#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181290 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/68/2236849.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236849_Fobs loop_ _publ_author_name 'Draguta, Sergiu' 'Khrustalev, Victor N.' 'Sandhu, Bhupinder' 'Antipin, Mikhail Yu.' 'Timofeeva, Tatiana V.' _publ_section_title ; 6-Methylpyridin-2-amine ; _journal_coeditor_code CV5366 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3466 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 100.952 _cell_angle_gamma 90.000 _cell_length_a 9.1006 _cell_length_b 6.2458 _cell_length_c 10.5598 _exptl_crystal_F_000 232.00 _reflns_d_resolution_high 0.7572 _cod_data_source_file cv5366Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 91.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 791.51 748.53 16.36 o 2 0 0 1343.90 1293.65 28.16 o 3 0 0 804.44 752.63 16.45 o 4 0 0 227.87 215.09 4.96 o 5 0 0 1.38 5.38 0.50 o 6 0 0 681.45 711.44 15.82 o 7 0 0 205.91 198.94 4.83 o 8 0 0 4.72 5.14 0.66 o 9 0 0 11.45 12.60 1.56 o 10 0 0 1.82 1.52 0.62 o 11 0 0 141.74 154.29 4.27 o 1 1 0 345.67 400.42 5.59 o 2 1 0 2221.73 2220.94 28.06 o 3 1 0 42.14 32.76 0.58 o 4 1 0 70.28 72.22 1.16 o 5 1 0 31.22 27.04 0.58 o 6 1 0 229.29 214.79 3.61 o 7 1 0 7.07 8.13 0.58 o 8 1 0 25.21 26.98 0.87 o 9 1 0 7.65 8.64 0.61 o 10 1 0 2.91 2.22 0.47 o 11 1 0 1.71 0.92 0.46 o 0 2 0 981.03 1156.13 26.64 o 1 2 0 554.85 627.03 8.79 o 2 2 0 429.91 481.90 6.76 o 3 2 0 243.40 246.85 3.56 o 4 2 0 42.10 42.45 0.77 o 5 2 0 2.69 2.73 0.29 o 6 2 0 0.02 0.02 0.23 o 7 2 0 70.80 65.91 1.51 o 8 2 0 102.10 99.06 1.97 o 9 2 0 12.85 12.42 0.76 o 10 2 0 12.45 10.51 0.70 o 11 2 0 3.36 2.80 0.54 o 1 3 0 294.41 373.04 4.81 o 2 3 0 67.90 81.23 1.29 o 3 3 0 112.66 119.93 1.85 o 4 3 0 2.40 1.62 0.25 o 5 3 0 7.60 8.49 0.40 o 6 3 0 176.85 167.82 2.59 o 7 3 0 1.85 1.21 0.34 o 8 3 0 66.88 71.54 2.62 o 9 3 0 26.46 26.97 1.11 o 10 3 0 10.62 9.17 0.80 o 0 4 0 927.72 1100.11 22.07 o 1 4 0 60.22 73.24 2.94 o 2 4 0 0.01 0.00 0.21 o 3 4 0 1.61 1.44 0.25 o 4 4 0 70.70 63.52 1.15 o 5 4 0 241.72 239.62 3.58 o 6 4 0 351.85 344.80 5.05 o 7 4 0 7.89 8.19 