#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/70/2237035.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237035_Fobs loop_ _publ_author_name 'Hamdouni, Noudjoud' 'Brihi, Ouarda' 'Medjroubi, Mohamed Larbi' 'Meinnel, Jean' 'Boudjada, Ali' _publ_section_title ; Iododurene ; _journal_coeditor_code SU2521 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3391 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _audit_creation_date 12-10-17 _audit_creation_method CRYSTALS _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_length_a 5.5099(3) _cell_length_b 11.8839(5) _cell_length_c 15.1704(6) _[local]_cod_data_source_file su2521Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 2 0 0 4569.39 5459.23 78.83 o 4 0 0 -5.19 5.20 3.98 < 6 0 0 705.27 614.00 17.41 o 1 1 0 1862.88 1947.59 25.08 o 2 1 0 5819.46 7026.64 72.18 o 3 1 0 985.95 1077.58 14.17 o 4 1 0 2428.27 2459.94 33.02 o 5 1 0 305.71 302.80 7.04 o 6 1 0 199.34 189.66 6.09 o 7 1 0 22.71 1.75 10.84 < 1 2 0 7733.52 9927.24 129.27 o 2 2 0 4058.48 4402.44 60.72 o 3 2 0 469.71 508.08 7.47 o 4 2 0 -9.28 0.02 3.15 < 5 2 0 360.61 340.15 7.56 o 6 2 0 -1.59 0.01 4.06 < 7 2 0 10.35 16.73 10.68 < 1 3 0 328.25 321.87 5.37 o 2 3 0 2783.45 2785.10 35.80 o 3 3 0 4582.65 4527.84 62.52 o 4 3 0 632.73 636.29 10.93 o 5 3 0 333.79 333.08 7.21 o 6 3 0 8.98 12.44 4.22 < 7 3 0 18.88 10.46 11.92 < 0 4 0 1596.56 1775.75 35.97 o 1 4 0 7919.02 8859.51 112.02 o 2 4 0 -3.14 0.44 2.70 < 3 4 0 897.62 908.35 14.09 o 4 4 0 100.26 96.91 4.11 o 5 4 0 37.63 45.79 4.06 o 6 4 0 5.99 1.60 4.07 < 1 5 0 2641.43 2710.35 36.48 o 2 5 0 483.86 415.53 8.26 o 3 5 0 3579.67 3652.94 49.97 o 4 5 0 119.44 127.60 4.65 o 5 5 0 439.35 371.14 9.08 o 6 5 0 -4.03 0.02 4.62 < 0 6 0 2080.44 1885.82 55.87 o 1 6 0 3910.93 4157.41 58.60 o 2 6 0 648.45 604.16 9.96 o 3 6 0 537.01 546.81 9.08 o 4 6 0 30.56 36.82 4.02 o 5 6 0 36.59 40.41 4.75 o 6 6 0 16.47 8.77 4.49 o 1 7 0 28.08 36.55 2.61 o 2 7 0 1411.48 1402.73 20.65 o 3 7 0 1038.81 985.12 15.26 o 4 7 0 364.33 341.11 8.04 o 5 7 0 106.08 103.07 4.87 o 6 7 0 5.22 1.48 5.80 < 0 8 0 5427.78 4757.82 127.07 o 1 8 0 570.88 615.73 11.44 o 2 8 0 931.18 931.47 15.14 o 3 8 0 263.72 249.75 6.13 o 4 8 0 -3.02 1.41 3.06 < 5 8 0 -1.22 0.30 7.53 < 6 8 0 18.08 35.84 5.57 o 1 9 0 5.89 