#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/70/2237093.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237093_Fobs loop_ _publ_author_name 'Tskhovrebov, Alexander' 'Haukka, Matti' _publ_section_title ; cis-Dichloridobis(2-isocyanophenyl 4-methoxybenzoate)palladium(II) chloroform monosolvate ; _journal_coeditor_code ZQ2184 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1476 _journal_page_last m1477 _journal_volume 68 _journal_year 2012 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 7.4457 _cell_length_b 12.1352 _cell_length_c 36.1109 _exptl_crystal_F_000 1608.00 _reflns_d_resolution_high 0.7098 _[local]_cod_data_source_file zq2184Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' alts1dx in P2(1)2(1)2(1) (colourless block)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 316.69 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 990.75 1043.90 36.70 o 6 0 0 3542.69 3727.13 114.69 o 8 0 0 2533.57 2530.85 175.33 o 1 1 0 10546.23 10391.01 177.97 o 2 1 0 19385.20 20091.59 272.80 o 3 1 0 12829.34 12237.05 128.77 o 4 1 0 58.70 41.74 15.34 o 5 1 0 545.30 528.84 26.33 o 6 1 0 1233.72 1156.57 39.41 o 7 1 0 1371.76 1453.44 84.10 o 8 1 0 1366.45 1295.10 115.78 o 9 1 0 525.61 560.81 100.32 o 10 1 0 202.88 154.10 219.41 o 0 2 0 6.83 11.39 5.89 o 1 2 0 19523.34 19271.65 280.68 o 2 2 0 17.87 35.72 8.37 o 3 2 0 14210.76 14355.57 218.86 o 4 2 0 921.47 954.29 32.39 o 5 2 0 6372.33 6774.87 96.56 o 6 2 0 46.18 107.61 29.29 o 7 2 0 228.64 233.98 49.59 o 8 2 0 819.35 979.59 108.22 o 9 2 0 247.84 190.32 99.35 o 10 2 0 383.40 138.89 161.55 o 1 3 0 2213.31 1882.13 58.86 o 2 3 0 19.73 25.64 13.50 o 3 3 0 8494.34 8925.88 120.87 o 4 3 0 9882.24 10321.47 150.57 o 5 3 0 205.39 190.58 26.72 o 6 3 0 4137.64 4173.09 83.58 o 7 3 0 1782.79 1504.95 66.37 o 8 3 0 0.39 15.39 56.99 o 9 3 0 939.20 864.13 192.88 o 10 3 0 37.08 93.72 157.91 o 0 4 0 2369.97 2513.87 53.45 o 1 4 0 596.80 517.35 19.00 o 2 4 0 81.45 51.07 17.62 o 3 4 0 218.91 270.81 20.68 o 4 4 0 2206.95 2335.82 55.81 o 5 4 0 87.97 84.24 27.06 o 6 4 0 191.92 226.34 39.49 o 7 4 0 1469.68 1378.40 66.97 o 8 4 0 1127.12 1205.45 111.55 o 9 4 0 76.07 163.46 152.06 o 10 4 0 299.91 132.80 129.50 o 1 5 0 267.74 221.91 27.31 o 2 5 0 11007.85 10546.95 216.50 o 3 5 0 505.00 431.41 29.81 o 4 5 0 18853.22 19280.20 282.25 o 5 5 0 71.30 84.36 24.90 o 6 5 0 5023.97 5310.83 121.16 o 7 5 0 57.25 14.17 49.20 o 8 5 0 2023.02 2033.38 127.92 o 9 5 0 500.43 648.64 155.87 o 10 5 0 56.73 172.31 296.97 o 0 6 0 10769.19 10181.50 316.92 o 1 6 0 9201.01 9411.52 220.62 o 2 6 0 10584.42 11044.15 210.19 o 3 6 0 16354.72 17058.28 299.43 o 4 6 0 1652.96 1692.71 48.61 o 5 6 0 7439.99 7815.84 137.15 o 6 6 