#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:32 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181291 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/69/2236953.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2236953_Fobs loop_ _publ_author_name 'Singh, Durga P.' 'Pratap, Seema' 'Gupta, Sushil K.' 'Butcher, Ray J.' _publ_section_title ; 3-[(Furan-2-yl)carbonyl]-1-(pyrimidin-2-yl)thiourea ; _journal_coeditor_code LH5548 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3300 _journal_page_last o3301 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 95.559 _cell_angle_gamma 90.000 _cell_length_a 5.6962 _cell_length_b 21.0530 _cell_length_c 8.7901 _exptl_crystal_F_000 512.00 _reflns_d_resolution_high 0.8070 _cod_data_source_file lh5548Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 3(III) in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 211.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 3221.83 3669.81 23.77 o 4 0 0 484.20 407.94 45.33 o 6 0 0 594.00 626.31 9.55 o 1 1 0 97.69 94.69 1.56 o 3 1 0 15.93 25.48 1.15 o 4 1 0 18.48 18.63 1.26 o 5 1 0 277.53 288.27 6.18 o 6 1 0 16.46 13.22 1.06 o 0 2 0 1200.09 1398.95 14.20 o 1 2 0 335.97 362.82 2.53 o 2 2 0 1928.49 1992.65 16.12 o 3 2 0 1910.77 2029.23 28.94 o 4 2 0 1479.87 1425.96 68.08 o 5 2 0 59.46 49.97 1.78 o 6 2 0 7.74 5.42 0.88 o 1 3 0 1418.84 1518.15 9.72 o 3 3 0 12.64 5.25 0.45 o 4 3 0 1002.73 882.44 22.44 o 5 3 0 0.63 0.40 0.52 o 6 3 0 77.51 72.46 3.06 o 0 4 0 695.39 773.29 17.40 o 1 4 0 3770.14 3912.47 23.52 o 2 4 0 31.73 35.52 0.84 o 3 4 0 408.25 350.54 7.20 o 4 4 0 194.55 152.21 6.11 o 5 4 0 38.75 36.35 1.58 o 6 4 0 85.78 94.13 2.81 o 1 5 0 2209.09 2386.39 26.37 o 2 5 0 1800.76 1926.68 24.20 o 3 5 0 1067.71 1129.42 25.16 o 4 5 0 387.00 349.23 7.52 o 5 5 0 11.82 12.69 1.19 o 6 5 0 260.51 293.82 5.98 o 0 6 0 16449.81 16508.93 157.07 o 2 6 0 96.07 87.87 2.76 o 3 6 0 52.23 51.04 1.48 o 4 6 0 363.49 359.72 6.84 o 5 6 0 323.22 301.72 6.10 o 6 6 0 145.53 166.93 4.36 o 1 7 0 1037.76 1087.74 6.75 o 2 7 0 161.37 215.81 4.61 o 3 7 0 1930.05 1991.72 59.25 o 4 7 0 58.02 49.72 1.85 o 5 7 0 432.37 421.96 7.23 o 6 7 0 84.03 89.44 3.31 o 0 8 0 978.37 1020.51 9.70 o 2 8 0 1743.96 1767.54 16.58 o 3 8 0 567.37 507.39 6.87 o 4 8 0 1138.50 1117.11 13.65 o 5 8 0 48.17 46.06 2.35 o 6 8 