#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181291 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236934.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236934_Fobs loop_ _publ_author_name 'Thanigaimani, Kaliyaperumal' 'Khalib, Nuridayanti Che' 'Arshad, Suhana' 'Razak, Ibrahim Abdul' _publ_section_title ; 2,6-Diamino-4-chloropyrimidine--benzoic acid (1/1) ; _journal_coeditor_code IS5218 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3442 _journal_page_last o3443 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.493 _cell_angle_gamma 90.000 _cell_length_a 8.7817 _cell_length_b 5.7032 _cell_length_c 24.0257 _exptl_crystal_F_000 552.00 _reflns_d_resolution_high 0.8412 _cod_data_source_file is5218Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_kty51a_0m in P2(1)/c (100K)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 160.67 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14.51 16.03 1.36 o 2 0 0 5.26 6.32 0.70 o 3 0 0 519.64 445.94 33.70 o 4 0 0 3.45 4.28 0.74 o 5 0 0 13.35 19.09 1.37 o 6 0 0 414.28 392.00 22.87 o 7 0 0 185.13 185.72 6.50 o 8 0 0 1342.14 1276.07 43.93 o 9 0 0 2819.51 2545.74 284.97 o 10 0 0 0.33 -0.55 1.46 o 1 1 0 3224.74 3215.44 165.90 o 2 1 0 1312.19 1310.66 37.01 o 3 1 0 223.03 175.82 6.51 o 4 1 0 2850.36 2840.71 73.63 o 5 1 0 18.20 14.27 0.93 o 6 1 0 316.62 314.86 10.66 o 7 1 0 95.63 102.97 3.63 o 8 1 0 175.81 185.72 6.04 o 9 1 0 50.97 51.11 2.41 o 10 1 0 97.97 89.24 3.65 o 0 2 0 517.16 537.13 36.96 o 1 2 0 838.17 908.59 54.80 o 2 2 0 663.05 722.87 39.42 o 3 2 0 362.12 438.85 16.11 o 4 2 0 9.34 10.41 0.91 o 5 2 0 13.92 18.48 1.03 o 6 2 0 217.85 224.71 7.79 o 7 2 0 926.61 955.62 46.42 o 8 2 0 11.53 11.59 1.62 o 9 2 0 80.88 83.30 5.64 o 1 3 0 31.44 25.90 2.75 o 2 3 0 244.34 263.98 10.60 o 3 3 0 35.19 26.60 1.89 o 4 3 0 164.28 164.65 7.73 o 5 3 0 28.93 23.32 1.96 o 6 3 0 17.64 13.78 1.64 o 7 3 0 175.05 176.47 5.76 o 8 3 0 94.27 86.12 3.57 o 9 3 0 6.07 6.36 3.17 o 0 4 0 796.85 725.96 41.09 o 1 4 0 523.10 511.80 22.93 o 2 4 0 1.99 1.69 0.78 o 3 4 0 102.36 108.75 5.28 o 4 4 0 222.05 263.49 10.00 o 5 4 0 0.04 1.53 1.39 o 6 4 0 28.95 18.08 2.08 o 7 4 0 229.95 226.06 7.30 o 8 4 0 67.18 70.52 4.01 o 1 5 0 173.41 205.67 11.81 o 2 5 0 301.81 301.60 14.53 o 3 5 0 158.34 158.62 8.23 o 4 5 0 743.21 728.27 31.23 o 5 5 0 328.29 287.47 15.41 o 6 5 0 1.78 3.08 1.89 o 7 5 0 1.43 1.80 1.78 o 0 6 0 692.43 545.67 54.03 o 1 6 0 160.13 178.44 9.99 o 2 6 0 13.20 23.34 5.30 o 3 6 0 2.70 5.21 