#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181291 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236929.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236929_Fobs loop_ _publ_author_name 'Thanigaimani, Kaliyaperumal' 'Khalib, Nuridayanti Che' 'Arshad, Suhana' 'Razak, Ibrahim Abdul' _publ_section_title ; 4-Chloro-6-methoxypyrimidin-2-amine--succinic acid (2/1) ; _journal_coeditor_code IS5213 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3343 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 82.337 _cell_angle_beta 88.952 _cell_angle_gamma 86.904 _cell_length_a 5.0094 _cell_length_b 8.5459 _cell_length_c 10.8736 _exptl_crystal_F_000 226.00 _reflns_d_resolution_high 0.7965 _cod_data_source_file is5213Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_kty87_0m in P-1 (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 149.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 545.66 559.28 10.09 o 2 0 0 140.26 131.84 1.56 o 3 0 0 64.37 69.40 0.98 o 4 0 0 9.53 10.40 0.41 o 5 0 0 236.01 233.04 2.53 o 6 0 0 98.84 98.69 1.36 o -6 1 0 0.43 0.36 0.20 o -5 1 0 5.78 4.84 0.32 o -4 1 0 31.51 30.24 0.51 o -3 1 0 1041.53 1107.08 11.74 o -2 1 0 3168.95 3272.44 41.76 o -1 1 0 3.70 3.50 0.17 o 0 1 0 311.20 346.38 7.90 o 1 1 0 159.98 161.29 1.90 o 2 1 0 33.13 36.89 0.67 o 3 1 0 248.29 243.19 2.57 o 4 1 0 18.98 18.51 0.40 o 5 1 0 174.82 171.42 1.83 o 6 1 0 1.25 1.49 0.29 o -6 2 0 10.81 9.24 0.42 o -5 2 0 5.25 3.35 0.25 o -4 2 0 140.85 142.99 1.75 o -3 2 0 11.24 19.18 0.55 o -2 2 0 128.11 121.27 1.25 o -1 2 0 31.70 35.12 1.11 o 0 2 0 120.83 108.79 2.62 o 1 2 0 1160.84 1190.12 19.05 o 2 2 0 999.49 919.79 7.29 o 3 2 0 84.13 81.16 0.81 o 4 2 0 135.64 127.49 1.24 o 5 2 0 4.18 4.50 0.26 o 6 2 0 445.66 450.08 4.35 o -5 3 0 206.39 196.20 2.40 o -4 3 0 256.93 254.24 2.91 o -2 3 0 525.85 621.92 6.54 o 0 3 0 648.05 629.86 11.95 o 1 3 0 432.86 429.34 4.14 o 2 3 0 22.12 16.47 0.33 o 3 3 0 209.89 210.00 1.69 o 4 3 0 276.57 283.96 2.49 o 5 3 0 129.19 131.07 1.34 o 6 3 0 101.40 101.82 1.31 o -5 4 0 62.45 53.09 1.07 o -4 4 0 1.22 0.43 0.13 o -3 4 0 6.76 7.14 0.62 o -2 4 0 394.93 425.95 4.58 o -1 4 0 82.60 81.27 1.22 o 0 4 0 326.91 307.04 3.81 o 1 4 0 20.40 22.05 0.36 o 2 4 0 95.13 81.70 0.83 o 3 4 0 252.91 252.94 