0.51 o 8 4 0 3.04 4.13 0.55 o 9 4 0 0.26 0.00 0.43 o 10 4 0 23.65 25.16 1.13 o 1 5 0 22.73 23.90 0.54 o 2 5 0 37.19 41.07 0.77 o 3 5 0 1.27 0.86 0.23 o 4 5 0 71.09 70.44 1.28 o 5 5 0 3.95 4.34 0.38 o 6 5 0 8.69 8.29 0.47 o 7 5 0 8.24 10.04 0.64 o 8 5 0 0.03 0.00 0.51 o 9 5 0 0.72 1.35 0.49 o 0 6 0 13.11 12.32 0.87 o 1 6 0 0.11 0.00 0.27 o 2 6 0 21.12 20.48 0.63 o 3 6 0 45.86 45.71 0.99 o 4 6 0 63.50 63.89 1.25 o 5 6 0 7.01 8.03 0.49 o 6 6 0 0.29 0.94 0.42 o 7 6 0 12.80 15.89 0.85 o 8 6 0 1.01 2.67 0.84 o 1 7 0 52.99 54.15 1.32 o 2 7 0 0.90 1.51 0.43 o 3 7 0 0.22 0.15 0.39 o 4 7 0 21.49 20.34 0.82 o 5 7 0 1.19 3.23 0.46 o 6 7 0 15.43 15.42 1.36 o 0 8 0 0.84 0.89 1.16 o 1 8 0 0.02 0.00 0.72 o 2 8 0 1.56 2.76 0.50 o -11 1 1 4.68 4.59 0.58 o -10 1 1 15.37 14.67 0.80 o -9 1 1 16.83 15.89 0.90 o -8 1 1 21.49 20.53 0.75 o -7 1 1 0.06 0.04 0.32 o -6 1 1 98.85 99.94 1.86 o -5 1 1 34.72 32.45 0.66 o -4 1 1 303.95 308.75 4.39 o -3 1 1 139.19 142.52 1.90 o -2 1 1 23.23 26.13 0.48 o -1 1 1 1151.17 1261.13 33.11 o 0 1 1 951.15 1185.45 17.39 o 1 1 1 2703.66 3000.29 41.64 o 2 1 1 1040.87 1072.35 14.90 o 3 1 1 317.16 341.88 4.63 o 4 1 1 21.18 17.77 0.37 o 5 1 1 65.51 66.75 1.00 o 6 1 1 5.56 3.86 0.25 o 7 1 1 51.87 50.17 1.16 o 8 1 1 16.32 16.54 0.71 o 9 1 1 18.85 19.15 0.91 o 10 1 1 0.88 0.24 0.40 o 11 1 1 6.38 7.12 0.65 o -11 2 1 0.70 0.93 0.46 o -10 2 1 9.32 8.15 0.64 o -9 2 1 20.40 21.91 0.85 o -8 2 1 8.03 7.29 0.55 o -7 2 1 18.75 17.91 0.70 o -6 2 1 3.42 3.29 0.34 o -5 2 1 139.50 136.76 1.90 o -4 2 1 52.37 58.85 1.03 o -3 2 1 168.08 160.68 2.64 o -2 2 1 6.98 4.98 0.24 o -1 2 1 1.54 1.82 0.13 o 0 2 1 1.34 1.49 0.15 o 1 2 1 12.09 8.67 0.31 o 2 2 1 71.14 64.79 1.02 o 3 2 1 117.68 118.26 1.79 o 4 2 1 0.01 0.14 0.18 o 5 2 1 0.01 0.18 0.20 o 6 2 1 55.03 50.41 0.94 o 7 2 1 3.02 2.41 0.39 o 8 2 1 68.09 64.42 1.46 o 9 2 1 0.15 0.15 0.39 o 10 2 1 1.84 3.17 0.57 o 11 2 1 2.92 2.57 0.62 o -11 3 1 126.29 142.49 3.35 o -10 3 1 0.53 0.00 0.51 o -9 3 1 50.34 49.58 2.33 o -8 3 1 0.04 0.00 0.40 o -7 3 1 94.01 90.65 1.77 o -6 3 1 0.16 0.61 0.30 o -5 3 1 573.67 551.67 7.84 o -4 3 1 124.04 121.78 1.90 o -3 3 1 1.27 1.60 0.24 o -2 3 1 8.54 9.54 0.33 o -1 3 1 58.75 63.14 0.94 o 0 3 1 449.74 539.64 8.31 o 1 3 1 36.63 38.94 0.93 o 2 3 1 157.09 177.45 2.61 o 3 3 1 45.52 37.27 0.72 o 4 3 1 64.44 58.62 1.04 o 5 3 1 11.45 10.43 0.43 o 6 3 1 522.32 504.79 7.22 o 7 3 1 102.17 99.90 1.92 o 8 3 1 29.91 31.10 1.11 o 9 3 1 0.18 0.05 0.44 o 10 3 1 12.81 14.46 0.95 o -10 4 1 18.43 21.63 1.11 o -9 4 1 0.33 0.10 0.44 o -8 4 1 1.89 2.63 0.49 o -7 4 1 1.26 0.97 0.59 o -6 4 1 125.35 124.80 2.02 o -5 4 1 349.20 333.06 4.88 o -4 4 1 31.07 31.63 0.73 o -3 4 1 99.70 100.49 1.63 o -2 4 1 133.61 131.84 1.86 o -1 4 1 14.86 19.29 0.57 o 0 4 1 167.85 199.12 2.68 o 1 4 1 177.17 176.25 2.85 o 2 4 1 26.32 27.34 0.56 o 3 4 1 21.31 17.75 0.52 o 4 4 1 31.39 26.47 0.65 o 5 4 1 98.02 92.20 1.56 o 6 4 1 11.66 10.82 0.53 o 7 4 1 37.52 35.53 0.95 o 8 4 1 15.18 14.21 0.82 o 9 4 1 0.06 0.93 0.48 o 10 4 1 7.90 7.32 0.76 o -9 5 1 5.61 6.24 0.70 o -8 5 1 2.58 2.82 0.52 o -7 5 1 1.91 1.65 0.38 o -6 5 1 0.07 0.25 0.28 o -5 5 1 12.29 13.20 0.59 o -4 5 1 107.14 105.88 1.76 o -3 5 1 308.39 300.38 4.02 o -2 5 1 0.56 0.14 0.21 o -1 5 1 0.31 0.51 0.25 o 0 5 1 1.64 0.90 0.21 o 1 5 1 120.33 133.79 2.62 o 2 5 1 1.88 1.96 0.25 o 3 5 1 161.55 145.91 2.08 o 4 5 1 9.76 8.47 0.42 o 5 5 1 1.79 1.85 0.31 o 6 5 1 4.75 4.89 0.44 o 7 5 1 20.43 20.59 0.74 o 8 5 1 36.39 37.24 1.57 o 9 5 1 0.23 0.32 0.59 o -8 6 1 2.01 2.40 0.69 o -7 6 1 4.80 6.19 0.62 o -6 6 1 16.52 17.08 1.15 o -5 6 1 100.18 96.82 1.70 o -4 6 1 0.03 0.32 0.37 o -3 6 1 24.32 24.68 0.71 o -2 6 1 11.48 10.20 0.49 o -1 6 1 1.62 1.46 0.31 o 0 6 1 0.28 0.45 0.28 o 1 6 1 41.27 36.95 0.85 o 2 6 1 1.09 0.67 0.30 o 3 6 1 0.03 0.09 0.28 o 4 6 1 4.75 3.90 0.40 o 5 6 1 2.03 2.61 0.39 o 6 6 1 26.97 29.34 0.90 o 7 6 1 0.74 1.04 0.56 o -6 7 1 5.03 4.36 0.53 o -5 7 1 196.47 191.26 3.42 o -4 7 1 3.78 4.21 0.50 o -3 7 1 2.77 2.82 0.46 o -2 7 1 0.20 0.00 0.37 o -1 7 1 4.83 4.68 0.63 o 0 7 1 48.06 48.60 1.24 o 1 7 1 45.80 40.37 1.17 o 2 7 1 6.51 5.89 0.54 o 3 7 1 8.63 9.71 0.62 o 4 7 1 34.53 35.46 1.04 o 5 7 1 0.98 1.06 0.38 o 6 7 1 117.87 126.16 2.19 o -2 8 1 0.40 0.84 0.45 o -1 8 1 14.63 13.27 0.77 o 0 8 1 37.69 35.55 1.39 o 1 8 1 4.75 