#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181291 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236952.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236952_Fobs loop_ _publ_author_name 'Samshuddin, Seranthimata' 'Narayana, Badiadka' 'Yathirajan, Hemmige S.' 'Gerber, Thomas' 'Hosten, Eric' 'Betz, Richard' _publ_section_title ; 4-Methoxy-4-methyl-6-phenyl-1,3-diazinane-2-thione ; _journal_coeditor_code LH5545 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3271 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 111.719 _cell_angle_gamma 90.000 _cell_length_a 10.1894 _cell_length_b 14.6889 _cell_length_c 9.2026 _exptl_crystal_F_000 504.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file lh5545Isup3.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' ca174_ma in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 88.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 26.87 17.96 2.24 o 2 0 0 548.02 501.88 3.24 o 3 0 0 36.62 37.00 0.43 o 4 0 0 463.94 506.63 3.91 o 5 0 0 8.89 4.46 0.30 o 6 0 0 47.62 71.50 0.97 o 7 0 0 6.60 7.33 0.46 o 8 0 0 67.88 66.37 1.06 o 9 0 0 612.01 612.77 6.18 o 10 0 0 669.21 653.27 9.80 o 11 0 0 4.29 3.32 1.16 o 12 0 0 90.59 83.02 2.74 o 2 1 0 4912.21 4815.27 23.06 o 3 1 0 472.27 486.66 2.14 o 4 1 0 34.52 46.00 0.53 o 5 1 0 45.07 32.04 0.42 o 6 1 0 668.47 672.11 3.72 o 7 1 0 157.89 150.13 1.14 o 8 1 0 1.76 1.11 0.30 o 9 1 0 571.93 535.29 6.79 o 10 1 0 172.44 166.71 2.40 o 11 1 0 146.77 141.49 2.49 o 12 1 0 44.79 53.59 1.70 o 0 2 0 1923.81 1933.66 15.07 o 1 2 0 5463.82 5092.95 45.32 o 2 2 0 103.48 114.17 0.63 o 3 2 0 39.70 40.87 0.51 o 4 2 0 215.68 209.46 1.29 o 5 2 0 124.13 154.23 1.18 o 6 2 0 138.10 156.71 1.25 o 7 2 0 2.50 2.50 0.29 o 8 2 0 35.67 35.81 0.72 o 9 2 0 166.28 161.67 1.91 o 10 2 0 0.53 0.61 0.47 o 11 2 0 0.29 0.11 0.50 o 12 2 0 0.56 1.07 0.88 o 1 3 0 2272.70 2332.57 10.61 o 2 3 0 6025.08 5840.68 26.14 o 3 3 0 2571.22 2557.88 13.54 o 4 3 0 0.12 -0.14 0.14 o 5 3 0 155.33 144.68 1.14 o 6 3 0 284.29 271.02 1.91 o 7 3 0 304.22 301.69 2.57 o 8 3 0 301.64 306.78 2.25 o 9 3 0 25.36 29.27 0.89 o 10 3 0 1.61 1.60 0.50 o 11 3 0 183.12 180.10 2.26 o 12 3 0 57.50 62.83 1.19 o 1 4 0 6184.31 6112.30 29.14 o 2 4 0 2032.66 1985.39 10.11 o 3 4 0 55.96 67.77 0.60 o 4 4 0 341.37 397.59 1.97 o 5 4 0 442.64 