.79 o 10 3 2 21.57 14.65 6.33 o 11 3 2 49.96 47.80 10.04 o 12 3 2 8.65 10.91 6.14 o 13 3 2 183.93 203.27 25.56 o 14 3 2 32.83 34.02 8.03 o -13 4 2 0.31 4.89 8.18 o -12 4 2 27.36 20.23 6.83 o -11 4 2 13.06 11.57 7.78 o -10 4 2 14.25 12.66 5.38 o -9 4 2 2.89 -4.10 4.10 o -8 4 2 0.18 -7.02 7.02 o -7 4 2 521.60 503.62 37.15 o -6 4 2 153.52 182.74 14.17 o -5 4 2 1177.81 1401.59 97.74 o -4 4 2 1966.92 2183.74 102.92 o -3 4 2 146.25 170.77 13.74 o -2 4 2 331.13 365.92 23.10 o -1 4 2 3012.27 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