#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236909.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236909_Fobs loop_ _publ_author_name 'Nyamori, Vincent O.' 'Keru, Godfrey' 'Omondi, Bernard' _publ_section_title ; (4-{[(Pyridin-4-yl)methylidene]amino}phenyl)ferrocene ; _journal_coeditor_code HG5267 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1535 _journal_volume 68 _journal_year 2012 _space_group_IT_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _cell_angle_alpha 90.000 _cell_angle_beta 93.044 _cell_angle_gamma 90.000 _cell_length_a 10.7200 _cell_length_b 7.4015 _cell_length_c 20.8517 _exptl_crystal_F_000 760.00 _reflns_d_resolution_high 0.7502 _[local]_cod_data_source_file hg5267Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 12bo_von_ker1_0ma in P2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 224.28 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 -9 0 71.07 77.62 7.12 o 2 -9 0 96.34 109.76 9.86 o 3 -9 0 96.02 96.98 10.05 o 4 -9 0 7.98 16.47 11.48 o 5 -9 0 262.22 247.58 21.46 o 0 -8 0 821.54 804.10 25.23 o 1 -8 0 772.47 781.35 20.65 o 2 -8 0 241.25 242.58 10.46 o 3 -8 0 465.35 460.84 17.61 o 4 -8 0 1336.56 1309.88 45.92 o 5 -8 0 125.53 135.81 10.52 o 6 -8 0 109.66 102.36 6.08 o 7 -8 0 627.02 637.95 17.81 o 8 -8 0 359.29 396.17 13.44 o 1 -7 0 582.01 558.51 19.54 o 2 -7 0 803.68 810.80 12.83 o 3 -7 0 1031.67 1030.15 16.43 o 4 -7 0 385.34 401.21 15.52 o 5 -7 0 158.60 177.03 11.37 o 6 -7 0 453.24 464.49 11.91 o 7 -7 0 144.79 147.90 6.94 o 8 -7 0 379.26 386.05 12.25 o 9 -7 0 776.83 763.73 21.44 o 10 -7 0 200.54 209.32 15.22 o 0 -6 0 593.39 494.66 24.46 o 1 -6 0 81.17 78.25 6.52 o 2 -6 0 38.74 40.16 2.02 o 3 -6 0 1348.31 1390.47 21.44 o 4 -6 0 599.25 608.13 10.90 o 5 -6 0 21.58 25.39 2.73 o 6 -6 0 118.35 108.77 5.35 o 7 -6 0 249.31 264.42 8.66 o 8 -6 0 857.01 854.73 19.20 o 9 -6 0 176.58 161.46 8.87 o 10 -6 0 192.62 192.40 10.08 o 11 -6 0 359.38 362.48 17.12 o 1 -5 0 1060.20 1039.85 37.69 o 2 -5 0 2553.80 2642.67 39.11 o 3 -5 0 409.94 411.54 7.44 o 4 -5 0 427.77 432.94 8.12 o 5 -5 0 436.55 439.31 6.77 o 6 -5 0 143.99 129.71 4.24 o 7 -5 0 451.74 446.96 8.94 o 8 -5 0 546.88 517.95 13.40 o 9 -5 0 645.83 666.12 20.65 o 10 -5 0 165.13 169.14 9.52 o 11 -5 0 94.04 94.17 7.90 o 12 -5 0 29.79 36.86 8.63 o 0 -4 0 3447.70 3266.43 