#------------------------------------------------------------------------------ #$Date: 2016-04-03 06:47:51 +0300 (Sun, 03 Apr 2016) $ #$Revision: 181292 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/70/2237086.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237086_Fobs loop_ _publ_author_name 'Brown, Shayne' 'Crundwell, Guy' _publ_section_title ; Di-\m-iodido-bis[(biphenyl-2-yl)(triphenylphosphane-\kP)palladium(II)] ; _journal_coeditor_code YK2076 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1526 _journal_volume 68 _journal_year 2012 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 133.962 _cell_angle_gamma 90.000 _cell_length_a 9.6957 _cell_length_b 20.0969 _cell_length_c 18.3718 _exptl_crystal_F_000 1272.00 _reflns_d_resolution_high 0.7501 _cod_data_source_file yk2076Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' 14c in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 303.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 75762.44 85464.80 699.64 o 3 0 0 52937.80 55188.82 704.23 o 4 0 0 148.23 268.96 93.48 o 5 0 0 10260.31 10018.59 154.84 o 6 0 0 8129.80 7917.38 164.59 o 7 0 0 1310.37 1103.94 136.49 o 8 0 0 1230.96 1320.71 159.43 o 9 0 0 102.55 255.20 174.34 o 2 1 0 417.09 486.15 32.13 o 3 1 0 6599.66 6727.42 66.50 o 4 1 0 539.83 546.46 65.10 o 5 1 0 1688.61 1933.73 89.92 o 6 1 0 378.83 367.89 103.34 o 7 1 0 187.94 142.33 101.99 o 8 1 0 634.60 649.99 98.36 o 9 1 0 61.93 89.07 112.02 o 2 2 0 10361.32 11306.31 177.55 o 3 2 0 34753.70 35504.75 399.98 o 4 2 0 935.20 862.59 65.86 o 5 2 0 5472.35 5406.04 141.65 o 6 2 0 3704.88 3432.35 288.17 o 7 2 0 1449.77 1250.21 103.19 o 8 2 0 542.33 588.85 100.79 o 9 2 0 9.95 321.15 173.76 o 2 3 0 39.52 108.41 19.77 o 3 3 0 4672.12 4932.65 60.24 o 4 3 0 807.88 674.27 59.51 o 5 3 0 11470.86 11578.00 437.85 o 6 3 0 2134.85 1907.74 96.79 o 7 3 0 1703.01 1500.02 101.32 o 8 3 0 3315.06 3150.38 309.68 o 9 3 0 401.42 376.20 168.60 o 1 4 0 668.07 1035.39 119.86 o 2 4 0 312.53 267.40 28.50 o 3 4 0 50.43 84.16 32.74 o 4 4 0 1899.41 2164.06 82.87 o 5 4 0 142.81 188.45 84.68 o 6 4 0 1.38 -38.57 91.73 o 7 4 0 571.02 641.67 99.78 o 8 4 0 1.32 181.34 105.12 o 9 4 0 89.40 286.74 167.45 o 1 5 0 1934.46 2330.77 35.84 o 2 5 0 371.92 492.29 26.91 o 3 5 0 6517.65 7690.07 178.07 o 4 5 0 592.15 427.18 64.29 o 5 5 0 6108.72 5501.08 395.41 o 6 5 0 4364.65 4050.88 269.53 o 7 5 0 829.39 836.61 164.01 o 8 5 0 2904.43 2632.98 105.57 o 9 5 0 