#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:09 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181290 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/68/2236879.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236879_Fobs loop_ _publ_author_name 'AlDamen, Murad A.' 'Haddad, Salim F.' _publ_section_title ; Bis{(E)-3-[(2-hydroxybenzylidene)amino]propyl}ammonium chloride ; _journal_coeditor_code GO2068 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3314 _journal_volume 68 _journal_year 2012 _space_group_IT_number 56 _symmetry_space_group_name_Hall '-P 2ab 2ac' _symmetry_space_group_name_H-M 'P c c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 4.9848 _cell_length_b 38.7140 _cell_length_c 10.3299 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.7998 _cod_data_source_file go2068Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' I P c c n R = 0.08' _shelx_refln_list_code 4 _shelx_f_calc_maximum 193.13 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z' 'x+1/2, -y, -z+1/2' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, y-1/2, -z' '-x-1/2, y, z-1/2' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 37298.93 37745.26 192.25 o 4 0 0 243.56 256.39 19.22 o 6 0 0 780.17 599.20 76.01 o 1 1 0 8556.18 7835.60 184.26 o 3 1 0 338.02 273.82 13.71 o 5 1 0 338.94 307.52 34.53 o 2 2 0 5560.79 5472.21 46.00 o 4 2 0 1928.19 1858.58 35.70 o 6 2 0 403.41 290.96 54.74 o 1 3 0 481.59 383.49 12.86 o 3 3 0 312.81 266.45 13.57 o 5 3 0 328.80 359.40 36.94 o 2 4 0 33.41 23.31 6.05 o 4 4 0 1666.30 1660.95 40.36 o 6 4 0 630.23 717.72 82.60 o 1 5 0 4285.16 4070.20 63.80 o 3 5 0 1110.00 1169.59 32.08 o 5 5 0 23.56 -2.20 12.85 o 2 6 0 5178.97 4704.18 50.09 o 4 6 0 1976.18 1943.75 46.04 o 6 6 0 2079.91 2065.33 139.59 o 1 7 0 8690.73 8240.48 56.69 o 3 7 0 0.87 7.15 4.29 o 5 7 0 17.11 3.31 16.31 o 0 8 0 1183.93 1165.94 29.58 o 2 8 0 4039.47 3802.18 47.11 o 4 8 0 2685.82 2588.79 54.23 o 6 8 0 909.84 995.99 98.00 o 1 9 0 3290.36 3096.01 33.10 o 3 9 0 114.91 111.03 11.45 o 5 9 0 45.02 60.97 25.87 o 0 10 0 9501.48 8874.17 90.79 o 2 10 0 7936.52 7509.33 82.78 o 4 10 0 1617.94 1593.96 43.55 o 6 10 0 9.86 63.72 31.06 o 1 11 0 1111.88 920.65 19.80 o 3 11 0 1531.56 1465.03 41.90 o 5 11 0 2004.29 1995.40 124.66 o 0 12 0 323.55 350.50 20.65 o 2 12 0 282.48 251.89 16.49 o 4 12 0 224.31 206.99 18.40 o 6 12 0 369.60 376.40 62.24 o 1 13 0 66.02 48.65 10.04 o 3 13 0 1622.43 1431.10 55.70 o 5 13 0 741.40 706.23 77.04 o 0 14 0 7766.21 7082.32 96.56 o 2 14 0 0.56 4.91 