0 4.63 5.59 0.60 o 1 9 0 102.38 91.54 1.69 o 2 9 0 63.75 71.59 2.05 o 3 9 0 271.84 250.91 4.80 o 4 9 0 1.37 1.27 0.66 o 5 9 0 67.34 71.00 2.79 o 6 9 0 1.12 2.21 0.49 o 0 10 0 2865.61 3035.92 47.39 o 1 10 0 368.39 436.08 5.01 o 2 10 0 1220.57 1354.74 24.73 o 3 10 0 14.81 16.74 1.20 o 4 10 0 1294.39 1266.65 15.01 o 5 10 0 10.14 9.03 1.13 o 6 10 0 135.67 150.92 3.71 o 1 11 0 3.46 2.98 0.41 o 2 11 0 3.96 5.47 0.69 o 3 11 0 199.85 212.81 4.45 o 4 11 0 34.31 30.37 1.90 o 5 11 0 22.08 23.04 2.09 o 6 11 0 167.45 182.56 4.04 o 0 12 0 4527.90 4713.69 74.41 o 1 12 0 127.42 136.40 2.84 o 2 12 0 133.81 130.17 4.69 o 3 12 0 383.36 412.50 14.01 o 4 12 0 0.48 0.05 0.59 o 5 12 0 45.52 40.74 2.21 o 6 12 0 45.51 49.68 2.00 o 1 13 0 13.14 16.44 1.01 o 2 13 0 21.83 22.32 1.30 o 3 13 0 1569.58 1607.96 14.03 o 4 13 0 37.35 38.09 2.09 o 5 13 0 41.06 44.77 2.21 o 6 13 0 5.57 3.66 0.92 o 0 14 0 316.96 383.90 22.21 o 1 14 0 8.96 13.86 1.07 o 2 14 0 0.38 1.72 0.46 o 3 14 0 1849.46 1822.86 17.62 o 4 14 0 7.15 10.40 1.32 o 5 14 0 431.93 444.87 8.69 o 1 15 0 1.56 1.79 0.41 o 2 15 0 2.32 0.92 0.53 o 3 15 0 225.52 215.86 3.83 o 4 15 0 80.49 61.77 3.23 o 5 15 0 22.29 26.51 2.58 o 0 16 0 551.76 620.98 10.69 o 1 16 0 3.68 2.93 0.54 o 2 16 0 91.55 87.84 2.73 o 3 16 0 13.55 13.55 0.99 o 4 16 0 451.92 393.65 13.05 o 5 16 0 62.48 68.46 4.81 o 1 17 0 2198.85 2078.11 24.23 o 2 17 0 39.34 35.00 1.71 o 3 17 0 22.06 20.09 1.33 o 4 17 0 412.36 346.35 10.30 o 5 17 0 185.07 208.91 16.94 o 0 18 0 1320.44 1402.93 114.94 o 1 18 0 2.18 2.44 0.79 o 2 18 0 5.71 5.86 0.95 o 3 18 0 137.50 134.86 3.01 o 4 18 0 14.29 12.91 1.39 o 5 18 0 23.30 20.15 1.83 o 1 19 0 192.98 177.08 5.58 o 2 19 0 91.93 92.45 2.83 o 3 19 0 18.82 17.63 1.37 o 4 19 0 2.47 2.90 0.79 o 0 20 0 194.37 184.54 8.70 o 1 20 0 289.15 280.04 5.98 o 2 20 0 288.21 291.79 6.07 o 3 20 0 127.76 131.48 3.36 o 4 20 0 6.61 6.31 0.79 o 1 21 0 34.87 35.47 1.93 o 2 21 0 32.09 34.34 3.66 o 3 21 0 22.47 20.39 1.48 o 4 21 0 57.97 74.64 3.21 o 0 22 0 88.62 88.84 5.50 o 1 22 0 66.37 68.99 3.39 o 2 22 0 450.00 474.45 9.05 o 3 22 0 196.68 212.20 13.28 o 1 23 0 343.76 313.51 12.13 o 2 23 0 67.02 76.93 3.24 o 3 23 0 9.00 8.70 1.37 o 0 24 0 195.01 201.82 8.24 o 1 24 0 0.99 0.92 0.65 o 2 24 0 6.00 4.27 0.76 o 1 25 0 0.61 1.03 0.46 o -5 0 1 100.31 102.96 4.95 o -3 0 1 1087.39 1046.83 