#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181290 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/68/2236832.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236832_Fobs loop_ _publ_author_name 'V\'ahovsk\'a, Lucia' 'Poto\N,N')iron(II) bis(tricyanomethanide) ; _journal_coeditor_code BX2428 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1524 _journal_page_last m1525 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.458 _cell_angle_beta 89.623 _cell_angle_gamma 82.323 _cell_length_a 9.3676 _cell_length_b 12.7079 _cell_length_c 18.1998 _exptl_crystal_F_000 892.00 _reflns_d_resolution_high 0.8107 _cod_data_source_file bx2428Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' exp_379t' _shelx_refln_list_code 4 _shelx_f_calc_maximum 267.40 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3709.87 3643.99 21.48 o 3 0 0 144.77 147.83 5.32 o 4 0 0 94.09 92.11 4.96 o 5 0 0 236.96 197.86 7.49 o 6 0 0 311.23 326.26 30.87 o 7 0 0 517.01 500.97 13.73 o 8 0 0 106.29 116.44 29.01 o 9 0 0 4.44 9.32 11.62 o 10 0 0 35.15 19.94 21.44 o 11 0 0 68.13 103.19 20.76 o -11 1 0 136.60 163.52 23.71 o -10 1 0 33.88 32.80 15.85 o -9 1 0 89.28 102.60 19.50 o -8 1 0 819.97 807.53 25.41 o -7 1 0 2.44 1.37 5.34 o -6 1 0 148.67 139.86 8.99 o -5 1 0 4.21 9.69 4.81 o -4 1 0 4.60 8.21 3.85 o -3 1 0 126.17 118.57 6.29 o -2 1 0 3397.02 3350.80 25.10 o 2 1 0 6587.07 6448.27 33.30 o 3 1 0 171.80 150.64 5.38 o 4 1 0 5.36 4.36 2.20 o 5 1 0 2218.35 2446.98 20.36 o 6 1 0 2917.08 2784.79 55.35 o 7 1 0 745.24 670.45 14.27 o 8 1 0 1362.27 1362.00 73.91 o 9 1 0 59.70 45.11 17.45 o 10 1 0 226.56 183.81 28.90 o 11 1 0 163.00 158.59 26.18 o -11 2 0 263.57 271.32 40.06 o -10 2 0 533.05 518.18 37.45 o -9 2 0 421.27 458.88 32.75 o -8 2 0 989.84 913.19 29.40 o -7 2 0 31.34 33.32 6.71 o -6 2 0 3111.66 3004.51 38.92 o -5 2 0 8.80 6.02 5.23 o -4 2 0 3183.09 3032.23 30.76 o -3 2 0 176.34 175.25 8.85 o -2 2 0 24648.93 25005.15 96.67 o -1 2 0 13.01 38.53 8.23 o 0 2 0 15155.16 16870.49 138.91 o 1 2 0 163.71 164.86 5.68 o 2 2 0 1009.99 1059.85 17.71 o 3 2 0 17.25 12.01 2.78 o 4 2 0 158.06 141.99 4.95 o 5 2 0 35.52 10.45 4.85 o 6 2 0 2220.31 2117.59 54.86 o 7 2 0 1136.36 1139.33 45.78 o 8 2 0 946.02 870.60 57.62 o 9 2 0 50.10 47.14 13.69 o 10 