446.96 2.83 o 6 4 0 105.19 130.99 1.14 o 7 4 0 173.93 173.09 1.44 o 8 4 0 29.10 30.00 0.66 o 9 4 0 1038.55 1034.17 7.16 o 10 4 0 30.98 30.37 0.88 o 11 4 0 2.20 1.02 0.49 o 12 4 0 7.83 8.83 0.63 o 1 5 0 445.62 498.15 2.48 o 2 5 0 25.05 27.00 0.38 o 3 5 0 760.58 823.19 4.80 o 4 5 0 52.20 44.45 0.77 o 5 5 0 23.99 27.99 0.62 o 6 5 0 255.34 256.49 1.71 o 7 5 0 71.41 75.24 0.83 o 8 5 0 264.17 262.44 2.08 o 9 5 0 6.25 4.80 0.51 o 10 5 0 1.30 1.06 0.46 o 11 5 0 13.13 9.38 0.63 o 12 5 0 5.16 4.62 0.59 o 0 6 0 2128.21 2268.15 14.76 o 1 6 0 19.10 17.84 0.34 o 2 6 0 389.28 411.23 2.30 o 3 6 0 35.31 33.16 0.47 o 4 6 0 180.54 187.77 1.26 o 5 6 0 2.22 5.85 0.33 o 6 6 0 68.75 66.88 0.74 o 7 6 0 138.13 142.35 1.35 o 8 6 0 204.86 205.37 1.98 o 9 6 0 26.94 29.38 1.25 o 10 6 0 31.01 28.34 0.90 o 11 6 0 60.30 64.18 1.22 o 12 6 0 0.91 0.78 0.55 o 1 7 0 329.64 347.93 1.85 o 2 7 0 899.13 979.33 5.17 o 3 7 0 873.73 919.92 4.92 o 4 7 0 434.54 455.25 2.63 o 5 7 0 524.29 503.41 3.57 o 6 7 0 237.60 230.68 2.01 o 7 7 0 228.34 237.31 1.91 o 8 7 0 0.14 0.20 0.41 o 9 7 0 30.10 25.22 0.81 o 10 7 0 101.17 94.42 1.38 o 11 7 0 14.28 12.33 0.84 o 0 8 0 4367.26 4409.67 32.84 o 2 8 0 754.61 805.48 4.74 o 3 8 0 225.25 200.99 1.34 o 4 8 0 1.07 0.05 0.22 o 5 8 0 14.74 15.22 0.56 o 6 8 0 92.71 81.59 0.95 o 7 8 0 35.80 30.20 0.80 o 8 8 0 125.77 120.69 1.47 o 9 8 0 251.24 259.72 2.84 o 10 8 0 8.57 7.34 0.70 o 11 8 0 4.99 3.46 0.79 o 1 9 0 165.55 176.93 1.50 o 2 9 0 0.54 0.44 0.21 o 3 9 0 718.49 743.61 4.49 o 4 9 0 190.83 177.51 1.57 o 5 9 0 519.77 469.61 3.08 o 6 9 0 91.46 93.60 1.03 o 7 9 0 269.30 258.14 2.32 o 8 9 0 52.66 52.78 1.19 o 9 9 0 4.42 6.71 0.68 o 10 9 0 36.28 31.76 1.13 o 11 9 0 79.39 82.23 1.69 o 0 10 0 228.62 224.27 2.07 o 1 10 0 314.85 329.23 2.17 o 2 10 0 2.38 3.27 0.27 o 3 10 0 675.66 676.89 4.18 o 4 10 0 47.34 48.04 1.11 o 5 10 0 18.39 20.11 0.66 o 6 10 0 851.46 856.80 5.43 o 7 10 0 230.46 214.65 2.39 o 8 10 0 5.76 6.69 0.62 o 9 10 0 0.64 0.86 0.54 o 10 10 0 66.11 70.71 1.49 o 1 11 0 7.06 9.96 0.59 o 2 11 0 25.01 27.62 0.67 o 3 11 0 418.81 422.85 2.83 o 4 11 0 447.59 476.85 3.15 o 5 11 0 471.58 477.17 3.20 o 6 11 0 240.32 219.67 3.01 o 7 11 0 25.10 25.96 0.94 o 8 11 0 0.08 0.07 0.61 o 9 11 0 0.02 -0.55 0.55 o 10 11 0 1.53 2.05 0.70 o 0 12 0 390.88 390.93 4.19 o 1 12 0 63.86 64.81 0.92 o 2 