#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236910.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236910_Fobs loop_ _publ_author_name 'Selvakumaran, N.' 'Sheeba, M. Mary' 'Karvembu, R.' 'Ng, Seik Weng' 'Tiekink, Edward R. T.' _publ_section_title ; 1-Benzoyl-3-(4-chlorophenyl)thiourea dichloromethane hemisolvate ; _journal_coeditor_code HG5268 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3313 _journal_volume 68 _journal_year 2012 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 117.690 _cell_angle_gamma 90.000 _cell_length_a 20.0800 _cell_length_b 16.0136 _cell_length_c 10.3752 _exptl_crystal_F_000 1368.00 _reflns_d_resolution_high 0.8004 _[local]_cod_data_source_file hg5268Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 268.43 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 539.35 375.83 10.58 o 4 0 0 1195.25 1014.98 12.88 o 6 0 0 3304.26 3702.32 30.95 o 8 0 0 3347.25 2730.87 50.49 o 10 0 0 16783.28 16090.38 130.76 o 12 0 0 10982.28 11194.30 126.05 o 14 0 0 29652.70 30782.79 413.59 o 16 0 0 919.36 984.25 47.59 o 18 0 0 1271.81 1415.88 37.73 o 20 0 0 5136.35 5300.10 83.62 o 1 1 0 2014.49 2428.01 13.91 o 3 1 0 5992.11 5695.94 61.46 o 5 1 0 3.00 47.33 2.67 o 7 1 0 3446.66 2774.09 21.95 o 9 1 0 4408.46 3944.27 53.98 o 11 1 0 2740.10 2918.32 42.50 o 13 1 0 394.81 364.92 17.74 o 15 1 0 632.13 615.57 20.65 o 17 1 0 812.27 849.99 30.98 o 19 1 0 96.89 95.34 9.39 o 21 1 0 916.24 918.48 20.25 o 0 2 0 1766.82 2106.17 14.18 o 2 2 0 10300.17 10367.79 33.19 o 4 2 0 38875.75 38170.91 476.99 o 6 2 0 58282.23 55131.07 155.07 o 8 2 0 12130.77 11772.85 54.44 o 10 2 0 17976.79 19024.79 108.75 o 12 2 0 7648.69 8156.10 75.47 o 14 2 0 985.67 1067.77 28.61 o 16 2 0 3399.51 3397.49 75.98 o 18 2 0 9.92 23.80 5.84 o 20 2 0 95.08 121.49 9.90 o 1 3 0 33201.38 29450.32 64.62 o 3 3 0 24875.97 24718.11 160.21 o 5 3 0 26.57 188.28 8.20 o 7 3 0 12532.90 11027.78 58.07 o 9 3 0 1387.33 1339.14 19.89 o 11 3 0 992.18 1101.93 26.39 o 13 3 0 95.32 121.67 5.95 o 15 3 0 5337.80 5412.07 50.67 o 17 3 0 5980.36 6171.34 75.60 o 19 3 0 577.40 603.57 17.51 o 21 3 0 2160.38 2130.09 47.01 o 0 4 0 70793.98 66697.77 158.00 o 2 4 0 770.79 648.69 9.59 o 4 4 0 26396.69 25060.37 72.81 o 6 4 0 651.53 859.72 27.08 o 8 4 0 2555.90 2266.33 32.61 o 10 4 0 1333.31 1003.03 24.12 o 12 4 0 36.79 16.54 3.59 o 14 4 0 7134.49 7173.29 59.13 o 16 4 0 2580.03 2653.04 51.25 o 18 4 0 183.12 174.64 18.95 o 20 4 0 1532.94 1497.14 45.62 o 1 5 0 22212.87 20179.34 88.79 o 3 5 0 1729.22 1621.93 17.14 o 5 5 0 2272.38 2766.42 23.60 o 7 5 0 246.36 375.37 27.54 o 9 5 0 19849.02 19267.86 84.91 o 11 5 0 3348.85 