2 0 346.82 331.98 31.25 o 11 2 0 129.03 124.41 21.59 o -10 3 0 44.05 18.35 16.97 o -9 3 0 767.88 745.23 41.50 o -8 3 0 82.75 84.53 12.48 o -7 3 0 1256.53 1202.55 28.45 o -6 3 0 336.22 399.22 23.74 o -5 3 0 678.82 619.34 18.64 o -4 3 0 1159.82 1156.01 22.92 o -3 3 0 8113.12 8590.48 55.54 o -2 3 0 2546.90 2373.89 25.72 o -1 3 0 712.77 725.80 14.69 o 0 3 0 1202.30 1327.95 28.62 o 1 3 0 1034.73 954.71 17.65 o 2 3 0 23791.29 24576.33 94.43 o 3 3 0 275.19 296.12 7.94 o 4 3 0 191.43 215.62 6.79 o 5 3 0 18.85 13.68 3.37 o 6 3 0 154.98 139.04 5.72 o 7 3 0 1107.07 1042.69 53.60 o 8 3 0 1607.78 1605.97 56.75 o 9 3 0 59.82 57.69 16.96 o 10 3 0 157.63 119.44 22.16 o 11 3 0 62.05 68.00 20.24 o -10 4 0 46.27 14.90 19.74 o -9 4 0 105.34 123.25 27.44 o -8 4 0 625.41 648.38 28.74 o -7 4 0 629.01 652.02 26.40 o -6 4 0 1.40 10.23 8.38 o -5 4 0 1698.22 1596.39 35.74 o -4 4 0 62.24 32.82 6.22 o -3 4 0 4698.66 5140.86 45.37 o -2 4 0 2833.84 2632.21 35.05 o -1 4 0 924.07 779.59 16.19 o 0 4 0 6813.04 7539.49 164.42 o 1 4 0 8.67 9.19 9.74 o 2 4 0 3193.37 2968.19 26.39 o 3 4 0 3903.95 4759.23 37.63 o 4 4 0 2692.86 2556.87 24.27 o 5 4 0 0.42 2.66 4.43 o 6 4 0 265.41 415.11 17.07 o 7 4 0 41.75 42.57 6.46 o 8 4 0 199.02 257.36 48.90 o 9 4 0 11.09 23.14 16.68 o 10 4 0 68.79 57.50 20.38 o 11 4 0 396.59 454.55 38.97 o -10 5 0 3.63 5.94 20.02 o -9 5 0 27.42 35.94 19.55 o -8 5 0 34.60 30.90 10.97 o -7 5 0 346.40 363.77 26.05 o -6 5 0 2389.21 2364.58 82.71 o -5 5 0 207.35 191.72 29.62 o -4 5 0 95.41 90.00 11.58 o -3 5 0 155.12 304.99 15.23 o -2 5 0 1081.65 1165.06 24.57 o -1 5 0 2253.60 2156.68 40.96 o 0 5 0 949.56 1113.68 33.58 o 1 5 0 4421.59 4243.04 31.54 o 2 5 0 4100.50 3983.99 32.73 o 3 5 0 5427.69 5696.23 47.06 o 4 5 0 380.44 352.67 16.78 o 5 5 0 563.35 492.33 14.10 o 6 5 0 2167.08 2147.09 28.50 o 7 5 0 14.67 13.05 4.16 o 8 5 0 22.47 79.96 33.01 o 9 5 0 12.28 23.34 19.63 o 10 5 0 42.08 60.14 19.76 o 11 5 0 43.14 49.22 20.43 o -9 6 0 542.52 584.24 53.92 o -8 6 0 45.23 54.40 14.01 o -7 6 0 194.35 225.82 23.23 o -6 6 0 79.24 155.68 33.34 o -5 6 0 107.94 112.20 24.39 o -4 6 0 40.84 45.50 9.04 o -3 6 0 15.88 29.97 7.17 o -2 6 0 176.30 203.51 12.70 o -1 6 0 789.30 746.71 19.80 o 0 6 0 33.70 42.20 7.33 o 1 6 0 1791.55 1674.49 35.97 o 2 6 0 928.84 