119.30 o 1 -4 0 1640.35 1731.59 37.75 o 2 -4 0 2897.33 3168.73 40.39 o 3 -4 0 2319.08 2481.75 33.81 o 4 -4 0 4865.78 4974.52 68.75 o 5 -4 0 230.98 240.03 3.91 o 6 -4 0 46.02 43.68 2.65 o 7 -4 0 338.53 321.58 6.44 o 8 -4 0 1863.63 1857.36 31.49 o 9 -4 0 743.94 734.09 15.09 o 10 -4 0 410.16 393.12 13.31 o 11 -4 0 420.64 432.67 14.59 o 12 -4 0 373.99 385.45 14.28 o 13 -4 0 118.35 112.13 11.15 o 1 -3 0 2243.36 2145.47 38.60 o 2 -3 0 2472.75 2788.29 38.19 o 3 -3 0 3190.40 3163.52 38.80 o 4 -3 0 1999.60 2151.47 22.80 o 5 -3 0 3409.67 3325.49 37.48 o 6 -3 0 144.13 138.05 3.43 o 7 -3 0 1253.20 1221.30 16.87 o 8 -3 0 210.74 214.06 5.40 o 9 -3 0 1418.27 1412.76 25.70 o 10 -3 0 394.22 377.42 9.63 o 11 -3 0 434.96 434.43 12.71 o 12 -3 0 215.60 210.25 10.45 o 13 -3 0 222.88 221.39 14.36 o 0 -2 0 32569.36 32704.74 1128.58 o 1 -2 0 2409.35 2560.70 34.75 o 2 -2 0 11662.20 12166.95 142.93 o 3 -2 0 828.38 919.33 10.81 o 4 -2 0 3814.10 3712.97 40.16 o 5 -2 0 77.15 88.42 2.57 o 6 -2 0 1104.65 1097.40 14.58 o 7 -2 0 334.62 324.86 5.78 o 8 -2 0 2457.85 2420.23 31.25 o 9 -2 0 642.69 651.59 10.42 o 10 -2 0 622.87 615.66 12.38 o 11 -2 0 127.20 129.47 6.42 o 12 -2 0 571.52 577.85 17.86 o 13 -2 0 201.93 214.86 20.71 o 1 -1 0 13804.75 14202.80 145.27 o 2 -1 0 14440.14 15026.03 149.36 o 3 -1 0 52.20 64.30 3.93 o 4 -1 0 451.96 480.09 6.69 o 5 -1 0 5245.59 5327.44 60.41 o 6 -1 0 428.44 431.22 6.73 o 7 -1 0 115.83 114.36 3.84 o 8 -1 0 47.75 44.51 2.72 o 9 -1 0 509.91 464.61 8.31 o 10 -1 0 561.33 566.28 9.57 o 11 -1 0 130.07 119.71 5.35 o 12 -1 0 337.18 333.19 11.15 o 13 -1 0 542.28 548.56 30.95 o 14 -1 0 84.09 86.85 15.47 o 1 0 0 5.04 2.59 0.36 o 2 0 0 151.89 131.71 2.09 o 3 0 0 8.70 8.29 1.21 o 4 0 0 5257.25 5015.74 57.45 o 5 0 0 171.32 173.17 3.46 o 6 0 0 546.97 493.04 7.43 o 7 0 0 126.25 120.79 3.77 o 8 0 0 485.92 439.86 7.74 o 9 0 0 963.02 1033.71 14.52 o 10 0 0 212.39 188.86 5.30 o 11 0 0 151.14 140.54 6.86 o 12 0 0 823.81 807.76 19.39 o 13 0 0 87.28 85.53 8.36 o 14 0 0 385.18 417.69 19.23 o 1 1 0 13715.95 13870.15 159.33 o 2 1 0 14323.47 14637.57 171.54 o 3 1 0 20.98 34.85 1.41 o 4 1 0 485.43 513.34 6.16 o 5 1 0 5154.08 5189.73 55.27 o 6 1 0 423.42 427.27 6.67 o 7 1 0 174.04 170.95 4.50 o 8 1 0 31.42 30.50 2.51 o 9 1 0 588.62 544.26 8.42 o 10 1 0 600.89 585.94 14.28 o 11 1 0 151.72 137.27 9.22 