4.73 0.57 o 2 8 1 16.40 15.70 0.77 o -12 0 2 12.92 10.93 1.13 o -11 0 2 2.27 1.43 0.68 o -10 0 2 27.23 26.78 1.38 o -9 0 2 17.97 17.35 1.47 o -8 0 2 10.82 11.16 1.24 o -7 0 2 26.71 28.71 1.16 o -6 0 2 51.90 60.80 1.76 o -5 0 2 1278.68 1199.97 38.04 o -4 0 2 106.06 105.30 2.41 o -3 0 2 0.22 0.00 0.27 o -2 0 2 320.24 294.69 5.32 o -1 0 2 2207.14 2189.39 39.05 o 0 0 2 318.46 332.58 12.26 o 1 0 2 3561.98 3636.20 156.14 o 2 0 2 985.63 1013.74 36.14 o 3 0 2 113.78 110.92 2.14 o 4 0 2 15.63 18.20 0.54 o 5 0 2 19.15 19.97 0.61 o 6 0 2 25.79 24.43 2.05 o 7 0 2 6.06 5.55 0.66 o 8 0 2 0.77 0.79 0.76 o 9 0 2 4.76 6.85 0.78 o 10 0 2 0.18 0.08 0.53 o 11 0 2 0.25 0.29 0.59 o -11 1 2 1.13 1.71 0.48 o -10 1 2 82.14 78.94 1.79 o -9 1 2 40.67 35.77 1.07 o -8 1 2 3.53 4.75 0.46 o -7 1 2 1.45 0.63 0.34 o -6 1 2 37.10 40.44 0.81 o -5 1 2 357.25 386.65 6.27 o -4 1 2 1.62 3.03 0.17 o -3 1 2 63.92 60.93 0.89 o -2 1 2 1631.63 1602.26 20.18 o -1 1 2 0.03 0.00 0.17 o 0 1 2 108.19 121.23 2.91 o 1 1 2 8280.40 8235.06 182.54 o 2 1 2 1064.07 1071.67 20.46 o 3 1 2 64.33 73.04 1.68 o 4 1 2 27.59 24.62 0.48 o 5 1 2 0.05 0.06 0.15 o 6 1 2 0.00 0.00 0.18 o 7 1 2 45.11 48.68 1.15 o 8 1 2 129.92 121.83 2.33 o 9 1 2 87.07 91.12 1.93 o 10 1 2 1.76 1.92 0.52 o 11 1 2 0.91 0.94 0.46 o -11 2 2 1.40 0.96 0.46 o -10 2 2 61.71 60.09 1.53 o -9 2 2 75.34 69.96 1.84 o -8 2 2 270.38 257.86 4.40 o -7 2 2 2.39 3.73 0.51 o -6 2 2 4.16 6.95 0.31 o -5 2 2 18.45 12.58 0.38 o -4 2 2 69.56 56.94 0.89 o -3 2 2 499.32 560.99 7.90 o -2 2 2 426.96 473.53 6.67 o -1 2 2 3.07 3.50 0.22 o 0 2 2 7.26 6.23 0.29 o 1 2 2 1088.25 1333.35 21.44 o 2 2 2 405.08 471.11 8.59 o 3 2 2 2116.22 2245.03 32.77 o 4 2 2 2.88 3.09 0.29 o 5 2 2 3.30 2.42 0.27 o 6 2 2 0.62 0.95 0.37 o 7 2 2 410.64 409.69 7.76 o 8 2 2 0.49 0.92 0.40 o 9 2 2 176.68 180.09 4.99 o 10 2 2 2.01 1.71 0.53 o -11 3 2 11.20 9.88 1.28 o -10 3 2 84.90 83.06 2.73 o -9 3 2 0.69 0.69 0.48 o -8 3 2 0.24 0.00 0.41 o -7 3 2 60.95 54.95 1.24 o -6 3 2 0.00 0.03 0.23 o -5 3 2 24.43 22.51 0.72 o -4 3 2 199.88 212.26 3.15 o -3 3 2 24.22 32.59 0.68 o -2 3 2 37.17 36.27 0.70 o -1 3 2 7.10 8.44 0.34 o 0 3 2 327.60 415.54 