1123.03 21.16 o 3 6 0 1063.75 1084.09 21.59 o 4 6 0 65.77 30.18 6.52 o 5 6 0 1708.04 1642.01 27.05 o 6 6 0 208.16 230.88 13.81 o 7 6 0 1251.39 1207.05 22.48 o 8 6 0 397.97 370.81 29.47 o 9 6 0 390.18 376.16 33.61 o 10 6 0 480.65 431.16 36.47 o 11 6 0 119.64 121.19 24.81 o -9 7 0 25.99 18.28 21.68 o -8 7 0 476.90 504.51 34.59 o -7 7 0 267.14 247.91 35.77 o -6 7 0 962.45 970.58 62.07 o -5 7 0 223.47 217.88 32.24 o -4 7 0 959.34 881.26 32.76 o -3 7 0 631.88 574.09 24.02 o -2 7 0 8.13 17.13 13.60 o -1 7 0 54.06 67.86 10.08 o 0 7 0 267.91 370.55 21.80 o 1 7 0 144.53 127.97 6.50 o 2 7 0 215.86 220.87 17.18 o 3 7 0 94.50 83.35 10.25 o 4 7 0 14.54 26.14 6.98 o 5 7 0 845.43 847.72 22.57 o 6 7 0 181.65 295.63 47.44 o 7 7 0 4.10 11.22 10.18 o 8 7 0 852.14 905.30 44.48 o 9 7 0 328.20 309.23 29.94 o 10 7 0 88.45 95.35 22.19 o -8 8 0 328.38 338.30 31.40 o -7 8 0 417.94 393.04 45.49 o -6 8 0 21.21 46.78 22.69 o -5 8 0 250.23 280.28 40.17 o -4 8 0 765.96 696.58 53.81 o -3 8 0 908.22 949.01 30.60 o -2 8 0 528.33 505.93 18.89 o -1 8 0 1901.82 1841.40 79.65 o 0 8 0 1175.59 1195.97 31.16 o 1 8 0 455.29 391.07 13.25 o 2 8 0 123.54 132.68 10.07 o 3 8 0 304.99 343.71 18.51 o 4 8 0 43.80 52.07 10.03 o 5 8 0 75.32 75.13 10.59 o 6 8 0 1393.86 1319.56 36.10 o 7 8 0 490.75 496.82 36.66 o 8 8 0 86.27 85.24 24.11 o 9 8 0 188.19 225.00 39.57 o 10 8 0 60.57 54.15 59.71 o -8 9 0 13.05 19.76 17.84 o -7 9 0 35.01 39.53 26.49 o -6 9 0 3.50 30.61 23.82 o -5 9 0 116.11 138.26 32.12 o -4 9 0 167.61 217.78 35.88 o -3 9 0 311.04 327.98 41.67 o -2 9 0 2407.98 2397.75 98.95 o -1 9 0 3446.73 3164.17 65.08 o 0 9 0 1904.90 2059.32 42.88 o 1 9 0 2716.99 2577.23 52.16 o 2 9 0 863.05 767.52 21.49 o 3 9 0 839.19 850.50 37.38 o 4 9 0 1158.77 1115.76 35.54 o 5 9 0 114.89 98.98 13.81 o 6 9 0 397.81 437.38 22.89 o 7 9 0 21.21 22.37 9.28 o 8 9 0 5.83 12.74 13.11 o 9 9 0 1.33 62.02 19.71 o 10 9 0 4.44 50.77 52.77 o -7 10 0 63.22 81.73 29.66 o -6 10 0 20.03 57.30 30.54 o -5 10 0 1.05 6.70 22.25 o -4 10 0 20.25 10.60 22.39 o -3 10 0 100.07 152.53 31.76 o -2 10 0 247.44 206.41 34.89 o -1 10 0 279.47 272.99 15.69 o 0 10 0 2021.23 2098.25 51.24 o 1 10 0 569.36 556.70 50.63 o 2 10 0 1322.61 1167.07 81.90 o 3 10 0 593.57 589.38 23.34 o 4 10 0 177.99 170.27 15.30 o 5 10 0 583.27 