#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236930.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236930_Fobs loop_ _publ_author_name 'Thanigaimani, Kaliyaperumal' 'Khalib, Nuridayanti Che' 'Arshad, Suhana' 'Razak, Ibrahim Abdul' _publ_section_title ; 4-Chloro-6-methoxypyrimidin-2-amine ; _journal_coeditor_code IS5214 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3318 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.550 _cell_angle_gamma 90.000 _cell_length_a 3.7683 _cell_length_b 16.4455 _cell_length_c 10.7867 _exptl_crystal_F_000 328.00 _reflns_d_resolution_high 0.6590 _[local]_cod_data_source_file is5214Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' kty84_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.84 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2500.57 2463.46 61.62 o 2 0 0 11.76 10.29 0.52 o 3 0 0 216.96 212.59 2.97 o 4 0 0 349.48 352.60 4.65 o 1 1 0 6016.46 6253.04 51.57 o 2 1 0 24.91 23.25 0.55 o 3 1 0 30.29 35.32 0.78 o 4 1 0 8.69 9.73 0.55 o 5 1 0 0.61 0.81 0.92 o 0 2 0 63.48 72.87 0.96 o 1 2 0 6173.93 6315.27 79.03 o 2 2 0 377.95 437.30 3.09 o 3 2 0 238.77 234.38 2.05 o 4 2 0 173.12 176.36 2.12 o 5 2 0 50.70 54.56 3.81 o 1 3 0 567.11 589.18 35.81 o 2 3 0 171.32 205.80 1.64 o 3 3 0 116.23 106.21 1.27 o 4 3 0 10.33 10.28 0.61 o 5 3 0 85.01 84.29 2.97 o 0 4 0 978.23 975.27 25.06 o 1 4 0 114.95 131.52 1.13 o 2 4 0 54.97 66.36 0.91 o 3 4 0 39.38 48.31 0.84 o 4 4 0 54.08 52.49 1.26 o 5 4 0 195.59 193.94 4.96 o 1 5 0 533.31 545.24 3.95 o 2 5 0 1978.79 2085.89 13.16 o 3 5 0 282.02 283.80 2.60 o 4 5 0 1.97 1.90 0.38 o 5 5 0 125.79 129.10 3.06 o 0 6 0 588.22 585.21 4.60 o 1 6 0 1777.99 1868.80 11.14 o 2 6 0 4.42 3.96 0.24 o 3 6 0 51.62 61.09 1.09 o 4 6 0 10.84 9.38 0.64 o 5 6 0 43.80 42.22 1.86 o 1 7 0 1085.84 1099.17 6.16 o 2 7 0 1760.10 1791.97 10.79 o 3 7 0 215.78 229.18 2.46 o 4 7 0 117.98 114.06 1.79 o 5 7 0 0.41 0.18 0.60 o 0 8 0 2270.51 2336.56 40.50 o 1 8 0 146.88 122.08 1.18 o 2 8 0 67.65 72.04 0.92 o 3 8 0 54.50 50.17 1.18 o 4 8 0 243.36 242.50 3.98 o 5 8 0 62.71 67.77 2.34 o 1 9 0 1422.86 1488.78 8.29 o 2 9 0 88.63 83.27 1.05 o 3 9 0 598.16 571.32 5.01 o 4 9 0 1.41 0.98 0.52 o 5 9 0 9.08 8.95 1.12 o 0 10 0 43.73 73.54 1.18 