683.39 788.53 171.47 o 0 6 0 7599.89 8678.43 104.77 o 1 6 0 12666.15 14008.74 172.86 o 2 6 0 8225.18 8290.41 43.16 o 3 6 0 12545.74 12836.38 303.38 o 4 6 0 1924.67 2090.23 64.46 o 5 6 0 4231.59 4016.03 153.69 o 6 6 0 2590.79 2332.30 91.28 o 7 6 0 116.65 180.09 115.84 o 8 6 0 592.74 645.34 92.58 o 9 6 0 223.40 404.87 158.28 o 1 7 0 12689.29 14290.93 173.41 o 2 7 0 1128.26 1154.40 63.66 o 3 7 0 3434.23 3524.96 70.92 o 4 7 0 1216.11 1389.41 43.76 o 5 7 0 23.48 -17.88 83.61 o 6 7 0 2730.16 2588.29 91.50 o 7 7 0 1.44 78.45 92.86 o 8 7 0 457.40 431.39 103.52 o 0 8 0 62837.65 61592.51 836.36 o 1 8 0 10990.19 12299.04 142.79 o 2 8 0 14068.11 13149.75 102.08 o 3 8 0 23543.02 22211.56 389.76 o 4 8 0 57.54 97.49 39.04 o 5 8 0 5240.87 5063.06 221.65 o 6 8 0 2178.00 2198.03 92.04 o 7 8 0 76.97 109.38 93.38 o 8 8 0 821.33 870.42 101.50 o 1 9 0 15652.63 16899.31 357.61 o 2 9 0 8502.00 8287.27 74.89 o 3 9 0 524.98 529.17 26.61 o 4 9 0 2999.86 3232.91 100.10 o 5 9 0 1073.31 1235.92 83.42 o 6 9 0 142.80 178.40 78.40 o 7 9 0 298.30 296.57 89.89 o 8 9 0 126.88 292.30 103.68 o 0 10 0 23475.95 22724.01 304.51 o 1 10 0 3878.91 4190.71 73.21 o 2 10 0 9044.26 8778.20 127.05 o 3 10 0 15355.31 14548.93 278.48 o 4 10 0 2074.86 2127.73 46.74 o 5 10 0 4796.51 4740.24 88.32 o 6 10 0 358.91 320.94 80.24 o 7 10 0 1167.95 1254.58 92.21 o 8 10 0 282.99 190.39 150.25 o 1 11 0 112.66 214.32 66.14 o 2 11 0 5177.85 4921.30 96.05 o 3 11 0 268.96 310.59 25.58 o 4 11 0 1174.56 1201.87 40.45 o 5 11 0 2946.59 2913.07 190.11 o 6 11 0 137.17 145.89 78.34 o 7 11 0 617.30 695.62 140.50 o 8 11 0 1261.97 1376.91 153.12 o 0 12 0 4683.21 4653.32 37.82 o 1 12 0 416.28 474.51 74.15 o 2 12 0 38.05 65.39 24.17 o 3 12 0 2105.78 2104.65 96.18 o 4 12 0 1501.76 1653.75 63.91 o 5 12 0 764.77 875.53 67.97 o 6 12 0 90.44 201.29 134.77 o 7 12 0 1196.74 1370.03 157.71 o 8 12 0 4.61 139.35 176.06 o 1 13 0 187.27 310.55 136.45 o 2 13 0 2.22 0.48 13.54 o 3 13 0 1468.85 1421.03 62.57 o 4 13 0 21.19 61.96 55.25 o 5 13 0 1917.84 1902.21 125.59 o 6 13 0 980.24 909.53 127.31 o 7 13 0 39.39 125.02 131.90 o 0 14 0 642.94 611.32 164.59 o 1 14 0 3183.90 2919.70 184.27 o 2 14 0 1622.98 1538.17 67.50 o 3 14 0 1364.05 1314.56 151.68 o 4 14 0 2429.74 2080.54 93.67 o 5 14 0 794.19 678.99 121.00 o 6 14 0 585.19 654.91 135.34 o 7 14 0 659.97 709.39 161.15 o 1 15 0 4373.15 4043.98 117.83 o 2 15 0 543.82 741.28 181.79 o 3 15 0 923.50 718.44 84.07 o 4 15 0 1957.07 1746.77 91.22 