#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/68/2236891.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236891_Fobs loop_ _publ_author_name 'Asiri, Abdullah M.' 'Arshad, Muhammad Nadeem' 'Zayed, Mohie E. M.' 'Alamry, Khalid A.' 'Bokhari, Tanveer Hussain' _publ_section_title ; (Z)-Ethyl 2-chloro-2-[2-(4-methylphenyl)hydrazinylidene]acetate ; _journal_coeditor_code HB6984 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3420 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.692 _cell_angle_gamma 90.000 _cell_length_a 4.6152 _cell_length_b 9.9444 _cell_length_c 26.3152 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.7941 _[local]_cod_data_source_file hb6984Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' pre_exp_35 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 68.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 10.68 17.31 0.63 o 2 0 0 518.71 445.50 4.71 o 3 0 0 0.64 0.61 0.31 o 4 0 0 10.52 9.27 0.68 o 5 0 0 17.37 19.48 1.07 o 1 1 0 550.84 513.72 2.63 o 2 1 0 164.65 142.11 1.39 o 3 1 0 18.36 14.67 0.95 o 4 1 0 11.17 12.72 0.55 o 5 1 0 181.56 210.00 16.93 o 0 2 0 45.16 61.84 1.75 o 1 2 0 310.30 326.38 2.48 o 2 2 0 1432.29 1452.27 8.71 o 3 2 0 22.80 21.39 1.25 o 4 2 0 0.99 0.47 0.22 o 5 2 0 119.34 127.63 6.63 o 1 3 0 171.14 152.31 1.38 o 2 3 0 127.27 131.00 1.88 o 3 3 0 507.40 475.39 10.78 o 4 3 0 18.05 19.52 0.73 o 5 3 0 3.83 4.29 0.50 o 0 4 0 2240.96 2138.94 17.40 o 1 4 0 2.92 2.30 0.31 o 2 4 0 553.39 560.38 5.87 o 3 4 0 0.01 -0.07 0.19 o 4 4 0 14.57 18.10 0.82 o 5 4 0 0.52 0.13 0.24 o 1 5 0 562.28 545.09 4.82 o 2 5 0 0.95 0.23 0.26 o 3 5 0 20.10 19.36 0.81 o 4 5 0 44.38 49.04 1.22 o 5 5 0 26.44 27.30 1.96 o 0 6 0 1943.43 1957.81 14.95 o 1 6 0 192.92 198.99 3.53 o 2 6 0 9.36 9.49 0.89 o 3 6 0 15.61 13.07 0.78 o 4 6 0 6.93 8.20 0.60 o 5 6 0 0.13 0.16 0.25 o 1 7 0 3.64 3.04 0.50 o 2 7 0 62.81 64.64 1.30 o 3 7 0 1.18 1.34 0.27 o 4 7 0 7.05 8.01 0.68 o 0 8 0 43.48 49.66 1.47 o 1 8 0 22.56 20.58 0.74 o 2 8 0 2.37 1.99 0.30 o 3 8 0 0.04 -0.03 0.18 o 4 8 0 33.33 31.66 1.01 o 1 9 0 96.29 93.96 1.69 o 2 9 0 3.49 5.03 0.35 o 3 9 0 0.00 -0.15 0.15 o 4 9 0 