612.89 29.53 o 6 10 0 269.29 235.83 17.71 o 7 10 0 255.60 267.13 19.57 o 8 10 0 180.13 197.52 23.75 o 9 10 0 179.66 162.08 23.76 o -6 11 0 218.13 219.25 41.81 o -5 11 0 628.85 608.36 61.31 o -4 11 0 638.59 703.37 65.98 o -3 11 0 542.26 593.31 59.72 o -2 11 0 515.71 497.22 54.57 o -1 11 0 1.99 21.45 22.42 o 0 11 0 42.40 24.60 21.13 o 1 11 0 201.56 183.30 33.31 o 2 11 0 79.48 75.79 27.51 o 3 11 0 580.77 533.72 20.55 o 4 11 0 139.66 142.62 14.35 o 5 11 0 97.94 122.06 15.23 o 6 11 0 246.33 251.69 18.57 o 7 11 0 412.77 396.21 29.79 o 8 11 0 464.33 475.39 34.55 o 9 11 0 4.16 18.00 12.12 o -5 12 0 379.35 358.64 52.71 o -4 12 0 341.36 327.37 49.38 o -3 12 0 294.03 339.53 50.22 o -2 12 0 146.46 146.34 34.43 o -1 12 0 85.72 78.55 29.49 o 0 12 0 127.88 146.17 31.07 o 1 12 0 221.64 185.82 36.04 o 2 12 0 29.47 62.92 26.81 o 3 12 0 201.49 230.06 37.84 o 4 12 0 5.14 17.20 21.16 o 5 12 0 0.14 -8.85 17.98 o 6 12 0 6.83 -15.18 15.18 o 7 12 0 189.13 201.70 37.81 o 8 12 0 34.85 28.75 19.67 o -4 13 0 109.75 69.33 33.13 o -3 13 0 618.48 642.27 67.96 o -2 13 0 174.54 182.93 40.03 o -1 13 0 369.20 448.80 57.48 o 0 13 0 33.88 11.30 23.44 o 1 13 0 217.06 195.33 39.68 o 2 13 0 388.10 392.17 51.12 o 3 13 0 345.12 360.97 47.83 o 4 13 0 653.91 645.89 60.16 o 5 13 0 116.06 93.94 29.83 o 6 13 0 62.18 61.84 26.51 o 7 13 0 12.35 34.54 25.13 o -2 14 0 334.40 348.00 53.21 o -1 14 0 21.08 7.08 25.60 o 0 14 0 79.51 55.75 28.77 o 1 14 0 173.76 175.44 38.92 o 2 14 0 475.08 445.87 55.47 o 3 14 0 244.23 312.63 47.13 o 4 14 0 378.61 379.07 50.08 o 5 14 0 359.99 399.20 50.67 o 0 15 0 8.28 33.35 33.02 o 1 15 0 101.43 66.59 30.93 o 2 15 0 397.08 382.39 55.97 o 3 15 0 247.04 283.36 47.22 o -5 -14 1 1.38 -9.94 21.31 o -4 -14 1 12.74 17.15 20.84 o -3 -14 1 15.02 16.06 26.20 o -2 -14 1 111.23 97.91 29.29 o -1 -14 1 18.47 -30.71 30.71 o 0 -14 1 209.05 221.78 43.16 o 1 -14 1 258.52 227.64 45.18 o 2 -14 1 208.85 216.37 43.69 o -7 -13 1 4.41 -8.35 19.87 o -6 -13 1 49.13 -12.80 21.98 o -5 -13 1 333.32 290.01 42.94 o -4 -13 1 664.39 603.77 57.64 o -3 -13 1 54.50 110.94 32.89 o -2 -13 1 10.56 29.34 23.33 o -1 -13 1 3.85 -3.63 23.90 o 0 -13 1 185.16 146.55 34.56 o 1 -13 1 36.20 20.13 26.53 o 2 -13 1 19.88 41.40 28.04 o 3 -13 1 343.08 396.20 55.00 o 4 -13 1 144.61 156.04 