0 359.61 257.37 56.57 o 7 6 0 4242.45 4123.42 183.31 o 8 6 0 789.91 751.68 128.55 o 9 6 0 281.83 375.23 148.91 o 1 7 0 625.50 647.32 41.54 o 2 7 0 1033.37 898.17 45.21 o 3 7 0 1670.99 1609.38 60.46 o 4 7 0 3934.16 3966.59 92.41 o 5 7 0 4594.49 4730.38 103.47 o 6 7 0 980.55 1128.09 113.68 o 7 7 0 70.04 190.24 259.21 o 8 7 0 609.14 636.58 226.55 o 9 7 0 23.38 -48.45 133.12 o 0 8 0 5250.33 5442.41 233.70 o 1 8 0 556.35 620.11 48.02 o 2 8 0 3412.36 3199.72 84.89 o 3 8 0 15.54 -10.25 31.64 o 4 8 0 7.02 -35.35 35.35 o 5 8 0 642.23 794.72 63.60 o 6 8 0 0.57 -6.23 119.91 o 7 8 0 1952.54 2127.06 155.22 o 8 8 0 398.70 306.15 184.71 o 9 8 0 1141.26 1331.30 206.37 o 1 9 0 54.69 60.63 29.33 o 2 9 0 3249.89 3339.17 103.10 o 3 9 0 433.54 379.40 44.44 o 4 9 0 4050.79 4030.57 112.57 o 5 9 0 35.08 55.49 60.72 o 6 9 0 1111.01 1183.42 106.48 o 7 9 0 0.09 15.20 92.33 o 8 9 0 157.49 235.74 185.73 o 0 10 0 24.68 -30.62 58.17 o 1 10 0 414.26 402.20 61.23 o 2 10 0 173.01 156.92 55.55 o 3 10 0 174.61 187.45 44.69 o 4 10 0 1734.22 1765.22 86.12 o 5 10 0 1867.22 2366.32 132.07 o 6 10 0 209.44 411.27 142.87 o 7 10 0 672.82 776.61 194.92 o 8 10 0 84.76 213.29 203.08 o 1 11 0 671.20 701.52 67.90 o 2 11 0 6935.14 7472.36 274.01 o 3 11 0 1217.52 1372.85 94.99 o 4 11 0 7643.93 8048.44 260.12 o 5 11 0 42.73 -105.11 105.11 o 6 11 0 2857.09 3587.11 314.32 o 7 11 0 31.38 -55.11 194.92 o 0 12 0 1889.25 2078.79 189.82 o 1 12 0 178.71 95.91 59.71 o 2 12 0 1083.00 984.35 127.05 o 3 12 0 1921.86 1819.19 125.12 o 4 12 0 213.09 134.21 117.87 o 1 13 0 6667.90 7406.38 293.31 o 2 13 0 0.75 -48.48 77.12 o 3 13 0 1178.19 1407.11 121.51 o 4 13 0 94.92 240.84 108.17 o 0 14 0 6610.48 7017.06 462.29 o 1 14 0 0.19 2.01 80.01 o 2 14 0 2009.31 2080.99 145.29 o 3 14 0 161.39 17.97 143.38 o 1 15 0 2100.61 2355.53 238.29 o 2 15 0 6.18 -100.25 304.11 o 3 15 0 163.31 276.44 152.57 o 4 15 0 199.45 -129.61 170.43 o 0 16 0 1209.92 1123.59 266.35 o 1 16 0 0.68 107.06 110.68 o 2 16 0 415.07 646.08 255.64 o 3 16 0 73.05 60.21 195.94 o 1 17 0 604.27 680.23 174.00 o 2 0 1 6951.03 6819.85 70.10 o 3 0 1 5431.24 5524.95 60.25 o 4 0 1 6222.88 6162.64 72.39 o 5 0 1 2095.73 2043.64 42.43 o 6 0 1 5553.18 5822.01 86.33 o 7 0 1 31.55 95.25 49.65 o 8 0 1 226.20 179.55 65.13 o 9 0 1 9.62 69.27 71.82 o 10 0 1 98.72 21.43 197.98 o -10 1 1 138.94 249.23 257.68 o -9 1 1 144.45 180.15 95.72 o -8 1 1 994.95 1123.28 88.84 o -7 1 1 541.27 500.01 52.37 o -6 1 1 106.05 142.94 26.06 o -5 1 1 4178.09 4348.41 66.21 o -4 1 1 1790.54 1766.62 35.61 o -3 1 1 15388.26 15336.18 159.95 o -2 1 1 37482.60 37847.80 810.14 o 2 1 1 36993.71 37489.08 421.91 o 3 1 1 15178.47 15111.26 157.39 o 4 1 1 2033.17 2047.45 37.06 o 5 1 1 3786.64 