15.65 3.57 < 2 9 0 1228.72 1264.49 20.52 o 3 9 0 -1.08 4.31 6.38 < 4 9 0 529.18 505.97 8.45 o 5 9 0 1.08 1.89 7.05 < 0 10 0 1934.90 1752.95 47.98 o 1 10 0 91.92 99.14 4.98 o 2 10 0 450.77 445.53 9.46 o 3 10 0 -0.33 4.62 3.68 < 4 10 0 10.90 14.76 3.46 o 5 10 0 -1.07 8.14 9.23 < 1 11 0 179.11 187.39 6.33 o 2 11 0 143.50 128.48 6.14 o 3 11 0 124.76 138.14 5.05 o 4 11 0 43.03 32.88 4.45 o 5 11 0 26.10 26.01 7.73 o 0 12 0 305.06 256.82 10.01 o 1 12 0 430.06 371.56 11.61 o 2 12 0 116.81 125.96 6.42 o 3 12 0 2.87 6.45 4.35 < 4 12 0 16.77 0.68 5.83 < 1 13 0 6.21 2.65 4.38 < 2 13 0 4.99 7.23 3.84 < 3 13 0 56.06 70.30 5.84 o 0 14 0 1.54 0.59 5.57 < 1 14 0 96.12 97.27 5.30 o 2 14 0 23.72 36.23 6.18 o 3 14 0 17.29 10.34 7.49 < 1 15 0 21.83 11.39 6.87 o 1 0 1 7930.18 0.00 163.34 x 2 0 1 302.01 335.58 9.96 o 3 0 1 1369.19 1340.85 18.68 o 4 0 1 232.12 230.87 5.31 o 5 0 1 78.77 89.12 4.11 o 6 0 1 37.03 50.80 4.46 o 7 0 1 69.85 58.26 12.18 o -7 1 1 15.21 20.63 8.03 < -6 1 1 51.11 54.56 4.14 o -5 1 1 808.45 713.24 12.43 o -4 1 1 217.68 226.07 9.71 o -3 1 1 4727.12 5050.94 60.66 o -2 1 1 955.78 1052.63 17.75 o -1 1 1 1971.13 2141.98 25.51 o 1 1 1 2235.88 2141.98 26.45 o 2 1 1 1047.49 1052.63 13.96 o 3 1 1 4630.60 5050.94 56.41 o 4 1 1 204.57 226.07 5.13 o 5 1 1 756.56 713.24 12.67 o 6 1 1 51.93 54.56 4.61 o 7 1 1 28.89 20.63 9.28 o -7 2 1 34.63 19.08 9.18 o -6 2 1 50.63 61.63 4.35 o -5 2 1 146.65 151.38 5.00 o -4 2 1 55.36 60.71 3.40 o -3 2 1 1116.32 1131.52 14.73 o -2 2 1 3766.38 3867.95 46.97 o -1 2 1 7545.80 9508.86 107.16 o 0 2 1 4497.73 0.00 108.54 x 1 2 1 7834.35 9508.86 126.49 o 2 2 1 3718.18 3867.95 51.59 o 3 2 1 1147.53 1131.53 16.13 o 4 2 1 48.23 60.71 3.48 o 5 2 1 151.58 151.38 4.95 o 6 2 1 55.92 61.63 4.46 o 7 2 1 17.19 19.08 7.66 < -7 3 1 12.13 11.96 11.67 < -6 3 1 58.26 55.42 4.38 o -5 3 1 120.65 128.09 4.69 o -4 3 1 1942.85 1808.51 26.41 o -3 3 1 1421.81 1439.35 19.87 o -2 3 1 4471.42 4770.57 56.77 o -1 3 1 2358.01 2272.28 30.52 o 0 3 1 286.87 324.95 5.87 o 1 3 1 2204.82 2272.28 31.86 o 2 3 1 4519.04 4770.56 61.56 o 3 3 1 1448.95 1439.35 20.97 o 4 3 1 1857.96 1808.51 26.34 o 5 3 1 125.68 128.09 4.83 o 6 3 1 58.51 55.42 4.38 o 7 3 1 24.21 11.96 8.62 < -6 4 1 76.52 74.86 5.08 o -5 4 1 18.40 19.58 3.82 o -4 4 1 5.96 20.09 3.45 < -3 4 1 