#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/68/2236894.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236894_Fobs loop_ _publ_author_name 'Sreenivasa, S.' 'ManojKumar, K.E.' 'Suchetan, P.A.' 'Srinivasan, T.' 'Palakshamurthy, B. S.' 'Velmurgan, D.' _publ_section_title ; 1-(2-Amino-6-methylpyrimidin-4-yl)-N,N-dimethylpiperidin-4-aminium chloride ; _journal_coeditor_code HB6988 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3371 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.968 _cell_angle_gamma 90.000 _cell_length_a 24.7908 _cell_length_b 8.2419 _cell_length_c 13.8764 _exptl_crystal_F_000 1168.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file hb6988Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' manc in C 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 361.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1638.66 1624.92 66.90 o 4 0 0 1422.93 1402.24 24.22 o 6 0 0 54.57 36.83 1.78 o 8 0 0 51275.21 42888.48 1156.54 o 10 0 0 29107.95 28935.39 754.08 o 12 0 0 6234.64 7978.93 133.97 o 14 0 0 1129.52 1137.81 31.04 o 16 0 0 2372.39 2228.33 40.85 o 18 0 0 1524.44 1318.82 38.53 o 20 0 0 2800.62 2833.82 51.81 o 22 0 0 258.63 212.33 8.48 o 24 0 0 69.40 49.24 8.56 o 26 0 0 522.32 546.85 20.34 o 28 0 0 118.49 123.61 13.91 o 1 1 0 3898.92 3743.32 27.99 o 3 1 0 34650.99 28336.13 1129.34 o 5 1 0 21848.36 21049.74 306.76 o 7 1 0 8556.26 8163.20 94.65 o 9 1 0 0.79 16.47 3.88 o 11 1 0 977.98 998.78 18.61 o 13 1 0 24568.28 25618.70 382.26 o 15 1 0 6051.17 6064.56 64.88 o 17 1 0 364.23 344.57 21.78 o 19 1 0 824.07 801.14 13.33 o 21 1 0 97.98 63.51 5.13 o 23 1 0 588.49 578.06 21.61 o 25 1 0 292.67 264.68 10.08 o 27 1 0 124.90 113.14 7.19 o 29 1 0 251.73 260.34 11.28 o 0 2 0 3157.97 3066.59 34.64 o 2 2 0 26709.13 24722.33 209.41 o 4 2 0 1848.77 1778.23 14.14 o 6 2 0 4.00 6.35 1.07 o 8 2 0 352.14 371.15 5.54 o 10 2 0 984.78 1005.41 12.42 o 12 2 0 4111.21 3873.09 42.21 o 14 2 0 795.81 761.18 10.61 o 16 2 0 71.38 102.13 3.47 o 18 2 0 38.57 62.03 3.54 o 20 2 0 5498.40 5449.36 77.23 o 22 2 0 2142.25 2145.38 30.22 o 24 2 0 87.58 100.90 5.31 o 26 2 0 49.76 26.24 6.05 o 28 2 0 645.54 650.63 21.19 o 1 3 0 447.12 500.54 5.14 o 3 3 0 763.41 848.99 7.46 o 5 3 0 860.14 1089.02 10.54 o 7 3 0 13081.78 13828.04 113.16 o 9 3 0 1481.91 1788.98 16.36 o 11 3 0 865.29 883.62 9.94 o 13 3 0 1431.97 1519.61 15.90 o 15 3 0 672.97 653.08 8.83 o 17 3 0 12296.84 12242.88 128.89 o 19 3 0 1718.83 1758.14 28.82 o 21 