3870.45 72.29 o 6 1 1 71.91 83.79 25.10 o 7 1 1 448.73 532.54 83.67 o 8 1 1 958.98 997.12 74.10 o 9 1 1 161.73 -96.54 96.54 o 10 1 1 141.62 217.32 162.96 o -10 2 1 68.92 -65.08 153.85 o -9 2 1 468.24 506.92 104.78 o -8 2 1 1040.39 976.47 96.13 o -7 2 1 2561.65 2635.23 81.18 o -6 2 1 1733.92 1711.25 51.09 o -5 2 1 7746.83 8215.62 111.43 o -4 2 1 15884.05 16388.49 240.80 o -3 2 1 14291.15 14457.55 182.68 o -2 2 1 16691.19 16743.69 321.27 o -1 2 1 23033.47 23937.17 673.50 o 0 2 1 697.78 624.14 18.92 o 1 2 1 23319.20 23594.63 400.40 o 2 2 1 16085.42 16254.92 234.39 o 3 2 1 14606.56 14535.43 200.42 o 4 2 1 15130.07 15413.86 187.88 o 5 2 1 7836.30 8274.22 108.89 o 6 2 1 1796.08 1727.06 47.15 o 7 2 1 2578.53 2557.61 99.36 o 8 2 1 1075.07 998.72 87.90 o 9 2 1 461.01 310.64 109.68 o 10 2 1 62.05 129.17 139.05 o -10 3 1 146.58 -116.34 202.06 o -9 3 1 1280.13 1621.92 150.61 o -8 3 1 1048.83 981.70 76.68 o -7 3 1 1189.52 1098.21 55.64 o -6 3 1 6752.58 6826.70 149.87 o -5 3 1 3878.86 3924.08 90.13 o -4 3 1 18402.42 19253.73 278.39 o -3 3 1 2417.23 2292.47 48.88 o -2 3 1 6313.02 5928.51 116.16 o -1 3 1 752.97 724.40 21.87 o 0 3 1 2811.33 2513.14 48.34 o 1 3 1 857.12 846.10 23.29 o 2 3 1 6771.92 6529.72 153.00 o 3 3 1 2550.04 2454.16 47.42 o 4 3 1 18846.83 20155.89 273.57 o 5 3 1 3783.08 3863.64 75.70 o 6 3 1 6895.90 7155.59 148.67 o 7 3 1 1148.35 1024.77 55.10 o 8 3 1 1031.70 913.95 100.26 o 9 3 1 1280.14 1398.12 128.68 o 10 3 1 141.17 279.14 132.88 o -10 4 1 397.88 240.67 393.41 o -9 4 1 358.79 465.20 118.90 o -8 4 1 1425.98 1491.34 113.38 o -7 4 1 528.79 580.54 50.41 o -6 4 1 6594.35 6869.95 152.28 o -5 4 1 2316.84 2306.44 61.45 o -4 4 1 3870.80 3971.36 77.46 o -3 4 1 4242.08 4241.42 103.19 o -2 4 1 1124.34 1081.33 37.70 o -1 4 1 2998.57 3065.13 61.14 o 0 4 1 2084.00 2272.08 36.23 o 1 4 1 2625.19 2647.58 49.22 o 2 4 1 1258.99 1216.80 37.20 o 3 4 1 3874.46 3849.81 82.32 o 4 4 1 3803.27 3790.35 72.42 o 5 4 1 2295.88 2275.93 58.44 o 6 4 1 6540.08 6742.26 123.77 o 7 4 1 585.97 559.72 52.07 o 8 4 1 1415.86 1704.21 150.11 o 9 4 1 345.91 475.51 115.95 o 10 4 1 378.69 282.68 254.11 o -10 5 1 424.62 504.13 278.60 o -9 5 1 753.16 647.15 118.21 o -8 5 1 1011.08 967.94 104.05 o -7 5 1 1311.22 1280.88 71.35 o -6 5 1 763.29 740.90 56.86 o -5 5 1 3049.08 3021.40 128.45 o -4 5 1 1228.46 1236.87 42.04 o -3 5 1 2247.64 2127.28 58.29 o -2 5 1 311.52 299.85 25.63 o -1 5 1 6451.05 6511.26 137.95 o 0 5 1 1.75 -9.69 11.53 o 1 5 1 6367.24 6483.04 103.67 o 2 5 1 397.47 444.03 30.78 o 3 5 1 2235.85 2173.41 68.19 o 4 5 1 1169.89 1225.98 50.48 o 5 5 1 3028.92 3068.55 78.29 o 6 5 1 747.04 822.07 55.54 o 7 5 1 1268.26 1302.53 82.63 o 8 5 1 975.38 855.83 104.54 o 9 