193.85 206.44 4.41 o -2 4 1 2916.42 3059.19 39.65 o -1 4 1 272.30 258.61 6.48 o 0 4 1 11961.60 12333.10 237.75 o 1 4 1 206.11 258.61 4.64 o 2 4 1 3042.68 3059.18 45.68 o 3 4 1 204.06 206.44 5.38 o 4 4 1 9.37 20.09 3.52 < 5 4 1 16.74 19.58 3.78 o 6 4 1 67.32 74.86 4.73 o -6 5 1 73.07 78.75 4.47 o -5 5 1 11.82 18.68 4.20 < -4 5 1 1096.85 1058.16 17.19 o -3 5 1 47.21 44.72 3.78 o -2 5 1 3298.82 3333.38 44.12 o -1 5 1 915.75 839.35 14.78 o 0 5 1 209.36 212.09 5.85 o 1 5 1 923.09 839.35 14.08 o 2 5 1 3259.92 3333.38 46.11 o 3 5 1 45.64 44.72 3.90 o 4 5 1 1119.56 1058.16 17.34 o 5 5 1 8.23 18.68 4.57 < 6 5 1 80.63 78.75 5.13 o -6 6 1 22.69 16.86 4.78 o -5 6 1 46.86 53.72 4.29 o -4 6 1 29.26 48.95 3.64 o -3 6 1 34.27 48.69 3.03 o -2 6 1 2297.27 2370.93 31.36 o -1 6 1 1376.91 1254.06 19.10 o 0 6 1 5743.89 5776.74 99.53 o 1 6 1 1189.40 1254.05 18.52 o 2 6 1 2351.98 2370.92 33.57 o 3 6 1 34.67 48.69 3.07 o 4 6 1 39.21 48.95 4.01 o 5 6 1 46.98 53.72 4.82 o 6 6 1 19.74 16.86 4.92 o -6 7 1 43.89 33.09 5.54 o -5 7 1 81.45 96.93 5.07 o -4 7 1 590.27 553.53 10.37 o -3 7 1 829.45 821.78 11.66 o -2 7 1 1320.11 1354.43 20.12 o -1 7 1 379.21 379.36 7.24 o 0 7 1 643.17 554.35 12.47 o 1 7 1 354.80 379.36 7.55 o 2 7 1 1278.80 1354.43 19.12 o 3 7 1 828.92 821.78 12.91 o 4 7 1 586.59 553.53 11.47 o 5 7 1 85.35 96.93 4.75 o 6 7 1 37.50 33.09 5.92 o -6 8 1 9.95 8.38 5.67 < -5 8 1 36.78 41.75 3.75 o -4 8 1 22.16 16.86 3.79 o -3 8 1 267.49 314.69 5.78 o -2 8 1 462.27 440.29 8.63 o -1 8 1 2705.42 2856.40 44.21 o 0 8 1 1826.37 1712.01 30.06 o 1 8 1 2756.79 2856.40 45.00 o 2 8 1 441.48 440.29 8.58 o 3 8 1 307.17 314.69 6.36 o 4 8 1 19.75 16.87 3.34 o 5 8 1 32.96 41.75 3.85 o 6 8 1 14.19 8.38 5.42 < -5 9 1 137.95 136.66 5.39 o -4 9 1 3.88 0.17 3.48 < -3 9 1 1273.37 1198.90 19.38 o -2 9 1 1.05 2.45 7.57 < -1 9 1 463.35 478.34 10.08 o 0 9 1 -7.57 0.36 3.73 < 1 9 1 456.02 478.33 8.93 o 2 9 1 -8.17 2.45 3.83 < 3 9 1 1238.45 1198.91 19.24 o 4 9 1 3.90 0.17 3.34 < 5 9 1 149.06 136.66 5.33 o -5 10 1 20.67 10.34 4.59 o -4 10 1 19.53 23.57 3.69 o -3 10 1 157.66 152.93 4.97 o -2 10 1 53.50 75.31 4.12 o -1 10 1 1647.36 1560.23 27.79 o 0 10 1 152.73 110.39 6.02 o 1 10 1 1661.16 1560.24 27.72 o 2 10 1 63.22 75.31 4.61 o 3 10 1 144.17 152.93 5.12 o 4 10 1 20.31 23.57 3.32 