o 12 1 0 389.39 377.66 11.60 o 13 1 0 545.57 537.01 17.38 o 14 1 0 78.79 78.93 8.64 o 0 2 0 30279.38 30916.97 1052.46 o 1 2 0 2433.38 2537.92 56.41 o 2 2 0 11675.41 11911.22 136.48 o 3 2 0 869.67 946.58 10.71 o 4 2 0 3705.94 3497.88 39.51 o 5 2 0 61.64 73.24 2.57 o 6 2 0 1108.24 1097.68 13.09 o 7 2 0 310.66 303.60 5.35 o 8 2 0 2539.92 2506.10 31.09 o 9 2 0 703.41 698.61 12.66 o 10 2 0 620.33 608.85 15.03 o 11 2 0 139.50 128.50 7.17 o 12 2 0 602.36 607.14 17.05 o 13 2 0 227.34 243.95 13.38 o 1 3 0 2178.07 2092.11 44.66 o 2 3 0 2635.45 2914.55 100.82 o 3 3 0 3264.47 3277.72 39.09 o 4 3 0 1932.50 2053.29 24.57 o 5 3 0 3457.97 3351.53 38.72 o 6 3 0 117.30 111.91 3.11 o 7 3 0 1328.73 1311.04 15.87 o 8 3 0 242.67 236.71 6.72 o 9 3 0 1429.55 1423.92 28.82 o 10 3 0 355.93 336.19 10.42 o 11 3 0 446.07 441.11 12.47 o 12 3 0 222.60 215.60 9.23 o 13 3 0 214.91 223.88 11.13 o 0 4 0 3487.84 3262.44 117.80 o 1 4 0 1665.71 1755.93 37.55 o 2 4 0 2839.05 3248.01 83.29 o 3 4 0 2329.40 2427.65 101.47 o 4 4 0 4927.32 5098.89 57.96 o 5 4 0 198.72 198.57 4.09 o 6 4 0 27.41 25.09 1.96 o 7 4 0 373.13 349.19 6.73 o 8 4 0 1683.02 1673.94 34.29 o 9 4 0 739.59 729.02 16.58 o 10 4 0 386.11 363.22 10.85 o 11 4 0 425.53 430.49 12.46 o 12 4 0 359.39 381.90 13.53 o 13 4 0 141.62 126.79 10.59 o 1 5 0 1065.13 1048.01 23.82 o 2 5 0 2597.92 2755.51 70.58 o 3 5 0 421.72 433.73 14.46 o 4 5 0 445.08 457.86 15.33 o 5 5 0 441.83 453.66 9.70 o 6 5 0 104.23 89.27 4.68 o 7 5 0 398.16 410.59 7.63 o 8 5 0 619.40 578.01 13.20 o 9 5 0 642.65 656.41 15.31 o 10 5 0 190.39 197.01 8.13 o 11 5 0 75.92 69.32 6.77 o 12 5 0 41.17 57.65 7.76 o 0 6 0 564.86 544.07 24.46 o 1 6 0 74.39 69.32 6.35 o 2 6 0 42.47 47.95 7.74 o 3 6 0 1380.08 1407.34 38.99 o 4 6 0 681.43 695.35 20.98 o 5 6 0 11.95 12.56 5.39 o 6 6 0 142.56 141.98 10.23 o 7 6 0 284.61 304.05 9.12 o 8 6 0 809.06 840.52 15.85 o 9 6 0 146.07 136.03 7.06 o 10 6 0 155.39 154.61 9.98 o 11 6 0 323.39 344.84 13.77 o 1 7 0 652.27 660.87 27.95 o 2 7 0 752.69 757.84 24.35 o 3 7 0 1036.93 1049.07 31.04 o 4 7 0 376.88 392.23 15.33 o 5 7 0 176.27 178.33 10.92 o 6 7 0 533.77 546.17 18.67 o 7 7 0 132.43 152.24 16.47 o 8 7 0 363.99 345.91 23.96 o 1 8 0 792.95 798.14 34.94 o 2 8 0 231.46 211.64 16.47 o 3 8 0 422.60 423.54 16.54 o 4 8 0 1332.97 1329.13 38.81 o 5 8 0 136.11 148.75 