12 0 67.91 58.31 0.87 o 3 12 0 143.20 136.40 1.26 o 4 12 0 11.01 8.11 0.87 o 5 12 0 8.93 4.90 0.57 o 6 12 0 168.81 153.95 1.94 o 7 12 0 8.75 5.78 0.62 o 8 12 0 35.61 35.82 1.14 o 9 12 0 28.40 26.48 1.09 o 1 13 0 282.86 273.67 2.29 o 2 13 0 28.10 27.65 0.64 o 3 13 0 4.25 2.41 0.40 o 4 13 0 237.57 229.04 2.43 o 5 13 0 268.66 248.09 2.63 o 6 13 0 19.78 19.22 1.67 o 7 13 0 12.51 11.58 0.74 o 8 13 0 51.37 49.57 2.15 o 9 13 0 164.17 183.35 2.42 o 0 14 0 197.87 178.75 4.19 o 1 14 0 247.67 233.29 2.08 o 2 14 0 372.51 376.15 2.99 o 3 14 0 210.52 206.64 2.92 o 4 14 0 0.02 -0.06 0.56 o 5 14 0 10.91 10.57 0.67 o 6 14 0 218.16 215.43 2.50 o 7 14 0 119.34 118.35 1.78 o 8 14 0 77.58 84.24 1.95 o 1 15 0 0.07 0.52 0.39 o 2 15 0 14.70 14.01 1.23 o 3 15 0 70.46 83.63 1.50 o 4 15 0 94.90 91.98 1.47 o 5 15 0 215.55 215.60 2.68 o 6 15 0 21.26 23.27 1.00 o 7 15 0 4.20 4.28 0.66 o 8 15 0 104.54 120.16 3.04 o 0 16 0 19.43 24.66 1.66 o 1 16 0 88.48 80.93 1.40 o 2 16 0 9.45 5.69 0.77 o 3 16 0 4.76 5.21 0.62 o 4 16 0 7.89 7.44 0.59 o 5 16 0 38.60 37.85 1.13 o 6 16 0 22.50 23.76 1.01 o 7 16 0 43.43 44.89 1.65 o 1 17 0 44.88 41.39 1.87 o 2 17 0 0.31 0.49 1.08 o 3 17 0 20.86 15.72 1.08 o 4 17 0 232.60 235.23 2.43 o 5 17 0 80.91 83.24 1.37 o 6 17 0 0.19 -0.15 0.60 o 0 18 0 2.11 0.83 1.00 o 1 18 0 21.15 26.01 1.26 o 2 18 0 123.34 114.31 2.62 o 3 18 0 98.74 105.72 3.40 o 4 18 0 7.36 7.08 0.87 o 1 19 0 1.81 1.12 0.76 o 2 19 0 1.09 0.83 1.08 o 3 19 0 86.30 97.50 2.14 o -12 1 1 9.21 7.38 0.91 o -11 1 1 1.62 2.22 0.55 o -10 1 1 346.44 341.91 4.49 o -9 1 1 488.16 464.85 3.49 o -8 1 1 33.63 35.67 0.58 o -7 1 1 7.94 10.79 0.41 o -6 1 1 33.26 33.65 0.71 o -5 1 1 158.32 169.57 1.14 o -4 1 1 577.02 608.10 3.04 o -3 1 1 1019.41 1134.30 4.39 o -2 1 1 3382.73 3121.35 12.75 o -1 1 1 139.28 159.23 0.92 o 1 1 1 2152.22 2110.38 9.56 o 2 1 1 1678.57 1699.52 7.78 o 3 1 1 2017.98 2055.36 13.26 o 4 1 1 2731.39 2836.08 16.45 o 5 1 1 145.38 131.66 1.20 o 6 1 1 242.02 237.96 1.69 o 7 1 1 17.14 16.74 0.50 o 8 1 1 0.19 0.33 0.33 o 9 1 1 6.43 4.25 0.43 o 10 1 1 43.75 38.92 1.09 o 11 1 1 0.01 0.76 0.61 o 12 1 1 55.32 52.28 1.26 o -12 2 1 52.47 55.79 1.39 o -11 2 1 92.76 82.06 1.43 o -10 2 1 6.48 5.79 0.60 o -9 2 1 144.71 143.03 3.64 o -8 2 1 506.52 519.34 3.80 o -7 2 1 173.93 173.19 1.41 o -6 2 1 2803.81 2850.26 16.45 o -5 