12.90 o -1 0 1 791.76 777.69 33.43 o 1 0 1 9210.55 8528.44 57.31 o 3 0 1 404.80 360.41 5.36 o 5 0 1 972.18 945.45 15.11 o -6 1 1 152.73 160.83 3.87 o -5 1 1 95.71 89.11 2.23 o -4 1 1 4.00 4.78 0.63 o -2 1 1 156.23 149.05 2.45 o -1 1 1 1053.53 990.97 14.20 o 0 1 1 3554.72 3392.66 44.88 o 2 1 1 2122.06 2103.35 14.62 o 3 1 1 1549.15 1605.19 27.11 o 4 1 1 147.88 138.68 3.59 o 5 1 1 247.10 237.92 4.10 o 6 1 1 6.38 4.13 0.67 o -6 2 1 257.27 268.06 5.87 o -5 2 1 115.38 112.70 2.78 o -4 2 1 463.57 439.09 12.14 o -3 2 1 505.74 530.50 10.82 o -2 2 1 3923.00 3959.37 54.15 o -1 2 1 6028.65 5719.22 32.43 o 0 2 1 371.52 409.35 5.82 o 1 2 1 1012.38 925.82 6.00 o 2 2 1 1797.89 1675.59 20.45 o 3 2 1 2006.27 2040.87 22.85 o 4 2 1 2.15 2.09 0.86 o 5 2 1 38.62 36.68 1.78 o 6 2 1 4.76 4.62 0.67 o -6 3 1 50.69 44.81 2.01 o -5 3 1 809.93 773.66 17.12 o -4 3 1 1932.43 1977.48 39.87 o -3 3 1 882.99 864.95 30.82 o -2 3 1 40.45 42.95 0.89 o -1 3 1 1451.53 1434.39 12.78 o 0 3 1 1998.54 2064.71 21.04 o 1 3 1 3068.37 2841.27 17.36 o 2 3 1 405.94 362.93 6.26 o 3 3 1 2302.48 2422.24 14.44 o 4 3 1 14.68 11.02 1.07 o 5 3 1 90.15 84.60 2.71 o 6 3 1 165.43 174.24 4.81 o -6 4 1 108.62 120.40 4.81 o -5 4 1 20.32 16.35 1.30 o -4 4 1 126.51 112.32 2.73 o -3 4 1 0.90 1.65 0.32 o -2 4 1 553.13 532.14 5.50 o -1 4 1 14604.09 15168.59 100.37 o 0 4 1 391.70 399.40 9.40 o 1 4 1 28.90 30.77 0.93 o 3 4 1 469.24 496.82 7.80 o 4 4 1 212.67 235.73 6.96 o 5 4 1 44.57 43.78 1.92 o 6 4 1 51.12 46.45 2.41 o -6 5 1 18.95 16.96 1.62 o -5 5 1 1001.68 931.66 11.42 o -4 5 1 4.22 5.87 0.78 o -3 5 1 1939.17 1996.04 51.16 o -2 5 1 45.10 54.16 1.45 o -1 5 1 44820.95 45108.42 695.81 o 0 5 1 381.03 417.24 3.16 o 1 5 1 2935.62 3238.24 44.76 o 2 5 1 116.76 143.69 2.59 o 3 5 1 1223.30 1242.60 18.44 o 4 5 1 55.03 66.07 5.04 o 5 5 1 546.46 536.76 8.65 o 6 5 1 73.28 70.09 2.91 o -6 6 1 161.17 172.16 8.70 o -5 6 1 8.10 7.60 0.92 o -4 6 1 76.77 80.63 2.63 o -3 6 1 4.65 4.41 0.47 o -1 6 1 1268.70 1584.97 8.04 o 0 6 1 170.05 170.15 2.82 o 1 6 1 23.88 27.50 0.86 o 2 6 1 83.87 118.09 1.66 o 3 6 1 31.87 41.08 1.30 o 4 6 1 97.34 99.91 2.98 o 5 6 1 199.11 192.43 7.90 o 6 6 1 4.58 5.53 0.97 o -6 7 1 62.30 63.46 2.91 o -5 7 1 263.60 263.12 5.61 o -4 7 1 321.93 318.15 4.89 o -3 7 1 312.89 303.95 5.52 o -2 7 1 0.26 2.03 0.37 o -1 7 1 4939.15 5531.38 69.22 