o 1 10 0 313.20 305.18 2.52 o 2 10 0 87.35 93.90 1.31 o 3 10 0 146.75 147.12 1.94 o 4 10 0 222.61 218.93 3.39 o 5 10 0 127.69 144.12 3.52 o 1 11 0 632.43 706.13 4.87 o 2 11 0 30.14 27.77 0.78 o 3 11 0 38.31 39.46 0.96 o 4 11 0 45.08 45.89 1.57 o 5 11 0 0.63 0.24 0.90 o 0 12 0 1621.81 1639.42 12.21 o 1 12 0 119.33 120.02 1.49 o 2 12 0 7.18 12.72 0.62 o 3 12 0 112.70 109.92 1.67 o 4 12 0 218.54 215.40 3.48 o 1 13 0 82.16 75.83 1.21 o 2 13 0 464.56 468.25 4.27 o 3 13 0 171.08 160.47 2.75 o 4 13 0 1.23 0.77 0.54 o 0 14 0 237.40 239.31 3.52 o 1 14 0 423.97 413.72 3.46 o 2 14 0 1.80 1.80 0.41 o 3 14 0 135.65 136.66 2.17 o 4 14 0 96.10 88.56 2.31 o 1 15 0 75.81 79.47 1.33 o 2 15 0 373.64 362.78 3.76 o 3 15 0 36.05 39.10 1.23 o 4 15 0 206.26 203.73 4.09 o 0 16 0 25.60 18.42 1.38 o 1 16 0 2.07 2.03 0.38 o 2 16 0 0.00 0.04 0.35 o 3 16 0 26.23 26.52 1.14 o 4 16 0 9.71 8.92 1.85 o 1 17 0 448.44 416.35 3.73 o 2 17 0 308.78 304.41 4.71 o 3 17 0 379.29 388.20 4.33 o 4 17 0 7.72 9.49 1.22 o 0 18 0 3.71 1.39 0.87 o 1 18 0 232.88 216.96 2.79 o 2 18 0 0.53 1.21 0.46 o 3 18 0 0.01 1.36 0.82 o 1 19 0 37.49 37.90 2.02 o 2 19 0 218.42 214.00 3.01 o 3 19 0 96.49 88.70 3.23 o 0 20 0 510.01 494.27 7.83 o 1 20 0 0.46 1.40 0.60 o 2 20 0 30.30 32.62 1.28 o 3 20 0 48.94 48.96 1.81 o 1 21 0 3.35 3.31 0.81 o 2 21 0 0.23 1.26 0.68 o 3 21 0 17.45 18.06 1.37 o 0 22 0 260.01 248.12 7.78 o 1 22 0 131.71 136.72 3.28 o 2 22 0 38.24 36.21 1.93 o 1 23 0 1.68 2.94 0.83 o 2 23 0 15.25 16.68 1.52 o 0 24 0 9.82 11.53 2.14 o 1 24 0 128.00 125.89 4.09 o -5 1 1 268.32 284.95 8.25 o -4 1 1 229.45 230.79 3.16 o -3 1 1 16.76 15.79 0.51 o -2 1 1 1000.85 999.17 6.12 o -1 1 1 30.85 20.25 0.48 o 0 1 1 55.61 62.71 0.80 o 1 1 1 553.96 539.97 4.07 o 2 1 1 10.00 5.00 0.30 o 3 1 1 242.10 230.59 2.23 o 4 1 1 87.59 88.20 1.46 o -5 2 1 81.54 87.87 3.03 o -4 2 1 34.59 32.71 0.98 o -3 2 1 45.21 43.26 0.78 o -2 2 1 340.29 366.44 2.48 o -1 2 1 57.65 76.87 0.88 o 0 2 1 2179.25 2173.77 30.70 o 1 2 1 17380.89 15823.69 170.88 o 2 2 1 560.17 560.94 3.79 o 3 2 1 36.41 45.62 1.87 o 4 2 1 46.70 49.00 1.09 o 5 2 1 65.57 64.89 3.58 o -5 3 1 148.83 155.11 4.14 o -4 3 1 0.03 1.66 0.80 o -3 3 1 22.42 22.65 0.58 o -2 3 1 198.12 192.04 1.55 o -1 3 1 4547.41 4607.60 