2 1 64.07 58.78 0.64 o -4 2 1 31.51 28.07 0.58 o -3 2 1 164.35 160.90 0.87 o -2 2 1 655.83 718.41 3.07 o -1 2 1 810.91 734.77 3.98 o 0 2 1 2776.19 2634.99 13.75 o 2 2 1 2507.54 2493.13 11.37 o 3 2 1 877.79 888.68 4.03 o 4 2 1 5.67 7.03 0.24 o 5 2 1 544.05 592.54 3.28 o 6 2 1 162.64 183.68 1.40 o 7 2 1 469.91 453.30 2.97 o 8 2 1 165.33 163.07 1.46 o 9 2 1 18.58 16.11 0.65 o 10 2 1 238.97 234.75 2.19 o 11 2 1 214.84 219.53 2.68 o 12 2 1 23.50 24.50 1.03 o -12 3 1 8.42 7.26 0.65 o -11 3 1 14.04 14.91 1.58 o -10 3 1 126.37 126.64 3.28 o -9 3 1 7.50 6.32 0.56 o -8 3 1 1.03 0.58 0.30 o -7 3 1 205.11 201.99 1.59 o -6 3 1 106.66 111.69 1.31 o -5 3 1 1031.34 1034.69 5.52 o -4 3 1 1000.36 983.13 4.81 o -3 3 1 10.35 10.19 0.22 o -2 3 1 1824.81 1934.38 9.52 o -1 3 1 2071.01 2053.63 10.06 o 0 3 1 644.57 627.93 3.03 o 1 3 1 1391.42 1354.78 6.78 o 2 3 1 1121.10 1122.11 5.09 o 3 3 1 2523.92 2698.92 14.47 o 4 3 1 3150.55 3516.08 17.79 o 5 3 1 346.62 358.10 1.97 o 6 3 1 52.39 53.71 0.63 o 7 3 1 11.09 13.50 0.57 o 8 3 1 18.48 21.89 0.93 o 9 3 1 4.10 5.91 0.47 o 10 3 1 18.77 17.27 0.83 o 11 3 1 10.68 11.59 0.67 o 12 3 1 11.25 10.16 0.91 o -12 4 1 23.20 23.13 0.88 o -11 4 1 5.36 5.06 0.59 o -10 4 1 64.28 63.30 1.26 o -9 4 1 39.02 40.76 1.03 o -8 4 1 384.52 381.86 2.67 o -7 4 1 139.32 146.27 1.65 o -6 4 1 271.19 309.63 1.94 o -5 4 1 268.56 273.00 1.70 o -4 4 1 72.36 84.65 0.76 o -3 4 1 202.96 221.57 1.34 o -2 4 1 111.20 117.95 1.32 o -1 4 1 69.37 70.00 0.49 o 0 4 1 5.21 7.64 0.19 o 1 4 1 664.25 664.58 3.50 o 2 4 1 1335.10 1382.72 6.69 o 3 4 1 353.72 329.94 1.91 o 4 4 1 227.76 289.31 1.75 o 5 4 1 477.30 474.59 2.53 o 6 4 1 22.23 25.42 0.49 o 7 4 1 4.10 5.14 0.36 o 8 4 1 27.58 28.48 0.72 o 9 4 1 119.55 125.47 1.56 o 10 4 1 0.05 -0.31 0.42 o 11 4 1 9.69 10.84 0.67 o -12 5 1 39.14 36.64 1.53 o -11 5 1 35.94 39.37 1.04 o -10 5 1 276.31 271.45 2.87 o -9 5 1 401.77 381.17 4.79 o -8 5 1 45.03 46.95 0.79 o -7 5 1 10.97 11.57 0.46 o -6 5 1 23.85 24.54 0.48 o -5 5 1 685.62 649.67 3.60 o -4 5 1 48.94 33.04 1.05 o -3 5 1 403.28 346.54 1.99 o -2 5 1 440.28 416.81 2.30 o -1 5 1 1146.16 1137.48 5.47 o 0 5 1 69.07 72.54 0.47 o 1 5 1 92.38 100.67 0.69 o 2 5 1 167.84 195.93 1.57 o 3 5 1 4251.26 4404.67 29.97 o 4 5 1 925.81 859.75 4.64 o 5 5 1 327.61 327.84 1.87 o 6 5 1 22.09 19.48 0.54 o 7 5 1 53.32 48.13 