2.27 o 4 4 0 125.76 125.38 1.24 o 5 4 0 67.81 68.60 0.84 o -5 5 0 2.70 2.59 0.27 o -4 5 0 29.52 29.14 0.59 o -3 5 0 267.99 252.14 3.31 o -2 5 0 0.10 0.55 0.17 o -1 5 0 105.70 109.62 1.61 o 0 5 0 129.91 122.28 1.49 o 1 5 0 0.32 0.62 0.08 o 2 5 0 0.02 0.10 0.05 o 3 5 0 75.21 73.54 0.77 o 4 5 0 15.97 17.33 0.35 o 5 5 0 2.37 1.90 0.20 o -5 6 0 1.27 1.10 0.21 o -4 6 0 191.62 179.36 2.22 o -3 6 0 22.68 19.79 0.53 o -2 6 0 294.93 295.06 4.59 o -1 6 0 0.54 0.42 0.24 o 0 6 0 15.35 15.87 0.37 o 1 6 0 840.82 887.56 7.58 o 2 6 0 566.33 586.13 5.10 o 3 6 0 15.83 16.22 0.37 o 4 6 0 61.51 59.77 0.91 o 5 6 0 5.57 5.50 0.48 o -4 7 0 97.28 89.90 1.33 o -3 7 0 1.16 2.17 0.25 o -2 7 0 23.20 24.82 0.62 o -1 7 0 2538.03 2588.94 26.25 o 0 7 0 137.23 135.59 1.50 o 1 7 0 73.29 68.17 0.89 o 2 7 0 4.95 5.13 0.21 o 3 7 0 73.34 74.27 1.21 o 4 7 0 43.92 41.77 0.84 o -3 8 0 237.06 252.53 3.48 o -2 8 0 1.48 1.82 0.24 o -1 8 0 29.06 30.95 1.19 o 0 8 0 113.83 108.11 1.17 o 1 8 0 1.55 1.86 0.18 o 2 8 0 0.35 -0.01 0.14 o 3 8 0 20.67 21.09 0.75 o 4 8 0 64.76 65.49 1.88 o -3 9 0 56.05 56.48 1.17 o -2 9 0 134.84 134.14 2.10 o -1 9 0 103.49 104.75 2.01 o 0 9 0 272.35 277.25 3.09 o 1 9 0 46.99 48.05 0.77 o 2 9 0 27.94 28.36 0.92 o 3 9 0 91.53 94.21 1.52 o -1 10 0 39.97 40.02 1.13 o 0 10 0 25.02 25.65 0.69 o 1 10 0 8.68 9.35 0.47 o 2 10 0 92.61 96.28 2.08 o -2 -10 1 109.19 108.55 2.27 o -1 -10 1 33.68 34.94 0.74 o 0 -10 1 5.18 4.03 0.37 o 1 -10 1 56.99 54.78 1.35 o -3 -9 1 10.11 10.79 0.66 o -2 -9 1 4.79 5.59 0.64 o -1 -9 1 8.42 8.70 0.39 o 0 -9 1 40.22 41.15 0.88 o 1 -9 1 194.25 194.43 2.64 o 2 -9 1 0.36 0.15 0.22 o -4 -8 1 0.23 0.24 0.51 o -3 -8 1 27.33 28.34 0.67 o -2 -8 1 34.53 38.13 1.01 o -1 -8 1 25.66 25.86 0.58 o 0 -8 1 3.83 3.51 0.32 o 1 -8 1 7.87 8.07 0.41 o 2 -8 1 163.43 158.74 2.31 o 3 -8 1 27.92 28.93 0.74 o -4 -7 1 2.63 3.09 0.28 o -3 -7 1 130.00 123.91 1.81 o -2 -7 1 3.25 2.99 0.18 o -1 -7 1 477.02 487.98 4.68 o 0 -7 1 48.79 50.61 0.82 o 1 -7 1 69.14 73.00 1.20 o 2 -7 1 32.44 34.03 0.61 o 3 -7 1 121.50 135.13 2.00 o 4 -7 1 72.90 80.52 1.20 o -5 -6 1 23.35 23.74 0.86 o -4 -6 1 17.55 17.74 0.52 o -3 -6 1 178.42 173.43 2.36 o -2 -6 1 65.79 62.36 0.68 o -1 -6 1 161.37 161.50 1.61 o 0 -6 1 98.40 94.96 1.22 o 1 -6 1 446.19 433.02 7.07 o 2 -6 1 