33.43 o 0 3 1 859.35 885.55 6.93 o 1 3 1 110.89 133.39 1.41 o 2 3 1 2334.74 2419.50 12.81 o 3 3 1 85.73 83.70 1.13 o 4 3 1 107.73 107.63 1.82 o 5 3 1 5.49 6.97 1.15 o -5 4 1 24.26 26.97 2.49 o -4 4 1 141.09 143.60 1.92 o -3 4 1 544.09 558.51 3.55 o -2 4 1 3.79 1.72 0.18 o -1 4 1 8.46 5.87 0.34 o 0 4 1 2621.40 2611.94 14.92 o 1 4 1 949.81 930.36 5.93 o 2 4 1 5279.61 5534.56 30.55 o 3 4 1 175.14 175.45 1.73 o 4 4 1 177.58 176.02 2.52 o 5 4 1 39.11 45.16 2.30 o -5 5 1 302.75 301.92 6.18 o -4 5 1 1.05 1.26 0.41 o -3 5 1 46.00 47.39 0.87 o -2 5 1 2.55 5.68 0.42 o -1 5 1 197.94 193.15 1.60 o 0 5 1 974.42 945.09 4.95 o 1 5 1 1175.91 1300.41 7.50 o 2 5 1 48.84 47.25 0.79 o 3 5 1 1351.12 1387.96 8.71 o 4 5 1 16.57 16.99 0.90 o 5 5 1 7.03 7.29 1.00 o -5 6 1 97.36 97.28 2.73 o -4 6 1 1067.87 1093.59 8.34 o -3 6 1 349.64 338.06 2.73 o -2 6 1 556.66 565.55 3.60 o -1 6 1 239.80 243.78 2.02 o 0 6 1 2017.27 2108.13 10.91 o 1 6 1 1567.98 1601.74 9.33 o 2 6 1 57.20 90.53 0.96 o 3 6 1 8.29 8.97 0.78 o 4 6 1 17.09 15.83 1.26 o 5 6 1 281.10 285.69 5.41 o -5 7 1 3.30 2.27 0.79 o -4 7 1 322.37 326.48 4.08 o -3 7 1 0.24 0.60 0.26 o -2 7 1 9.53 11.09 0.42 o -1 7 1 181.46 179.72 1.30 o 0 7 1 389.92 445.44 3.63 o 1 7 1 89.92 111.37 1.28 o 2 7 1 8.08 8.19 0.56 o 3 7 1 743.91 761.93 6.02 o 4 7 1 19.18 19.32 0.89 o 5 7 1 1.99 1.41 0.61 o -5 8 1 1.47 0.91 0.69 o -4 8 1 45.91 48.67 1.51 o -3 8 1 1142.66 1130.18 9.05 o -2 8 1 93.85 79.00 0.99 o -1 8 1 322.82 342.68 2.17 o 0 8 1 9.82 5.11 0.33 o 1 8 1 0.16 2.55 0.24 o 2 8 1 28.13 27.87 0.64 o 3 8 1 3.63 3.93 0.42 o 4 8 1 304.72 299.67 3.20 o 5 8 1 10.55 11.34 1.05 o -5 9 1 29.95 31.19 1.78 o -4 9 1 30.72 32.97 2.22 o -3 9 1 6.81 5.97 0.79 o -2 9 1 60.16 62.52 1.54 o -1 9 1 963.38 1020.49 5.15 o 0 9 1 1934.15 2086.11 10.58 o 1 9 1 113.23 128.42 1.39 o 2 9 1 668.16 673.46 4.76 o 3 9 1 420.98 409.32 4.96 o 4 9 1 441.01 444.32 4.60 o 5 9 1 13.24 12.12 1.30 o -5 10 1 0.04 0.12 0.75 o -4 10 1 9.93 9.19 0.88 o -3 10 1 41.46 39.97 0.99 o -2 10 1 31.24 34.66 0.73 o -1 10 1 260.66 281.07 1.83 o 0 10 1 151.14 163.98 1.36 o 1 10 1 34.76 34.59 0.73 o 2 10 1 4.15 3.70 0.41 o 3 10 1 1.39 1.22 0.32 o 4 10 1 20.40 18.03 1.02 o 5 10 1 60.28 59.02 2.26 o -5 11 1 128.59 136.79 3.48 o -4 