3499.33 51.92 o 13 5 0 14520.32 14759.05 83.24 o 15 5 0 480.22 451.41 21.98 o 17 5 0 396.49 417.11 19.83 o 19 5 0 5528.83 5667.78 72.81 o 21 5 0 29.27 43.43 7.05 o 0 6 0 115.95 145.26 9.65 o 2 6 0 26791.08 27125.43 76.41 o 4 6 0 52.50 60.77 3.90 o 6 6 0 12741.08 11311.12 77.83 o 8 6 0 19459.76 18903.07 124.17 o 10 6 0 1146.53 1346.09 32.19 o 12 6 0 846.25 1001.40 21.73 o 14 6 0 171.39 213.22 15.68 o 16 6 0 3649.62 3620.69 66.76 o 18 6 0 1810.84 1766.12 35.98 o 20 6 0 1655.92 1725.97 44.93 o 1 7 0 8005.14 9035.06 55.86 o 3 7 0 5437.64 5184.78 36.41 o 5 7 0 4558.06 4418.24 52.83 o 7 7 0 12699.96 11851.23 88.49 o 9 7 0 3393.25 3900.05 65.13 o 11 7 0 434.65 455.59 17.33 o 13 7 0 4517.61 4465.85 47.53 o 15 7 0 1423.85 1368.20 37.96 o 17 7 0 100.12 91.39 9.39 o 19 7 0 5727.01 5602.60 193.42 o 0 8 0 1806.62 1291.21 32.47 o 2 8 0 11673.13 12625.69 85.07 o 4 8 0 2572.94 2645.35 54.39 o 6 8 0 770.40 555.78 19.70 o 8 8 0 1967.77 1769.51 37.28 o 10 8 0 1533.97 1436.45 30.69 o 12 8 0 3006.03 3090.84 46.46 o 14 8 0 1185.33 1198.16 54.44 o 16 8 0 1035.83 1024.24 45.67 o 18 8 0 145.02 145.86 14.30 o 20 8 0 506.06 473.94 18.59 o 1 9 0 21468.23 22377.61 143.20 o 3 9 0 5043.26 4841.16 76.18 o 5 9 0 17.24 13.25 5.57 o 7 9 0 692.43 789.97 25.57 o 9 9 0 18111.27 18000.13 110.39 o 11 9 0 2968.91 3060.40 47.02 o 13 9 0 5789.59 5663.55 121.62 o 15 9 0 638.42 575.91 36.40 o 17 9 0 2.12 13.64 7.21 o 19 9 0 1768.36 1590.39 84.51 o 0 10 0 1517.12 2310.86 48.52 o 2 10 0 1928.50 1896.61 47.91 o 4 10 0 30.79 32.20 7.48 o 6 10 0 2504.76 2234.16 42.55 o 8 10 0 17.98 35.70 5.91 o 10 10 0 1902.93 1923.53 37.42 o 12 10 0 674.74 711.23 44.91 o 14 10 0 1796.01 1878.46 67.89 o 16 10 0 1182.00 1141.69 45.72 o 18 10 0 67.89 71.25 6.02 o 1 11 0 41.13 40.77 7.37 o 3 11 0 2617.80 2566.65 60.36 o 5 11 0 2593.72 2399.88 35.04 o 7 11 0 10284.77 9630.13 142.44 o 9 11 0 1474.81 1504.59 109.53 o 11 11 0 1616.69 1633.79 69.82 o 13 11 0 224.39 218.81 24.66 o 15 11 0 905.68 869.85 42.02 o 17 11 0 685.64 702.61 29.27 o 0 12 0 23.85 14.47 6.54 o 2 12 0 999.93 991.98 22.94 o 4 12 0 0.13 6.31 3.22 o 6 12 0 4511.75 4580.78 46.31 o 8 12 0 2.34 26.99 13.67 o 10 12 0 3265.45 3381.59 101.23 o 12 12 0 191.70 194.50 24.03 o 14 12 0 25.53 36.55 10.89 o 16 12 0 1696.17 1571.77 46.40 o 1 13 0 1949.00 1980.56 43.11 o 3 13 0 168.36 200.33 21.98 o 5 13 0 35.17 42.26 5.22 o 7 13 0 2392.31 2282.28 51.55 o 9 13 0 147.94 162.04 23.98 o 11 13 0 157.92 171.80 22.69 o 13 13 0 118.51 128.28 17.98 o 15 13 0 1308.11 1289.26 43.11 o 0 14 0 3566.71 3510.05 83.38 o 2 14 0 412.82 376.26 19.48 o 4 14 0 1020.28 831.84 24.57 o 6 14 0 9.56 8.97 4.32 o 8 