o 5 10 1 16.04 10.34 5.02 o -5 11 1 33.31 44.56 7.29 o -4 11 1 63.88 71.38 4.29 o -3 11 1 132.13 131.61 5.22 o -2 11 1 208.69 220.61 7.75 o -1 11 1 89.71 75.59 5.21 o 0 11 1 11.30 13.61 3.60 o 1 11 1 73.45 75.59 4.87 o 2 11 1 218.53 220.61 6.86 o 3 11 1 132.31 131.61 5.64 o 4 11 1 66.13 71.38 4.71 o 5 11 1 50.51 44.56 6.52 o -4 12 1 2.37 1.12 4.39 < -3 12 1 37.83 47.44 4.16 o -2 12 1 89.54 101.65 5.69 o -1 12 1 177.34 162.20 7.02 o 0 12 1 645.59 549.37 11.73 o 1 12 1 167.08 162.20 6.68 o 2 12 1 93.80 101.65 5.18 o 3 12 1 39.46 47.44 4.37 o 4 12 1 2.78 1.12 5.41 < -3 13 1 21.37 7.55 5.64 o -2 13 1 69.70 74.81 5.83 o -1 13 1 9.06 10.71 4.59 < 0 13 1 8.06 1.99 3.86 < 1 13 1 10.41 10.71 4.95 < 2 13 1 63.73 74.81 5.35 o 3 13 1 18.33 7.55 6.80 < -2 14 1 71.73 64.44 7.39 o -1 14 1 15.62 15.70 5.98 < 0 14 1 184.15 176.64 6.10 o 1 14 1 13.58 15.70 4.70 < 2 14 1 69.39 64.44 6.64 o -1 15 1 3.65 6.98 7.61 < 0 15 1 -0.50 0.01 4.75 < 1 15 1 10.95 6.98 6.01 < 1 0 2 241.39 244.52 4.64 o 2 0 2 6721.57 6939.43 97.38 o 3 0 2 859.20 816.97 11.89 o 4 0 2 -5.26 11.31 2.96 < 5 0 2 7.26 7.09 3.43 < 6 0 2 6.20 18.73 4.66 < 7 0 2 -8.27 0.93 11.71 < -7 1 2 4.61 2.61 7.95 < -6 1 2 102.50 102.40 4.66 o -5 1 2 79.24 77.41 4.43 o -4 1 2 2696.55 2564.61 36.36 o -3 1 2 1009.06 953.65 15.67 o -2 1 2 5231.11 5718.07 73.50 o -1 1 2 2221.88 2164.21 25.75 o 1 1 2 2048.79 2164.21 26.68 o 2 1 2 5283.17 5718.08 68.03 o 3 1 2 986.62 953.65 13.82 o 4 1 2 2685.00 2564.61 33.53 o 5 1 2 88.15 77.41 4.28 o 6 1 2 98.21 102.40 5.60 o 7 1 2 9.91 2.61 10.29 < -7 2 2 34.66 23.51 10.70 o -6 2 2 74.15 78.56 4.26 o -5 2 2 161.96 158.15 5.04 o -4 2 2 31.93 34.32 3.43 o -3 2 2 368.43 417.38 6.67 o -2 2 2 4095.34 4146.41 54.40 o -1 2 2 6859.89 7280.53 103.81 o 0 2 2 8036.12 9134.47 153.28 o 1 2 2 6592.11 7280.53 99.72 o 2 2 2 4062.18 4146.41 55.29 o 3 2 2 432.18 417.39 6.67 o 4 2 2 26.52 34.32 2.87 o 5 2 2 172.52 158.15 5.03 o 6 2 2 76.61 78.56 5.36 o 7 2 2 13.51 23.51 9.53 < -6 3 2 35.41 41.35 4.30 o -5 3 2 466.75 431.67 9.24 o -4 3 2 337.35 316.03 6.78 o -3 3 2 2782.54 2782.76 36.74 o -2 3 2 135.21 244.63 3.09 o -1 3 2 2703.17 2787.99 36.98 o 0 3 2 473.52 454.64 7.65 o 1 3 2 2982.18 2788.00 40.86 o 2 3 2 131.72 244.63 3.75 o 3 3 2 2750.52 2782.76 40.50 o 4 3 2 312.08 316.03 10.23 o 