0.77 o 8 5 1 85.56 81.83 1.47 o 9 5 1 13.03 16.09 0.67 o 10 5 1 45.73 51.60 1.04 o 11 5 1 20.17 22.05 0.83 o -12 6 1 7.21 7.22 1.14 o -11 6 1 131.32 140.40 4.38 o -10 6 1 36.48 35.43 0.94 o -9 6 1 3.41 2.84 0.47 o -8 6 1 364.39 350.80 2.34 o -7 6 1 432.46 427.32 2.65 o -6 6 1 167.72 149.39 1.09 o -5 6 1 244.52 232.97 1.68 o -4 6 1 108.88 79.34 0.78 o -3 6 1 297.83 333.47 2.48 o -2 6 1 862.67 930.20 4.90 o -1 6 1 971.82 1054.57 4.75 o 0 6 1 577.25 582.98 2.89 o 1 6 1 417.81 430.90 2.38 o 2 6 1 693.83 681.32 3.65 o 3 6 1 912.44 947.10 5.02 o 4 6 1 5.09 2.87 0.25 o 5 6 1 173.96 193.98 1.37 o 6 6 1 0.24 1.61 0.29 o 7 6 1 126.48 131.76 1.30 o 8 6 1 122.05 113.26 1.39 o 9 6 1 38.27 39.23 0.96 o 10 6 1 146.63 150.64 1.76 o 11 6 1 15.54 15.20 0.75 o -12 7 1 141.31 155.35 2.32 o -11 7 1 57.67 53.71 1.38 o -10 7 1 70.47 70.38 2.17 o -9 7 1 38.21 45.27 1.09 o -8 7 1 30.18 29.88 0.65 o -7 7 1 44.79 41.85 0.63 o -6 7 1 181.99 179.26 1.33 o -5 7 1 373.77 354.88 2.67 o -4 7 1 171.33 208.70 1.52 o -3 7 1 173.10 198.23 1.43 o -2 7 1 170.01 189.16 1.49 o -1 7 1 490.53 483.60 2.46 o 0 7 1 664.48 710.05 3.79 o 1 7 1 132.02 154.27 0.93 o 2 7 1 274.99 288.73 1.87 o 3 7 1 0.55 0.26 0.17 o 4 7 1 34.07 30.89 0.55 o 5 7 1 39.33 42.01 0.65 o 6 7 1 22.36 19.16 0.62 o 7 7 1 1.59 2.50 0.37 o 8 7 1 1.38 2.28 0.48 o 9 7 1 65.91 68.36 1.40 o 10 7 1 0.38 0.84 0.48 o 11 7 1 26.92 28.04 1.01 o -11 8 1 174.28 174.90 2.38 o -10 8 1 35.88 37.43 1.15 o -9 8 1 116.62 113.97 1.74 o -8 8 1 167.01 161.44 1.72 o -7 8 1 0.29 0.10 0.36 o -6 8 1 251.29 234.74 1.66 o -5 8 1 31.40 25.59 0.84 o -4 8 1 229.38 229.33 1.68 o -3 8 1 14.07 11.44 0.47 o -2 8 1 160.87 146.93 1.26 o -1 8 1 0.50 2.65 0.23 o 0 8 1 357.17 326.64 1.90 o 1 8 1 1830.70 1854.52 10.03 o 2 8 1 490.88 473.98 2.92 o 3 8 1 100.11 100.18 0.82 o 4 8 1 9.13 6.91 0.27 o 5 8 1 2.15 2.25 0.30 o 6 8 1 0.98 -0.33 0.33 o 7 8 1 57.32 45.60 0.96 o 8 8 1 146.03 137.56 1.97 o 9 8 1 40.38 42.39 0.96 o 10 8 1 5.67 5.20 0.55 o 11 8 1 37.87 37.08 1.22 o -11 9 1 87.48 91.88 2.26 o -10 9 1 65.27 67.11 1.48 o -9 9 1 77.33 72.77 1.39 o -8 9 1 17.27 16.82 1.08 o -7 9 1 6.76 5.05 0.55 o -6 9 1 170.55 172.58 1.48 o -5 9 1 55.86 69.98 0.84 o -4 9 1 380.74 335.52 2.30 o -3 9 1 1014.70 1002.26 6.04 o -2 9 1 304.46 291.37 2.40 o -1 9 1 393.79 399.28 2.52 o 0 9 1 294.60 285.55 