14 0 2864.03 2899.38 54.99 o 10 14 0 7593.19 7550.53 139.05 o 12 14 0 3063.08 3121.23 80.17 o 14 14 0 398.99 398.50 24.22 o 1 15 0 85.21 100.66 10.70 o 3 15 0 192.77 164.83 11.21 o 5 15 0 2199.65 2215.93 38.41 o 7 15 0 5951.82 5854.28 102.00 o 9 15 0 2469.59 2436.04 75.50 o 11 15 0 1205.95 1179.27 47.46 o 13 15 0 11.63 8.62 6.11 o 0 16 0 457.23 393.67 27.70 o 2 16 0 1388.44 1280.54 26.62 o 4 16 0 48.55 38.15 5.74 o 6 16 0 1021.16 883.38 21.83 o 8 16 0 1963.51 1883.08 50.58 o 10 16 0 198.55 192.86 18.17 o 12 16 0 627.92 619.91 42.91 o 1 17 0 835.43 810.31 20.29 o 3 17 0 62.34 85.02 8.77 o 5 17 0 458.52 414.89 13.98 o 7 17 0 415.11 476.58 17.57 o 9 17 0 0.44 -0.49 4.14 o 11 17 0 0.96 1.37 7.42 o 0 18 0 374.08 282.26 13.06 o 2 18 0 404.26 371.31 12.59 o 4 18 0 45.94 64.37 5.37 o 6 18 0 69.32 52.40 8.45 o 8 18 0 1390.75 1304.60 34.01 o 1 19 0 1544.59 1617.94 37.45 o 3 19 0 91.12 87.58 5.33 o 5 19 0 10.56 8.61 4.12 o -21 1 1 1120.10 1128.17 25.63 o -19 1 1 3451.39 3534.81 51.45 o -17 1 1 145.36 173.58 23.16 o -15 1 1 1242.38 1211.76 27.83 o -13 1 1 545.72 497.26 30.00 o -11 1 1 49.61 100.44 6.67 o -9 1 1 3890.55 3762.61 31.57 o -7 1 1 8953.58 9458.42 51.55 o -5 1 1 2126.11 2173.95 16.41 o -3 1 1 7.53 23.62 5.43 o -1 1 1 4286.44 4082.91 10.39 o 1 1 1 1232.39 1167.57 9.53 o 3 1 1 7159.42 7006.33 37.30 o 5 1 1 101.64 110.73 4.38 o 7 1 1 1788.01 2049.03 51.71 o 9 1 1 19.28 35.41 5.09 o 11 1 1 1785.36 1950.92 37.84 o 13 1 1 175.36 177.66 8.22 o 15 1 1 40.98 41.39 6.13 o 17 1 1 244.95 259.39 16.24 o 19 1 1 0.37 1.31 3.44 o -22 2 1 110.67 90.47 9.67 o -20 2 1 606.88 597.71 21.01 o -18 2 1 1618.83 1746.69 43.66 o -16 2 1 263.58 298.53 18.55 o -14 2 1 7.47 9.49 2.95 o -12 2 1 528.06 576.13 20.95 o -10 2 1 281.86 227.88 8.45 o -8 2 1 1636.17 1777.02 17.88 o -6 2 1 7032.74 7181.86 33.85 o -4 2 1 2666.82 2580.24 18.52 o -2 2 1 6942.28 6081.04 29.55 o 0 2 1 1711.25 1418.38 12.46 o 2 2 1 2110.67 2096.74 15.98 o 4 2 1 872.34 793.06 11.40 o 6 2 1 56.43 78.32 4.09 o 8 2 1 8.47 19.43 3.93 o 10 2 1 715.73 747.41 17.61 o 12 2 1 43.31 80.41 5.60 o 14 2 1 43.55 50.86 4.40 o 16 2 1 1268.88 1292.37 36.22 o 18 2 1 295.45 317.55 16.32 o 20 2 1 66.03 67.78 9.38 o -21 3 1 158.26 154.10 14.99 o -19 3 1 2664.99 2800.27 74.90 o -17 3 1 1579.42 1669.98 42.95 o -15 3 1 3837.47 4007.86 64.96 o -13 3 1 97.99 91.22 12.42 o -11 3 1 874.08 871.15 17.44 o -9 3 1 195.92 172.17 7.03 o -7 3 1 3011.88 3067.85 29.25 o -5 3 1 52771.89 50181.86 138.33 o -3 3 1 2.13 7.39 2.61 o -1 3 1 8128.62 7376.51 55.69 o 1 3 1 1680.11 1492.98 17.52 o 3 3 1 1458.21 1306.52 14.91 o 5 3 1 119.83 109.85 3.85 o 7 3 1 2024.03 2189.62 37.14 