11 1 5.11 3.89 0.70 o -3 11 1 80.50 80.95 1.36 o -2 11 1 1840.42 1812.09 10.25 o -1 11 1 657.92 642.21 4.16 o 0 11 1 542.73 534.49 3.29 o 1 11 1 30.33 39.22 0.83 o 2 11 1 751.95 738.57 5.79 o 3 11 1 463.35 468.32 5.66 o 4 11 1 185.88 185.74 3.12 o 5 11 1 0.17 -0.51 0.79 o -5 12 1 54.35 60.85 6.30 o -4 12 1 7.23 7.97 0.74 o -3 12 1 81.53 80.61 1.41 o -2 12 1 11.68 10.67 0.76 o -1 12 1 71.52 70.01 1.11 o 0 12 1 139.36 149.22 1.38 o 1 12 1 5.89 8.44 0.65 o 2 12 1 7.34 11.40 0.67 o 3 12 1 140.65 131.59 2.00 o 4 12 1 11.96 12.63 1.05 o -4 13 1 10.25 11.07 1.24 o -3 13 1 236.27 241.33 2.69 o -2 13 1 41.04 37.69 0.93 o -1 13 1 949.48 923.05 6.24 o 0 13 1 141.46 128.72 1.30 o 1 13 1 0.06 0.17 0.27 o 2 13 1 30.20 27.88 0.91 o 3 13 1 303.29 301.98 3.38 o 4 13 1 54.92 55.09 1.45 o -4 14 1 172.47 179.12 2.80 o -3 14 1 259.76 259.34 2.88 o -2 14 1 249.85 250.12 4.05 o -1 14 1 178.62 165.61 1.91 o 0 14 1 185.04 176.45 1.76 o 1 14 1 880.10 815.26 5.78 o 2 14 1 75.85 74.35 1.48 o 3 14 1 103.13 100.38 1.85 o 4 14 1 42.65 41.29 2.19 o -4 15 1 13.37 13.13 1.33 o -3 15 1 5.67 4.64 0.59 o -2 15 1 199.40 200.39 2.60 o -1 15 1 95.56 89.41 1.40 o 0 15 1 48.21 44.81 1.00 o 1 15 1 9.47 6.43 0.52 o 2 15 1 242.57 215.77 3.31 o 3 15 1 2.00 3.19 0.81 o 4 15 1 3.44 3.46 0.77 o -4 16 1 60.24 56.99 2.25 o -3 16 1 156.10 147.22 2.38 o -2 16 1 68.28 71.39 2.02 o -1 16 1 7.14 6.50 0.57 o 0 16 1 870.45 807.16 5.85 o 1 16 1 157.89 175.82 2.13 o 2 16 1 363.60 365.90 3.89 o 3 16 1 0.08 0.08 0.43 o 4 16 1 93.11 87.62 3.38 o -4 17 1 1.00 0.28 0.78 o -3 17 1 44.17 49.73 1.45 o -2 17 1 16.93 15.78 0.91 o -1 17 1 4.93 5.52 0.57 o 0 17 1 12.28 13.86 0.92 o 1 17 1 103.32 89.13 1.52 o 2 17 1 13.20 11.99 0.82 o 3 17 1 0.49 0.92 0.50 o 4 17 1 0.23 0.22 0.86 o -3 18 1 66.96 63.83 1.92 o -2 18 1 0.14 0.30 0.40 o -1 18 1 0.25 1.00 0.54 o 0 18 1 0.77 2.80 0.59 o 1 18 1 357.22 362.57 3.50 o 2 18 1 62.80 60.18 1.53 o 3 18 1 29.07 28.21 1.74 o -3 19 1 0.49 0.05 0.63 o -2 19 1 380.64 389.44 4.30 o -1 19 1 479.21 464.46 5.25 o 0 19 1 157.74 153.82 2.69 o 1 19 1 14.13 12.84 0.96 o 2 19 1 145.64 142.91 2.42 o 3 19 1 47.79 48.25 2.17 o -3 20 1 49.73 53.69 2.19 o -2 20 1 126.32 122.96 2.27 o -1 20 1 5.24 7.71 0.82 o 0 20 1 23.02 24.03 1.35 o 1 20 1 