1.73 o 1 9 1 64.60 56.99 0.54 o 2 9 1 542.72 531.70 3.27 o 3 9 1 2.02 1.84 0.22 o 4 9 1 765.76 725.25 4.05 o 5 9 1 2.97 3.98 0.54 o 6 9 1 238.50 238.05 2.14 o 7 9 1 289.71 261.16 2.68 o 8 9 1 48.68 46.97 0.97 o 9 9 1 23.75 19.51 0.96 o 10 9 1 0.02 0.51 0.60 o -11 10 1 2.10 2.19 0.69 o -10 10 1 79.22 84.18 2.31 o -9 10 1 3.31 2.30 0.60 o -8 10 1 3.98 5.07 0.60 o -7 10 1 1.72 0.49 0.40 o -6 10 1 974.19 917.60 6.30 o -5 10 1 319.78 327.53 2.34 o -4 10 1 101.31 104.02 1.04 o -3 10 1 129.00 123.91 1.11 o -2 10 1 36.02 45.96 0.70 o -1 10 1 138.14 157.84 1.38 o 0 10 1 70.45 78.17 0.79 o 1 10 1 93.15 107.80 0.81 o 2 10 1 15.88 14.31 0.40 o 3 10 1 41.89 42.91 1.03 o 4 10 1 186.51 191.10 1.38 o 5 10 1 15.20 12.26 0.95 o 6 10 1 9.63 10.77 0.54 o 7 10 1 1.66 2.20 0.52 o 8 10 1 15.96 12.32 0.72 o 9 10 1 13.66 13.66 0.85 o 10 10 1 109.28 107.30 1.83 o -10 11 1 44.06 41.05 1.23 o -9 11 1 2.40 1.50 0.60 o -8 11 1 0.38 0.09 0.52 o -7 11 1 7.01 6.25 0.61 o -6 11 1 22.62 15.91 0.67 o -5 11 1 46.81 45.79 1.01 o -4 11 1 97.09 93.29 1.02 o -3 11 1 96.67 96.31 0.99 o -2 11 1 183.44 175.28 1.57 o -1 11 1 31.31 25.71 0.59 o 0 11 1 1.73 1.45 0.29 o 1 11 1 0.27 0.63 0.27 o 2 11 1 26.69 21.70 0.54 o 3 11 1 1481.14 1511.80 9.80 o 4 11 1 899.22 895.48 5.44 o 5 11 1 40.25 42.36 0.87 o 6 11 1 125.85 119.17 1.66 o 7 11 1 20.32 21.99 0.93 o 8 11 1 24.45 23.01 1.03 o 9 11 1 5.29 4.86 0.68 o -10 12 1 3.08 1.20 0.68 o -9 12 1 127.99 128.80 2.22 o -8 12 1 5.49 4.98 0.65 o -7 12 1 33.88 33.29 1.05 o -6 12 1 2.50 1.61 0.51 o -5 12 1 821.64 835.98 5.80 o -4 12 1 1.76 1.65 0.40 o -3 12 1 56.61 56.89 0.89 o -2 12 1 6.67 6.24 0.39 o -1 12 1 282.26 275.90 2.26 o 0 12 1 1117.18 1081.98 6.39 o 1 12 1 248.35 255.66 1.85 o 2 12 1 3.67 4.79 0.39 o 3 12 1 2.49 0.50 0.33 o 4 12 1 170.99 160.11 2.47 o 5 12 1 21.09 19.91 0.90 o 6 12 1 8.89 9.16 0.71 o 7 12 1 37.87 29.71 0.99 o 8 12 1 45.34 45.32 1.23 o 9 12 1 166.84 179.08 2.41 o -9 13 1 4.42 4.03 0.72 o -8 13 1 0.36 -0.57 0.57 o -7 13 1 2.09 1.12 0.57 o -6 13 1 1.93 1.36 0.52 o -5 13 1 145.53 136.57 1.50 o -4 13 1 50.56 49.08 0.90 o -3 13 1 4.53 5.92 0.43 o -2 13 1 428.97 422.30 3.72 o -1 13 1 355.13 359.89 2.83 o 0 13 1 35.87 41.34 0.82 o 1 13 1 364.59 345.80 2.72 o 2 13 1 0.01 0.10 0.36 o 3 13 1 101.94 93.49 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