5 1 751.93 558.89 147.59 o 10 5 1 407.69 250.70 167.97 o -9 6 1 1011.29 1147.34 161.75 o -8 6 1 308.02 287.52 110.68 o -7 6 1 1053.94 999.14 102.24 o -6 6 1 1011.90 887.25 59.09 o -5 6 1 955.35 1002.20 45.31 o -4 6 1 31.92 66.65 24.59 o -3 6 1 1089.35 1097.69 39.82 o -2 6 1 3299.31 3117.68 71.32 o -1 6 1 4146.84 4079.81 128.64 o 0 6 1 14598.69 13917.48 313.73 o 1 6 1 3955.66 3767.60 95.94 o 2 6 1 3034.47 2953.28 76.85 o 3 6 1 1109.29 1108.58 45.73 o 4 6 1 44.29 24.07 23.33 o 5 6 1 1030.30 967.11 47.65 o 6 6 1 979.21 969.08 61.44 o 7 6 1 1068.74 1075.38 84.80 o 8 6 1 319.12 163.80 113.57 o 9 6 1 1007.21 791.92 165.97 o -9 7 1 585.24 745.24 274.52 o -8 7 1 663.63 732.00 125.12 o -7 7 1 558.17 769.47 175.53 o -6 7 1 510.48 541.76 55.39 o -5 7 1 831.10 875.33 53.75 o -4 7 1 3024.23 3028.21 68.26 o -3 7 1 1334.17 1281.77 82.34 o -2 7 1 5910.18 5781.25 111.97 o -1 7 1 5820.70 5686.68 186.99 o 0 7 1 8218.06 7889.02 193.69 o 1 7 1 6097.26 5804.27 120.19 o 2 7 1 5811.56 5750.10 179.56 o 3 7 1 1360.67 1356.73 56.43 o 4 7 1 3004.28 2982.98 69.67 o 5 7 1 832.62 768.85 44.29 o 6 7 1 491.40 534.98 67.85 o 7 7 1 552.39 428.05 134.71 o 8 7 1 628.91 694.30 142.11 o 9 7 1 592.76 312.50 136.74 o -9 8 1 596.17 462.29 250.03 o -8 8 1 680.08 593.94 205.12 o -7 8 1 619.19 750.08 154.10 o -6 8 1 334.23 291.12 146.44 o -5 8 1 74.17 26.47 32.51 o -4 8 1 990.92 958.98 52.08 o -3 8 1 3436.58 3322.99 79.02 o -2 8 1 5271.71 5061.27 114.04 o -1 8 1 5747.65 5902.27 273.50 o 0 8 1 13468.12 13048.03 349.53 o 1 8 1 5916.80 5780.56 124.87 o 2 8 1 5154.33 5300.25 125.73 o 3 8 1 3634.97 3722.74 162.82 o 4 8 1 988.10 960.56 52.45 o 5 8 1 84.32 71.50 32.54 o 6 8 1 371.66 329.70 77.95 o 7 8 1 647.00 500.78 211.25 o 8 8 1 726.35 811.31 227.57 o 9 8 1 596.33 330.65 278.60 o -8 9 1 347.77 203.08 186.75 o -7 9 1 324.27 281.66 156.14 o -6 9 1 417.20 503.43 95.75 o -5 9 1 372.67 313.63 74.06 o -4 9 1 716.45 613.92 56.50 o -3 9 1 3730.51 3964.80 95.02 o -2 9 1 4127.96 4319.59 149.70 o -1 9 1 6931.67 6899.21 158.94 o 0 9 1 2454.54 2517.49 104.60 o 1 9 1 7019.02 6928.02 187.20 o 2 9 1 4178.25 4201.98 116.51 o 3 9 1 3956.81 4175.91 111.10 o 4 9 1 693.19 753.85 51.30 o 5 9 1 361.37 349.60 51.39 o 6 9 1 422.05 493.14 89.00 o 7 9 1 352.88 308.20 184.71 o 8 9 1 398.20 286.76 185.73 o -8 10 1 204.87 126.54 200.02 o -7 10 1 361.20 461.27 167.36 o -6 10 1 73.78 97.86 77.93 o -5 10 1 773.73 748.13 95.68 o -4 10 1 14.51 63.47 51.50 o -3 10 1 441.08 611.84 71.99 o -2 10 1 147.90 226.49 73.99 o -1 10 1 8322.09 8919.99 232.76 o 0 10 1 1306.48 1430.03 88.33 o 1 10 1 8250.69 8779.37 204.46 o 2 10 1 102.55 93.66 49.43 o 3 10 1 442.92 442.24 66.71 o 4 10 1 11.34 29.45 50.71 o 5 10 1 806.65 