118.12 109.47 2.34 o 2 20 1 0.18 0.83 0.52 o 3 20 1 12.25 13.98 1.20 o -3 21 1 63.40 62.49 2.38 o -2 21 1 321.59 301.58 5.09 o -1 21 1 251.61 260.29 4.55 o 0 21 1 224.02 226.57 4.14 o 1 21 1 4.59 3.87 0.84 o 2 21 1 34.71 34.22 1.55 o 3 21 1 287.76 280.84 4.44 o -2 22 1 2.34 1.91 0.81 o -1 22 1 31.17 33.66 2.01 o 0 22 1 20.93 21.73 1.53 o 1 22 1 41.83 38.01 1.82 o 2 22 1 76.19 75.37 2.57 o -2 23 1 153.38 151.85 3.66 o -1 23 1 266.09 265.95 4.84 o 0 23 1 9.41 10.85 3.31 o 1 23 1 4.23 6.97 1.06 o 2 23 1 150.99 162.47 3.84 o -1 24 1 32.36 34.30 1.92 o 0 24 1 19.93 22.31 2.02 o 1 24 1 0.07 0.13 0.65 o -5 0 2 0.77 1.65 1.01 o -4 0 2 801.49 846.48 11.03 o -3 0 2 668.47 654.68 6.53 o -2 0 2 3.11 1.77 0.29 o -1 0 2 911.29 975.78 10.14 o 0 0 2 1228.29 1295.85 20.17 o 1 0 2 3193.99 3293.96 101.68 o 2 0 2 2379.51 2414.26 19.87 o 3 0 2 500.08 501.84 5.44 o 4 0 2 174.24 193.28 3.22 o 5 0 2 40.85 45.21 2.11 o -5 1 2 23.94 25.13 1.96 o -4 1 2 15.09 16.89 0.99 o -3 1 2 775.16 783.66 4.55 o -2 1 2 8.54 7.55 0.31 o -1 1 2 1184.77 1202.05 9.37 o 1 1 2 1647.99 1632.73 23.30 o 2 1 2 92.43 82.31 1.37 o 3 1 2 14.32 14.14 0.58 o 4 1 2 73.25 72.73 1.47 o 5 1 2 18.20 16.65 1.29 o -5 2 2 10.26 12.05 1.43 o -4 2 2 18.69 19.61 0.90 o -3 2 2 427.98 432.53 2.88 o -2 2 2 2013.31 2045.78 16.33 o -1 2 2 143.73 147.79 2.47 o 0 2 2 174.14 172.41 2.42 o 1 2 2 381.39 371.43 3.61 o 2 2 2 2001.05 2073.00 11.96 o 3 2 2 796.53 827.12 5.65 o 4 2 2 0.39 0.85 0.36 o 5 2 2 61.57 63.08 2.05 o -5 3 2 312.35 318.04 6.32 o -4 3 2 551.50 557.98 5.73 o -3 3 2 90.19 89.54 1.06 o -2 3 2 103.28 120.59 1.06 o -1 3 2 1294.58 1249.06 8.33 o 0 3 2 2541.53 2475.96 21.65 o 1 3 2 720.85 806.00 5.97 o 2 3 2 711.06 740.43 5.10 o 3 3 2 67.07 55.57 0.92 o 4 3 2 4.81 6.18 0.65 o 5 3 2 42.89 44.25 1.74 o -5 4 2 6.76 7.19 1.23 o -4 4 2 14.73 13.36 0.91 o -3 4 2 307.12 323.69 2.38 o -2 4 2 135.34 133.23 1.25 o -1 4 2 1691.35 1690.14 10.70 o 0 4 2 679.68 654.24 4.39 o 1 4 2 572.15 583.52 5.24 o 2 4 2 238.52 286.95 2.11 o 3 4 2 27.99 32.39 0.80 o 4 4 2 4.15 5.11 0.56 o 5 4 2 0.31 -0.03 0.49 o -5 5 2 31.25 35.23 2.10 o -4 5 2 358.47 344.81 4.36 o -3 5 2 107.84 109.31 1.22 o -2 5 2 338.81 340.25 2.41 o -1 5 2 397.06 389.44 2.68 o 0 5 2 2431.18 2332.03 14.47 o 