3 0 296.06 285.18 11.28 o 23 3 0 26.77 26.90 5.33 o 25 3 0 403.66 409.87 12.08 o 27 3 0 25.02 35.39 7.16 o 0 4 0 435.10 333.65 5.89 o 2 4 0 329.69 301.83 3.83 o 4 4 0 11576.08 12621.12 95.00 o 6 4 0 1589.69 1650.84 15.73 o 8 4 0 44.07 43.09 2.41 o 10 4 0 55.06 64.57 2.95 o 12 4 0 739.56 851.62 10.74 o 14 4 0 640.35 722.06 12.42 o 16 4 0 1427.27 1490.67 21.75 o 18 4 0 7.15 4.64 3.87 o 20 4 0 1030.81 1117.84 26.46 o 22 4 0 103.49 91.40 7.46 o 24 4 0 207.49 202.45 8.96 o 26 4 0 206.64 245.52 21.29 o 1 5 0 571.09 529.24 6.74 o 3 5 0 17.77 8.49 1.21 o 5 5 0 188.16 208.39 3.53 o 7 5 0 1307.37 1185.01 13.60 o 9 5 0 372.76 417.44 7.94 o 11 5 0 7.70 3.18 2.12 o 13 5 0 8.72 2.53 3.24 o 15 5 0 98.40 109.26 4.97 o 17 5 0 798.39 816.24 17.28 o 19 5 0 581.80 578.90 17.36 o 21 5 0 271.41 285.11 10.21 o 23 5 0 598.19 647.12 19.96 o 25 5 0 2.80 1.18 4.09 o 0 6 0 38.40 32.53 2.57 o 2 6 0 4.02 4.00 1.26 o 4 6 0 628.61 601.45 10.02 o 6 6 0 39.83 42.34 2.60 o 8 6 0 5.97 1.74 1.60 o 10 6 0 143.72 179.18 5.56 o 12 6 0 660.76 763.59 19.78 o 14 6 0 14.74 17.89 4.41 o 16 6 0 129.98 102.81 10.70 o 18 6 0 0.08 0.88 4.11 o 20 6 0 920.06 934.55 20.18 o 22 6 0 1.64 0.00 5.55 o 1 7 0 49.31 58.06 4.40 o 3 7 0 2271.03 2315.91 27.70 o 5 7 0 229.78 239.08 8.17 o 7 7 0 65.64 72.81 3.50 o 9 7 0 997.72 1047.96 17.36 o 11 7 0 120.90 115.26 6.33 o 13 7 0 0.44 2.14 3.26 o 15 7 0 372.17 360.11 13.99 o 17 7 0 53.45 61.99 5.56 o 19 7 0 3.21 14.84 4.71 o 0 8 0 187.50 211.93 13.91 o 2 8 0 298.62 310.65 15.52 o 4 8 0 26.34 26.65 4.88 o 6 8 0 1120.39 1098.94 19.74 o 8 8 0 18.48 19.65 3.22 o 10 8 0 245.76 228.84 8.84 o 12 8 0 35.40 61.63 5.56 o 14 8 0 100.49 114.45 6.99 o 16 8 0 37.72 64.51 5.95 o 1 9 0 296.94 315.62 17.13 o 3 9 0 978.69 945.29 24.59 o 5 9 0 181.98 195.52 10.60 o 7 9 0 312.75 338.54 13.23 o 9 9 0 39.77 39.86 6.05 o 11 9 0 399.29 454.88 15.84 o -29 1 1 77.17 72.55 7.19 o -27 1 1 88.82 90.53 8.69 o -25 1 1 0.51 0.00 3.46 o -23 1 1 9.01 6.37 5.06 o -21 1 1 138.72 118.76 5.32 o -19 1 1 1090.85 1054.21 14.49 o -17 1 1 19.12 21.04 1.90 o -15 1 1 474.28 470.56 8.31 o -13 1 1 5706.65 5915.77 109.69 o -11 1 1 990.61 1287.86 16.96 o -9 1 1 120.70 94.58 11.77 o -7 1 1 4378.72 4322.56 52.93 o -5 1 1 10708.43 10246.04 104.84 o -3 1 1 5942.00 6117.76 51.99 o -1 1 1 1907.80 1750.39 14.14 o 1 1 1 46.19 28.20 0.96 o 3 1 1 8585.82 9092.81 110.46 o 5 1 1 1083.85 1084.30 12.15 o 7 1 1 0.82 9.63 2.14 o 9 1 1 1789.94 1859.58 23.26 o 11 1 1 93.94 133.45 3.76 o 13 1 1 