5.29 o 4 14 0 3.10 7.85 6.90 o 1 15 0 134.86 102.75 9.41 o 3 15 0 41.32 22.66 7.50 o 5 15 0 121.67 160.19 39.23 o 0 16 0 669.63 508.76 28.46 o 2 16 0 6197.97 6134.25 87.20 o 4 16 0 1728.25 1496.17 65.56 o 1 17 0 7436.07 7369.53 77.43 o 3 17 0 4711.31 4469.07 136.09 o 5 17 0 945.04 788.57 81.20 o 0 18 0 5835.05 5715.83 99.56 o 2 18 0 128.76 93.68 21.77 o 4 18 0 14.12 12.97 9.54 o 1 19 0 2625.73 2409.78 47.26 o 3 19 0 1219.34 1082.00 42.93 o 5 19 0 410.95 463.93 60.39 o 0 20 0 811.12 849.59 40.99 o 2 20 0 186.00 131.75 15.00 o 4 20 0 8.01 13.98 11.64 o 1 21 0 143.70 216.85 15.55 o 3 21 0 77.20 87.27 12.98 o 5 21 0 280.30 231.42 44.58 o 0 22 0 2.33 88.25 15.02 o 2 22 0 985.49 982.56 40.07 o 4 22 0 3197.64 3102.42 104.04 o 1 23 0 1939.49 1886.12 46.40 o 3 23 0 651.38 585.25 34.04 o 5 23 0 17.86 27.61 22.80 o 0 24 0 1232.84 1256.38 54.33 o 2 24 0 1534.49 1435.32 50.32 o 4 24 0 947.78 866.29 56.43 o 1 25 0 770.27 754.27 30.90 o 3 25 0 128.85 112.91 16.48 o 5 25 0 114.89 130.18 25.72 o 0 26 0 2330.08 2410.80 78.28 o 2 26 0 1157.44 1121.02 46.38 o 4 26 0 268.66 174.77 26.65 o 1 27 0 322.08 286.76 20.20 o 3 27 0 82.76 63.68 15.13 o 5 27 0 67.00 79.24 21.06 o 0 28 0 3301.69 3367.82 96.43 o 2 28 0 1781.50 1635.06 58.04 o 4 28 0 852.31 795.09 57.53 o 1 29 0 213.67 240.47 19.25 o 3 29 0 12.56 11.76 9.07 o 0 30 0 1657.38 1614.91 69.64 o 2 30 0 2665.14 2640.77 76.61 o 4 30 0 971.25 903.12 62.83 o 1 31 0 2246.21 2165.73 58.75 o 3 31 0 125.29 120.67 18.44 o 0 32 0 2558.08 2610.12 92.06 o 2 32 0 113.81 91.55 17.79 o 4 32 0 65.19 47.96 16.30 o 1 33 0 2666.27 2736.59 88.27 o 3 33 0 260.97 264.10 27.40 o 0 34 0 399.58 487.69 42.15 o 2 34 0 641.80 683.43 42.11 o 4 34 0 294.86 315.31 42.84 o 1 35 0 575.94 566.29 32.53 o 3 35 0 176.26 158.01 21.65 o 0 36 0 974.54 1021.19 62.11 o 2 36 0 583.65 688.56 46.04 o 4 36 0 652.82 622.09 62.72 o 1 37 0 808.10 766.67 45.70 o 3 37 0 9.39 8.62 8.61 o 0 38 0 700.10 722.34 54.67 o 2 38 0 575.49 509.16 38.58 o 1 39 0 89.17 83.78 17.11 o 3 39 0 24.36 12.99 14.02 o 0 40 0 404.47 421.95 68.19 o 2 40 0 432.36 453.81 38.03 o 1 41 0 234.70 224.44 26.99 o 3 41 0 79.93 68.14 21.81 o 0 42 0 24.71 53.92 17.88 o 2 42 0 94.56 116.73 20.97 o 1 43 0 675.11 661.68 47.12 o 0 44 0 1.69 -4.63 28.81 o 2 44 0 44.37 48.28 16.32 o 1 45 0 112.87 109.00 20.74 o 0 46 0 175.04 273.53 38.65 o 1 47 0 108.96 184.99 27.20 o 0 48 0 0.92 10.46 13.22 o 1 1 1 2960.24 3035.27 30.84 o 2 1 1 47.46 83.92 4.51 o 3 1 1 441.24 513.14 12.61 o 4 1 1 38.29 49.17 4.79 o 5 1 1 7.37 0.81 7.62 o 6 1 1 1.87 