41.05 o -8 -12 1 25.95 33.47 20.79 o -7 -12 1 98.61 151.65 33.48 o -6 -12 1 333.77 332.92 39.16 o -5 -12 1 564.05 562.18 53.96 o -4 -12 1 1731.96 1783.41 91.29 o -3 -12 1 447.71 465.68 49.76 o -2 -12 1 95.46 51.44 22.61 o -1 -12 1 107.94 84.04 29.95 o 0 -12 1 59.52 44.30 28.00 o 1 -12 1 6.48 -0.86 22.59 o 2 -12 1 20.51 29.55 26.41 o 3 -12 1 31.68 39.30 31.92 o 4 -12 1 10.08 12.70 23.54 o 5 -12 1 51.33 64.54 32.52 o -8 -11 1 0.15 -20.32 20.32 o -7 -11 1 118.76 130.00 19.00 o -6 -11 1 301.93 274.53 19.65 o -5 -11 1 372.87 320.80 38.65 o -4 -11 1 285.20 277.37 37.86 o -3 -11 1 1112.78 1056.88 67.95 o -2 -11 1 470.10 486.91 49.11 o -1 -11 1 366.75 341.69 22.25 o 0 -11 1 36.30 30.78 8.31 o 1 -11 1 232.38 233.41 38.49 o 2 -11 1 393.45 469.05 52.31 o 3 -11 1 433.90 448.72 54.62 o 4 -11 1 43.01 65.23 29.66 o 5 -11 1 147.41 204.99 42.53 o 6 -11 1 11.57 16.11 21.01 o -9 -10 1 155.36 178.71 23.71 o -8 -10 1 54.80 67.57 17.36 o -7 -10 1 56.16 90.68 16.61 o -6 -10 1 7.42 14.86 9.71 o -5 -10 1 302.46 319.65 21.67 o -4 -10 1 32.75 25.99 20.77 o -3 -10 1 19.60 10.27 18.24 o -2 -10 1 24.11 29.25 18.83 o -1 -10 1 283.02 268.64 19.62 o 0 -10 1 9.29 3.51 6.15 o 1 -10 1 2.61 9.65 7.64 o 2 -10 1 835.54 1048.55 71.74 o 3 -10 1 1133.88 1159.15 76.00 o 4 -10 1 658.79 670.22 60.79 o 5 -10 1 696.12 669.63 62.46 o 6 -10 1 385.65 345.64 49.37 o 7 -10 1 39.74 26.74 20.77 o -10 -9 1 275.84 304.86 33.65 o -9 -9 1 225.57 302.82 31.76 o -8 -9 1 55.94 89.09 18.03 o -7 -9 1 753.17 751.17 29.65 o -6 -9 1 393.75 373.31 23.48 o -5 -9 1 12.86 25.17 9.78 o -4 -9 1 18.47 31.31 9.71 o -3 -9 1 9.28 21.26 7.54 o -2 -9 1 25.89 15.99 16.14 o -1 -9 1 451.65 431.82 23.34 o 0 -9 1 884.27 880.94 30.65 o 1 -9 1 886.79 867.29 60.75 o 2 -9 1 912.53 885.49 62.36 o 3 -9 1 1653.65 1611.83 84.43 o 4 -9 1 1051.36 1037.95 70.38 o 5 -9 1 457.51 385.97 46.97 o 6 -9 1 160.79 198.80 36.41 o 7 -9 1 164.83 201.83 37.55 o 8 -9 1 46.50 61.42 18.19 o -10 -8 1 183.02 253.63 44.60 o -9 -8 1 5.01 33.63 47.76 o -8 -8 1 429.35 455.28 27.77 o -7 -8 1 1844.11 1873.73 40.70 o -6 -8 1 469.31 438.73 21.53 o -5 -8 1 451.38 424.12 20.41 o -4 -8 1 412.39 428.59 21.62 o -3 -8 1 486.10 472.23 20.72 o -2 -8 1 46.00 67.30 9.01 o -1 -8 1 489.33 482.22 23.09 o 0 -8 1 0.42 15.22 7.86 o 1 -8 1 15.16 