16.49 15.60 0.71 o 0 10 0 0.18 3.03 2.43 o 1 10 0 71.53 69.06 1.20 o 2 10 0 0.30 0.21 0.15 o 3 10 0 0.79 0.69 0.19 o 1 11 0 10.40 8.98 0.44 o 2 11 0 2.27 2.39 0.24 o 0 12 0 2.46 1.81 0.27 o 1 12 0 0.81 1.25 0.17 o -5 1 1 0.17 1.93 0.36 o -4 1 1 174.77 184.26 3.15 o -3 1 1 130.61 123.65 2.70 o -2 1 1 579.03 569.02 5.35 o -1 1 1 462.70 501.02 2.12 o 0 1 1 2046.41 1911.73 10.80 o 1 1 1 16.29 13.07 0.28 o 2 1 1 1431.73 1320.59 4.64 o 3 1 1 265.33 273.03 3.54 o 4 1 1 104.84 110.38 1.91 o 5 1 1 99.07 112.74 3.10 o -5 2 1 7.38 9.39 0.57 o -4 2 1 11.73 12.37 0.59 o -3 2 1 90.13 83.78 2.48 o -2 2 1 151.97 179.50 1.60 o 0 2 1 214.19 206.06 2.31 o 1 2 1 3156.31 3137.27 18.35 o 2 2 1 460.51 443.88 3.84 o 3 2 1 0.20 1.21 0.40 o 4 2 1 0.31 -0.13 0.25 o 5 2 1 6.22 7.33 0.73 o -5 3 1 1.76 3.80 0.50 o -4 3 1 11.75 12.14 0.54 o -3 3 1 42.04 43.30 2.12 o -2 3 1 237.75 238.79 2.80 o -1 3 1 1122.61 1144.79 7.31 o 0 3 1 429.50 431.18 3.58 o 1 3 1 340.55 328.39 2.16 o 2 3 1 5.92 4.29 0.30 o 3 3 1 106.29 95.46 3.71 o 4 3 1 89.30 93.13 1.81 o 5 3 1 24.74 30.32 1.14 o -5 4 1 6.54 5.18 0.50 o -4 4 1 35.34 41.06 1.11 o -3 4 1 35.35 34.29 0.83 o -2 4 1 5.96 5.38 0.72 o -1 4 1 1437.26 1440.80 6.57 o 0 4 1 2921.06 2836.46 15.65 o 1 4 1 1932.45 1946.87 9.38 o 2 4 1 91.35 86.55 1.77 o 3 4 1 0.20 0.17 0.22 o 4 4 1 151.34 155.20 2.33 o 5 4 1 0.44 0.52 0.28 o -5 5 1 6.63 7.33 0.90 o -4 5 1 68.55 63.59 1.40 o -3 5 1 0.17 0.51 0.27 o -2 5 1 105.04 93.64 3.16 o -1 5 1 278.81 262.41 3.60 o 0 5 1 81.74 81.19 1.73 o 1 5 1 43.76 47.21 1.31 o 2 5 1 1.98 3.34 0.48 o 3 5 1 36.09 34.06 1.03 o 4 5 1 10.50 9.96 0.71 o 5 5 1 8.61 7.00 1.10 o -5 6 1 4.00 4.22 0.34 o -4 6 1 0.24 0.12 0.21 o -3 6 1 8.62 8.57 0.63 o -2 6 1 239.87 240.28 4.30 o -1 6 1 825.96 811.98 6.49 o 0 6 1 216.92 275.11 3.33 o 1 6 1 30.02 26.26 1.30 o 2 6 1 17.68 16.85 1.17 o 3 6 1 9.72 10.84 0.60 o 4 6 1 0.42 0.46 0.26 o 5 6 1 0.38 -0.22 0.25 o -4 7 1 7.73 8.22 0.56 o -3 7 1 12.31 10.68 0.58 o -2 7 1 7.51 8.36 0.45 o -1 7 1 9.80 10.61 0.83 o 0 7 1 7.50 12.54 0.80 o 1 7 1 0.15 0.37 0.25 o 2 7 1 19.27 18.20 0.72 o 3 7 1 8.34 7.15 0.49 o 4 7 1 52.50 54.18 1.59 o -4 8 1 0.30 0.16 