9707.13 11342.92 171.84 o 15 1 1 1124.98 1274.36 23.06 o 17 1 1 0.51 0.00 1.40 o 19 1 1 20.09 28.83 2.28 o 21 1 1 70.49 98.55 4.43 o 23 1 1 368.24 369.12 8.90 o 25 1 1 34.25 22.06 4.33 o 27 1 1 29.68 24.96 4.87 o 29 1 1 1.61 0.00 4.88 o -28 2 1 81.21 85.06 8.68 o -26 2 1 9.52 0.00 5.14 o -24 2 1 356.73 345.20 13.62 o -22 2 1 3310.18 3170.36 49.01 o -20 2 1 202.53 233.22 8.61 o -18 2 1 592.07 602.71 11.18 o -16 2 1 351.61 298.96 5.89 o -14 2 1 1003.16 857.64 12.84 o -12 2 1 1192.39 1228.59 13.94 o -10 2 1 746.21 758.85 8.41 o -8 2 1 9.04 7.78 1.62 o -6 2 1 14158.40 13760.54 119.30 o -4 2 1 2910.37 3104.08 24.24 o -2 2 1 5144.24 5065.58 38.92 o 0 2 1 8123.51 7833.83 61.22 o 2 2 1 13043.22 12382.19 101.89 o 4 2 1 610.25 658.60 7.76 o 6 2 1 4108.24 4086.34 41.62 o 8 2 1 965.21 932.44 14.81 o 10 2 1 115.76 121.67 2.90 o 12 2 1 1.18 0.00 0.96 o 14 2 1 928.92 897.81 11.94 o 16 2 1 1406.66 1470.28 18.35 o 18 2 1 363.81 409.29 7.62 o 20 2 1 410.19 393.35 7.81 o 22 2 1 9.80 3.52 2.59 o 24 2 1 33.81 39.96 4.41 o 26 2 1 0.14 6.23 3.60 o 28 2 1 350.03 309.65 13.99 o -27 3 1 288.75 290.93 14.32 o -25 3 1 154.60 142.67 7.55 o -23 3 1 91.67 86.22 5.67 o -21 3 1 113.11 121.71 6.30 o -19 3 1 428.61 457.08 11.60 o -17 3 1 10361.37 10571.95 143.69 o -15 3 1 0.73 3.39 1.62 o -13 3 1 115.31 127.74 3.49 o -11 3 1 52.50 73.60 2.58 o -9 3 1 13352.99 13881.99 120.74 o -7 3 1 5637.73 5682.03 48.00 o -5 3 1 1195.24 1376.46 11.00 o -3 3 1 516.05 643.01 6.14 o -1 3 1 401.90 375.40 5.92 o 1 3 1 10229.02 9999.22 79.88 o 3 3 1 9555.83 9882.23 82.59 o 5 3 1 1938.86 1854.20 16.90 o 7 3 1 4931.00 5289.18 53.95 o 9 3 1 4233.18 4139.48 36.48 o 11 3 1 1446.76 1224.09 13.01 o 13 3 1 3274.28 3160.28 35.49 o 15 3 1 14.90 9.53 1.78 o 17 3 1 2732.65 2737.04 31.95 o 19 3 1 1664.11 1769.68 22.28 o 21 3 1 699.30 691.47 15.42 o 23 3 1 529.49 598.48 17.68 o 25 3 1 0.27 0.00 3.22 o 27 3 1 11.63 13.91 4.41 o -26 4 1 192.80 222.06 9.59 o -24 4 1 416.09 437.07 13.05 o -22 4 1 210.10 229.40 9.13 o -20 4 1 321.38 359.68 13.10 o -18 4 1 780.82 810.56 20.72 o -16 4 1 63.66 52.44 4.51 o -14 4 1 109.04 110.62 9.42 o -12 4 1 954.06 905.90 13.02 o -10 4 1 2329.16 2374.93 25.38 o -8 4 1 162.73 185.21 3.07 o -6 4 1 35.38 59.17 1.76 o -4 4 1 9581.54 9217.58 84.38 o -2 4 1 4555.11 4245.52 34.95 o 0 4 1 2046.07 2075.46 20.72 o 2 4 1 12.69 16.74 1.19 o 4 4 1 765.83 661.30 7.83 o 6 4 1 657.38 489.72 6.20 o 8 4 1 3588.36 3546.95 40.58 o 10 4 1 1174.40 1082.16 14.71 o 12 4 1 222.15 196.03 