o 9 3 1 4814.36 5190.42 60.73 o 11 3 1 452.03 481.95 18.24 o 13 3 1 4.59 9.51 2.62 o 15 3 1 94.37 112.80 8.89 o 17 3 1 1089.52 1103.69 25.97 o 19 3 1 1521.09 1617.80 49.05 o -22 4 1 118.54 101.05 9.89 o -20 4 1 3806.21 3966.25 79.72 o -18 4 1 18.46 30.25 10.22 o -16 4 1 2375.28 2569.52 52.61 o -14 4 1 1100.26 1219.10 23.54 o -12 4 1 2480.47 2552.87 61.28 o -10 4 1 4.70 12.73 2.94 o -8 4 1 1164.17 1183.90 20.24 o -6 4 1 6319.68 6167.85 99.70 o -4 4 1 1401.08 1157.50 10.60 o -2 4 1 371.84 354.09 8.28 o 0 4 1 778.79 767.45 9.88 o 2 4 1 5921.91 5929.37 32.50 o 4 4 1 4321.21 4499.07 81.06 o 6 4 1 2476.36 2056.73 23.76 o 8 4 1 383.46 443.54 15.60 o 10 4 1 20.26 38.43 4.62 o 12 4 1 2965.16 2918.11 31.31 o 14 4 1 1524.85 1610.34 31.92 o 16 4 1 4460.45 4496.27 50.98 o 18 4 1 33.58 34.51 9.37 o 20 4 1 1197.47 1131.60 33.81 o -21 5 1 4.75 6.91 4.69 o -19 5 1 1253.49 1316.70 48.85 o -17 5 1 2563.82 2559.34 68.64 o -15 5 1 781.88 769.15 19.50 o -13 5 1 7.87 10.98 2.97 o -11 5 1 1747.67 1766.23 33.07 o -9 5 1 1487.80 1499.80 42.23 o -7 5 1 4309.82 3804.55 34.72 o -5 5 1 4314.72 4148.30 287.58 o -3 5 1 4975.81 5000.08 24.38 o -1 5 1 6195.49 5806.32 70.29 o 1 5 1 294.34 281.40 21.74 o 3 5 1 373.00 375.76 10.93 o 5 5 1 2376.27 2154.05 24.19 o 7 5 1 99.46 65.72 6.59 o 9 5 1 2295.19 2505.27 33.47 o 11 5 1 1370.62 1417.12 24.26 o 13 5 1 2842.79 2893.35 44.03 o 15 5 1 147.17 108.35 10.88 o 17 5 1 22.51 22.12 4.59 o 19 5 1 1553.83 1586.43 45.81 o -22 6 1 970.18 934.77 24.99 o -20 6 1 4055.47 3962.96 70.89 o -18 6 1 624.07 601.31 22.60 o -16 6 1 1454.37 1424.76 38.73 o -14 6 1 764.92 780.30 19.88 o -12 6 1 4128.06 4447.30 45.21 o -10 6 1 6905.12 6684.77 146.36 o -8 6 1 153.10 225.33 11.91 o -6 6 1 7251.56 7928.16 63.11 o -4 6 1 1131.58 1116.18 12.52 o -2 6 1 2945.94 3172.30 24.76 o 0 6 1 1786.96 1691.00 22.77 o 2 6 1 1749.13 1977.81 26.00 o 4 6 1 32.17 29.78 4.45 o 6 6 1 439.87 551.27 18.92 o 8 6 1 9065.81 9320.88 75.94 o 10 6 1 2521.56 2525.84 31.99 o 12 6 1 3481.62 3637.05 74.86 o 14 6 1 223.81 222.37 15.48 o 16 6 1 1027.55 991.33 29.62 o 18 6 1 112.88 144.14 10.25 o 20 6 1 1597.58 1448.01 32.58 o -21 7 1 181.44 160.92 12.52 o -19 7 1 2676.47 2590.74 60.31 o -17 7 1 964.22 911.08 29.56 o -15 7 1 23.03 33.12 7.56 o -13 7 1 1242.40 1281.01 25.74 o -11 7 1 5949.11 6084.07 61.08 o -9 7 1 421.95 420.16 17.62 o -7 7 1 5.77 14.01 3.85 o -5 7 1 24285.16 25653.15 97.62 o -3 7 1 758.10 702.92 12.53 o -1 7 1 41305.93 41666.63 315.98 o 1 7 1 977.23 1013.14 19.60 o 3 7 1 7538.45 7147.09 56.93 o 5 7 1 1867.30 1950.49 25.27 o 7 7 1 335.34 412.07 17.95 o 9 7 1 243.72 158.17 8.18 o 11 7 1 12.42 28.23 4.96 