597.21 585.84 7.21 o 3 -6 1 11.84 16.08 0.56 o 4 -6 1 92.71 98.58 1.35 o -5 -5 1 107.96 112.45 1.58 o -4 -5 1 67.82 66.17 0.80 o -3 -5 1 23.61 23.71 0.39 o -2 -5 1 63.71 70.93 0.67 o -1 -5 1 963.16 948.27 7.97 o 0 -5 1 114.73 101.12 1.37 o 1 -5 1 699.05 736.55 12.05 o 2 -5 1 104.79 103.24 3.59 o 3 -5 1 247.48 253.41 3.29 o 4 -5 1 8.85 8.55 0.32 o 5 -5 1 1.67 1.02 0.20 o -5 -4 1 73.10 69.01 0.84 o -4 -4 1 41.24 44.22 0.52 o -3 -4 1 51.59 46.72 0.54 o -2 -4 1 35.49 39.22 0.69 o -1 -4 1 183.64 174.14 1.47 o 0 -4 1 290.57 282.94 3.54 o 1 -4 1 267.95 274.17 2.63 o 2 -4 1 76.09 83.99 1.25 o 3 -4 1 20.80 20.65 0.45 o 4 -4 1 132.19 114.95 1.46 o 5 -4 1 58.42 59.20 0.94 o -6 -3 1 37.19 36.80 0.61 o -5 -3 1 43.89 44.74 0.63 o -4 -3 1 16.03 15.46 0.32 o -3 -3 1 552.36 536.04 3.86 o -2 -3 1 116.35 103.77 0.96 o -1 -3 1 677.87 653.90 8.16 o 0 -3 1 133.32 123.42 3.43 o 1 -3 1 1638.77 1747.55 25.18 o 2 -3 1 0.06 1.36 0.15 o 3 -3 1 208.49 196.22 3.93 o 4 -3 1 246.57 232.29 2.66 o 5 -3 1 191.45 183.95 2.25 o -6 -2 1 21.29 21.35 0.84 o -5 -2 1 115.26 118.89 1.24 o -4 -2 1 112.41 109.86 1.10 o -3 -2 1 18.02 12.72 0.21 o -2 -2 1 437.99 471.69 4.17 o -1 -2 1 3241.10 3284.43 40.84 o 0 -2 1 2.37 3.49 0.21 o 1 -2 1 29.00 37.37 0.88 o 2 -2 1 612.94 652.06 7.09 o 3 -2 1 254.30 251.24 3.20 o 4 -2 1 76.52 78.24 1.05 o 5 -2 1 3.05 2.89 0.22 o 6 -2 1 4.16 2.93 0.27 o -6 -1 1 45.45 43.13 0.81 o -5 -1 1 18.30 18.49 0.51 o -4 -1 1 182.22 184.02 1.79 o -3 -1 1 6.85 7.78 0.22 o -2 -1 1 36.14 40.68 0.86 o -1 -1 1 501.25 470.69 5.94 o 0 -1 1 262.22 258.33 4.01 o 1 -1 1 4465.47 4566.22 58.42 o 2 -1 1 294.76 360.42 3.54 o 3 -1 1 185.61 196.07 2.17 o 4 -1 1 0.05 0.01 0.09 o 5 -1 1 0.01 0.14 0.26 o 6 -1 1 114.38 113.07 1.59 o -6 0 1 2.88 2.43 0.28 o -5 0 1 7.04 7.03 0.31 o -4 0 1 54.62 59.55 0.85 o -3 0 1 53.88 59.14 0.75 o -2 0 1 2382.52 2325.07 26.24 o -1 0 1 94.93 89.73 2.95 o 0 0 1 4.85 4.00 0.15 o 2 0 1 2.43 0.29 0.29 o 3 0 1 82.68 78.87 0.93 o 4 0 1 102.90 105.24 1.23 o 5 0 1 170.10 176.45 1.99 o 6 0 1 47.33 46.77 0.81 o -6 1 1 21.55 19.39 0.57 o -5 1 1 10.24 11.14 0.46 o -4 1 1 149.81 145.95 1.64 o -3 1 1 139.36 127.09 2.47 o -2 1 1 70.25 74.43 0.96 o -1 1 1 87.23 94.43 2.53 o 1 1 1 1443.45 1460.91 18.74 o 2 1 1 3.63 6.86 0.43 o 3 1 1 245.91 231.94 