12.78 9.55 o 1 2 1 10231.36 10266.71 42.89 o 2 2 1 2447.41 2469.24 28.52 o 3 2 1 2655.95 2803.23 28.04 o 4 2 1 212.66 217.31 8.98 o 5 2 1 2.11 16.46 7.67 o 6 2 1 4.90 30.91 17.56 o 1 3 1 1222.89 1296.00 17.62 o 2 3 1 1143.60 1127.52 15.22 o 3 3 1 53.34 151.87 21.43 o 4 3 1 0.18 9.25 4.05 o 5 3 1 66.09 58.63 12.30 o 6 3 1 42.66 57.20 19.45 o 1 4 1 6718.81 6684.47 39.93 o 2 4 1 0.00 4.04 4.49 o 3 4 1 703.86 738.24 15.36 o 4 4 1 55.38 57.02 5.44 o 5 4 1 18.37 12.78 8.24 o 6 4 1 26.17 20.29 11.51 o 1 5 1 769.45 735.56 8.70 o 2 5 1 1.94 1.28 1.80 o 3 5 1 236.09 288.39 10.83 o 4 5 1 58.10 62.86 5.58 o 5 5 1 10.35 18.35 23.19 o 6 5 1 9.48 5.29 12.93 o 1 6 1 9.93 9.89 1.76 o 2 6 1 3.10 2.19 1.81 o 3 6 1 536.13 566.11 14.72 o 4 6 1 4.40 3.64 3.74 o 5 6 1 20.10 11.27 29.47 o 6 6 1 41.63 41.64 16.78 o 1 7 1 264.12 226.17 5.93 o 2 7 1 63.30 50.45 4.15 o 3 7 1 33.38 30.14 8.94 o 4 7 1 2.02 3.44 3.89 o 5 7 1 2.00 29.93 12.82 o 6 7 1 21.42 86.81 23.60 o 1 8 1 161.08 134.71 5.07 o 2 8 1 7.85 7.44 2.37 o 3 8 1 151.14 122.57 7.29 o 4 8 1 15.84 20.92 4.98 o 5 8 1 348.17 373.16 30.50 o 6 8 1 42.52 59.67 20.92 o 1 9 1 7.59 10.77 2.55 o 2 9 1 360.20 352.73 9.61 o 3 9 1 70.22 67.06 5.75 o 4 9 1 87.06 95.76 8.95 o 5 9 1 199.89 224.13 27.41 o 6 9 1 35.38 59.21 19.11 o 1 10 1 1185.83 1080.00 15.18 o 2 10 1 212.63 209.53 7.76 o 3 10 1 173.16 168.16 7.62 o 4 10 1 386.01 357.17 16.19 o 5 10 1 57.92 81.69 15.39 o 6 10 1 38.73 99.81 26.16 o 1 11 1 594.72 544.80 11.47 o 2 11 1 3.32 4.42 2.45 o 3 11 1 48.59 51.99 5.03 o 4 11 1 1.32 30.33 7.60 o 5 11 1 91.94 164.42 19.76 o 6 11 1 51.93 149.95 30.39 o 1 12 1 113.85 115.51 5.92 o 2 12 1 9.56 16.21 3.12 o 3 12 1 1106.74 1112.96 24.06 o 4 12 1 266.64 245.02 16.05 o 5 12 1 818.53 828.51 39.33 o 6 12 1 284.29 324.26 41.13 o 1 13 1 134.29 136.24 7.70 o 2 13 1 864.56 864.26 19.08 o 3 13 1 75.83 69.73 12.48 o 4 13 1 99.57 108.11 11.56 o 5 13 1 8.16 198.72 48.60 o 1 14 1 440.91 457.64 13.85 o 2 14 1 508.84 520.80 17.42 o 3 14 1 188.33 178.97 12.89 o 4 14 1 100.68 96.19 11.01 o 5 14 1 522.86 471.30 30.89 o 1 15 1 1068.63 1105.18 21.86 o 2 15 1 16.24 15.67 5.48 o 3 15 1 20.90 19.61 5.40 o 4 15 1 27.86 38.53 8.28 o 5 15 1 110.63 208.72 35.37 o 1 16 1 485.84 508.64 15.60 o 2 16 1 75.08 105.50 8.82 o 3 16 1 327.19 333.30 15.75 o 4 16 1 351.54 337.30 20.00 o 5 16 1 65.05 94.97 15.19 o 1 17 1 130.60 137.45 9.19 o 2 17 1 928.15 893.05 24.33 o 3 17 1 114.33 122.05 10.26 o 4 17 1 0.58 6.74 6.93 o 5 17 1 198.39 242.09 25.64 o 1 18 1 1379.22 1533.81 28.00 o 2 18 1 44.04 53.21 