0.22 o -3 8 1 1.53 1.60 0.25 o -2 8 1 14.42 12.15 0.54 o -1 8 1 167.35 160.54 2.33 o 0 8 1 52.39 49.56 1.04 o 1 8 1 39.11 43.77 0.95 o 2 8 1 7.10 6.19 0.45 o 3 8 1 0.64 0.39 0.21 o 4 8 1 0.08 0.62 0.25 o -3 9 1 8.88 8.70 0.42 o -2 9 1 3.02 2.95 0.29 o -1 9 1 13.07 12.35 0.63 o 0 9 1 20.26 18.01 0.76 o 1 9 1 95.36 92.79 1.69 o 2 9 1 0.24 0.27 0.18 o 3 9 1 14.92 14.00 0.52 o 4 9 1 1.60 1.11 0.24 o -3 10 1 1.95 3.13 0.24 o -2 10 1 1.79 1.93 0.22 o -1 10 1 7.76 7.42 0.53 o 0 10 1 27.98 24.50 0.87 o 1 10 1 10.09 10.87 0.50 o 2 10 1 0.73 0.91 0.22 o 3 10 1 1.47 1.53 0.30 o -2 11 1 23.58 19.48 0.60 o -1 11 1 1.70 1.50 0.22 o 0 11 1 20.90 19.27 0.59 o 1 11 1 0.35 0.50 0.17 o 2 11 1 17.89 17.18 0.57 o -1 12 1 0.94 1.01 0.17 o 0 12 1 21.07 18.56 0.57 o 1 12 1 1.07 0.77 0.14 o -5 0 2 4.10 6.38 0.72 o -4 0 2 48.90 52.98 2.39 o -3 0 2 313.80 310.98 5.43 o -2 0 2 496.31 465.10 5.88 o -1 0 2 1649.88 1555.19 6.53 o 2 0 2 30.84 22.55 1.16 o 3 0 2 32.16 25.90 1.55 o 4 0 2 121.89 122.70 2.37 o -5 1 2 21.47 23.30 1.36 o -4 1 2 38.06 40.74 0.93 o -3 1 2 3.79 6.11 0.68 o -2 1 2 22.84 26.53 0.97 o -1 1 2 932.43 1046.17 7.25 o 0 1 2 15.71 22.45 0.44 o 1 1 2 3910.58 3564.70 19.08 o 2 1 2 34.11 40.41 0.78 o 3 1 2 33.10 30.19 1.18 o 4 1 2 38.10 38.65 0.84 o -5 2 2 21.82 26.97 0.93 o -4 2 2 19.33 21.46 0.77 o -3 2 2 4.28 4.36 0.59 o -2 2 2 1387.75 1356.83 7.41 o 0 2 2 762.49 726.32 6.14 o 1 2 2 23.95 24.77 0.51 o 2 2 2 117.30 114.68 1.47 o 3 2 2 88.21 80.64 3.10 o 4 2 2 0.57 0.34 0.22 o 5 2 2 2.40 7.72 0.89 o -5 3 2 64.15 69.72 1.50 o -4 3 2 9.29 13.04 0.56 o -3 3 2 56.43 50.99 2.31 o -2 3 2 583.84 524.72 5.10 o -1 3 2 371.63 369.67 2.74 o 0 3 2 69.85 71.37 1.26 o 1 3 2 357.47 392.15 2.35 o 2 3 2 4.04 2.51 0.27 o 3 3 2 318.52 307.22 5.94 o 4 3 2 832.76 861.69 5.29 o 5 3 2 0.63 1.02 0.47 o -5 4 2 0.35 0.78 0.29 o -4 4 2 26.74 25.96 0.78 o -3 4 2 96.65 96.29 1.78 o -2 4 2 1132.67 1218.97 7.82 o -1 4 2 1589.39 1744.34 6.64 o 0 4 2 122.06 103.20 1.85 o 1 4 2 54.38 62.53 1.05 o 2 4 2 19.34 20.24 0.86 o 3 4 2 41.93 40.74 1.17 o 4 4 2 63.65 72.34 2.03 o 5 4 2 2.70 2.98 0.52 o -5 5 2 22.84 22.43 2.06 o -4 5 2 2.29 4.12 0.42 o -3 5 2 16.72 15.51 0.64 o -2 5 2 303.79 330.61 5.17 o -1 5 2 736.63 851.32 5.95 o 0 5 2 300.90 306.03 3.43 o 1 5 2 316.09 311.00 3.60 o 2 5 2 242.68 242.88 3.05 o 3 5 2 2.24 3.17 0.38 o 4 5 2 62.17 62.68 2.55 o 5 5 2 0.04 -0.09 0.27 o -5 6 2 1.61 1.66 0.24 o -4 6 2 0.39 0.61 0.22 o -3 6 2 0.83 0.58 0.33 o -2 6 2 168.99 164.01 3.96 o -1 6 2 1.00 1.54 0.42 o 0 6 2 158.55 173.09 2.91 o 1 6 2 361.88 369.31 4.52 o 2 6 2 17.63 21.30 1.35 o 3 6 2 282.92 283.81 2.89 o 4 6 2 0.07 -0.17 0.34 o 5 6 2 1.93 2.02 0.34 o -4 7 2 2.02 2.67 0.29 o -3 7 2 19.81 21.90 0.98 o -2 7 2 29.37 25.70 0.75 o -1 7 2 131.54 129.14 2.85 o 0 7 2 545.28 556.61 5.23 o 1 7 2 5.95 7.61 0.72 o 2 7 2 61.75 57.01 1.09 o 3 7 2 57.80 65.47 1.39 o 4 7 2 8.33 13.69 0.92 o -4 8 2 18.11 20.57 0.80 o -3 8 2 2.59 2.42 0.29 o -2 8 2 208.61 198.30 2.82 o -1 8 2 58.59 60.17 1.36 o 0 8 2 41.89 43.02 0.97 o 1 8 2 28.02 27.91 0.76 o 2 8 2 11.51 12.28 0.62 o 3 8 2 3.12 2.32 0.29 o 4 8 2 2.98 3.43 0.37 o -3 9 2 2.36 1.87 0.32 o -2 9 2 3.25 1.98 0.25 o -1 9 2 0.03 -0.01 0.21 o 0 9 2 0.20 0.46 0.21 o 1 9 2 29.74 33.78 1.03 o 2 9 2 1.26 1.18 0.28 o 3 9 2 7.47 6.61 0.49 o 4 9 2 1.34 1.26 0.26 o -3 10 2 2.63 3.14 0.24 o -2 10 2 3.70 2.92 0.25 o -1 10 2 18.07 18.58 0.71 o 0 10 2 12.86 14.71 0.67 o 1 10 2 8.58 8.46 0.45 o 2 10 2 13.37 13.54 0.54 o 3 10 2 16.19 16.44 0.65 o -2 11 2 3.43 4.20 0.29 o -1 11 2 0.26 0.50 0.23 o 0 11 2 3.45 3.36 0.32 o 1 11 2 0.75 0.65 0.15 o 2 11 2 8.30 7.59 0.39 o -1 12 2 0.46 0.61 0.15 o 0 12 2 6.57 7.54 0.32 o 1 12 2 0.96 0.92 0.14 o -5 1 3 6.57 8.90 0.59 o -4 1 3 36.90 35.96 0.80 o -3 1 3 321.63 297.06 4.67 o -2 1 3 528.60 594.38 5.29 o -1 1 3 7.14 8.16 0.23 o 0 1 3 1466.15 1346.31 5.29 o 1 1 3 74.93 63.23 0.72 o 2 1 3 743.71 703.69 6.02 o 3 1 3 598.34 586.48 6.82 o 4 1 3 29.83 29.98 0.85 o -5 2 3 24.14 25.50 0.80 o -4 2 3 1.35 1.99 0.29 o -3 2 3 36.06 31.98 1.53 o -2 2 3 620.13 649.71 3.62 o -1 2 3 989.83 1058.04 3.90 o 1 2 3 15.33 23.87 0.47 o 2 2 3 239.04 232.23 2.35 o 3 2 3 94.02 86.58 3.25 o 4 2 3 33.95 29.61 1.32 o 5 2 3 0.04 0.67 0.45 o -5 3 3 12.85 14.81 0.86 o -4 3 3 8.21 8.66 0.60 o -3 3 3 13.61 15.30 1.68 o -2 