1 5 2 71.23 49.69 0.89 o 2 5 2 4.55 4.17 0.40 o 3 5 2 1076.53 1089.63 7.93 o 4 5 2 330.98 318.47 3.55 o 5 5 2 27.97 28.40 1.60 o -5 6 2 84.78 87.34 3.25 o -4 6 2 21.78 19.39 1.30 o -3 6 2 0.49 0.49 0.25 o -2 6 2 5.06 6.84 0.40 o -1 6 2 15.72 22.35 0.43 o 0 6 2 20.67 38.32 0.47 o 1 6 2 101.48 118.15 1.52 o 2 6 2 100.00 105.84 1.22 o 3 6 2 466.17 493.28 4.39 o 4 6 2 81.32 79.15 1.82 o 5 6 2 2.13 2.95 0.67 o -5 7 2 75.25 81.15 3.16 o -4 7 2 32.50 30.61 1.49 o -3 7 2 12.05 11.87 0.61 o -2 7 2 60.13 57.79 0.79 o -1 7 2 863.38 819.86 4.23 o 0 7 2 871.51 823.58 5.05 o 1 7 2 2069.78 2218.27 15.70 o 2 7 2 0.01 -0.21 0.22 o 3 7 2 183.27 177.13 2.31 o 4 7 2 984.16 983.01 10.09 o 5 7 2 214.67 210.71 3.46 o -5 8 2 26.59 28.55 1.82 o -4 8 2 200.26 197.47 3.69 o -3 8 2 1862.32 1893.58 11.63 o -2 8 2 130.69 130.94 1.35 o -1 8 2 420.20 446.87 2.52 o 0 8 2 595.29 632.36 3.55 o 1 8 2 285.98 298.26 2.92 o 2 8 2 125.04 125.97 2.19 o 3 8 2 7.90 5.87 0.54 o 4 8 2 7.40 6.60 0.76 o 5 8 2 59.60 54.43 1.90 o -5 9 2 107.01 104.60 2.97 o -4 9 2 305.34 308.19 4.89 o -3 9 2 292.05 284.12 2.46 o -2 9 2 436.98 444.71 3.17 o -1 9 2 561.32 569.47 3.14 o 0 9 2 491.05 508.91 3.27 o 1 9 2 60.91 56.79 0.91 o 2 9 2 2.92 3.53 0.40 o 3 9 2 25.16 24.34 0.99 o 4 9 2 5.78 6.32 0.66 o 5 9 2 45.26 46.08 2.02 o -5 10 2 2.08 1.59 0.90 o -4 10 2 44.94 47.75 1.87 o -3 10 2 41.55 40.01 1.04 o -2 10 2 3053.81 2996.08 16.11 o -1 10 2 118.53 103.21 0.96 o 0 10 2 3.04 4.13 0.30 o 1 10 2 620.16 603.57 4.29 o 2 10 2 583.52 566.63 4.67 o 3 10 2 63.62 56.51 1.50 o 4 10 2 5.35 5.68 0.92 o 5 10 2 250.40 261.24 4.78 o -5 11 2 10.95 10.95 1.28 o -4 11 2 0.62 1.14 0.54 o -3 11 2 135.92 135.76 2.00 o -2 11 2 30.18 32.36 0.75 o -1 11 2 175.71 167.78 1.46 o 0 11 2 1.68 0.86 0.24 o 1 11 2 4.32 2.02 0.31 o 2 11 2 80.17 78.42 1.38 o 3 11 2 83.38 81.49 3.42 o 4 11 2 0.51 0.34 0.51 o 5 11 2 37.14 35.78 2.09 o -5 12 2 23.42 25.21 2.25 o -4 12 2 3.54 3.26 0.57 o -3 12 2 183.03 186.90 2.24 o -2 12 2 28.42 33.58 0.86 o -1 12 2 523.99 524.31 3.62 o 0 12 2 34.84 33.95 0.79 o 1 12 2 937.68 905.90 6.14 o 2 12 2 650.53 592.23 5.03 o 3 12 2 53.38 53.04 1.27 o 4 12 2 27.65 30.27 2.08 o -4 13 2 28.11 26.10 1.27 o -3 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