o 5 15 0 61.67 -175.89 275.84 o 6 15 0 1018.48 1107.38 146.81 o 7 15 0 50.10 154.84 147.96 o 0 16 0 3802.35 3930.02 186.38 o 1 16 0 1725.21 1407.88 197.27 o 2 16 0 3242.04 2967.76 418.35 o 3 16 0 868.28 720.90 94.34 o 4 16 0 592.10 482.05 90.79 o 5 16 0 1411.77 1361.44 103.33 o 6 16 0 189.20 125.65 194.41 o 7 16 0 6.72 77.42 142.22 o 1 17 0 5148.35 5235.82 200.14 o 2 17 0 3077.27 3590.52 189.25 o 3 17 0 563.67 588.76 174.62 o 4 17 0 2943.92 2908.96 97.92 o 5 17 0 140.27 88.66 135.34 o 6 17 0 494.26 414.66 110.49 o 7 17 0 113.19 17.20 162.87 o 0 18 0 494.64 662.36 173.19 o 1 18 0 1060.72 1243.86 202.44 o 2 18 0 1950.91 2160.85 193.26 o 3 18 0 391.31 512.69 142.79 o 4 18 0 36.84 227.10 192.11 o 5 18 0 1070.84 966.50 107.32 o 6 18 0 0.04 -120.15 120.15 o 1 19 0 2262.34 2154.54 164.01 o 2 19 0 982.03 611.32 200.72 o 3 19 0 91.72 168.60 165.16 o 4 19 0 767.51 978.92 160.57 o 5 19 0 369.31 441.00 178.92 o 6 19 0 86.81 -47.02 203.01 o 0 20 0 95.62 255.20 193.83 o 1 20 0 88.69 102.65 206.45 o 2 20 0 1143.70 917.56 209.89 o 3 20 0 37.55 325.16 182.36 o 4 20 0 229.96 494.91 176.06 o 5 20 0 300.78 241.43 180.07 o 1 21 0 15.20 204.16 165.73 o 2 21 0 31.75 -84.87 189.25 o 3 21 0 19.75 269.53 192.11 o 4 21 0 0.37 380.79 199.57 o 5 21 0 101.91 358.99 220.79 o 0 22 0 41.01 509.24 213.33 o 1 22 0 1.55 165.16 214.48 o 2 22 0 149.61 -125.02 168.60 o 3 22 0 71.92 -204.16 204.16 o 4 22 0 292.95 1101.07 218.49 o 1 23 0 613.41 929.60 194.98 o 2 23 0 211.68 119.28 220.21 o 3 23 0 55.18 -197.85 197.85 o 4 23 0 507.17 1601.14 230.54 o 0 24 0 16.53 329.17 208.17 o 1 24 0 21.57 421.50 204.16 o 2 24 0 2.56 -46.45 223.08 o 3 24 0 16.73 -120.43 180.07 o 1 25 0 646.80 1306.37 241.43 o 2 25 0 287.08 407.17 199.57 o -9 1 1 1080.31 1055.02 121.29 o -8 1 1 737.63 712.38 102.63 o -7 1 1 149.35 172.91 87.86 o -6 1 1 13973.29 13871.03 262.36 o -5 1 1 9430.86 8889.93 97.82 o -4 1 1 9129.98 9983.63 83.73 o -3 1 1 86015.63 92230.02 798.85 o -2 1 1 8229.85 8798.89 191.04 o 1 1 1 5224.26 6514.06 71.92 o 2 1 1 63165.33 68820.92 948.81 o 3 1 1 8663.72 8977.92 78.40 o 4 1 1 3974.16 3895.20 81.05 o 5 1 1 10626.27 10679.64 120.58 o 6 1 1 4.93 25.30 92.87 o 7 1 1 39.83 -26.95 96.03 o 8 1 1 527.87 384.33 116.77 o -9 2 1 558.88 623.64 115.21 o -8 2 1 1825.20 1838.77 101.95 o -7 2 1 32.99 19.95 94.01 o -6 2 1 1125.28 1101.48 94.36 o -5 2 1 1709.91 1795.63 81.46 o -4 2 1 205.98 242.18 59.51 o -3 2 1 61.39 171.40 45.15 o -2 2 1 55.98 96.02 