o 0 7 1 466.02 529.86 7.40 o 1 7 1 640.66 755.40 9.75 o 2 7 1 2872.11 3269.05 36.25 o 3 7 1 192.13 224.28 7.78 o 4 7 1 222.80 203.34 4.24 o 5 7 1 8.76 9.09 1.20 o 6 7 1 70.24 77.77 3.06 o -6 8 1 59.83 58.39 2.59 o -5 8 1 549.54 537.39 11.22 o -4 8 1 403.22 423.58 9.85 o -3 8 1 90.74 88.35 2.24 o -1 8 1 1152.05 1392.23 17.29 o 0 8 1 500.23 562.04 6.66 o 1 8 1 146.99 173.01 3.11 o 3 8 1 86.29 85.68 2.34 o 4 8 1 4.26 4.21 0.64 o 5 8 1 3.00 1.95 0.67 o 6 8 1 4.77 5.50 0.97 o -6 9 1 75.40 76.76 2.91 o -5 9 1 99.89 90.42 3.15 o -4 9 1 2960.55 2747.51 93.39 o -3 9 1 132.72 148.03 3.25 o -2 9 1 926.38 1042.41 9.57 o -1 9 1 318.90 355.64 7.40 o 0 9 1 49.45 47.92 1.28 o 1 9 1 66.43 74.97 2.39 o 2 9 1 1.67 1.72 0.57 o 3 9 1 136.22 151.53 5.73 o 4 9 1 223.69 214.48 5.32 o 5 9 1 69.20 59.60 3.12 o 6 9 1 383.39 432.59 18.77 o -6 10 1 29.95 29.65 1.48 o -5 10 1 92.64 94.70 3.15 o -4 10 1 249.63 237.80 12.03 o -3 10 1 22.18 27.93 1.53 o -1 10 1 346.98 364.95 5.04 o 0 10 1 9.61 12.59 0.61 o 1 10 1 592.79 606.96 6.54 o 2 10 1 406.82 460.42 10.41 o 3 10 1 444.10 395.70 11.02 o 4 10 1 2.38 4.66 0.94 o 5 10 1 313.67 302.67 11.76 o 6 10 1 66.49 83.34 4.35 o -6 11 1 108.77 104.81 8.26 o -5 11 1 661.67 667.39 11.28 o -4 11 1 67.22 61.33 3.06 o -3 11 1 54.75 53.45 2.27 o -2 11 1 122.86 139.30 4.94 o -1 11 1 3499.99 3850.92 40.82 o 0 11 1 167.65 182.92 2.50 o 1 11 1 83.63 84.35 2.15 o 2 11 1 635.10 663.61 10.17 o 3 11 1 140.38 156.30 5.04 o 4 11 1 401.52 378.92 7.13 o 5 11 1 13.81 13.87 1.49 o 6 11 1 20.89 28.66 2.75 o -6 12 1 263.26 291.05 5.01 o -5 12 1 101.88 100.64 7.56 o -4 12 1 16.83 13.69 1.16 o -3 12 1 22.14 22.39 1.75 o -2 12 1 1330.02 1426.04 16.94 o -1 12 1 324.78 354.24 6.08 o 0 12 1 3271.81 3569.23 65.29 o 1 12 1 436.80 438.80 6.21 o 2 12 1 529.45 530.48 9.19 o 3 12 1 506.02 503.85 8.10 o 4 12 1 606.39 608.94 9.32 o 5 12 1 122.86 130.49 4.85 o 6 12 1 41.65 55.05 2.29 o -6 13 1 0.48 0.27 0.31 o -5 13 1 406.53 419.05 41.67 o -4 13 1 54.69 54.13 2.37 o -3 13 1 354.04 349.52 7.27 o -2 13 1 666.38 727.23 10.95 o -1 13 1 1181.20 1247.70 10.58 o 0 13 1 79.76 92.34 1.98 o 1 13 1 84.79 78.77 2.27 o 2 13 1 13.08 9.90 1.06 o 3 13 1 77.78 67.91 2.55 o 4 13 1 52.81 49.91 2.10 o 5 13 1 1.92 1.49 0.46 o -5 14 1 130.38 121.15 4.58 o -4 14 1 78.74 73.10 3.51 o -3 14 1 423.13 415.64 6.04 o -2 14 