15.97 o 6 8 0 118.64 121.79 14.97 o 7 8 0 661.09 700.81 34.94 o 4 9 0 3.95 0.50 10.48 o 5 9 0 307.94 317.46 22.46 o -5 -9 1 178.37 169.71 18.47 o -4 -9 1 393.00 342.42 23.46 o -3 -9 1 683.07 666.23 23.99 o -2 -9 1 178.64 174.59 18.47 o -1 -9 1 32.30 28.72 7.74 o 0 -9 1 291.20 315.11 12.10 o 1 -9 1 257.57 244.84 13.41 o 2 -9 1 989.65 973.34 43.93 o 3 -9 1 77.77 71.38 13.48 o 4 -9 1 44.17 46.42 13.48 o 5 -9 1 81.74 104.82 15.97 o -8 -8 1 685.11 680.39 19.33 o -7 -8 1 35.65 46.31 5.37 o -6 -8 1 64.08 70.36 5.09 o -5 -8 1 293.07 306.98 21.96 o -4 -8 1 1065.76 1087.57 35.44 o -3 -8 1 68.32 58.59 9.98 o -2 -8 1 918.28 888.61 22.93 o -1 -8 1 638.28 621.62 31.25 o 0 -8 1 262.40 246.40 10.08 o 1 -8 1 99.52 111.49 7.39 o 2 -8 1 1091.46 1053.24 26.80 o 3 -8 1 703.13 721.51 24.18 o 4 -8 1 214.28 205.33 11.98 o 5 -8 1 22.81 29.49 8.98 o 6 -8 1 257.14 254.97 8.35 o 7 -8 1 513.15 537.30 13.96 o 8 -8 1 239.41 222.95 10.16 o -10 -7 1 214.77 234.15 18.47 o -9 -7 1 125.13 104.87 9.58 o -8 -7 1 31.13 18.09 5.44 o -7 -7 1 1427.46 1435.80 29.81 o -6 -7 1 1118.41 1057.95 22.03 o -5 -7 1 580.16 574.77 20.11 o -4 -7 1 469.91 455.96 16.90 o -3 -7 1 2324.29 2331.51 34.89 o -2 -7 1 156.25 159.13 3.99 o -1 -7 1 101.58 110.95 4.76 o 0 -7 1 132.40 125.53 7.30 o 1 -7 1 1650.37 1581.05 36.69 o 2 -7 1 548.50 538.04 9.30 o 3 -7 1 0.71 0.68 2.18 o 4 -7 1 606.64 630.03 21.52 o 5 -7 1 380.10 388.68 16.19 o 6 -7 1 90.56 75.39 6.84 o 7 -7 1 174.19 165.04 7.24 o 8 -7 1 974.54 963.97 21.64 o 9 -7 1 776.70 780.61 23.25 o -11 -6 1 260.66 255.27 11.90 o -10 -6 1 211.62 202.73 10.27 o -9 -6 1 266.87 275.60 10.97 o -8 -6 1 1164.83 1165.86 25.27 o -7 -6 1 133.18 124.50 5.93 o -6 -6 1 63.81 55.99 3.87 o -5 -6 1 899.65 914.70 16.75 o -4 -6 1 1373.93 1382.55 21.65 o -3 -6 1 97.81 94.40 3.53 o -2 -6 1 207.82 203.95 4.42 o -1 -6 1 54.57 51.46 3.52 o 0 -6 1 443.93 391.97 20.96 o 1 -6 1 56.78 57.33 2.97 o 2 -6 1 990.91 1035.71 16.03 o 3 -6 1 475.13 476.23 8.47 o 4 -6 1 2214.46 2267.10 33.69 o 5 -6 1 71.45 75.97 3.33 o 6 -6 1 732.08 731.30 16.22 o 7 -6 1 140.68 144.83 6.61 o 8 -6 1 833.12 821.29 19.08 o 9 -6 1 472.64 454.62 12.62 o 10 -6 1 621.29 614.03 24.22 o 11 -6 1 90.56 88.64 10.05 o -12 -5 1 224.45 232.76 14.00 o -11 -5 1 180.89 199.58 10.57 o -10 -5 1 246.97 248.98 10.71 o -9 -5 1 387.25 384.96 12.81 o -8 -5 1 201.10 