2.80 o 4 6 0 45.36 47.78 6.69 o -10 1 1 0.25 1.83 0.95 o -9 1 1 104.97 102.77 3.97 o -8 1 1 103.81 103.12 3.86 o -7 1 1 137.82 149.51 6.88 o -6 1 1 614.61 639.92 18.24 o -5 1 1 488.31 504.16 13.01 o -4 1 1 476.27 485.92 12.45 o -2 1 1 582.28 471.99 14.49 o -1 1 1 184.43 168.13 7.87 o 0 1 1 7736.39 6981.72 295.87 o 1 1 1 1194.55 1225.45 47.97 o 2 1 1 92.94 118.42 6.34 o 3 1 1 5.38 8.50 1.03 o 4 1 1 9.43 9.97 0.96 o 5 1 1 1257.59 1269.92 34.16 o 7 1 1 31.50 31.57 1.90 o 8 1 1 110.34 108.77 4.19 o 9 1 1 347.75 338.01 10.07 o 10 1 1 94.55 93.83 5.12 o -9 2 1 69.57 68.95 3.55 o -8 2 1 285.67 312.98 12.89 o -7 2 1 2023.20 1920.62 58.68 o -6 2 1 176.53 181.45 5.87 o -5 2 1 36.87 30.17 1.36 o -4 2 1 177.86 178.24 5.44 o -3 2 1 186.06 219.74 9.36 o -2 2 1 0.07 -0.58 0.29 o -1 2 1 113.06 106.61 4.81 o 0 2 1 335.75 296.54 14.76 o 1 2 1 4802.97 4835.88 190.79 o 2 2 1 5811.87 5784.23 310.61 o 3 2 1 13.62 5.77 0.97 o 4 2 1 18.64 38.64 1.95 o 5 2 1 377.64 439.59 10.89 o 6 2 1 38.04 37.52 2.02 o 7 2 1 14.25 16.13 1.47 o 8 2 1 61.23 62.71 2.79 o 9 2 1 86.45 98.76 3.51 o -9 3 1 142.75 135.26 5.97 o -8 3 1 3.64 2.36 1.10 o -7 3 1 54.26 56.70 4.95 o -6 3 1 17.23 22.04 3.19 o -5 3 1 18.95 20.86 1.82 o -4 3 1 986.91 1086.54 54.27 o -3 3 1 231.93 189.37 7.16 o -2 3 1 401.07 401.68 19.52 o -1 3 1 2441.51 2472.06 102.20 o 0 3 1 195.36 219.40 10.18 o 1 3 1 776.21 755.57 30.73 o 2 3 1 13.00 18.35 1.52 o 3 3 1 66.17 82.94 4.27 o 4 3 1 798.44 859.65 29.12 o 5 3 1 437.12 439.91 14.75 o 6 3 1 37.94 44.39 2.47 o 7 3 1 558.33 551.52 16.86 o 8 3 1 257.43 261.55 10.68 o 9 3 1 12.61 13.97 2.34 o -8 4 1 0.70 -1.62 1.21 o -7 4 1 30.12 31.94 3.03 o -6 4 1 4.46 3.38 2.65 o -5 4 1 216.14 215.31 11.40 o -4 4 1 415.12 482.36 17.02 o -3 4 1 29.25 28.88 2.16 o -2 4 1 0.01 -0.16 0.62 o -1 4 1 14.01 11.70 1.81 o 0 4 1 344.47 345.58 14.19 o 1 4 1 0.10 -0.34 0.72 o 2 4 1 128.37 134.34 5.69 o 3 4 1 105.29 92.66 6.85 o 4 4 1 35.54 38.20 3.42 o 5 4 1 650.57 627.55 23.80 o 6 4 1 98.20 92.46 5.00 o 7 4 1 2.72 0.02 1.28 o 8 4 1 7.55 12.51 2.10 o -7 5 1 63.12 66.09 6.73 o -6 5 1 1.41 1.19 1.45 o -5 5 1 37.63 24.11 5.67 o -4 5 1 61.42 78.44 5.33 o -3 5 1 40.37 33.33 3.56 o -2 5 1 6.59 8.92 2.66 o -1 5 1 0.10 2.08 1.55 o 0 5 1 30.22 22.44 3.16 o 1 5 1 31.23 27.41 5.00 o 2 5 1 70.22 78.82 6.69 o 3 5 1 32.50 34.42 3.31 o 5 5 1 10.05 7.29 5.78 o 6 5 1 30.54 35.88 7.84 o -4 6 1 1.74 3.06 7.73 o -3 6 1 27.89 21.76 4.33 o -2 6 1 1.49 2.75 2.07 o -1 6 1 174.36 180.44 8.94 o 0 6 1 296.09 