7.28 o 3 18 1 165.43 146.22 11.04 o 4 18 1 7.62 43.75 10.88 o 5 18 1 164.04 187.17 28.58 o 1 19 1 41.51 97.36 9.06 o 2 19 1 71.50 93.32 9.25 o 3 19 1 17.96 23.17 5.98 o 4 19 1 882.14 932.76 34.30 o 5 19 1 214.25 159.32 25.74 o 1 20 1 1316.96 1405.14 28.49 o 2 20 1 882.11 832.92 25.02 o 3 20 1 296.77 289.48 16.27 o 4 20 1 50.84 97.02 12.98 o 5 20 1 18.15 28.20 15.40 o 1 21 1 170.87 197.44 11.95 o 2 21 1 94.39 104.41 10.10 o 3 21 1 106.22 109.80 10.84 o 4 21 1 383.83 397.76 23.37 o 5 21 1 14.79 7.10 9.62 o 1 22 1 67.23 59.26 6.84 o 2 22 1 211.79 185.43 12.86 o 3 22 1 465.33 460.46 21.21 o 4 22 1 5.03 27.50 8.90 o 5 22 1 119.99 112.36 23.53 o 1 23 1 243.54 257.59 13.41 o 2 23 1 319.93 304.11 16.42 o 3 23 1 446.25 451.52 21.22 o 4 23 1 480.60 429.69 24.77 o 5 23 1 15.72 24.86 25.03 o 1 24 1 53.40 74.14 7.88 o 2 24 1 47.85 48.83 7.50 o 3 24 1 113.48 134.50 12.26 o 4 24 1 27.01 39.57 10.64 o 5 24 1 43.97 10.63 10.87 o 1 25 1 24.82 30.29 5.59 o 2 25 1 0.97 7.19 5.60 o 3 25 1 54.25 47.78 7.98 o 4 25 1 75.87 76.15 13.00 o 5 25 1 4.13 -2.49 9.65 o 1 26 1 40.63 35.95 5.84 o 2 26 1 199.98 168.72 13.08 o 3 26 1 28.29 34.43 8.15 o 4 26 1 62.81 54.08 11.02 o 5 26 1 0.06 11.51 12.42 o 1 27 1 154.50 146.19 11.20 o 2 27 1 7.70 18.48 6.54 o 3 27 1 267.07 245.95 16.88 o 4 27 1 37.88 44.37 10.42 o 5 27 1 7.40 -1.21 10.88 o 1 28 1 214.85 235.33 14.38 o 2 28 1 286.78 263.45 17.26 o 3 28 1 1.76 13.13 6.68 o 4 28 1 90.88 83.53 15.01 o 5 28 1 27.79 18.33 15.39 o 1 29 1 614.26 629.79 23.31 o 2 29 1 730.95 716.92 27.94 o 3 29 1 475.20 421.31 22.49 o 4 29 1 211.25 179.32 20.14 o 1 30 1 162.01 165.80 12.76 o 2 30 1 26.19 29.64 7.83 o 3 30 1 17.28 17.95 7.54 o 4 30 1 9.03 26.07 10.01 o 1 31 1 65.05 69.75 8.71 o 2 31 1 145.31 124.77 12.58 o 3 31 1 6.32 3.93 6.76 o 4 31 1 96.96 96.81 15.48 o 1 32 1 16.28 11.23 5.22 o 2 32 1 148.97 180.33 15.60 o 3 32 1 23.82 24.05 7.49 o 4 32 1 8.52 0.17 7.88 o 1 33 1 26.67 27.29 6.52 o 2 33 1 845.24 834.41 32.44 o 3 33 1 266.36 246.35 18.82 o 4 33 1 23.70 -3.93 14.81 o 1 34 1 149.13 170.98 13.84 o 2 34 1 336.90 383.65 22.89 o 3 34 1 31.71 22.29 6.65 o 4 34 1 31.94 31.54 14.28 o 1 35 1 5.00 7.02 5.85 o 2 35 1 750.25 684.41 30.36 o 3 35 1 0.69 0.01 7.35 o 4 35 1 28.35 16.13 10.29 o 1 36 1 60.43 55.34 8.49 o 2 36 1 221.28 217.68 17.89 o 3 36 1 1.36 -1.37 6.41 o 4 36 1 48.63 66.13 13.31 o 1 37 1 49.52 60.49 8.75 o 2 37 1 3.41 17.23 7.14 o 3 37 1 99.21 89.09 13.24 o 1 38 1 6.28 13.57 6.64 o 2 38 1 3.41 12.66 7.77 o 3 38 1 2.23 3.13 8.76 o 1 39 1 9.82 3.14 5.69 o 2 39 1 