177.42 8.75 o -7 -5 1 88.98 84.66 4.11 o -6 -5 1 719.37 729.04 11.20 o -5 -5 1 480.85 478.53 7.40 o -4 -5 1 320.86 330.53 6.75 o -3 -5 1 2979.95 3033.61 44.78 o -2 -5 1 185.33 175.54 3.58 o -1 -5 1 206.44 211.30 5.71 o 0 -5 1 93.69 80.12 4.96 o 1 -5 1 2357.29 2308.60 41.72 o 2 -5 1 304.08 323.91 5.81 o 3 -5 1 173.12 178.13 4.40 o 4 -5 1 2676.05 2819.89 41.61 o 5 -5 1 679.31 686.38 9.47 o 6 -5 1 264.18 261.24 5.47 o 7 -5 1 466.03 492.17 9.97 o 8 -5 1 40.57 41.61 4.52 o 9 -5 1 1032.37 1075.74 27.18 o 10 -5 1 139.05 136.10 8.53 o 11 -5 1 276.29 276.15 12.12 o 12 -5 1 216.80 251.07 15.20 o -13 -4 1 54.24 48.30 9.23 o -12 -4 1 415.59 414.80 14.26 o -11 -4 1 27.56 30.58 6.28 o -10 -4 1 69.43 68.74 6.67 o -9 -4 1 168.37 157.67 6.59 o -8 -4 1 1039.24 1033.63 19.89 o -7 -4 1 134.96 133.00 4.25 o -6 -4 1 586.82 587.54 8.84 o -5 -4 1 352.93 345.85 5.28 o -4 -4 1 1943.37 1919.52 25.59 o -3 -4 1 1067.76 1122.17 17.08 o -2 -4 1 1821.78 1881.40 26.04 o -1 -4 1 1041.38 1073.80 18.19 o 0 -4 1 4810.03 5222.67 129.87 o 1 -4 1 98.01 120.04 3.29 o 2 -4 1 10347.08 10728.88 135.73 o 3 -4 1 2135.18 2166.87 29.90 o 4 -4 1 14053.20 14642.39 198.81 o 5 -4 1 162.73 186.89 3.47 o 6 -4 1 1129.71 1105.39 16.03 o 7 -4 1 169.11 167.74 4.57 o 8 -4 1 65.95 67.00 4.03 o 9 -4 1 20.37 21.64 3.97 o 10 -4 1 723.16 735.60 20.65 o 11 -4 1 2.44 -1.67 5.19 o 12 -4 1 25.99 29.45 8.03 o -13 -3 1 69.53 81.45 10.48 o -12 -3 1 61.03 58.25 6.98 o -11 -3 1 348.91 343.46 10.91 o -10 -3 1 432.90 421.89 10.64 o -9 -3 1 474.55 481.28 11.11 o -8 -3 1 773.59 787.93 12.06 o -7 -3 1 2416.61 2345.65 28.60 o -6 -3 1 462.58 451.51 6.88 o -5 -3 1 80.55 78.72 2.50 o -4 -3 1 230.09 252.66 3.72 o -3 -3 1 4733.49 4671.29 56.27 o -2 -3 1 432.31 397.44 6.65 o -1 -3 1 170.43 172.78 4.14 o 0 -3 1 272.54 282.26 9.48 o 1 -3 1 3759.14 3683.74 54.11 o 2 -3 1 8999.63 9635.74 128.08 o 3 -3 1 133.84 145.88 2.99 o 4 -3 1 9539.71 10342.15 108.26 o 5 -3 1 10707.35 10966.11 120.91 o 6 -3 1 173.77 181.29 3.81 o 7 -3 1 382.96 361.69 6.12 o 8 -3 1 846.93 835.16 13.53 o 9 -3 1 438.05 454.35 10.84 o 10 -3 1 146.12 148.59 6.58 o 11 -3 1 1066.08 1083.16 24.21 o 12 -3 1 33.38 23.14 6.30 o 13 -3 1 521.17 534.24 20.63 o -13 -2 1 39.21 44.95 8.51 o -12 -2 1 1240.68 1211.53 31.07 o -11 -2 1 309.65 307.90 9.28 o -10 -2 1 98.49 97.06 4.97 o -9 -2 1 357.98 