277.24 23.25 o 1 6 1 200.14 168.37 10.55 o 2 6 1 39.41 54.01 5.20 o 3 6 1 0.66 5.62 2.76 o 4 6 1 6.76 9.96 6.74 o -10 0 2 0.08 0.71 1.44 o -9 0 2 412.15 392.16 18.23 o -8 0 2 192.94 185.82 9.80 o -7 0 2 369.83 410.39 15.24 o -6 0 2 215.01 240.08 10.44 o -5 0 2 65.67 43.97 5.09 o -4 0 2 278.78 284.38 10.54 o -3 0 2 50.75 66.36 2.62 o -2 0 2 4296.14 3153.68 152.55 o -1 0 2 263.90 154.86 9.09 o 1 0 2 1739.57 1770.93 78.16 o 2 0 2 967.17 867.96 46.68 o 3 0 2 1404.86 1301.62 59.34 o 4 0 2 619.16 611.08 21.25 o 5 0 2 1409.52 1416.38 75.60 o 6 0 2 743.23 796.87 39.19 o 7 0 2 162.11 159.64 5.76 o 8 0 2 111.61 108.94 4.90 o 9 0 2 80.93 82.38 5.60 o 10 0 2 1129.03 1105.97 67.58 o -10 1 2 65.99 61.49 3.36 o -9 1 2 233.79 224.25 7.18 o -8 1 2 146.15 148.21 5.04 o -7 1 2 105.61 105.95 3.49 o -6 1 2 787.70 815.81 28.87 o -5 1 2 308.74 321.37 9.06 o -4 1 2 1324.09 1497.12 45.09 o -3 1 2 2570.80 1860.34 107.42 o -2 1 2 17204.58 19373.99 771.41 o -1 1 2 376.95 367.43 39.54 o 0 1 2 6613.34 6064.02 422.15 o 1 1 2 1007.90 1067.01 36.18 o 2 1 2 1030.33 1031.42 29.72 o 3 1 2 15.84 16.51 0.90 o 4 1 2 60.93 51.70 2.09 o 5 1 2 1944.23 1878.83 82.95 o 6 1 2 50.64 52.87 2.81 o 7 1 2 1335.70 1312.65 32.69 o 8 1 2 88.94 90.81 3.28 o 9 1 2 193.76 182.38 6.01 o 10 1 2 46.30 49.24 3.03 o -9 2 2 57.86 59.34 4.86 o -8 2 2 0.39 -0.44 0.86 o -7 2 2 59.16 55.57 2.77 o -6 2 2 357.63 412.63 14.17 o -5 2 2 77.51 88.63 2.75 o -4 2 2 72.67 95.85 3.76 o -3 2 2 44.67 35.35 7.22 o -2 2 2 3249.44 3329.48 377.65 o -1 2 2 367.25 366.24 16.55 o 0 2 2 887.35 874.58 29.88 o 1 2 2 14.93 16.51 1.46 o 2 2 2 135.30 129.33 6.34 o 3 2 2 578.65 627.26 28.79 o 4 2 2 1583.80 1737.54 81.05 o 5 2 2 246.89 259.71 7.36 o 6 2 2 143.04 145.83 5.94 o 7 2 2 39.92 40.16 2.90 o 8 2 2 36.43 37.74 1.96 o 9 2 2 12.92 13.76 1.39 o -9 3 2 0.11 -1.43 1.13 o -8 3 2 0.58 -0.56 0.90 o -7 3 2 265.18 266.39 8.25 o -6 3 2 35.11 33.35 1.96 o -5 3 2 84.72 92.39 4.09 o -4 3 2 34.83 29.46 5.61 o -3 3 2 435.72 433.65 15.13 o -2 3 2 97.18 114.14 8.51 o -1 3 2 155.57 138.95 7.27 o 0 3 2 15.90 23.67 2.32 o 1 3 2 136.52 129.84 13.92 o 2 3 2 1247.78 1339.31 46.64 o 3 3 2 159.03 162.81 7.62 o 4 3 2 11.06 16.84 1.96 o 5 3 2 26.53 26.46 4.60 o 6 3 2 30.77 36.94 2.61 o 7 3 2 7.07 8.66 1.62 o 8 3 2 2.77 2.40 1.55 o 9 3 2 20.82 24.83 2.87 o -8 4 2 17.83 15.98 2.21 o -7 4 2 180.80 177.02 7.13 o -6 4 2 470.25 458.76 20.34 o -5 4 2 2.63 1.06 1.36 o -4 4 2 328.40 373.92 13.81 o -3 4 2 59.74 67.36 4.34 o -2 4 2 565.65 545.42 21.07 