o 13 7 1 6526.36 6592.20 126.20 o 15 7 1 216.82 214.15 22.11 o 17 7 1 64.00 87.91 11.67 o 19 7 1 2129.23 2181.83 45.64 o -20 8 1 606.65 621.85 26.33 o -18 8 1 12.52 20.60 5.02 o -16 8 1 9922.76 10202.60 117.65 o -14 8 1 1101.07 1056.62 35.11 o -12 8 1 6577.67 6858.55 59.43 o -10 8 1 66.61 50.13 6.30 o -8 8 1 350.00 404.20 14.47 o -6 8 1 4004.65 3928.18 42.39 o -4 8 1 2600.75 2903.51 40.86 o -2 8 1 2400.57 2901.15 61.04 o 0 8 1 2449.70 2668.70 46.70 o 2 8 1 4487.88 4734.20 46.08 o 4 8 1 3120.84 3471.98 40.41 o 6 8 1 53.79 22.46 6.30 o 8 8 1 34.04 71.02 10.01 o 10 8 1 2310.80 2341.10 49.43 o 12 8 1 4396.55 4231.37 104.16 o 14 8 1 205.78 231.90 24.19 o 16 8 1 1972.95 2105.83 43.28 o 18 8 1 185.67 157.44 9.38 o -19 9 1 85.83 62.35 8.27 o -17 9 1 4711.91 4669.51 61.01 o -15 9 1 578.20 577.76 25.06 o -13 9 1 2226.01 2365.72 60.44 o -11 9 1 6598.27 6775.17 59.77 o -9 9 1 1002.92 991.46 24.25 o -7 9 1 10597.99 10495.20 91.23 o -5 9 1 737.90 763.12 23.17 o -3 9 1 6000.54 5965.47 85.25 o -1 9 1 1990.54 2037.95 30.58 o 1 9 1 35.74 113.71 9.03 o 3 9 1 8889.19 8573.86 102.11 o 5 9 1 7404.06 7724.54 103.88 o 7 9 1 12031.74 12382.63 108.78 o 9 9 1 5475.83 5295.36 74.36 o 11 9 1 2544.76 2555.55 82.53 o 13 9 1 3782.51 3706.69 96.55 o 15 9 1 34.40 22.38 9.13 o 17 9 1 1565.85 1673.93 41.46 o -18 10 1 295.57 277.98 18.84 o -16 10 1 11.73 9.76 7.88 o -14 10 1 149.57 147.10 20.62 o -12 10 1 33.39 73.09 17.29 o -10 10 1 683.27 685.16 19.38 o -8 10 1 224.47 238.42 15.14 o -6 10 1 191.86 177.04 12.37 o -4 10 1 51.34 49.63 9.30 o -2 10 1 17.23 22.29 6.20 o 0 10 1 5389.76 5460.80 71.66 o 2 10 1 2275.18 2236.17 67.34 o 4 10 1 417.30 429.49 24.89 o 6 10 1 721.72 689.39 31.51 o 8 10 1 2959.32 2955.16 56.16 o 10 10 1 124.57 116.92 19.62 o 12 10 1 1415.61 1476.54 62.74 o 14 10 1 489.36 488.59 33.33 o 16 10 1 262.85 284.64 17.37 o -17 11 1 237.14 210.78 18.19 o -15 11 1 248.69 237.37 23.61 o -13 11 1 1812.02 1870.07 72.36 o -11 11 1 1994.67 1941.47 78.57 o -9 11 1 2683.45 2721.06 76.30 o -7 11 1 2941.83 2892.92 49.96 o -5 11 1 2602.10 2496.65 64.09 o -3 11 1 1832.59 1904.41 52.28 o -1 11 1 16571.06 16508.58 147.13 o 1 11 1 584.29 566.96 18.26 o 3 11 1 7088.17 7344.97 140.67 o 5 11 1 41.47 43.14 7.96 o 7 11 1 3613.31 3578.36 49.10 o 9 11 1 1858.06 1821.76 72.53 o 11 11 1 841.86 838.19 48.26 o 13 11 1 3718.05 3747.20 93.72 o 15 11 1 2887.56 2727.77 67.68 o 17 11 1 22.31 8.66 4.10 o -18 12 1 22.07 22.61 4.91 o -16 12 1 353.16 366.55 24.87 o -14 12 1 4645.98 4666.99 104.44 o -12 12 1 2780.57 2723.95 89.61 o -10 12 1 634.02 676.10 47.76 o -8 12 1 349.85 319.61 15.43 o -6 12 1 41.88 54.24 6.05 o -4 12 1 