#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/70/2237071.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237071_Fobs loop_ _publ_author_name 'Ng, Seik Weng' _publ_section_title ; Tetrakis(triphenylphosphane-\kP)silver(I) trifluoroacetate ethanol monosolvate ; _journal_coeditor_code XU5640 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1536 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 89.403 _cell_angle_beta 85.465 _cell_angle_gamma 87.780 _cell_length_a 11.8005 _cell_length_b 14.5169 _cell_length_c 18.4830 _exptl_crystal_F_000 1360.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file xu5640Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' P-1 peak 0.86 A, hole 0.68 A from Ag1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 431.71 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 2512.12 2382.24 65.52 o 5 0 0 5145.15 5506.83 128.78 o 6 0 0 13250.48 13850.87 284.60 o 7 0 0 6822.52 6678.51 118.09 o 8 0 0 326.97 272.78 25.30 o 9 0 0 1061.09 1015.30 44.29 o 10 0 0 894.25 871.92 60.35 o 11 0 0 545.58 563.77 42.81 o 12 0 0 2097.02 2168.05 115.25 o 13 0 0 1955.63 2182.37 121.15 o 14 0 0 598.88 724.53 88.30 o 15 0 0 22.97 -18.09 42.82 o -15 1 0 611.95 639.90 86.05 o -14 1 0 432.13 359.87 46.45 o -13 1 0 786.58 593.80 74.70 o -12 1 0 195.61 158.96 28.16 o -11 1 0 108.14 71.79 21.03 o -10 1 0 2117.61 2266.32 127.37 o -9 1 0 237.42 272.80 27.32 o -8 1 0 11.71 6.98 12.04 o 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1549.20 57.56 o 7 3 0 1257.99 1161.48 53.07 o 8 3 0 1406.16 1530.26 50.77 o 9 3 0 350.30 388.51 31.84 o 10 3 0 1152.18 914.48 58.91 o 11 3 0 102.24 118.86 41.26 o 12 3 0 760.22 783.18 85.30 o 13 3 0 693.99 508.58 74.20 o 14 3 0 620.97 726.15 92.94 o 15 3 0 134.08 147.19 54.96 o -14 4 0 7.13 20.75 42.10 o -13 4 0 705.09 763.40 85.47 o -12 4 0 104.26 131.71 23.71 o -11 4 0 1573.16 1473.78 75.00 o -10 4 0 2257.97 2269.73 72.93 o -9 4 0 1523.65 1513.97 57.70 o -8 4 0 3541.77 3713.07 86.75 o -7 4 0 3402.75 3242.75 93.56 o -6 4 0 2122.51 2131.42 54.54 o -5 4 0 7.51 28.38 10.19 o -4 4 0 111.70 15.06 8.06 o -3 4 0 22311.05 22993.13 308.76 o -2 4 0 3011.24 3036.32 88.33 o -1 4 0 22235.57 22191.66 436.26 o 0 4 0 3465.10 3427.92 47.37 o 1 4 0 6921.50 6724.51 105.55 o 2 4 0 9702.95 10725.24 156.11 o 3 4 0 3155.82 2923.61 56.22 o 4 4 0 13478.09 13708.89 198.04 o 5 4 0 2510.86 2210.16 51.10 o 6 4 0 4137.58 4783.56 121.68 o 7 4 0 4884.19 5176.63 100.39 o 8 4 0 3632.14 3731.45 84.53 o 9 4 0 824.36 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326.89 347.81 67.66 o -14 6 0 828.73 1031.02 107.51 o -13 6 0 1375.09 1580.95 109.89 o -12 6 0 1940.02 2102.65 120.72 o -11 6 0 117.16 104.19 41.31 o -10 6 0 711.70 849.32 83.63 o -9 6 0 3186.97 3233.18 87.68 o -8 6 0 2893.32 2706.78 91.83 o -7 6 0 405.18 384.01 28.35 o -6 6 0 2387.11 2252.08 60.88 o -5 6 0 1228.47 1314.88 37.16 o -4 6 0 292.55 365.25 16.80 o -3 6 0 11998.40 12321.93 278.38 o -2 6 0 14416.20 13844.81 302.25 o -1 6 0 10039.37 9830.47 225.80 o 0 6 0 7499.01 7416.18 94.60 o 1 6 0 2268.46 2001.59 38.15 o 2 6 0 2931.03 2988.53 87.06 o 3 6 0 2039.75 1886.99 48.19 o 4 6 0 16687.50 17991.44 338.37 o 5 6 0 5337.69 5278.35 97.75 o 6 6 0 1164.96 1441.26 38.38 o 7 6 0 15.92 10.32 12.36 o 8 6 0 35.40 50.96 16.73 o 9 6 0 1268.71 1260.91 50.67 o 10 6 0 4244.14 4226.38 159.20 o 11 6 0 3779.50 