o -1 4 2 68.14 73.61 5.82 o 0 4 2 125.71 124.06 6.06 o 1 4 2 21.93 19.20 2.28 o 2 4 2 577.36 587.79 21.34 o 3 4 2 41.72 31.85 6.54 o 4 4 2 332.27 314.74 14.52 o 5 4 2 76.42 50.35 4.56 o 6 4 2 258.02 268.56 10.53 o 7 4 2 5.56 -0.61 1.29 o 8 4 2 0.23 -0.23 1.23 o -7 5 2 1.61 0.48 1.51 o -6 5 2 35.09 40.90 3.53 o -5 5 2 45.94 41.27 4.36 o -4 5 2 0.77 -0.21 1.31 o -3 5 2 113.96 106.68 6.23 o -2 5 2 539.78 533.36 24.21 o -1 5 2 770.68 816.26 35.47 o 0 5 2 867.91 846.97 33.96 o 1 5 2 307.49 297.90 12.97 o 2 5 2 249.11 259.25 12.79 o 3 5 2 2.75 1.25 1.94 o 4 5 2 80.84 66.03 5.88 o 5 5 2 1.42 0.71 3.54 o 6 5 2 18.96 25.74 3.68 o -4 6 2 94.12 85.68 8.36 o -3 6 2 25.83 28.59 9.31 o -2 6 2 407.31 392.53 30.88 o -1 6 2 7.15 12.40 2.29 o 0 6 2 317.01 302.38 13.42 o 1 6 2 61.82 73.65 10.88 o 2 6 2 36.86 46.41 7.12 o 3 6 2 33.46 50.21 10.34 o 4 6 2 16.03 13.13 6.89 o -10 1 3 210.42 207.06 14.86 o -9 1 3 2.09 1.06 0.81 o -8 1 3 115.07 119.34 4.25 o -7 1 3 230.66 237.35 6.44 o -6 1 3 46.89 45.05 1.96 o -5 1 3 0.31 1.84 0.46 o -4 1 3 1550.92 1472.24 53.25 o -3 1 3 1180.30 1079.26 32.77 o -2 1 3 23878.95 22764.39 1139.87 o -1 1 3 239.08 233.38 9.03 o 0 1 3 379.48 371.49 21.35 o 1 1 3 2.86 6.36 0.89 o 2 1 3 134.85 130.46 4.07 o 3 1 3 920.04 954.34 23.08 o 4 1 3 676.95 703.20 18.49 o 5 1 3 2644.07 2635.39 58.74 o 6 1 3 8.86 8.32 1.10 o 7 1 3 304.71 299.68 8.22 o 8 1 3 1.04 -0.45 0.68 o 9 1 3 32.25 33.28 2.30 o 10 1 3 12.24 13.77 1.56 o -9 2 3 236.11 253.40 8.72 o -8 2 3 59.39 63.02 3.26 o -7 2 3 21.32 20.59 1.69 o -6 2 3 112.84 115.67 3.70 o -5 2 3 168.76 151.43 4.36 o -4 2 3 245.32 257.72 7.26 o -3 2 3 1162.46 1240.95 41.30 o -2 2 3 1415.90 1300.28 51.84 o -1 2 3 3640.72 3624.33 158.93 o 0 2 3 1611.60 1528.86 59.90 o 1 2 3 376.07 396.38 21.98 o 2 2 3 113.52 134.25 5.65 o 3 2 3 23.02 45.09 2.22 o 4 2 3 1177.19 1245.97 28.27 o 5 2 3 957.31 980.40 25.45 o 6 2 3 700.33 682.23 18.23 o 7 2 3 507.74 502.29 12.73 o 8 2 3 199.42 210.45 5.98 o 9 2 3 67.29 74.91 3.02 o -9 3 3 420.87 409.62 13.44 o -8 3 3 95.37 85.82 3.56 o -7 3 3 300.33 312.50 9.15 o -6 3 3 329.80 348.03 13.97 o -5 3 3 144.14 152.06 6.23 o -4 3 3 266.79 234.02 34.99 o -3 3 3 0.54 0.55 0.76 o -2 3 3 61.69 56.97 4.05 o -1 3 3 1129.34 1208.45 44.83 o 0 3 3 628.55 631.05 27.03 o 1 3 3 91.18 145.56 9.32 o 2 3 3 1512.41 1616.54 55.28 o 3 3 3 1111.07 1121.77 32.95 o 4 3 3 173.11 181.16 7.00 o 5 3 3 17.49 16.27 2.34 o 6 3 3 108.35 101.26 4.37 o 7 3 3 187.47 186.03 6.88 o 8 3 3 53.70 56.22 4.01 o 9 3 