28.58 20.81 o 2 -8 1 16.94 74.19 23.57 o 3 -8 1 266.97 284.33 37.72 o 4 -8 1 177.44 157.85 30.76 o 5 -8 1 28.90 125.18 33.44 o 6 -8 1 39.29 30.58 21.14 o 7 -8 1 100.69 104.01 29.78 o 8 -8 1 0.68 -7.74 15.99 o -10 -7 1 49.23 38.34 15.92 o -9 -7 1 64.25 85.47 20.36 o -8 -7 1 499.10 469.43 34.96 o -7 -7 1 627.42 663.63 52.74 o -6 -7 1 2802.19 2804.02 38.10 o -5 -7 1 1918.80 1782.58 32.34 o -4 -7 1 1284.20 1241.78 29.38 o -3 -7 1 1579.07 1487.08 35.02 o -2 -7 1 362.98 303.48 12.09 o -1 -7 1 2008.57 2431.90 47.41 o 0 -7 1 3585.67 3639.00 101.74 o 1 -7 1 2264.80 2310.75 84.73 o 2 -7 1 1318.00 1316.92 66.80 o 3 -7 1 438.53 396.13 39.72 o 4 -7 1 75.53 80.88 23.86 o 5 -7 1 1456.54 1420.80 74.68 o 6 -7 1 315.38 297.02 36.21 o 7 -7 1 28.71 27.07 21.64 o 8 -7 1 14.59 23.32 13.36 o 9 -7 1 11.17 29.04 21.93 o -11 -6 1 0.52 -14.36 17.91 o -10 -6 1 456.86 448.68 37.49 o -9 -6 1 267.46 292.70 28.86 o -8 -6 1 372.61 352.11 39.84 o -7 -6 1 364.86 385.59 19.57 o -6 -6 1 1.50 13.98 7.38 o -5 -6 1 957.67 886.11 22.87 o -4 -6 1 2233.42 2309.18 37.10 o -3 -6 1 406.25 342.55 14.47 o -2 -6 1 313.31 282.60 9.82 o -1 -6 1 215.41 242.81 21.51 o 0 -6 1 1122.17 947.91 49.04 o 1 -6 1 412.11 373.54 34.05 o 2 -6 1 689.54 677.68 45.19 o 3 -6 1 823.92 683.99 46.73 o 4 -6 1 1.78 8.00 17.13 o 5 -6 1 817.84 810.05 53.23 o 6 -6 1 1200.76 1066.87 62.65 o 7 -6 1 573.50 588.34 34.43 o 8 -6 1 71.98 86.89 16.91 o 9 -6 1 24.51 33.05 19.48 o -11 -5 1 129.57 181.08 29.60 o -10 -5 1 1817.28 1799.77 77.53 o -9 -5 1 909.48 842.61 46.45 o -8 -5 1 1057.09 1008.92 46.37 o -7 -5 1 723.91 672.59 17.88 o -6 -5 1 754.49 804.47 19.17 o -5 -5 1 3.89 4.15 4.41 o -4 -5 1 1200.16 1648.25 37.49 o -3 -5 1 364.00 416.30 13.24 o -2 -5 1 570.20 532.67 12.48 o -1 -5 1 575.67 749.97 17.17 o 0 -5 1 6.20 17.34 13.18 o 1 -5 1 528.27 463.06 23.31 o 2 -5 1 661.84 621.47 28.06 o 3 -5 1 143.77 199.05 14.56 o 4 -5 1 2596.95 2496.85 85.54 o 5 -5 1 110.48 142.34 16.68 o 6 -5 1 177.68 194.55 19.51 o 7 -5 1 1270.63 1283.01 38.32 o 8 -5 1 260.72 263.67 23.93 o 9 -5 1 62.66 88.25 23.34 o 10 -5 1 72.13 47.27 19.38 o -11 -4 1 61.30 100.62 23.15 o -10 -4 1 33.23 60.20 19.93 o -9 -4 1 8.74 25.75 15.81 o -8 -4 1 109.33 109.47 18.61 o -7 -4 1 1144.63 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