3550.38 152.03 o 12 6 0 2513.92 2336.92 125.71 o 13 6 0 391.95 350.66 67.35 o 14 6 0 82.37 50.15 42.58 o -13 7 0 503.84 517.33 77.42 o -12 7 0 867.95 1036.72 100.11 o -11 7 0 1194.70 1121.59 99.21 o -10 7 0 200.04 118.91 39.95 o -9 7 0 47.38 59.56 33.56 o -8 7 0 2.48 38.43 29.93 o -7 7 0 34.53 42.04 29.60 o -6 7 0 0.12 26.85 10.34 o -5 7 0 666.02 807.60 26.66 o -4 7 0 722.14 786.68 55.18 o -3 7 0 1007.33 1022.78 59.51 o -2 7 0 2551.44 2899.94 101.38 o -1 7 0 258.68 284.53 34.77 o 0 7 0 62.90 109.52 15.58 o 1 7 0 5058.57 5194.00 75.92 o 2 7 0 125.41 139.62 22.90 o 3 7 0 49.50 113.02 12.61 o 4 7 0 166.49 190.78 16.08 o 5 7 0 3299.17 3325.15 68.32 o 6 7 0 21.01 11.03 10.06 o 7 7 0 888.84 861.43 32.68 o 8 7 0 222.46 247.32 41.69 o 9 7 0 1289.29 1242.47 51.70 o 10 7 0 316.54 393.59 60.43 o 11 7 0 45.15 35.63 36.55 o 12 7 0 143.91 108.35 45.16 o 13 7 0 95.75 -1.16 38.70 o 14 7 0 0.63 -51.46 35.81 o -13 8 0 333.30 321.34 66.12 o -12 8 0 159.91 155.87 52.81 o -11 8 0 253.84 322.12 60.76 o -10 8 0 379.59 391.47 63.07 o -9 8 0 751.88 731.89 76.92 o -8 8 0 3564.90 3367.62 141.23 o -7 8 0 2859.05 2618.67 118.45 o -6 8 0 674.69 598.64 64.62 o -5 8 0 2921.46 3022.53 118.81 o -4 8 0 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1109.86 1386.06 37.71 o 3 9 0 212.43 238.11 19.40 o 4 9 0 17.12 38.83 12.02 o 5 9 0 666.78 650.07 31.07 o 6 9 0 129.52 131.03 17.45 o 7 9 0 424.24 472.85 34.41 o 8 9 0 94.87 88.03 18.57 o 9 9 0 178.87 140.56 41.96 o 10 9 0 238.38 214.55 49.89 o 11 9 0 279.36 279.74 57.42 o 12 9 0 258.88 155.78 54.95 o 13 9 0 128.43 99.92 51.45 o -12 10 0 218.30 331.92 67.79 o -11 10 0 1831.23 1834.19 120.82 o -10 10 0 2991.22 3166.06 152.94 o -9 10 0 1172.92 1407.79 98.13 o -8 10 0 65.24 80.71 37.87 o -7 10 0 1781.58 1688.01 101.12 o -6 10 0 1130.49 1223.74 84.29 o -5 10 0 61.70 95.93 35.81 o -4 10 0 774.26 895.06 70.68 o -3 10 0 84.67 120.69 36.13 o -2 10 0 728.32 876.63 76.75 o -1 10 0 1842.57 2042.30 97.35 o 0 10 0 58.72 101.38 12.08 o 1 10 0 3708.12 3635.80 77.90 o 2 10 0 2466.32 2310.00 51.68 o 3 10 0 2777.92 2783.58 73.62 o 4 10 0 2108.78 2096.65 51.19 o 5 10 0 1210.15 1268.03 41.16 o 6 10 0 406.69 375.95 30.11 o 7 10 0 3.03 15.85 12.67 o 8 10 0 905.51 995.07 41.94 o 9 10 0 584.11 728.88 78.59 o 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338.01 350.83 32.77 o 5 13 0 1.01 -10.90 13.42 o 6 13 0 23.11 20.06 15.93 o 7 13 0 42.91 70.42 19.20 o 8 13 0 286.59 344.96 39.39 o 9 13 0 5.13 3.18 56.20 o 10 13 0 37.59 92.26 44.06 o 11 13 0 44.92 12.93 40.39 o -9 14 0 539.82 819.78 105.46 o -8 14 0 417.69 402.79 73.49 o -7 14 0 370.15 442.35 76.82 o -6 14 0 166.90 160.14 51.57 o -5 14 0 463.11 579.65 80.48 o -4 14 0 333.60 331.88 61.93 o -3 14 0 1718.38 1842.74 114.62 o -2 14 0 1997.39 2010.49 116.93 o -1 14 0 222.64 333.30 59.78 o 0 14 0 154.91 100.08 40.32 o 1 14 0 5.82 14.21 32.02 o 2 14 0 970.02 871.80 59.29 o 3 14 0 309.70 353.03 39.49 o 4 14 0 963.75 836.04 55.69 o 5 14 0 481.60 485.42 44.39 o 6 14 0 39.69 36.83 18.02 o 7 14 0 53.44 29.95 23.72 o 8 14 0 559.72 599.41 52.77 o 9 14 0 1612.68 1840.38 79.63 o 10 14 0 1224.59 1305.50 114.46 o -8 15 0 213.10 176.11 60.65 o -7 15 0 7.18 27.88 42.08 o -6 15 0 811.89 673.14 89.97 o -5 15 0 1268.05 1354.65 123.91 o -4 15 0 802.36 609.69 81.35 o -3 15 0 251.42 207.50 55.85 o -2 15 0 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