8.20 o 1 3 2 787.81 940.37 16.67 o 2 3 2 12.61 9.83 0.32 o 3 3 2 101.35 97.64 1.55 o 4 3 2 49.15 41.33 0.81 o 5 3 2 62.39 62.11 1.50 o 6 3 2 11.41 11.18 0.47 o 7 3 2 171.17 169.19 3.00 o 8 3 2 13.77 15.51 0.87 o 9 3 2 7.10 9.16 0.75 o 10 3 2 7.14 6.88 0.71 o -10 4 2 41.15 44.89 2.62 o -9 4 2 1.67 2.55 0.56 o -8 4 2 8.19 8.66 0.70 o -7 4 2 2.45 3.72 0.44 o -6 4 2 35.80 36.80 1.22 o -5 4 2 168.31 161.24 2.53 o -4 4 2 110.98 112.73 1.84 o -3 4 2 4.09 3.68 0.33 o -2 4 2 0.35 0.59 0.24 o -1 4 2 6.24 8.90 0.36 o 0 4 2 1.41 1.87 0.27 o 1 4 2 110.36 119.24 1.87 o 2 4 2 75.76 84.69 1.26 o 3 4 2 7.09 10.15 0.40 o 4 4 2 9.26 8.74 0.40 o 5 4 2 28.40 24.65 0.69 o 6 4 2 16.57 16.49 0.55 o 7 4 2 26.34 26.18 1.24 o 8 4 2 0.93 0.91 0.44 o 9 4 2 0.49 0.62 0.49 o -9 5 2 3.32 4.89 0.65 o -8 5 2 0.12 0.00 0.46 o -7 5 2 0.88 0.91 0.42 o -6 5 2 0.00 0.17 0.28 o -5 5 2 123.60 120.06 2.00 o -4 5 2 78.90 77.31 1.40 o -3 5 2 1.26 1.55 0.26 o -2 5 2 17.64 17.90 0.58 o -1 5 2 5.49 6.50 0.40 o 0 5 2 0.02 0.00 0.23 o 1 5 2 36.38 43.83 1.02 o 2 5 2 37.12 41.15 1.15 o 3 5 2 17.58 16.23 0.55 o 4 5 2 10.59 9.40 0.55 o 5 5 2 6.20 6.79 0.48 o 6 5 2 39.77 38.79 1.01 o 7 5 2 10.68 11.65 1.17 o 8 5 2 0.01 0.00 0.80 o -8 6 2 1.02 1.38 0.68 o -7 6 2 0.10 0.77 0.46 o -6 6 2 7.37 8.19 0.56 o -5 6 2 66.43 59.86 1.21 o -4 6 2 25.89 27.67 0.76 o -3 6 2 326.27 325.14 4.80 o -2 6 2 88.42 92.19 1.63 o -1 6 2 8.22 9.39 0.49 o 0 6 2 17.86 19.26 0.68 o 1 6 2 33.48 30.90 0.78 o 2 6 2 82.24 73.40 1.36 o 3 6 2 19.19 18.06 0.62 o 4 6 2 32.12 28.52 0.78 o 5 6 2 2.50 3.55 0.39 o 6 6 2 12.37 15.44 0.73 o 7 6 2 5.70 7.50 0.68 o -6 7 2 0.93 1.14 0.42 o -5 7 2 36.10 35.14 1.05 o -4 7 2 58.55 57.59 1.39 o -3 7 2 2.63 2.65 0.48 o -2 7 2 2.19 1.76 0.46 o -1 7 2 0.03 0.47 0.42 o 0 7 2 11.82 10.66 1.20 o 1 7 2 1.28 1.24 0.35 o 2 7 2 12.70 10.26 0.54 o 3 7 2 26.70 27.74 0.80 o 4 7 2 5.14 4.88 0.44 o 5 7 2 5.16 4.59 0.55 o -2 8 2 0.05 0.09 0.78 o -1 8 2 3.17 3.94 0.71 o 0 8 2 5.32 5.38 0.70 o 1 8 2 4.93 5.92 0.70 o 2 8 2 5.82 5.69 0.66 o -11 1 3 9.54 8.80 0.69 o -10 1 3 20.03 17.41 0.96 o -9 1 3 10.53 8.68 0.62 o -8 1 3 122.98 113.82 2.20 o -7 1 3 17.15 15.10 0.80 