1 153.64 151.77 5.25 o -1 14 1 241.05 253.54 5.08 o 0 14 1 205.24 193.81 4.43 o 1 14 1 0.96 1.99 0.35 o 2 14 1 461.49 468.00 9.05 o 3 14 1 499.30 461.56 7.59 o 4 14 1 7.95 7.01 0.96 o 5 14 1 14.15 19.26 1.39 o -5 15 1 118.81 104.05 3.89 o -4 15 1 171.01 168.60 5.41 o -3 15 1 368.59 345.44 5.51 o -2 15 1 258.85 245.88 6.69 o -1 15 1 894.18 931.23 11.00 o 0 15 1 414.25 508.24 15.85 o 1 15 1 665.17 707.47 9.85 o 2 15 1 17.20 15.17 1.39 o 3 15 1 288.31 284.20 6.43 o 4 15 1 62.01 46.43 3.89 o 5 15 1 0.66 1.53 0.53 o -5 16 1 56.61 60.67 5.50 o -4 16 1 11.89 7.59 1.01 o -3 16 1 322.86 313.33 6.88 o -2 16 1 0.99 1.90 0.67 o -1 16 1 145.77 141.88 3.42 o 0 16 1 77.16 101.21 3.17 o 1 16 1 173.62 183.70 3.98 o 2 16 1 19.62 19.30 1.30 o 3 16 1 313.04 293.66 10.71 o 4 16 1 226.87 197.37 9.62 o 5 16 1 21.19 24.32 1.52 o -5 17 1 9.54 9.70 1.10 o -4 17 1 10.05 9.59 1.26 o -3 17 1 821.82 801.05 9.45 o -2 17 1 121.38 111.47 3.68 o -1 17 1 480.59 428.11 7.54 o 0 17 1 69.15 74.49 2.99 o 1 17 1 161.43 165.46 3.86 o 2 17 1 995.91 928.89 10.77 o 3 17 1 6.84 6.10 0.92 o 4 17 1 357.63 313.79 8.25 o 5 17 1 6.21 6.87 1.37 o -5 18 1 0.31 0.46 0.32 o -4 18 1 16.85 16.24 1.83 o -3 18 1 116.62 107.96 2.72 o -2 18 1 285.13 257.53 5.70 o -1 18 1 19.84 16.00 1.48 o 0 18 1 180.34 178.33 5.98 o 1 18 1 28.26 29.05 1.53 o 2 18 1 430.28 417.87 7.93 o 3 18 1 123.78 122.46 3.48 o 4 18 1 12.20 12.60 1.62 o -4 19 1 14.24 14.07 1.21 o -3 19 1 18.87 18.17 1.42 o -2 19 1 0.04 0.86 0.59 o -1 19 1 150.97 142.53 5.34 o 0 19 1 15.72 15.76 1.76 o 1 19 1 0.52 0.37 0.41 o 2 19 1 1150.62 1148.15 13.02 o 3 19 1 44.54 40.08 2.28 o 4 19 1 551.86 496.02 23.35 o -4 20 1 40.88 39.34 2.26 o -3 20 1 0.14 0.73 0.92 o -2 20 1 0.84 0.46 0.65 o -1 20 1 3.62 4.64 0.79 o 0 20 1 13.90 14.00 1.62 o 1 20 1 108.65 114.07 3.21 o 2 20 1 677.91 679.80 9.41 o 3 20 1 466.71 482.10 9.48 o 4 20 1 3.75 4.21 0.73 o -4 21 1 49.98 53.87 5.27 o -3 21 1 110.72 105.20 4.17 o -2 21 1 31.99 28.91 1.85 o -1 21 1 162.26 155.44 5.15 o 0 21 1 266.50 251.42 6.80 o 1 21 1 3.38 3.66 0.97 o 2 21 1 4.65 6.41 1.10 o 3 21 1 158.07 168.27 4.03 o -3 22 1 108.90 103.71 5.04 o -2 22 1 663.76 672.34 8.87 o -1 22 1 186.85 169.97 7.56 o 0 22 1 342.71 326.09 7.45 o 1 22 1 0.27 0.92 0.86 o 2 22 1 77.57 79.52 3.39 o 3 22 1 68.44 62.08 2.74 o -3 23 1 100.95 120.58 4.58 o -2 23 