355.63 6.76 o -8 -2 1 945.53 926.38 12.59 o -7 -2 1 344.19 343.64 6.13 o -6 -2 1 2516.65 2598.96 33.01 o -5 -2 1 150.13 170.60 3.50 o -4 -2 1 2555.68 2523.98 26.94 o -3 -2 1 615.41 661.05 7.78 o -2 -2 1 56.45 61.72 2.05 o -1 -2 1 231.60 262.64 3.88 o 0 -2 1 15671.45 16331.43 433.95 o 1 -2 1 8141.33 8658.91 108.71 o 2 -2 1 12779.56 13638.28 162.53 o 3 -2 1 90.46 95.72 2.12 o 4 -2 1 1701.99 1741.18 19.55 o 5 -2 1 989.52 1082.27 12.55 o 6 -2 1 4684.29 4621.71 54.11 o 7 -2 1 539.38 563.17 8.61 o 8 -2 1 52.47 47.28 2.85 o 9 -2 1 1019.26 1037.61 14.32 o 10 -2 1 1208.51 1254.55 21.96 o 11 -2 1 293.48 311.79 9.00 o 12 -2 1 279.08 267.52 11.73 o 13 -2 1 17.76 20.85 7.80 o -14 -1 1 20.04 31.45 13.48 o -13 -1 1 415.75 417.79 25.46 o -12 -1 1 484.62 492.33 15.63 o -11 -1 1 2133.94 2129.40 31.57 o -10 -1 1 11.97 6.36 2.80 o -9 -1 1 198.00 182.22 4.81 o -8 -1 1 727.82 775.44 11.68 o -7 -1 1 6089.82 6095.13 72.97 o -6 -1 1 798.20 894.44 12.83 o -5 -1 1 75.57 60.35 2.26 o -4 -1 1 972.55 1005.46 12.56 o -3 -1 1 822.70 776.25 8.46 o -2 -1 1 1136.18 1249.81 13.55 o -1 -1 1 373.91 380.35 4.75 o 0 -1 1 372.05 357.76 5.14 o 1 -1 1 22624.05 23815.86 253.17 o 2 -1 1 41655.11 42868.13 427.50 o 3 -1 1 177.64 187.55 3.01 o 4 -1 1 1632.24 1753.79 20.02 o 5 -1 1 5862.53 5921.62 67.91 o 6 -1 1 587.96 624.55 9.09 o 7 -1 1 640.37 655.13 9.52 o 8 -1 1 143.26 129.17 3.99 o 9 -1 1 1337.44 1325.22 17.70 o 10 -1 1 1025.66 1055.22 14.89 o 11 -1 1 488.75 508.03 10.69 o 12 -1 1 20.76 18.84 5.58 o 13 -1 1 420.45 393.83 24.96 o 14 -1 1 126.18 157.73 18.47 o -14 0 1 0.05 -3.06 8.29 o -13 0 1 338.35 369.81 14.50 o -12 0 1 722.89 722.81 17.90 o -11 0 1 82.45 76.05 5.27 o -10 0 1 1160.48 1157.61 16.30 o -9 0 1 277.12 264.87 5.78 o -8 0 1 1796.90 1660.07 21.63 o -7 0 1 621.64 681.30 9.87 o -6 0 1 3.57 -1.74 1.74 o -5 0 1 695.99 782.77 10.00 o -4 0 1 1069.79 991.04 12.08 o -3 0 1 282.32 253.12 3.66 o -2 0 1 5282.65 5498.57 55.29 o -1 0 1 494.51 421.98 10.27 o 1 0 1 518.02 458.58 4.71 o 2 0 1 11919.11 11794.67 111.05 o 3 0 1 61.62 43.86 1.72 o 4 0 1 3204.76 2974.77 34.46 o 5 0 1 130.76 132.68 3.17 o 6 0 1 4844.77 4852.28 59.11 o 7 0 1 21.56 16.88 2.06 o 8 0 1 935.69 927.07 12.95 o 9 0 1 511.96 522.63 8.50 o 10 0 1 168.56 152.29 4.86 o 11 0 1 123.51 107.91 5.84 o 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