2.48 o 4 1 1 232.30 230.62 2.26 o 5 1 1 149.52 148.72 1.62 o 6 1 1 20.15 21.53 0.55 o -6 2 1 124.23 117.52 1.68 o -5 2 1 181.00 176.44 2.22 o -4 2 1 169.12 157.52 1.93 o -3 2 1 93.56 81.83 1.81 o -2 2 1 725.44 783.56 12.53 o 0 2 1 1700.43 1788.16 44.55 o 1 2 1 421.10 413.06 5.41 o 2 2 1 1158.96 1167.90 10.20 o 3 2 1 0.05 0.18 0.12 o 4 2 1 170.08 165.72 1.71 o 5 2 1 41.35 41.97 0.67 o 6 2 1 271.58 266.04 2.74 o -5 3 1 86.12 81.56 1.23 o -4 3 1 0.58 0.56 0.14 o -3 3 1 44.02 26.71 0.82 o -2 3 1 265.02 273.57 3.44 o -1 3 1 289.83 316.35 4.98 o 0 3 1 180.44 189.16 2.09 o 1 3 1 11.57 9.73 0.19 o 2 3 1 368.19 343.34 2.94 o 3 3 1 101.93 119.91 1.13 o 4 3 1 145.15 144.17 1.38 o 5 3 1 59.69 62.41 0.87 o 6 3 1 52.40 51.78 1.13 o -5 4 1 59.49 54.14 0.93 o -4 4 1 179.36 182.29 2.22 o -3 4 1 15.43 14.64 0.50 o -2 4 1 544.65 589.38 7.19 o -1 4 1 145.27 131.40 2.12 o 0 4 1 2829.63 3161.35 26.46 o 1 4 1 370.89 402.92 3.53 o 2 4 1 39.13 38.71 0.46 o 3 4 1 33.02 28.82 0.40 o 4 4 1 189.10 190.48 1.76 o 5 4 1 4.02 4.25 0.23 o -5 5 1 52.48 56.22 0.98 o -4 5 1 6.54 7.91 0.45 o -3 5 1 618.50 620.41 7.68 o -2 5 1 1161.50 1171.35 22.02 o -1 5 1 231.90 234.44 2.75 o 0 5 1 167.93 172.70 1.45 o 1 5 1 273.66 274.05 2.12 o 2 5 1 324.31 321.41 2.33 o 3 5 1 80.61 79.43 0.81 o 4 5 1 118.50 126.00 1.36 o 5 5 1 22.04 21.54 0.46 o -5 6 1 116.50 121.33 1.71 o -4 6 1 120.74 131.93 1.76 o -3 6 1 0.80 0.76 0.18 o -2 6 1 238.39 241.92 3.22 o -1 6 1 33.37 31.75 0.47 o 0 6 1 961.49 980.50 8.35 o 1 6 1 78.55 89.42 0.82 o 2 6 1 423.64 401.50 3.09 o 3 6 1 16.97 17.87 0.33 o 4 6 1 43.56 43.20 0.65 o 5 6 1 27.90 27.71 0.79 o -4 7 1 36.58 35.32 0.74 o -3 7 1 129.88 127.52 1.96 o -2 7 1 5.60 6.90 0.38 o -1 7 1 9.45 10.88 0.45 o 0 7 1 145.19 142.84 1.57 o 1 7 1 114.99 114.09 1.08 o 2 7 1 3.10 5.08 0.27 o 3 7 1 2.14 2.87 0.45 o 4 7 1 113.29 116.64 2.29 o -3 8 1 0.38 0.10 0.23 o -2 8 1 329.16 328.58 4.36 o -1 8 1 6.27 5.96 0.37 o 0 8 1 5.14 5.37 0.28 o 1 8 1 49.29 49.82 0.76 o 2 8 1 20.90 21.97 0.51 o 3 8 1 105.39 107.68 1.64 o 4 8 1 263.59 267.07 3.56 o -3 9 1 0.20 0.02 0.22 o -2 9 1 102.19 98.29 1.68 o -1 9 1 9.47 8.13 0.45 o 0 9 1 30.10 30.48 0.64 o 1 9 1 175.60 175.59 2.19 o 2 9 1 23.25 24.91 0.90 o 3 9 1 49.42 54.00 1.03 o -1 10 1 5.93 6.40 0.64 o 0 10 1 86.00 