4.96 o 14 4 1 108.34 95.47 4.53 o 16 4 1 6094.86 5898.80 72.22 o 18 4 1 966.40 966.33 16.13 o 20 4 1 351.74 366.50 11.09 o 22 4 1 337.30 330.31 10.63 o 24 4 1 573.17 637.46 19.20 o 26 4 1 877.59 959.72 21.35 o -25 5 1 25.03 22.82 5.04 o -23 5 1 11.08 7.18 4.24 o -21 5 1 330.43 355.31 13.38 o -19 5 1 24.12 20.11 4.09 o -17 5 1 878.14 827.05 17.48 o -15 5 1 1097.24 1030.56 19.76 o -13 5 1 6.96 11.46 3.26 o -11 5 1 1418.99 1453.10 21.59 o -9 5 1 43.57 69.54 3.31 o -7 5 1 4890.73 4973.17 44.91 o -5 5 1 16.72 6.48 1.19 o -3 5 1 39.93 34.75 1.75 o -1 5 1 5.16 5.49 1.26 o 1 5 1 1375.69 1327.55 13.98 o 3 5 1 4002.44 3876.82 36.40 o 5 5 1 904.43 894.65 11.23 o 7 5 1 156.80 175.58 3.69 o 9 5 1 56.97 43.77 2.90 o 11 5 1 5950.33 5798.27 65.21 o 13 5 1 1123.75 1119.89 17.52 o 15 5 1 2.51 0.29 2.31 o 17 5 1 2073.88 2164.63 30.48 o 19 5 1 1600.22 1582.43 28.22 o 21 5 1 649.28 655.12 16.04 o 23 5 1 231.67 257.92 12.47 o 25 5 1 333.79 409.72 13.05 o -22 6 1 150.31 135.02 7.99 o -20 6 1 1207.33 1186.67 24.05 o -18 6 1 3.68 7.01 3.88 o -16 6 1 20.17 8.81 3.60 o -14 6 1 344.89 310.89 10.04 o -12 6 1 814.64 773.01 15.97 o -10 6 1 444.92 375.79 8.93 o -8 6 1 70.38 63.78 3.20 o -6 6 1 402.02 365.18 7.64 o -4 6 1 5389.22 5289.87 59.50 o -2 6 1 1577.21 1557.95 15.71 o 0 6 1 13.98 27.68 1.92 o 2 6 1 530.91 524.11 7.14 o 4 6 1 598.72 532.11 8.71 o 6 6 1 120.41 125.48 4.06 o 8 6 1 283.46 275.69 6.60 o 10 6 1 1.13 3.80 2.11 o 12 6 1 55.11 43.03 3.54 o 14 6 1 22.51 36.11 3.76 o 16 6 1 178.62 202.57 7.21 o 18 6 1 620.78 623.87 15.21 o 20 6 1 95.52 92.96 7.35 o 22 6 1 30.69 32.02 9.63 o -19 7 1 65.70 67.10 6.12 o -17 7 1 218.34 222.13 9.23 o -15 7 1 41.72 43.85 4.87 o -13 7 1 301.42 242.63 9.05 o -11 7 1 951.04 918.03 15.99 o -9 7 1 444.63 462.50 9.65 o -7 7 1 206.26 183.89 5.72 o -5 7 1 759.06 780.45 13.95 o -3 7 1 115.61 128.34 9.82 o -1 7 1 3258.52 3171.08 40.91 o 1 7 1 412.20 408.87 7.87 o 3 7 1 51.84 48.22 3.03 o 5 7 1 6.38 1.61 1.86 o 7 7 1 34.86 24.54 2.62 o 9 7 1 1176.24 1049.78 17.50 o 11 7 1 0.05 0.00 2.59 o 13 7 1 33.48 30.40 3.86 o 15 7 1 1.77 0.00 4.48 o 17 7 1 17.50 23.83 4.51 o 19 7 1 1.04 3.75 4.82 o -16 8 1 17.67 15.33 5.63 o -14 8 1 27.20 15.68 4.51 o -12 8 1 77.16 79.45 6.12 o -10 8 1 645.97 642.68 13.18 o -8 8 1 25.74 29.85 4.33 o -6 8 1 5.13 13.42 4.88 o -4 8 1 695.66 645.93 25.15 o -2 8 1 1709.11 1674.45 39.07 o 0 8 1 1129.89 1107.87 26.49 o 2 8 1 59.82 78.03 6.53 o 4 8 1 153.03 154.23 7.19 o 6 8 1 126.28 151.39 5.66 o 8 8 