1 12.58 14.32 1.13 o -1 23 1 231.32 231.08 5.80 o 0 23 1 0.20 0.92 0.37 o 1 23 1 46.55 46.93 2.21 o 2 23 1 13.45 13.28 1.10 o -2 24 1 26.52 32.98 1.94 o -1 24 1 28.32 30.45 1.94 o 0 24 1 143.71 134.28 3.48 o 1 24 1 182.49 185.46 6.41 o 2 24 1 0.76 1.37 0.92 o -1 25 1 218.40 225.70 5.04 o 0 25 1 9.04 6.09 0.67 o 1 25 1 42.18 43.06 1.94 o -6 0 2 1139.56 1252.74 18.09 o -4 0 2 2260.97 2383.50 53.58 o -2 0 2 7007.98 6905.77 61.60 o 0 0 2 209.61 280.88 4.35 o 2 0 2 4480.23 4691.89 36.62 o 4 0 2 578.87 689.51 12.14 o 6 0 2 519.49 496.84 10.99 o -6 1 2 0.24 1.18 0.67 o -5 1 2 162.46 155.61 3.71 o -4 1 2 15.65 13.63 0.93 o -3 1 2 171.38 168.92 5.39 o -2 1 2 1673.70 1833.49 13.02 o -1 1 2 16.88 22.12 1.59 o 0 1 2 6.37 10.46 0.41 o 1 1 2 279.49 294.12 2.44 o 2 1 2 730.47 700.08 8.48 o 3 1 2 72.22 68.85 2.31 o 4 1 2 515.16 535.17 7.44 o 5 1 2 94.07 81.95 2.72 o 6 1 2 144.36 144.45 3.25 o -6 2 2 395.07 430.71 6.87 o -5 2 2 902.63 896.11 9.67 o -4 2 2 55.63 52.23 1.93 o -3 2 2 7.66 6.70 0.61 o -2 2 2 2964.52 3136.94 22.59 o -1 2 2 980.43 1001.45 26.51 o 0 2 2 4396.25 4639.56 51.06 o 1 2 2 555.52 520.64 3.73 o 2 2 2 9.01 12.39 0.52 o 3 2 2 263.36 218.77 4.74 o 4 2 2 32.18 38.56 2.28 o 5 2 2 131.40 126.45 4.36 o 6 2 2 61.49 54.62 1.93 o -6 3 2 188.75 199.21 4.40 o -5 3 2 4.42 3.93 1.37 o -4 3 2 196.36 216.11 3.68 o -3 3 2 785.77 873.13 22.59 o -2 3 2 256.18 275.48 3.56 o -1 3 2 70.31 70.06 2.09 o 0 3 2 2397.75 2375.20 22.66 o 1 3 2 27.28 26.84 0.85 o 2 3 2 14.01 6.00 0.46 o 3 3 2 64.04 70.13 1.92 o 4 3 2 14.22 13.17 1.21 o 5 3 2 13.91 9.46 1.37 o 6 3 2 41.23 49.05 1.93 o -6 4 2 0.55 0.27 0.76 o -5 4 2 1018.19 972.85 14.08 o -4 4 2 330.10 328.13 5.68 o -3 4 2 9.87 5.93 0.51 o -2 4 2 463.03 499.79 11.24 o -1 4 2 200.20 217.17 3.85 o 0 4 2 613.09 691.83 15.07 o 1 4 2 565.77 561.17 5.38 o 2 4 2 303.92 320.14 5.56 o 3 4 2 636.47 622.68 9.06 o 4 4 2 31.96 25.57 1.43 o 5 4 2 202.81 170.02 14.65 o 6 4 2 0.36 1.37 0.65 o -6 5 2 21.09 19.01 1.62 o -5 5 2 610.16 554.40 10.04 o -4 5 2 3.77 1.26 0.46 o -3 5 2 48.70 48.60 1.81 o -2 5 2 61.90 75.92 1.65 o -1 5 2 2537.14 2561.36 50.67 o 0 5 2 6046.51 6434.87 45.89 o 1 5 2 65.17 58.69 1.10 o 2 5 2 650.85 650.90 6.77 o 3 5 2 11.81 15.65 0.97 o 4 5 2 886.65 830.23 10.55 o 5 5 2 191.80 138.50 11.91 o 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