8.75 4.52 6.53 o 3 39 1 5.53 -1.16 8.92 o 1 40 1 20.94 13.52 6.04 o 2 40 1 2.85 -0.54 6.60 o 3 40 1 7.92 -2.28 13.03 o 1 41 1 2.23 -2.60 6.06 o 2 41 1 5.35 4.22 5.79 o 3 41 1 0.95 -10.85 10.85 o 1 42 1 23.90 39.24 7.72 o 2 42 1 76.80 76.78 11.34 o 3 42 1 0.21 3.08 8.19 o 1 43 1 36.58 39.61 7.89 o 2 43 1 7.57 7.10 6.40 o 1 44 1 20.37 16.54 6.43 o 2 44 1 14.52 3.76 9.72 o 1 45 1 5.22 4.03 5.50 o 2 45 1 10.27 4.61 6.80 o 1 46 1 6.13 6.27 9.69 o 1 47 1 4.79 15.91 8.61 o 0 0 2 9136.61 10938.61 127.00 o 1 0 2 17999.82 17872.97 53.33 o 2 0 2 595.02 481.81 17.00 o 3 0 2 7.96 82.48 19.98 o 4 0 2 52.26 64.74 13.27 o 5 0 2 1060.16 1248.88 54.83 o 6 0 2 111.65 119.28 41.37 o 0 1 2 36.30 42.62 5.18 o 1 1 2 4056.26 4018.42 48.19 o 2 1 2 738.01 665.72 11.52 o 3 1 2 762.19 805.16 16.20 o 4 1 2 356.93 366.96 18.93 o 5 1 2 369.56 588.05 24.88 o 6 1 2 10.98 23.37 11.35 o 0 2 2 8733.18 8932.92 105.74 o 1 2 2 6451.25 6690.53 45.83 o 2 2 2 185.36 194.26 6.30 o 3 2 2 1544.45 1467.69 25.92 o 4 2 2 366.14 364.73 18.71 o 5 2 2 398.41 548.38 23.88 o 6 2 2 13.93 49.89 18.33 o 0 3 2 14030.78 15179.92 109.98 o 1 3 2 30685.69 30869.57 88.71 o 2 3 2 391.90 415.69 10.05 o 3 3 2 1820.30 1743.20 46.93 o 4 3 2 0.16 11.93 6.03 o 5 3 2 509.96 681.93 28.89 o 6 3 2 99.08 83.16 21.86 o 0 4 2 6040.61 6077.46 114.40 o 1 4 2 32307.26 32033.97 87.98 o 2 4 2 573.13 691.14 13.60 o 3 4 2 1740.12 1774.03 26.86 o 4 4 2 156.44 139.12 9.46 o 5 4 2 582.98 750.75 33.34 o 6 4 2 7.00 56.16 21.89 o 0 5 2 9151.92 9602.74 91.03 o 1 5 2 2.43 73.61 16.64 o 2 5 2 0.67 9.30 3.14 o 3 5 2 2457.84 2499.07 38.73 o 4 5 2 257.85 230.10 12.94 o 5 5 2 843.60 921.48 40.81 o 6 5 2 128.21 159.23 44.13 o 0 6 2 4851.33 5167.38 54.51 o 1 6 2 2289.20 2238.95 18.09 o 2 6 2 11.79 11.23 2.84 o 3 6 2 1217.24 1333.37 29.59 o 4 6 2 108.85 134.57 11.74 o 5 6 2 2.08 287.56 65.39 o 6 6 2 107.80 239.42 35.35 o 0 7 2 767.01 685.15 20.78 o 1 7 2 3136.48 2980.67 20.54 o 2 7 2 239.12 242.76 12.83 o 3 7 2 1221.35 1096.35 27.39 o 4 7 2 684.76 700.36 21.38 o 5 7 2 622.76 631.22 34.30 o 6 7 2 398.08 419.28 45.31 o 0 8 2 9781.50 9826.16 82.49 o 1 8 2 96.58 105.39 4.40 o 2 8 2 1049.37 960.66 34.34 o 3 8 2 256.20 325.69 16.08 o 4 8 2 66.53 181.26 13.31 o 5 8 2 117.13 324.31 38.92 o 6 8 2 93.87 332.97 45.16 o 0 9 2 412.14 360.66 16.65 o 1 9 2 917.42 859.65 13.13 o 2 9 2 1939.32 1796.83 38.98 o 3 9 2 1425.39 1335.25 31.30 o 4 9 2 851.05 829.00 24.21 o 5 9 2 638.77 746.76 37.97 o 6 9 2 415.90 478.04 49.57 o 0 10 2 2803.82 2701.98 45.37 o 1 10 2 239.16 246.03 7.60 o 2 10 2 