5 3 2 445.62 431.67 9.22 o 6 3 2 40.44 41.35 4.86 o -6 4 2 5.37 3.05 3.94 < -5 4 2 66.76 80.92 4.12 o -4 4 2 237.01 256.55 5.92 o -3 4 2 690.40 673.34 10.05 o -2 4 2 281.13 258.83 4.96 o -1 4 2 6843.54 7150.11 95.46 o 0 4 2 1376.87 1640.97 21.53 o 1 4 2 6807.66 7150.10 108.84 o 2 4 2 249.66 258.82 7.49 o 3 4 2 693.50 673.34 11.99 o 4 4 2 251.68 256.55 6.57 o 5 4 2 62.73 80.92 4.59 o 6 4 2 4.97 3.05 4.74 < -6 5 2 10.82 6.18 4.75 < -5 5 2 412.53 388.69 8.22 o -4 5 2 56.68 43.79 4.40 o -3 5 2 2285.61 2307.69 28.99 o -2 5 2 1092.47 1133.83 15.68 o -1 5 2 1667.98 1818.76 24.86 o 0 5 2 551.90 580.61 9.95 o 1 5 2 1711.35 1818.76 24.84 o 2 5 2 1217.65 1133.83 17.11 o 3 5 2 2270.14 2307.69 34.31 o 4 5 2 37.47 43.79 4.98 o 5 5 2 414.42 388.69 8.68 o 6 5 2 10.61 6.18 4.57 < -6 6 2 28.71 33.42 7.00 o -5 6 2 30.01 35.44 4.01 o -4 6 2 66.29 78.15 3.77 o -3 6 2 389.64 390.23 6.70 o -2 6 2 124.53 141.84 3.75 o -1 6 2 5833.10 6158.64 85.59 o 0 6 2 3137.02 2944.66 49.47 o 1 6 2 5925.32 6158.65 87.99 o 2 6 2 125.47 141.84 3.70 o 3 6 2 394.39 390.23 7.52 o 4 6 2 71.55 78.15 4.81 o 5 6 2 29.65 35.44 4.12 o 6 6 2 41.36 33.42 5.28 o -6 7 2 12.08 15.92 6.48 < -5 7 2 138.74 127.93 5.52 o -4 7 2 532.01 537.90 9.24 o -3 7 2 896.46 872.06 12.72 o -2 7 2 1669.64 1623.23 24.04 o -1 7 2 770.53 827.69 12.90 o 0 7 2 149.67 144.93 4.92 o 1 7 2 764.17 827.69 12.76 o 2 7 2 1654.98 1623.23 23.95 o 3 7 2 908.57 872.06 13.91 o 4 7 2 542.88 537.90 10.86 o 5 7 2 138.31 127.93 5.45 o 6 7 2 14.73 15.92 5.20 < -6 8 2 7.02 7.28 5.96 < -5 8 2 11.86 6.41 4.06 < -4 8 2 7.94 8.22 3.35 < -3 8 2 139.96 126.16 4.12 o -2 8 2 1429.66 1416.35 21.20 o -1 8 2 546.43 638.49 10.76 o 0 8 2 2234.87 2052.91 34.29 o 1 8 2 543.98 638.48 10.60 o 2 8 2 1443.12 1416.35 22.20 o 3 8 2 126.77 126.16 4.33 o 4 8 2 7.12 8.22 4.49 < 5 8 2 12.28 6.41 3.98 o 6 8 2 -3.78 7.28 5.90 < -5 9 2 9.76 12.12 3.91 < -4 9 2 329.88 317.09 6.81 o -3 9 2 6.59 1.65 3.32 < -2 9 2 528.93 551.96 9.26 o -1 9 2 141.18 171.77 5.16 o 0 9 2 108.80 101.38 4.58 o 1 9 2 161.02 171.77 4.80 o 2 9 2 547.38 551.96 9.99 o 3 9 2 -0.10 1.65 3.20 < 4 9 2 323.42 317.09 6.63 o 5 9 2 2.89 12.12 4.33 < -5 10 2 6.97 5.43 4.39 < -4 10 2 8.83 4.07 3.32 < -3 10 2 17.31 25.43 3.83 o -2 10 2 584.02 601.52 10.65 o -1 10 2 88.56 81.95 5.23 o 0 10 