1 27.44 25.51 3.69 o 10 8 1 809.26 729.11 14.28 o 12 8 1 972.65 970.89 17.36 o 14 8 1 53.97 65.06 5.75 o 16 8 1 0.12 1.07 4.88 o -11 9 1 83.59 77.07 10.70 o -9 9 1 0.03 5.26 4.36 o -7 9 1 0.02 4.82 4.54 o -5 9 1 519.88 528.97 17.02 o -3 9 1 624.12 625.41 23.01 o -1 9 1 186.56 194.22 10.60 o 1 9 1 0.02 8.03 4.54 o 3 9 1 695.04 788.66 22.32 o 5 9 1 37.38 38.37 6.05 o 7 9 1 64.88 73.79 7.57 o 9 9 1 192.95 193.67 13.91 o 11 9 1 76.78 74.00 7.57 o -28 0 2 769.56 709.24 22.67 o -26 0 2 773.38 875.30 24.18 o -24 0 2 1300.37 1349.58 31.40 o -22 0 2 144.81 139.15 12.84 o -20 0 2 292.14 270.81 17.13 o -18 0 2 113.99 190.86 7.12 o -16 0 2 5630.14 5805.68 99.51 o -14 0 2 106.27 119.58 4.68 o -12 0 2 1210.17 1346.34 39.07 o -10 0 2 12807.71 13434.38 190.88 o -8 0 2 11343.02 10749.85 153.33 o -6 0 2 9316.38 10081.02 144.30 o -4 0 2 7940.80 6835.72 102.80 o -2 0 2 6482.49 5999.47 65.97 o 0 0 2 31792.79 29013.92 490.74 o 2 0 2 86403.29 66098.74 5316.57 o 4 0 2 1700.10 2119.63 37.09 o 6 0 2 6791.23 7081.75 118.83 o 8 0 2 879.56 1003.93 24.08 o 10 0 2 7555.71 8686.70 162.16 o 12 0 2 166.37 174.48 6.05 o 14 0 2 4930.80 5290.27 91.20 o 16 0 2 709.33 629.04 14.74 o 18 0 2 118.60 136.01 6.05 o 20 0 2 2072.38 2073.92 58.87 o 22 0 2 126.52 181.72 7.92 o 24 0 2 1527.74 1435.38 42.82 o 26 0 2 243.98 274.02 17.13 o 28 0 2 161.65 127.61 12.84 o -29 1 2 39.83 32.46 6.12 o -27 1 2 100.97 104.87 8.32 o -25 1 2 120.13 133.30 7.61 o -23 1 2 29.12 10.69 5.80 o -21 1 2 2213.79 2330.40 32.06 o -19 1 2 363.13 383.37 9.42 o -17 1 2 393.14 389.70 7.48 o -15 1 2 3061.40 3134.41 32.46 o -13 1 2 4033.58 4140.41 42.88 o -11 1 2 702.32 874.69 13.16 o -9 1 2 2149.85 1969.52 19.69 o -7 1 2 1406.30 1531.38 23.33 o -5 1 2 2310.02 2472.12 23.13 o -3 1 2 10389.75 9915.75 82.18 o -1 1 2 172.65 312.18 3.30 o 1 1 2 446.54 673.27 7.19 o 3 1 2 4238.59 4028.74 39.87 o 5 1 2 2288.77 2394.06 25.90 o 7 1 2 9729.75 9620.26 111.47 o 9 1 2 7559.84 7734.40 81.19 o 11 1 2 28.94 10.40 1.74 o 13 1 2 1522.21 1500.44 18.08 o 15 1 2 30.41 20.49 1.67 o 17 1 2 578.35 593.79 9.17 o 19 1 2 1296.61 1238.80 24.51 o 21 1 2 845.38 748.30 15.42 o 23 1 2 765.59 651.60 19.54 o 25 1 2 105.53 113.11 6.90 o 27 1 2 653.95 687.45 16.47 o -28 2 2 40.61 36.86 7.46 o -26 2 2 1.44 0.00 4.09 o -24 2 2 748.85 690.68 16.66 o -22 2 2 829.47 872.15 15.42 o -20 2 2 2244.22 2155.99 100.20 o -18 2 2 2.77 1.62 2.97 o -16 2 2 420.98 499.62 7.77 o -14 2 2 257.38 183.87 3.74 o -12 2 2 31.79 14.27 1.17 o -10 2 2 