3 29.61 27.42 3.04 o -8 4 3 3.72 4.70 1.73 o -7 4 3 73.64 61.72 5.01 o -6 4 3 24.20 14.34 2.26 o -5 4 3 44.45 49.27 3.70 o -4 4 3 24.22 22.54 2.26 o -3 4 3 0.04 -0.13 0.82 o -2 4 3 27.18 35.26 2.47 o -1 4 3 342.49 351.17 18.27 o 0 4 3 22.86 24.92 2.54 o 1 4 3 0.40 0.71 0.84 o 2 4 3 218.73 256.04 13.26 o 3 4 3 38.89 37.88 3.18 o 4 4 3 0.16 -0.32 0.99 o 5 4 3 7.79 7.75 2.03 o 6 4 3 6.98 13.09 2.22 o 7 4 3 68.40 61.99 4.26 o 8 4 3 24.21 19.38 2.29 o -7 5 3 7.78 5.13 1.98 o -6 5 3 24.63 27.82 8.77 o -5 5 3 1.25 0.07 1.48 o -4 5 3 1.48 2.74 1.60 o -3 5 3 9.62 12.23 2.88 o -2 5 3 81.15 67.32 4.70 o -1 5 3 503.27 525.04 21.73 o 0 5 3 13.55 12.56 2.05 o 1 5 3 12.23 13.68 2.69 o 2 5 3 3.42 2.33 2.66 o 3 5 3 138.52 129.98 10.05 o 4 5 3 53.59 53.01 7.33 o 5 5 3 23.38 16.95 2.96 o 6 5 3 71.44 75.59 5.84 o -4 6 3 106.44 123.64 10.46 o -3 6 3 0.17 3.27 2.40 o -2 6 3 172.19 211.76 17.18 o -1 6 3 0.16 1.96 1.41 o 0 6 3 11.53 16.19 2.69 o 1 6 3 202.56 204.14 18.69 o 2 6 3 1.76 6.71 2.79 o 3 6 3 86.34 60.64 8.39 o 4 6 3 18.82 31.84 9.14 o -10 0 4 625.74 579.21 26.13 o -9 0 4 0.57 0.65 1.45 o -8 0 4 934.15 984.20 44.87 o -7 0 4 3.04 3.16 1.10 o -6 0 4 37.51 34.47 2.87 o -5 0 4 26.60 39.18 2.06 o -4 0 4 2141.26 1916.48 76.73 o -3 0 4 142.53 129.18 4.59 o -1 0 4 7.50 7.98 1.53 o 0 0 4 1061.23 1108.86 65.36 o 1 0 4 16.03 14.32 1.34 o 2 0 4 10375.73 9553.81 337.40 o 3 0 4 1190.20 1332.86 46.98 o 4 0 4 121.88 128.68 4.49 o 5 0 4 1377.98 1458.82 44.27 o 6 0 4 394.35 388.96 13.04 o 7 0 4 1122.19 1095.09 33.91 o 8 0 4 7.89 11.90 1.57 o 9 0 4 58.22 52.14 7.90 o 10 0 4 285.66 294.75 22.64 o -10 1 4 5.81 6.47 1.54 o -9 1 4 0.45 0.29 0.70 o -8 1 4 8.31 7.80 1.32 o -7 1 4 42.81 43.20 2.03 o -6 1 4 530.48 534.76 16.09 o -5 1 4 36.65 48.73 2.13 o -4 1 4 953.15 955.29 42.86 o -3 1 4 251.52 247.58 9.24 o -2 1 4 25815.74 30011.74 2696.77 o -1 1 4 1876.55 1773.66 67.24 o 0 1 4 1546.27 1508.45 98.66 o 1 1 4 695.58 704.90 23.84 o 2 1 4 2048.03 1974.32 37.81 o 3 1 4 395.76 388.78 8.28 o 4 1 4 21.55 14.86 1.12 o 5 1 4 893.96 941.07 21.21 o 6 1 4 1818.78 1971.41 61.34 o 7 1 4 1331.87 1382.92 34.33 o 8 1 4 190.56 201.39 8.73 o 9 1 4 866.65 871.14 26.72 o 10 1 4 10.07 9.77 1.40 o -9 2 4 22.63 22.45 2.80 o -8 2 4 36.95 33.49 2.51 o -7 2 4 8.67 8.90 1.28 o -6 2 4 8.95 12.41 1.84 o -5 2 4 176.64 194.41 10.30 o -4 2 4 594.78 669.91 23.27 o -3 2 4 2046.78 1912.13 61.02 o -2 2 4 393.22 452.15 13.33 o -1 2 4 3.44 1.40 0.54 o 0 2 4 43.08 34.72 3.12 o 1 2 4 187.87 209.74 11.90 o 2 