2 3012.53 2598.77 46.04 o 1 10 2 89.32 81.95 5.04 o 2 10 2 573.60 601.52 11.39 o 3 10 2 29.23 25.43 4.33 o 4 10 2 6.37 4.07 3.36 < 5 10 2 1.36 5.43 4.98 < -4 11 2 156.11 160.14 5.18 o -3 11 2 97.36 109.83 4.64 o -2 11 2 289.12 303.79 7.91 o -1 11 2 110.58 104.90 4.77 o 0 11 2 13.11 17.05 3.55 o 1 11 2 107.19 104.90 4.99 o 2 11 2 297.54 303.79 7.40 o 3 11 2 103.68 109.83 5.57 o 4 11 2 169.09 160.14 6.01 o -4 12 2 23.95 20.00 5.30 o -3 12 2 14.70 14.07 4.10 o -2 12 2 66.35 68.99 4.95 o -1 12 2 503.20 464.96 11.20 o 0 12 2 74.58 61.41 4.94 o 1 12 2 482.26 464.96 11.00 o 2 12 2 69.24 68.99 4.68 o 3 12 2 14.21 14.07 4.20 o 4 12 2 19.89 20.00 6.84 < -3 13 2 105.16 108.53 5.98 o -2 13 2 5.75 3.66 4.59 < -1 13 2 51.54 51.07 5.05 o 0 13 2 33.09 42.46 4.48 o 1 13 2 48.20 51.07 5.36 o 2 13 2 5.74 3.66 4.74 < 3 13 2 95.72 108.53 6.41 o -2 14 2 34.40 33.69 7.57 o -1 14 2 114.98 98.96 6.36 o 0 14 2 0.31 0.18 3.75 < 1 14 2 113.63 98.96 6.12 o 2 14 2 29.97 33.69 5.70 o -1 15 2 28.32 15.30 6.96 o 0 15 2 17.10 0.44 6.78 < 1 15 2 19.12 15.30 7.00 < 1 0 3 7508.02 8503.83 150.88 o 2 0 3 526.24 561.86 7.72 o 3 0 3 1292.42 1274.28 17.09 o 4 0 3 342.13 353.36 7.16 o 5 0 3 12.62 33.20 5.36 < 6 0 3 15.27 7.50 3.80 o 7 0 3 29.24 18.98 10.13 < -7 1 3 1.56 0.40 7.19 < -6 1 3 4.38 6.25 4.14 < -5 1 3 712.16 676.59 12.73 o -4 1 3 376.29 367.33 7.11 o -3 1 3 4442.71 4536.82 55.79 o -2 1 3 1415.91 1462.31 17.63 o -1 1 3 5671.49 5529.62 87.43 o 0 1 3 1669.96 1562.85 22.03 o 1 1 3 5827.66 5529.62 76.32 o 2 1 3 1394.80 1462.31 18.76 o 3 1 3 4456.88 4536.82 55.89 o 4 1 3 395.95 367.33 7.59 o 5 1 3 751.58 676.59 11.48 o 6 1 3 -4.13 6.25 3.97 < 7 1 3 6.98 0.40 10.10 < -7 2 3 47.50 41.77 8.55 o -6 2 3 51.07 53.23 5.14 o -5 2 3 31.86 44.35 3.91 o -4 2 3 190.45 202.10 4.85 o -3 2 3 318.94 336.63 6.08 o -2 2 3 1642.30 1747.43 20.79 o -1 2 3 9170.13 10361.63 156.98 o 0 2 3 7044.28 7214.68 110.63 o 1 2 3 9507.24 10361.63 171.36 o 2 2 3 1598.17 1747.43 20.30 o 3 2 3 289.55 336.63 5.92 o 4 2 3 217.92 202.10 5.33 o 5 2 3 32.99 44.35 4.08 o 6 2 3 45.49 53.23 4.30 o 7 2 3 46.59 41.77 8.80 o -6 3 3 30.19 31.80 4.08 o -5 3 3 198.49 176.90 5.78 o -4 3 3 1836.69 1823.73 24.21 o -3 3 3 654.11 726.86 9.86 o -2 3 3 5381.23 5563.54 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