23.54 o 1 2 1 90.66 153.67 17.36 o 2 2 1 17638.41 20026.15 158.98 o 3 2 1 4595.42 4766.88 51.81 o 4 2 1 5462.16 5529.21 86.19 o 5 2 1 5931.21 6190.24 155.98 o 6 2 1 1041.65 1033.89 94.08 o 7 2 1 3397.94 3160.77 118.42 o 8 2 1 1467.08 1455.54 118.34 o -9 3 1 246.63 361.09 115.03 o -8 3 1 163.48 295.32 105.55 o -7 3 1 347.96 352.77 110.68 o -6 3 1 2346.36 2110.00 122.72 o -5 3 1 2727.69 2430.14 63.86 o -4 3 1 1659.67 1583.61 62.46 o -3 3 1 15389.36 16444.20 105.66 o -2 3 1 1498.42 2051.49 19.20 o 1 3 1 11765.74 13108.32 141.56 o 2 3 1 8245.58 9078.87 155.36 o 3 3 1 793.61 613.88 21.56 o 4 3 1 381.53 419.34 55.25 o 5 3 1 2063.82 1963.07 100.59 o 6 3 1 398.80 382.31 96.70 o 7 3 1 35.77 71.61 99.60 o 8 3 1 80.31 177.14 115.87 o -9 4 1 1111.37 1164.48 123.01 o -8 4 1 3896.36 3885.95 295.34 o -7 4 1 37.72 42.31 97.20 o -6 4 1 2980.17 2977.98 230.25 o -5 4 1 4836.07 4332.83 87.60 o -4 4 1 4620.44 4861.28 98.92 o -3 4 1 19.39 83.81 25.31 o -2 4 1 2273.06 3088.60 28.49 o -1 4 1 13996.71 14289.98 446.35 o 0 4 1 2274.11 3145.90 71.95 o 1 4 1 30443.03 34605.60 1029.67 o 2 4 1 16535.92 16765.60 270.68 o 3 4 1 4884.84 5220.08 104.29 o 4 4 1 7133.84 5991.54 320.78 o 5 4 1 10495.18 9918.50 709.10 o 6 4 1 1587.69 1539.62 98.29 o 7 4 1 5280.85 4693.57 482.29 o 8 4 1 2643.37 2615.30 353.55 o -9 5 1 99.21 214.34 107.81 o -8 5 1 176.68 349.51 96.08 o -7 5 1 515.89 564.02 114.12 o -6 5 1 972.16 1018.44 93.07 o -5 5 1 332.28 322.01 76.75 o -4 5 1 1445.58 1562.07 60.08 o -3 5 1 5355.75 5561.03 103.93 o -2 5 1 4456.04 3697.80 35.29 o -1 5 1 35698.25 39221.86 478.85 o 0 5 1 39.45 162.89 27.32 o 1 5 1 3620.81 3796.40 63.66 o 2 5 1 152.42 163.03 16.04 o 3 5 1 10044.26 11598.86 211.04 o 4 5 1 7.76 9.62 47.28 o 5 5 1 11.71 44.82 89.64 o 6 5 1 1304.93 1183.66 99.21 o 7 5 1 61.19 18.98 104.74 o 8 5 1 38.93 111.29 146.24 o -9 6 1 600.10 743.82 109.64 o -8 6 1 1572.55 1644.22 99.97 o -7 6 1 194.05 253.94 106.95 o -6 6 1 943.37 863.75 111.83 o -5 6 1 921.09 811.77 80.57 o -4 6 1 2512.30 2734.87 63.37 o -3 6 1 83.65 135.41 24.36 o -2 6 1 876.44 967.44 29.86 o -1 6 1 2165.71 2562.33 74.00 o 0 6 1 8469.01 8380.81 74.33 o 1 6 1 6820.23 6122.98 67.10 o 2 6 1 578.20 598.25 19.74 o 3 6 1 7948.39 8350.94 281.58 o 4 6 1 2505.59 2362.67 116.10 o 5 6 1 5996.26 5294.10 269.25 o 6 6 1 665.42 637.69 93.80 o 7 6 1 2542.21 2453.95 152.54 o 8 6 1 1207.81 1284.36 266.95 o -9 7 1 613.44 701.36 155.98 o -8 7 1 1248.72 1432.35 104.58 o -7 7 1 457.51 