1736.74 1595.55 32.71 o 3 10 2 43.51 70.13 16.66 o 4 10 2 267.28 315.34 16.93 o 5 10 2 707.61 873.43 43.63 o 6 10 2 14.10 156.90 35.95 o 0 11 2 10005.82 9675.73 88.37 o 1 11 2 392.56 309.40 8.83 o 2 11 2 356.95 281.65 9.00 o 3 11 2 501.70 432.37 10.48 o 4 11 2 1.30 22.19 7.34 o 5 11 2 854.80 881.96 41.40 o 0 12 2 153.72 184.62 14.41 o 1 12 2 832.99 819.73 14.79 o 2 12 2 41.09 92.44 10.12 o 3 12 2 503.37 445.54 15.18 o 4 12 2 16.53 37.32 8.15 o 5 12 2 31.50 262.08 32.24 o 0 13 2 5978.74 5747.12 72.90 o 1 13 2 3542.97 3300.45 37.79 o 2 13 2 5150.09 4784.28 39.14 o 3 13 2 1017.41 938.43 19.72 o 4 13 2 872.32 805.86 29.44 o 5 13 2 90.25 128.58 17.17 o 0 14 2 1.06 42.13 11.60 o 1 14 2 81.48 126.52 14.49 o 2 14 2 126.86 137.06 15.67 o 3 14 2 591.91 552.63 19.17 o 4 14 2 946.97 962.09 32.97 o 5 14 2 203.68 225.61 21.75 o 0 15 2 7038.46 6949.17 84.56 o 1 15 2 2733.57 2680.39 34.64 o 2 15 2 2088.13 1983.05 34.57 o 3 15 2 3.69 19.21 4.83 o 4 15 2 1346.80 1457.97 41.08 o 5 15 2 10.43 48.43 11.57 o 0 16 2 271.42 365.58 21.94 o 1 16 2 135.62 217.29 16.77 o 2 16 2 2013.11 1944.85 35.23 o 3 16 2 30.49 30.19 5.97 o 4 16 2 1549.14 1537.23 42.63 o 5 16 2 13.19 16.38 9.31 o 0 17 2 442.94 441.78 23.44 o 1 17 2 2523.52 2469.29 35.27 o 2 17 2 10.10 48.32 7.31 o 3 17 2 309.76 269.99 15.75 o 4 17 2 29.69 102.24 20.10 o 5 17 2 30.91 34.67 18.22 o 0 18 2 263.03 243.62 18.39 o 1 18 2 4.09 46.03 8.03 o 2 18 2 0.21 5.66 4.74 o 3 18 2 27.29 43.18 8.06 o 4 18 2 51.47 75.66 11.37 o 5 18 2 196.32 239.11 27.86 o 0 19 2 24.20 41.87 15.14 o 1 19 2 420.24 374.92 14.83 o 2 19 2 816.80 832.35 24.91 o 3 19 2 1231.19 1213.99 32.11 o 4 19 2 719.04 669.73 30.97 o 5 19 2 595.08 681.90 44.41 o 0 20 2 3249.54 3500.98 87.33 o 1 20 2 651.21 587.49 18.82 o 2 20 2 1168.82 1081.76 29.15 o 3 20 2 1740.32 1691.68 38.53 o 4 20 2 23.96 52.99 10.29 o 5 20 2 148.11 201.55 37.75 o 0 21 2 7384.35 7946.49 112.58 o 1 21 2 40.63 47.40 7.34 o 2 21 2 1609.00 1502.92 34.88 o 3 21 2 1.43 23.26 7.78 o 4 21 2 334.25 355.60 22.27 o 5 21 2 394.29 380.64 42.27 o 0 22 2 7.88 166.03 27.59 o 1 22 2 703.80 700.71 21.53 o 2 22 2 168.17 192.17 13.67 o 3 22 2 1.14 19.33 6.83 o 4 22 2 175.79 170.34 16.05 o 5 22 2 0.59 21.83 44.39 o 0 23 2 229.92 188.72 15.71 o 1 23 2 480.15 483.95 18.47 o 2 23 2 375.04 323.61 17.01 o 3 23 2 862.13 827.78 28.73 o 4 23 2 164.02 171.93 16.41 o 5 23 2 116.90 103.42 25.65 o 0 24 2 0.35 6.82 6.21 o 1 24 2 102.62 115.63 10.32 o 2 24 2 11.44 10.78 5.49 o 3 24 2 87.56 148.43 14.09 o 4 24 2 2.43 12.19 9.05 o 5 24 2 187.49 