3 3 1.02 0.57 0.25 o -1 3 3 61.16 52.14 0.93 o 0 3 3 231.76 233.13 1.81 o 1 3 3 1027.11 1074.36 5.54 o 2 3 3 370.96 370.95 3.21 o 3 3 3 295.00 283.77 4.82 o 4 3 3 1.18 7.40 0.68 o 5 3 3 1.10 0.82 0.42 o -5 4 3 8.88 7.26 0.41 o -4 4 3 0.43 0.57 0.20 o -3 4 3 305.52 290.42 2.42 o -2 4 3 2817.59 2738.22 17.80 o -1 4 3 163.70 201.78 2.23 o 0 4 3 2884.88 2841.30 9.68 o 1 4 3 254.56 239.85 2.10 o 2 4 3 0.60 0.82 0.18 o 3 4 3 0.66 0.52 0.18 o 4 4 3 5.15 6.12 0.74 o 5 4 3 6.86 4.76 0.65 o -5 5 3 0.27 1.46 0.30 o -4 5 3 1.21 2.38 0.33 o -3 5 3 2.28 3.43 0.38 o -2 5 3 0.06 0.18 0.29 o -1 5 3 765.40 856.75 6.02 o 0 5 3 26.46 29.83 1.04 o 1 5 3 3.05 3.18 0.38 o 2 5 3 51.43 54.53 1.61 o 3 5 3 628.28 595.35 8.92 o 4 5 3 8.08 8.36 0.78 o 5 5 3 0.33 0.39 0.28 o -5 6 3 3.46 4.21 0.34 o -4 6 3 1.77 1.28 0.26 o -3 6 3 5.70 6.59 0.60 o -2 6 3 8.64 11.01 1.07 o -1 6 3 608.57 606.77 5.65 o 0 6 3 197.57 214.42 3.26 o 1 6 3 136.92 123.40 2.62 o 2 6 3 29.12 28.58 1.17 o 3 6 3 65.31 67.21 1.42 o 4 6 3 1.70 2.29 0.53 o 5 6 3 6.29 5.83 0.50 o -4 7 3 0.14 0.27 0.19 o -3 7 3 49.28 44.29 1.37 o -2 7 3 107.84 103.38 1.49 o -1 7 3 23.94 25.24 1.26 o 0 7 3 20.41 23.76 1.11 o 1 7 3 15.87 15.46 1.12 o 2 7 3 1.09 0.37 0.58 o 3 7 3 71.65 73.19 1.47 o 4 7 3 5.13 6.28 0.59 o -4 8 3 0.02 -0.09 0.21 o -3 8 3 0.08 -0.07 0.20 o -2 8 3 35.93 37.69 1.04 o -1 8 3 95.64 107.48 1.91 o 0 8 3 0.76 1.62 0.26 o 1 8 3 98.31 98.76 1.43 o 2 8 3 41.09 42.83 1.11 o 3 8 3 0.85 0.49 0.21 o 4 8 3 0.71 0.65 0.23 o -3 9 3 6.67 5.72 0.34 o -2 9 3 0.72 1.46 0.28 o -1 9 3 33.71 31.75 1.08 o 0 9 3 0.39 0.33 0.19 o 1 9 3 67.82 66.27 1.43 o 2 9 3 13.82 14.10 0.68 o 3 9 3 61.94 69.53 1.39 o 4 9 3 2.75 1.72 0.28 o -3 10 3 9.34 6.56 0.48 o -2 10 3 1.18 0.87 0.17 o -1 10 3 5.59 4.87 0.39 o 0 10 3 5.38 5.67 0.44 o 1 10 3 5.76 7.52 0.43 o 2 10 3 6.93 7.84 0.42 o 3 10 3 1.80 2.10 0.28 o -2 11 3 6.10 6.56 0.35 o -1 11 3 27.46 22.28 0.83 o 0 11 3 11.71 11.12 0.52 o 1 11 3 0.64 0.66 0.16 o 2 11 3 6.02 7.02 0.54 o -1 12 3 11.46 8.90 0.39 o 0 12 3 0.40 0.38 0.12 o 1 12 3 4.46 3.68 0.41 o -5 0 4 25.83 27.85 1.43 o -4 0 4 0.05 -0.08 0.30 o -3 0 4 1438.22 1411.84 14.43 o -2 