506.20 106.09 o -6 7 1 7725.12 7471.37 199.86 o -5 7 1 4234.13 3903.22 83.40 o -4 7 1 6488.38 6815.36 106.38 o -3 7 1 31308.86 31214.54 228.01 o -2 7 1 2806.88 2910.18 33.26 o -1 7 1 18472.37 19155.42 162.46 o 0 7 1 30794.11 32415.62 257.68 o 1 7 1 1242.92 1028.46 71.97 o 2 7 1 8878.21 7828.59 44.36 o 3 7 1 10509.83 11032.08 339.78 o 4 7 1 178.88 183.97 47.51 o 5 7 1 6339.50 6030.16 106.51 o 6 7 1 1073.80 969.15 98.92 o 7 7 1 133.89 230.10 136.49 o 8 7 1 252.99 236.01 108.42 o -9 8 1 50.34 113.55 138.21 o -8 8 1 74.58 102.20 92.72 o -7 8 1 1150.11 1230.73 90.61 o -6 8 1 277.80 287.00 80.91 o -5 8 1 333.83 367.89 74.93 o -4 8 1 7548.45 7650.92 109.84 o -3 8 1 262.46 292.72 22.35 o -2 8 1 5491.11 6184.04 56.35 o -1 8 1 10292.81 10528.37 117.46 o 0 8 1 4907.85 5841.43 110.76 o 1 8 1 3875.39 4131.96 85.45 o 2 8 1 513.08 482.98 33.64 o 3 8 1 6365.52 6738.05 261.50 o 4 8 1 79.34 86.47 45.95 o 5 8 1 389.97 302.68 85.12 o 6 8 1 736.89 613.94 86.42 o 7 8 1 168.69 198.79 190.11 o 8 8 1 0.13 23.79 112.08 o -8 9 1 1292.65 1395.19 104.00 o -7 9 1 0.51 65.43 84.87 o -6 9 1 6674.26 6444.87 99.47 o -5 9 1 4092.78 4075.28 85.27 o -4 9 1 3564.67 3742.82 81.84 o -3 9 1 32468.66 31625.10 393.67 o -2 9 1 9638.78 8928.97 122.47 o -1 9 1 25961.48 26635.02 361.04 o 0 9 1 41407.02 41125.93 575.19 o 1 9 1 4710.98 4569.80 56.39 o 2 9 1 12501.87 12449.58 93.48 o 3 9 1 4428.24 4397.94 131.92 o 4 9 1 1132.27 1168.77 48.48 o 5 9 1 4744.27 4634.08 96.13 o 6 9 1 83.85 92.62 88.46 o 7 9 1 331.07 316.51 93.67 o 8 9 1 24.20 81.65 106.76 o -8 10 1 429.84 502.94 165.16 o -7 10 1 1247.26 1270.02 83.44 o -6 10 1 323.03 381.23 73.69 o -5 10 1 3951.30 3874.34 82.36 o -4 10 1 4580.07 4707.07 122.33 o -3 10 1 2004.56 2027.64 26.97 o -2 10 1 7985.04 8020.61 143.55 o -1 10 1 5550.20 6383.59 103.06 o 0 10 1 3067.69 3458.86 39.65 o 1 10 1 2913.25 3089.77 56.72 o 2 10 1 8995.80 8490.37 82.79 o 3 10 1 1194.66 1251.61 59.02 o 4 10 1 3481.92 3385.78 122.06 o 5 10 1 2082.18 2166.33 129.89 o 6 10 1 283.48 312.72 121.58 o 7 10 1 424.15 461.89 114.69 o -8 11 1 793.54 941.64 158.28 o -7 11 1 675.93 833.85 85.82 o -6 11 1 1026.05 963.61 75.16 o -5 11 1 1326.78 1350.81 69.73 o -4 11 1 10.00 22.36 26.94 o -3 11 1 6819.27 6638.26 127.06 o -2 11 1 706.58 650.70 63.08 o -1 11 1 8157.20 8018.98 193.99 o 0 11 1 2244.72 2084.19 62.25 o 1 11 1 205.65 199.40 22.96 o 2 11 1 7751.62 7223.18 134.77 o 3 11 1 337.49 337.06 26.23 o 4 11 1 2401.38 2662.79 75.25 