88.76 1.49 o 1 10 1 79.17 83.02 2.35 o 2 10 1 3.26 2.06 0.38 o -1 -10 2 104.62 109.29 1.58 o 0 -10 2 71.08 70.57 1.85 o 1 -10 2 52.07 50.74 1.03 o -3 -9 2 0.35 -0.52 0.26 o -2 -9 2 6.35 5.77 0.36 o -1 -9 2 49.44 52.77 0.93 o 0 -9 2 56.16 56.53 2.39 o 1 -9 2 2.05 1.75 0.32 o 2 -9 2 224.13 231.22 3.04 o -4 -8 2 19.24 20.92 0.63 o -3 -8 2 1.16 0.60 0.20 o -2 -8 2 11.85 11.08 0.40 o -1 -8 2 129.10 132.82 1.54 o 0 -8 2 1695.84 1749.69 21.04 o 1 -8 2 121.00 124.48 2.75 o 2 -8 2 0.70 1.15 0.25 o 3 -8 2 27.85 25.01 0.66 o -4 -7 2 9.91 10.60 0.46 o -3 -7 2 222.77 227.67 3.04 o -2 -7 2 619.74 646.80 6.15 o -1 -7 2 10.72 9.91 0.34 o 0 -7 2 19.65 18.38 1.75 o 1 -7 2 261.17 265.24 3.46 o 2 -7 2 0.71 0.63 0.17 o 3 -7 2 250.82 236.70 3.17 o 4 -7 2 2.41 2.45 0.22 o -5 -6 2 13.80 9.37 1.39 o -4 -6 2 19.95 23.28 0.60 o -3 -6 2 3.91 3.54 0.26 o -2 -6 2 1.20 0.77 0.13 o -1 -6 2 25.78 27.63 0.53 o 0 -6 2 18.86 17.83 0.57 o 1 -6 2 0.07 0.27 0.10 o 2 -6 2 241.68 227.26 2.96 o 3 -6 2 94.10 92.53 1.17 o 4 -6 2 3.62 5.07 0.28 o -5 -5 2 48.55 50.44 1.29 o -4 -5 2 127.52 126.48 1.83 o -3 -5 2 2.03 1.06 0.14 o -2 -5 2 49.19 53.10 0.72 o -1 -5 2 93.92 82.76 1.03 o 0 -5 2 83.12 81.35 1.48 o 1 -5 2 349.66 369.84 6.99 o 2 -5 2 69.68 70.48 1.37 o 3 -5 2 5.82 3.62 0.31 o 4 -5 2 189.90 165.09 1.98 o 5 -5 2 103.82 106.82 1.44 o -5 -4 2 54.00 54.67 0.77 o -4 -4 2 71.11 71.09 0.73 o -3 -4 2 0.51 0.27 0.10 o -2 -4 2 248.42 226.20 1.81 o -1 -4 2 340.02 311.22 2.90 o 0 -4 2 4.55 3.49 0.17 o 1 -4 2 143.26 164.09 5.45 o 2 -4 2 2.92 3.90 0.24 o 3 -4 2 296.34 288.14 3.76 o 4 -4 2 293.17 268.52 3.02 o 5 -4 2 172.85 166.01 2.04 o -5 -3 2 31.28 32.90 0.53 o -4 -3 2 53.76 50.69 0.57 o -3 -3 2 275.70 267.00 2.17 o -2 -3 2 117.90 124.79 1.00 o -1 -3 2 13.03 13.32 0.21 o 0 -3 2 98.36 100.66 1.60 o 1 -3 2 241.57 243.58 3.07 o 2 -3 2 37.25 32.85 0.90 o 3 -3 2 277.20 291.17 3.24 o 4 -3 2 4.28 3.44 0.32 o 5 -3 2 1.66 0.86 0.16 o -6 -2 2 37.63 38.11 0.66 o -5 -2 2 23.71 26.84 0.47 o -4 -2 2 56.51 58.08 0.69 o -3 -2 2 183.88 183.08 1.50 o -2 -2 2 25.47 26.10 0.32 o -1 -2 2 523.28 530.60 5.12 o 0 -2 2 18.67 15.64 0.37 o 1 -2 2 2741.53 2875.75 44.30 o 2 -2 2 1708.79 1814.28 27.14 o 3 -2 2 22.33 23.28 0.42 o 4 -2 2 0.00 0.12 0.10 o 5 -2 2 6.25 6.37 0.29 o 6 -2 2 32.01 32.48 