196.93 33.78 o 0 25 2 21.70 19.02 7.58 o 1 25 2 1275.64 1237.55 30.37 o 2 25 2 2.24 3.34 5.24 o 3 25 2 1418.10 1355.67 37.96 o 4 25 2 111.39 98.36 12.61 o 5 25 2 677.48 663.75 57.88 o 0 26 2 1029.07 1013.77 37.08 o 1 26 2 501.44 549.31 21.37 o 2 26 2 42.22 49.40 8.33 o 3 26 2 809.43 813.85 30.28 o 4 26 2 52.41 41.50 9.92 o 5 26 2 381.39 404.51 47.18 o 0 27 2 77.14 89.69 13.44 o 1 27 2 2006.67 1984.17 39.93 o 2 27 2 252.01 243.37 15.98 o 3 27 2 641.48 579.72 25.95 o 4 27 2 46.07 31.53 9.43 o 5 27 2 218.76 286.51 39.47 o 0 28 2 334.61 344.42 22.84 o 1 28 2 20.01 100.91 11.30 o 2 28 2 37.41 45.60 8.09 o 3 28 2 165.66 189.83 17.65 o 4 28 2 108.17 84.65 13.22 o 0 29 2 1429.96 1458.16 47.10 o 1 29 2 368.07 372.07 18.42 o 2 29 2 248.91 229.46 16.24 o 3 29 2 76.14 74.17 11.03 o 4 29 2 45.66 38.89 8.34 o 0 30 2 34.42 100.80 15.01 o 1 30 2 733.41 729.47 25.86 o 2 30 2 251.59 269.48 17.75 o 3 30 2 111.01 103.54 13.92 o 4 30 2 109.50 115.68 17.11 o 0 31 2 865.20 914.43 45.06 o 1 31 2 110.08 181.62 14.36 o 2 31 2 388.45 364.29 21.00 o 3 31 2 387.15 410.44 26.28 o 4 31 2 40.49 38.73 10.45 o 0 32 2 118.30 201.33 23.10 o 1 32 2 1419.65 1510.54 38.60 o 2 32 2 0.08 4.01 6.51 o 3 32 2 488.08 464.74 28.54 o 4 32 2 11.16 8.75 9.70 o 0 33 2 1763.73 1865.40 66.61 o 1 33 2 2377.79 2428.14 49.51 o 2 33 2 238.72 202.78 16.25 o 3 33 2 347.82 359.51 25.56 o 4 33 2 91.36 96.19 15.75 o 0 34 2 1090.03 1132.88 53.31 o 1 34 2 168.27 309.96 19.28 o 2 34 2 13.96 12.35 6.24 o 3 34 2 637.98 594.86 32.61 o 4 34 2 61.95 68.13 13.51 o 0 35 2 10.43 50.69 16.14 o 1 35 2 899.26 928.82 31.85 o 2 35 2 97.43 93.10 11.74 o 3 35 2 102.36 130.29 16.86 o 4 35 2 0.24 -9.06 9.06 o 0 36 2 282.57 305.57 29.33 o 1 36 2 599.60 653.60 27.38 o 2 36 2 110.17 142.56 15.15 o 3 36 2 10.42 21.57 8.66 o 4 36 2 26.56 30.71 10.37 o 0 37 2 1052.65 1028.64 53.10 o 1 37 2 2.70 28.03 7.49 o 2 37 2 726.28 775.26 33.61 o 3 37 2 465.96 440.66 29.16 o 0 38 2 109.65 180.73 25.00 o 1 38 2 0.14 8.50 5.40 o 2 38 2 29.65 54.32 15.18 o 3 38 2 93.30 126.99 16.29 o 0 39 2 710.05 713.83 46.16 o 1 39 2 74.49 59.11 9.59 o 2 39 2 269.16 271.08 20.60 o 3 39 2 107.75 131.94 16.65 o 0 40 2 148.74 225.80 26.83 o 1 40 2 2.66 10.07 6.88 o 2 40 2 7.69 13.32 6.99 o 3 40 2 39.07 66.70 13.06 o 0 41 2 11.01 18.64 10.80 o 1 41 2 86.85 87.90 11.09 o 2 41 2 103.16 96.37 13.51 o 3 41 2 139.45 124.32 17.00 o 0 42 2 117.76 129.36 21.42 o 1 42 2 65.64 75.44 10.86 o 2 42 2 69.21 83.38 12.82 o 0 43 2 61.28 78.99 16.43 o 1 43 2 168.20 235.08 18.54 o 2 43 2 2.25 4.19 8.51 o 0 