o -6 1 3 13.35 11.43 0.46 o -5 1 3 95.60 103.68 1.48 o -4 1 3 444.88 454.63 5.84 o -3 1 3 1.67 4.41 0.21 o -2 1 3 802.87 892.12 11.27 o -1 1 3 59.44 65.65 1.02 o 0 1 3 287.39 330.24 4.73 o 1 1 3 252.89 271.20 6.68 o 2 1 3 1436.43 1441.37 20.43 o 3 1 3 160.18 175.31 2.57 o 4 1 3 48.30 49.76 0.88 o 5 1 3 14.49 16.63 0.42 o 6 1 3 37.40 34.63 0.67 o 7 1 3 20.16 18.53 0.70 o 8 1 3 41.99 45.22 1.38 o 9 1 3 49.09 48.30 1.55 o 10 1 3 15.30 14.78 0.80 o -11 2 3 1.62 1.44 0.50 o -10 2 3 63.08 68.02 1.64 o -9 2 3 4.42 1.88 0.44 o -8 2 3 42.21 40.85 1.09 o -7 2 3 8.46 6.91 0.40 o -6 2 3 2.45 3.79 0.27 o -5 2 3 51.76 57.14 0.93 o -4 2 3 138.95 137.75 1.90 o -3 2 3 995.09 1132.91 19.91 o -2 2 3 94.19 97.45 1.51 o -1 2 3 120.65 132.68 2.26 o 0 2 3 0.01 0.00 0.14 o 1 2 3 62.35 72.86 1.64 o 2 2 3 393.80 421.15 5.95 o 3 2 3 0.03 0.04 0.17 o 4 2 3 377.49 366.88 5.26 o 5 2 3 6.43 6.05 0.45 o 6 2 3 11.75 11.25 0.56 o 7 2 3 90.01 93.24 1.80 o 8 2 3 11.25 11.28 0.75 o 9 2 3 22.43 21.61 1.00 o 10 2 3 0.01 0.00 0.48 o -11 3 3 3.63 4.24 0.72 o -10 3 3 45.08 45.50 2.16 o -9 3 3 51.72 53.38 1.36 o -8 3 3 23.70 19.47 0.78 o -7 3 3 31.73 27.14 0.84 o -6 3 3 5.15 6.31 0.52 o -5 3 3 31.15 37.31 0.81 o -4 3 3 5.95 4.93 0.33 o -3 3 3 1.96 1.17 0.23 o -2 3 3 6.53 6.31 0.30 o -1 3 3 2.00 1.14 0.20 o 0 3 3 0.58 0.53 0.17 o 1 3 3 180.73 209.07 3.05 o 2 3 3 24.76 36.43 0.69 o 3 3 3 251.38 242.49 3.54 o 4 3 3 102.15 105.43 1.70 o 5 3 3 2.63 2.91 0.31 o 6 3 3 3.89 4.75 0.36 o 7 3 3 10.18 12.29 0.61 o 8 3 3 83.62 78.25 2.57 o 9 3 3 0.42 1.06 0.48 o 10 3 3 7.63 8.87 0.78 o -10 4 3 20.21 25.51 1.47 o -9 4 3 1.81 1.70 0.52 o -8 4 3 0.06 0.46 0.48 o -7 4 3 0.00 0.42 0.49 o -6 4 3 36.76 35.23 0.83 o -5 4 3 23.11 23.25 0.66 o -4 4 3 167.02 167.13 2.59 o -3 4 3 80.13 83.65 1.44 o -2 4 3 146.59 152.15 2.12 o -1 4 3 7.76 8.43 0.40 o 0 4 3 32.62 31.51 0.69 o 1 4 3 0.12 0.30 0.47 o 2 4 3 2.33 4.61 0.33 o 3 4 3 0.18 0.19 0.22 o 4 4 3 73.41 61.76 1.12 o 5 4 3 10.90 9.32 0.44 o 6 4 3 7.68 7.97 0.58 o 7 4 3 28.16 26.79 1.04 o 8 4 3 3.05 2.66 0.54 o 9 4 3 1.97 3.22 0.58 o -9 5 3 11.28 12.65 0.91 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