2 4 54.70 59.69 2.69 o 3 2 4 38.53 27.97 1.61 o 4 2 4 591.59 582.29 15.58 o 5 2 4 1704.22 1844.55 62.39 o 6 2 4 42.90 48.42 2.67 o 7 2 4 52.06 52.25 2.89 o 8 2 4 119.86 109.92 3.98 o 9 2 4 42.71 43.32 2.49 o -9 3 4 178.28 167.35 8.95 o -8 3 4 19.04 19.91 2.30 o -7 3 4 32.02 27.16 1.97 o -6 3 4 60.92 68.69 3.15 o -5 3 4 30.89 35.39 3.00 o -4 3 4 37.29 40.39 8.74 o -3 3 4 21.04 29.08 3.10 o -2 3 4 131.34 113.44 4.00 o -1 3 4 116.11 129.60 5.14 o 0 3 4 522.48 541.06 23.60 o 1 3 4 27.78 21.21 2.67 o 2 3 4 71.09 113.54 5.62 o 3 3 4 40.57 51.67 2.81 o 4 3 4 91.89 93.10 5.17 o 5 3 4 0.84 0.16 0.94 o 6 3 4 235.85 227.00 7.89 o 7 3 4 60.52 57.36 4.73 o 8 3 4 40.04 37.60 6.41 o 9 3 4 0.02 2.04 1.55 o -8 4 4 18.11 18.80 2.25 o -7 4 4 94.04 106.79 8.71 o -6 4 4 4.00 2.68 1.28 o -5 4 4 12.93 13.78 2.01 o -4 4 4 19.65 22.74 4.87 o -3 4 4 290.37 306.53 21.23 o -2 4 4 420.65 379.43 15.02 o -1 4 4 302.85 282.01 11.44 o 0 4 4 844.18 849.62 37.31 o 1 4 4 251.34 233.87 11.31 o 2 4 4 377.01 396.51 17.97 o 3 4 4 139.00 141.37 7.38 o 4 4 4 0.90 -0.26 1.11 o 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2 25 95.32 90.94 4.65 o -1 2 25 175.43 181.78 7.86 o 0 2 25 387.25 418.89 22.99 o 1 2 25 162.39 173.47 8.82 o 2 2 25 65.77 62.55 4.42 o 3 2 25 7.26 12.59 1.78 o -2 3 25 11.84 12.85 1.84 o -1 3 25 17.12 15.89 1.96 o 0 3 25 5.78 5.38 1.56 o 1 3 25 84.47 83.46 5.08 o -5 0 26 117.39 116.74 9.14 o -4 0 26 356.86 397.61 25.42 o -3 0 26 31.55 24.60 3.58 o -2 0 26 24.46 25.40 3.68 o -1 0 26 71.74 74.17 6.43 o 0 0 26 266.82 287.00 18.92 o 1 0 26 443.35 472.82 29.92 o 2 0 26 190.71 160.31 11.80 o 3 0 26 231.50 210.97 14.94 o -4 1 26 861.56 892.72 41.41 o -3 1 26 139.07 148.77 7.30 o -2 1 26 47.48 47.19 3.41 o -1 1 26 0.76 0.00 0.94 o 0 1 26 102.90 104.53 5.86 o 1 1 26 164.17 154.91 6.45 o 2 1 26 6.82 4.00 1.28 o 3 1 26 412.61 458.94 16.84 o -3 2 26 86.94 86.99 4.52 o -2 2 26 0.00 0.22 1.00 o -1 2 26 1.73 0.90 1.13 o 0 2 26 66.62 75.70 4.21 o 1 2 26 6.90 8.24 1.91 o 2 2 26 107.57 108.24 5.10 o -3 1 27 164.97 173.01 12.50 o -2 1 27 104.09 106.06 4.66 o -1 1 27 25.36 33.53 4.06 o 0 1 27 20.61 22.03 2.51 o 1 1 27 181.64 185.65 13.30 o 2 1 27 120.61 136.67 7.44 o -2 2 27 68.62 75.25 4.19 o -1 2 27 8.30 10.24 1.66 o 0 2 27 104.40 108.19 5.36 o -3 0 28 138.80 142.08 10.59 o -2 0 28 25.21 20.41 3.35 o -1 0 28 154.12 144.90 10.76 o 0 0 28 44.54 47.58 5.10 o 1 0 28 1.23 2.37 1.87 o -2 1 28 17.97 17.89 1.73 o -1 1 28 271.76 286.35 13.45 o 0 1 28 282.01 288.09 13.58 o