862.11 107.98 o 6 10 1 75.83 163.28 130.63 o 7 10 1 338.84 26.53 182.67 o 8 10 1 204.38 683.74 225.53 o -6 11 1 1020.33 967.72 145.93 o -4 11 1 1993.79 2178.80 175.53 o -3 11 1 1013.66 1079.77 108.17 o -2 11 1 3037.29 3031.85 155.82 o -1 11 1 314.01 418.78 97.97 o 0 11 1 4323.08 4398.48 148.13 o 1 11 1 384.11 322.01 48.89 o 2 11 1 2986.25 3073.35 147.12 o 3 11 1 1053.24 957.11 105.62 o 4 11 1 2037.93 2226.38 93.58 o 5 11 1 138.23 305.90 146.95 o 6 11 1 1053.96 906.22 194.92 o -5 12 1 570.08 467.40 146.95 o -4 12 1 1958.91 2023.84 250.54 o -3 12 1 1145.04 1349.06 227.57 o -2 12 1 928.84 1177.52 220.43 o -1 12 1 2645.65 2700.45 290.85 o 0 12 1 555.16 647.01 99.50 o 1 12 1 2653.90 2771.05 210.23 o 2 12 1 909.41 893.35 99.53 o 3 12 1 1123.75 1289.99 146.44 o 4 12 1 1956.09 2282.40 156.47 o 6 12 1 1764.15 1866.52 236.76 o -4 13 1 501.43 468.96 118.89 o -3 13 1 2527.67 2659.84 330.14 o -2 13 1 552.39 554.17 95.16 o -1 13 1 307.85 288.83 88.27 o 0 13 1 537.53 585.52 87.76 o 1 13 1 314.94 371.33 79.94 o 2 13 1 545.37 710.14 164.81 o 3 13 1 2560.46 2693.50 294.42 o 4 13 1 520.71 565.01 108.97 o -4 14 1 1813.54 1913.47 255.13 o -3 14 1 331.51 187.56 194.92 o -2 14 1 1230.81 1367.82 194.92 o -1 14 1 296.70 207.37 74.06 o 0 14 1 360.48 281.84 112.26 o 1 14 1 317.81 366.30 118.89 o 2 14 1 1249.90 1443.44 134.25 o 3 14 1 360.19 107.93 89.88 o 4 14 1 1848.48 2382.90 243.90 o 5 14 1 366.56 385.75 188.80 o 6 14 1 391.90 583.73 229.62 o -3 15 1 885.66 962.06 138.28 o -2 15 1 312.60 364.82 97.97 o -1 15 1 183.79 280.55 105.63 o 0 15 1 200.23 341.56 102.44 o 1 15 1 175.32 227.39 83.33 o 2 15 1 356.30 278.66 103.16 o 3 15 1 846.05 731.24 213.29 o 4 15 1 278.82 365.34 154.10 o -3 16 1 817.08 767.79 202.06 o -2 16 1 1247.41 1318.29 170.78 o -1 16 1 364.64 322.48 201.04 o 0 16 1 44.90 91.28 114.24 o 1 16 1 343.89 500.22 121.95 o 2 16 1 1264.99 1256.05 157.23 o 3 16 1 814.13 478.62 218.39 o -1 17 1 160.31 116.68 119.30 o 0 17 1 1.56 531.69 187.77 o 1 17 1 176.76 302.07 174.51 o 2 0 2 1846.63 1859.90 25.32 o 3 0 2 8167.10 7950.66 88.00 o 4 0 2 2048.69 2063.81 33.96 o 5 0 2 3736.30 3830.98 60.32 o 6 0 2 891.34 843.42 36.80 o 7 0 2 115.62 46.48 52.54 o 8 0 2 10.36 -6.44 60.23 o 9 0 2 751.98 811.47 87.60 o 10 0 2 7.62 -77.28 149.73 o -10 1 2 1503.64 1908.36 209.42 o -9 1 2 137.10 109.26 94.26 o -8 1 2 789.61 748.72 75.79 o -7 1 2 172.43 182.33 36.47 o -6 1 2 20.48 22.65 24.05 o -5 1 2 1206.29 1181.56 37.72 o -4 1 2 6048.70 6099.29 83.33 o -3 1 2 462.77 446.17 15.57 o -2 1 2 45991.46 46760.83 609.96 o -1 1 2 8783.66 8436.42 395.55 o 1 1 2 8566.94 8584.17 98.27 o 2 1 2 43658.54 43834.52 575.79 o 3 1 2 414.63 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