o 5 11 1 572.76 628.51 73.44 o 6 11 1 1243.47 1417.85 88.54 o 7 11 1 477.59 691.61 155.98 o -8 12 1 628.54 566.02 144.52 o -7 12 1 136.89 151.40 136.49 o -6 12 1 1284.05 1191.11 131.90 o -5 12 1 438.75 395.88 63.00 o -4 12 1 1.67 -36.85 52.57 o -3 12 1 34.91 16.85 44.93 o -2 12 1 462.52 550.61 55.31 o -1 12 1 4102.14 4045.92 49.68 o 0 12 1 366.02 425.52 30.54 o 1 12 1 125.22 130.72 22.46 o 2 12 1 5852.71 5410.06 82.40 o 3 12 1 1454.59 1343.16 39.32 o 4 12 1 958.42 1075.20 68.93 o 5 12 1 4760.62 5015.37 133.91 o 6 12 1 34.43 107.24 122.15 o 7 12 1 912.53 1091.89 162.87 o -8 13 1 17.63 0.00 174.34 o -7 13 1 1139.68 1263.94 151.97 o -6 13 1 77.76 118.14 121.58 o -5 13 1 121.64 112.97 116.42 o -4 13 1 1608.22 1553.76 124.41 o -3 13 1 105.93 96.35 34.33 o -2 13 1 18.27 82.42 57.75 o -1 13 1 50.91 35.72 83.44 o 0 13 1 2260.70 2052.22 97.84 o 1 13 1 1073.63 933.42 45.64 o 2 13 1 174.75 249.65 70.19 o 3 13 1 4284.56 4125.41 133.47 o 4 13 1 284.80 365.27 60.09 o 5 13 1 1.29 252.90 126.16 o 6 13 1 2018.92 2089.16 153.69 o 7 13 1 178.44 243.73 139.93 o -8 14 1 143.78 111.25 162.87 o -7 14 1 110.63 155.41 134.77 o -6 14 1 748.73 843.58 137.06 o -5 14 1 127.17 153.69 116.99 o -4 14 1 893.07 671.95 91.78 o -3 14 1 116.63 57.99 81.14 o -2 14 1 2146.44 2273.37 186.67 o -1 14 1 749.20 637.25 97.62 o 0 14 1 2149.16 1931.74 68.04 o 1 14 1 1647.64 1509.23 92.04 o 2 14 1 1750.18 1550.52 78.80 o 3 14 1 1496.25 1369.17 49.64 o 4 14 1 0.63 40.14 103.23 o 5 14 1 1321.65 1332.18 133.05 o 6 14 1 332.60 391.11 137.06 o 7 14 1 378.96 274.69 167.45 o -8 15 1 235.17 187.53 169.17 o -7 15 1 513.06 527.02 156.56 o -6 15 1 782.60 891.75 139.35 o -5 15 1 271.07 -13.71 225.38 o -4 15 1 1117.70 895.14 89.78 o -3 15 1 2143.41 1995.86 84.55 o -2 15 1 734.95 1025.06 432.11 o -1 15 1 2694.91 2634.49 51.45 o 0 15 1 4023.58 3912.04 254.05 o 1 15 1 0.94 89.69 141.36 o 2 15 1 759.40 750.16 145.66 o 3 15 1 2699.21 2381.06 88.84 o 4 15 1 7.22 -125.13 260.36 o 5 15 1 317.51 355.55 129.61 o 6 15 1 1413.67 1384.37 135.91 o 7 15 1 9.54 97.49 158.85 o -7 16 1 752.43 671.54 145.66 o -6 16 1 237.57 17.84 132.19 o -5 16 1 631.93 576.96 98.65 o -4 16 1 2360.63 2091.78 89.90 o -3 16 1 13.32 147.13 179.50 o -2 16 1 3108.25 3061.11 269.53 o -1 16 1 2639.03 2723.60 148.81 o 0 16 1 738.50 982.82 145.56 o 1 16 1 5152.31 4331.45 203.58 o 2 16 1 112.00 150.65 121.00 o 3 16 1 2206.21 2196.51 88.15 o 4 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