825.57 927.09 27.65 o -2 12 1 325.23 319.00 16.19 o 0 12 1 150.05 122.94 15.61 o 2 12 1 339.50 376.22 15.13 o 4 12 1 699.46 689.90 17.98 o 6 12 1 1612.85 1599.22 45.02 o 8 12 1 9390.16 9307.75 164.08 o 10 12 1 655.95 664.45 43.10 o 12 12 1 138.93 144.83 20.02 o 14 12 1 139.64 128.59 16.08 o 16 12 1 26.51 47.69 7.67 o -17 13 1 2931.28 2853.15 50.98 o -15 13 1 133.94 148.93 17.01 o -13 13 1 1481.00 1512.55 60.61 o -11 13 1 7572.36 7434.34 149.60 o -9 13 1 1008.90 1260.46 65.32 o -7 13 1 13787.53 14271.86 98.22 o -5 13 1 84.31 72.49 7.07 o -3 13 1 6297.65 6294.17 76.99 o -1 13 1 991.01 1031.07 31.52 o 1 13 1 2277.80 2493.94 48.72 o 3 13 1 20883.63 21044.20 119.90 o 5 13 1 6961.39 6787.88 67.38 o 7 13 1 602.66 542.14 24.52 o 9 13 1 4962.20 5062.57 116.82 o 11 13 1 1466.06 1503.91 59.82 o 13 13 1 3120.00 3094.37 74.36 o 15 13 1 3435.63 3623.01 62.78 o -16 14 1 602.36 665.42 25.45 o -14 14 1 6.94 17.54 7.88 o -12 14 1 325.94 328.01 28.83 o -10 14 1 1748.97 1858.64 74.26 o -8 14 1 1230.04 1195.46 36.97 o -6 14 1 526.72 508.32 19.31 o -4 14 1 1814.61 1850.31 42.43 o -2 14 1 212.98 188.76 14.21 o 0 14 1 72.24 46.76 8.52 o 2 14 1 5487.94 5415.41 72.86 o 4 14 1 292.99 268.60 13.92 o 6 14 1 699.01 736.64 21.48 o 8 14 1 462.37 458.29 34.53 o 10 14 1 107.03 119.16 17.97 o 12 14 1 2427.35 2469.97 65.31 o 14 14 1 40.13 44.04 7.80 o -15 15 1 892.13 902.17 29.00 o -13 15 1 2935.92 3164.18 71.05 o -11 15 1 299.27 254.96 24.75 o -9 15 1 2578.31 2516.46 47.89 o -7 15 1 4358.92 4372.72 70.36 o -5 15 1 1723.73 1671.57 34.30 o -3 15 1 506.09 588.68 19.09 o -1 15 1 10946.46 10972.79 119.19 o 1 15 1 28.46 22.41 6.27 o 3 15 1 3036.59 3083.05 68.63 o 5 15 1 250.92 264.58 12.99 o 7 15 1 267.80 234.23 14.93 o 9 15 1 7599.48 7602.02 122.28 o 11 15 1 1400.97 1345.32 42.45 o 13 15 1 983.05 1044.31 31.82 o -14 16 1 1027.94 1056.85 28.81 o -12 16 1 811.09 829.61 34.04 o -10 16 1 4083.56 4276.50 89.50 o -8 16 1 9.04 12.84 7.40 o -6 16 1 237.48 239.26 12.19 o -4 16 1 488.38 610.77 20.11 o -2 16 1 12.61 10.40 3.78 o 0 16 1 3926.33 4191.39 62.45 o 2 16 1 420.15 367.92 18.50 o 4 16 1 16.73 59.36 10.81 o 6 16 1 2833.56 3012.86 67.51 o 8 16 1 612.37 633.68 32.18 o 10 16 1 2322.64 2323.05 35.88 o 12 16 1 1088.66 1061.12 28.45 o -11 17 1 430.80 431.13 21.71 o -9 17 1 16.08 22.75 7.87 o -7 17 1 2912.34 3096.34 47.50 o -5 17 1 400.66 354.31 13.60 o -3 17 1 901.50 889.25 20.55 o -1 17 1 13.89 8.84 3.48 o 1 17 1 688.67 739.08 19.80 o 3 17 1 2106.07 2117.66 39.15 o 5 17 1 667.22 653.33 19.45 o 7 17 1 47.34 35.93 5.28 o 9 17 1 224.17 213.72 9.90 o -10 18 1 1510.01 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