0 4 2040.48 1999.80 24.08 o 0 0 4 776.39 760.82 12.90 o 2 0 4 122.34 124.50 2.60 o 3 0 4 583.76 561.09 22.22 o 4 0 4 53.68 62.40 1.69 o -5 1 4 0.04 -0.05 0.29 o -4 1 4 48.25 48.93 1.04 o -3 1 4 114.58 99.34 2.73 o -2 1 4 54.95 63.86 1.36 o -1 1 4 4721.49 4432.02 21.26 o 1 1 4 48.48 45.09 0.68 o 2 1 4 595.11 574.80 4.57 o 3 1 4 654.75 649.87 7.30 o 4 1 4 7.32 3.85 0.50 o -5 2 4 19.56 17.97 0.83 o -4 2 4 24.02 19.47 0.67 o -3 2 4 0.56 1.01 0.37 o -2 2 4 1291.99 1320.49 5.85 o 0 2 4 177.84 159.36 1.52 o 1 2 4 198.82 190.23 1.47 o 2 2 4 57.93 55.79 1.12 o 3 2 4 4.39 5.14 0.52 o 4 2 4 106.97 115.97 2.55 o 5 2 4 9.06 13.36 1.02 o -5 3 4 0.77 1.28 0.26 o -4 3 4 14.30 17.71 0.73 o -3 3 4 8.90 11.01 1.47 o -2 3 4 969.76 1098.20 7.81 o -1 3 4 2.92 4.99 0.46 o 0 3 4 1807.51 1655.07 11.04 o 1 3 4 28.64 28.93 0.56 o 2 3 4 816.33 804.52 4.83 o 3 3 4 3.46 2.23 0.50 o 4 3 4 270.30 289.50 4.19 o 5 3 4 20.54 17.85 1.18 o -5 4 4 0.88 0.68 0.40 o -4 4 4 3.88 3.42 0.31 o -3 4 4 53.95 56.23 1.24 o -2 4 4 250.07 237.02 3.91 o -1 4 4 499.77 472.89 5.42 o 0 4 4 65.59 54.12 1.19 o 1 4 4 15.73 12.97 0.40 o 2 4 4 304.05 310.63 2.78 o 3 4 4 0.27 0.10 0.17 o 4 4 4 44.79 48.58 1.75 o 5 4 4 0.10 0.52 0.37 o -5 5 4 2.44 3.57 0.44 o -4 5 4 10.47 12.11 0.64 o -3 5 4 58.43 59.50 1.23 o -2 5 4 22.04 21.03 1.20 o -1 5 4 16.60 8.23 0.62 o 0 5 4 44.06 47.22 1.32 o 1 5 4 316.11 308.62 3.51 o 2 5 4 893.73 836.44 9.48 o 3 5 4 320.42 317.05 3.33 o 4 5 4 0.99 0.67 0.36 o 5 5 4 0.03 -0.09 0.25 o -5 6 4 4.67 4.89 0.33 o -4 6 4 2.55 2.28 0.33 o -3 6 4 301.02 293.99 5.54 o -2 6 4 92.13 96.40 3.06 o -1 6 4 72.18 88.40 2.17 o 0 6 4 16.04 12.32 0.82 o 1 6 4 71.07 67.00 2.37 o 2 6 4 31.33 31.31 0.87 o 3 6 4 7.87 9.17 0.57 o 4 6 4 1.10 0.53 0.56 o -4 7 4 0.41 0.23 0.18 o -3 7 4 15.27 17.42 0.89 o -2 7 4 0.32 0.41 0.19 o -1 7 4 30.01 31.61 0.97 o 0 7 4 296.19 305.24 3.91 o 1 7 4 102.19 108.36 2.17 o 2 7 4 71.95 68.70 1.66 o 3 7 4 158.81 156.85 2.12 o 4 7 4 13.94 16.05 0.84 o -4 8 4 0.23 0.52 0.16 o -3 8 4 0.49 0.53 0.24 o -2 8 4 115.24 109.42 2.21 o -1 8 4 155.38 152.05 2.38 o 0 8 4 54.99 52.05 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