44 2 18.12 34.70 13.70 o 1 44 2 57.62 59.17 9.69 o 2 44 2 19.13 10.55 8.02 o 0 45 2 20.01 60.46 17.15 o 1 45 2 21.45 26.79 8.04 o 2 45 2 115.44 148.23 16.68 o 0 46 2 57.93 92.28 20.17 o 1 46 2 60.31 65.04 10.82 o 0 47 2 90.32 121.07 22.67 o 1 47 2 91.79 124.61 16.19 o 1 1 3 5294.65 5402.32 57.64 o 2 1 3 5982.73 5983.52 64.98 o 3 1 3 206.03 169.64 7.80 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28.41 9.16 o 1 8 3 74.78 95.28 6.21 o 2 8 3 42.80 50.89 7.70 o 3 8 3 41.64 31.55 5.34 o 4 8 3 639.23 667.82 28.75 o 5 8 3 157.03 112.13 13.07 o 1 9 3 167.30 209.59 9.16 o 2 9 3 790.41 796.17 25.04 o 3 9 3 54.28 50.83 6.64 o 4 9 3 395.93 481.04 42.94 o 5 9 3 0.00 15.27 7.11 o 1 10 3 905.72 964.52 18.56 o 2 10 3 753.61 644.05 28.19 o 3 10 3 433.96 395.87 17.87 o 4 10 3 496.97 521.38 26.32 o 5 10 3 31.35 23.23 7.29 o 1 11 3 639.16 699.88 16.31 o 2 11 3 0.01 17.31 7.01 o 3 11 3 162.56 164.19 12.20 o 4 11 3 162.93 196.94 24.01 o 5 11 3 111.87 105.05 15.55 o 1 12 3 6.68 24.90 4.99 o 2 12 3 1929.97 1815.83 25.81 o 3 12 3 4.03 20.80 8.88 o 4 12 3 274.70 269.25 17.75 o 5 12 3 34.10 5.88 9.99 o 1 13 3 2594.45 2848.93 38.13 o 2 13 3 8.24 18.63 3.74 o 3 13 3 625.72 579.00 23.14 o 4 13 3 10.19 22.78 7.56 o 5 13 3 1.32 10.13 10.12 o 1 14 3 981.51 1127.72 24.97 o 2 14 3 55.70 74.12 4.91 o 3 14 3 105.82 79.77 7.72 o 4 14 3 59.21 57.16 9.69 o 5 14 3 46.26 37.07 12.15 o 1 15 3 281.94 306.81 13.64 o 2 15 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376.25 21.89 o 4 10 4 511.11 487.49 25.81 o 5 10 4 916.22 849.74 37.39 o 0 11 4 3271.39 3269.62 61.44 o 1 11 4 404.35 509.41 23.31 o 2 11 4 271.96 187.44 7.63 o 3 11 4 517.78 642.16 29.83 o 4 11 4 99.85 137.41 16.79 o 5 11 4 308.66 518.00 37.57 o 0 12 4 2525.76 2645.04 56.07 o 1 12 4 8169.12 8304.38 68.29 o 2 12 4 55.89 42.40 4.42 o 3 12 4 4398.19 4110.35 73.33 o 4 12 4 21.52 55.41 13.00 o 5 12 4 942.84 865.33 48.70 o 0 13 4 568.36 677.70 29.18 o 1 13 4 106.85 189.70 15.92 o 2 13 4 555.13 484.51 15.08 o 3 13 4 349.52 478.13 30.40 o 4 13 4 578.71 593.20 33.37 o 5 13 4 84.70 206.52 26.00 o 0 14 4 289.12 287.87 23.72 o 1 14 4 4896.34 4848.91 54.36 o 2 14 4 516.46 516.42 14.71 o 3 14 4 699.26 634.86 25.47 o 4 14 4 171.77 200.85 21.11 o 5 14 4 130.21 110.35 14.73 o 0 15 4 133.96 91.45 12.52 o 1 15 4 895.32 981.05 25.49 o 2 15 4 30.04 27.04 4.46 o 3 15 4 69.22 130.43 17.65 o 4 15 4 275.77 249.12 26.08 o 5 15 4 9.00 63.64 12.49 o 0 16 4 1197.28 1203.22 40.74 o 1 16 4 1566.39 1507.45 31.92 o 2 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