0.89 o -6 -1 2 157.22 160.52 1.98 o -5 -1 2 1.96 2.33 0.19 o -4 -1 2 82.83 83.83 1.04 o -3 -1 2 11.47 11.46 0.21 o -2 -1 2 145.88 153.13 1.31 o -1 -1 2 22476.65 21185.30 443.98 o 0 -1 2 859.29 842.39 13.54 o 1 -1 2 222.71 220.54 3.73 o 2 -1 2 14.82 9.46 0.23 o 3 -1 2 5.50 5.23 0.18 o 4 -1 2 185.93 179.56 1.91 o 5 -1 2 191.88 197.53 2.35 o 6 -1 2 4.52 4.38 0.28 o -6 0 2 18.45 16.74 0.54 o -5 0 2 19.67 17.79 0.50 o -4 0 2 337.06 350.90 3.20 o -3 0 2 1564.01 1591.39 13.58 o -2 0 2 28.66 28.65 0.33 o -1 0 2 5.78 3.90 0.17 o 0 0 2 302.51 300.77 4.70 o 1 0 2 148.09 129.63 1.55 o 2 0 2 833.34 823.60 8.73 o 3 0 2 0.98 0.63 0.10 o 4 0 2 468.16 465.70 4.60 o 5 0 2 24.82 24.80 0.60 o 6 0 2 0.07 0.47 0.18 o -6 1 2 5.51 4.61 0.34 o -5 1 2 39.76 39.86 0.77 o -4 1 2 0.90 1.38 0.15 o -3 1 2 58.47 48.59 0.62 o -2 1 2 65.53 65.29 0.76 o -1 1 2 157.22 137.49 1.87 o 0 1 2 1711.60 1697.00 25.88 o 2 1 2 241.34 233.36 2.63 o 3 1 2 319.57 311.62 2.79 o 4 1 2 31.66 30.92 0.49 o 5 1 2 669.53 684.74 6.25 o 6 1 2 10.59 10.16 0.40 o -6 2 2 89.96 87.23 1.39 o -5 2 2 157.18 159.66 2.07 o -4 2 2 56.44 59.12 0.92 o -3 2 2 469.61 507.89 4.98 o -2 2 2 133.42 135.98 1.59 o -1 2 2 396.37 356.97 5.42 o 0 2 2 151.81 157.15 2.63 o 1 2 2 316.27 295.30 5.77 o 2 2 2 519.54 536.03 4.98 o 3 2 2 1068.34 1092.05 10.69 o 4 2 2 249.71 253.81 2.47 o 5 2 2 94.33 95.44 1.16 o 6 2 2 191.67 189.62 2.07 o -5 3 2 0.63 0.33 0.19 o -4 3 2 6.31 6.44 0.31 o -2 3 2 21.89 19.06 0.49 o -1 3 2 639.36 663.53 8.00 o 1 3 2 710.19 720.24 14.36 o 2 3 2 390.82 414.11 4.60 o 3 3 2 182.81 189.24 1.72 o 4 3 2 99.71 102.22 1.16 o 5 3 2 0.60 0.36 0.16 o 6 3 2 20.14 18.06 0.75 o -5 4 2 4.15 4.23 0.30 o -4 4 2 157.48 153.47 2.42 o -3 4 2 14.34 12.99 0.59 o -2 4 2 172.89 175.93 2.84 o -1 4 2 405.69 411.64 5.09 o 0 4 2 2.65 3.33 0.19 o 1 4 2 56.86 53.74 0.54 o 2 4 2 133.84 134.01 1.33 o 3 4 2 28.32 35.86 0.67 o 4 4 2 2.20 1.65 0.17 o 5 4 2 7.86 8.33 0.29 o -5 5 2 76.04 75.17 1.22 o -4 5 2 82.92 78.52 1.19 o -3 5 2 144.70 145.30 2.10 o -2 5 2 32.11 34.65 0.73 o -1 5 2 15.70 22.97 0.42 o 0 5 2 500.21 563.13 4.50 o 1 5 2 1050.58 1133.39 8.92 o 2 5 2 11.25 11.35 0.21 o 3 5 2 202.14 192.81 1.70 o 4 5 2 16.37 17.79 0.39 o 5 5 2 7.98 7.97 0.31 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