200.26 238.45 3.66 o -8 2 2 8135.95 8227.56 82.68 o -6 2 2 736.47 608.42 5.94 o -4 2 2 25064.71 24690.68 195.56 o -2 2 2 1763.02 1820.94 15.46 o 0 2 2 82.01 132.62 2.30 o 2 2 2 2050.74 2222.01 18.86 o 4 2 2 2008.46 2400.77 21.29 o 6 2 2 7462.69 7852.26 71.32 o 8 2 2 231.96 299.10 5.40 o 10 2 2 1164.73 1089.79 13.45 o 12 2 2 551.25 582.71 8.48 o 14 2 2 2726.10 2713.44 34.36 o 16 2 2 103.58 119.35 3.76 o 18 2 2 1381.00 1346.10 19.92 o 20 2 2 1506.36 1524.94 19.90 o 22 2 2 296.21 290.05 6.77 o 24 2 2 247.54 230.65 8.61 o 26 2 2 27.92 27.28 5.14 o 28 2 2 28.18 13.91 7.49 o -27 3 2 1.45 1.86 5.64 o -25 3 2 1.67 2.14 7.49 o -23 3 2 1.54 0.00 3.05 o -21 3 2 0.47 0.00 2.31 o -19 3 2 97.56 87.67 4.62 o -17 3 2 295.97 309.71 7.64 o -15 3 2 411.46 444.52 6.94 o -13 3 2 5.31 17.21 2.57 o -11 3 2 1169.34 1319.57 15.02 o -9 3 2 188.63 284.83 4.29 o -7 3 2 3844.92 3890.53 30.62 o -5 3 2 184.78 330.89 4.02 o -3 3 2 412.13 477.97 5.17 o -1 3 2 225.85 316.42 4.10 o 1 3 2 978.09 952.49 9.96 o 3 3 2 14527.67 14877.82 121.09 o 5 3 2 4934.97 4602.48 47.31 o 7 3 2 8300.65 8717.14 87.63 o 9 3 2 81.27 142.14 2.39 o 11 3 2 208.71 236.70 4.32 o 13 3 2 1465.02 1477.18 18.21 o 15 3 2 167.95 171.77 4.51 o 17 3 2 65.93 54.31 3.18 o 19 3 2 1810.43 1820.09 25.94 o 21 3 2 63.18 77.90 4.53 o 23 3 2 14.83 11.84 3.46 o 25 3 2 43.86 45.66 4.87 o 27 3 2 7.86 14.57 4.88 o 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1931.09 18.86 o -7 5 2 329.79 403.57 6.01 o -5 5 2 642.15 547.92 7.45 o -3 5 2 1382.46 1327.99 13.29 o -1 5 2 826.47 929.06 10.60 o 1 5 2 3707.93 3783.17 52.66 o 3 5 2 29.00 27.18 1.68 o 5 5 2 154.98 183.93 4.40 o 7 5 2 225.25 255.95 6.08 o 9 5 2 9.50 11.68 2.28 o 11 5 2 123.05 136.28 5.47 o 13 5 2 96.21 73.04 4.71 o 15 5 2 145.88 147.95 6.01 o 17 5 2 35.97 48.82 4.13 o 19 5 2 953.56 1026.05 20.80 o 21 5 2 204.53 228.32 9.23 o 23 5 2 3.22 1.74 3.60 o -22 6 2 89.47 86.63 7.80 o -20 6 2 815.59 874.22 19.90 o -18 6 2 19.87 15.07 4.24 o -16 6 2 401.69 396.61 11.71 o -14 6 2 4152.00 3840.09 57.88 o -12 6 2 17.90 22.88 3.32 o -10 6 2 182.35 164.40 4.73 o -8 6 2 316.84 290.54 6.65 o -6 6 2 4299.14 4439.65 50.96 o -4 6 2 3195.93 3177.49 31.88 o -2 6 2 257.34 254.15 4.80 o 0 6 2 588.99 555.30 7.25 o 2 6 2 499.87 471.64 8.27 o 4 6 2 4753.35 4715.81 51.73 o 6 6 2 504.94 504.06 8.40 o 8 6 2 24.10 16.59 2.53 o 10 6 2 252.44 260.97 7.56 o 12 6 2 506.41 450.28 10.15 o 14 6 2 1068.58 909.25 16.06 o 16 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