#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/70/2237095.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237095_Fobs loop_ _publ_author_name 'Yan, Biao' 'Li, Hong-Ya' 'Zhao, Ning-Ning' 'Li, Jie' 'Ma, Hai-Xia' _publ_section_title ; 3,3-Dinitroazetidinium chloride ; _journal_coeditor_code ZQ2187 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first o3376 _journal_volume 68 _journal_year 2012 _space_group_IT_number 36 _symmetry_space_group_name_Hall 'C 2c -2' _symmetry_space_group_name_H-M 'C m c 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 6.6807 _cell_length_b 10.4409 _cell_length_c 9.9707 _exptl_crystal_F_000 376.00 _reflns_d_resolution_high 0.7597 _[local]_cod_data_source_file zq2187Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' sa in Cmc2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 131.97 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, z+1/2' '-x, y, z' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, z+1/2' '-x+1/2, y+1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 3 5 -11 150.17 154.67 5.45 o 3 5 -10 17.72 18.57 2.11 o 2 6 -10 113.90 113.31 4.33 o 3 7 -10 195.64 188.77 6.22 o 1 5 -9 511.67 500.74 11.93 o 3 5 -9 80.00 77.75 3.40 o 2 6 -9 30.01 29.98 2.20 o 4 6 -9 9.84 8.12 1.95 o 3 7 -9 66.63 69.56 3.55 o 2 8 -9 92.94 93.69 4.07 o 1 5 -8 53.01 56.52 2.46 o 3 5 -8 31.37 33.61 2.30 o 5 5 -8 11.48 9.85 1.88 o 2 6 -8 308.89 313.93 8.13 o 4 6 -8 221.44 223.77 6.78 o 1 7 -8 267.97 260.07 6.79 o 3 7 -8 206.74 200.43 6.18 o 2 8 -8 3.72 2.47 1.64 o 4 8 -8 5.28 3.52 2.08 o 3 9 -8 145.32 150.14 5.51 o 2 10 -8 139.27 140.66 5.44 o 0 4 -7 6.13 5.12 0.90 o 1 5 -7 345.16 329.89 7.99 o 3 5 -7 791.68 773.00 17.84 o 5 5 -7 120.23 127.33 4.60 o 2 6 -7 69.52 60.74 2.76 o 4 6 -7 19.80 21.26 2.11 o 1 7 -7 229.71 219.02 6.07 o 3 7 -7 36.24 34.24 2.42 o 5 7 -7 82.98 94.42 4.11 o 2 8 -7 238.83 253.29 7.21 o 4 8 -7 196.54 213.04 6.70 o 1 9 -7 101.12 100.43 4.02 o 3 9 -7 122.91 123.28 4.86 o 2 10 -7 118.89 121.59 4.81 o 1 3 -6 1142.54 1207.64 25.44 o 3 3 -6 144.97 147.80 4.92 o 1 5 -6 95.24 104.47 3.31 o 3 5 -6 86.59 78.63 3.29 o 5 5 -6 13.29 13.32 1.78 o 2 6 -6 111.15 112.14 3.69 o 4 6 -6 31.07 34.02 1.78 o 6 6 -6 255.08 261.10 7.80 o 1 7 -6 1099.15 1089.11 24.29 o 3 7 -6 377.07 369.28 7.34 o 5 7 -6 349.47 360.68 7.54 o 0 8 -6 250.26 263.15 6.98 o 2 8 -6 156.40 160.69 5.00 o 4 8 -6 132.07 145.65 3.95 o 1 9 -6 138.70 135.62 4.64 o 3 9 -6 111.12 108.69 4.39 o 5 9 -6 46.70 51.28 4.62 o 2 10 -6 12.59 8.46 1.98 o 4 10 -6 2.10 2.38 3.11 o 1 11 -6 39.67 44.69 3.07 o 3 1 -5 210.56 192.12 5.50 o 2 2 -5 2626.47 2690.52 66.32 o 1 3 -5 970.98 1092.77 22.56 o 3 3 -5 718.33 727.45 19.01 o 2 4 -5 968.98 999.52 25.56 o 4 4 -5 450.58 469.93 12.83 o 6 4 -5 269.78 270.73 7.49 o 1 5 -5 580.91 580.45 16.04 o 3 5 -5 1043.32 1056.67 45.75 o 5 5 -5 241.25 234.04 5.12 o 7 5 -5 39.20 38.61 2.95 o 0 6 -5 249.91 236.44 5.92 o 2 6 -5 86.28 92.23 2.51 o 4 6 -5 75.65 79.28 6.38 o 6 6 -5 57.04 58.18 3.12 o 1 7 -5 50.22 46.56 1.58 o 3 7 -5 324.03 330.76 9.86 o 5 7 -5 11.32 13.07 1.60 o 0 8 -5 330.30 325.19 8.09 o 2 8 -5 191.84 190.78 5.64 o 4 8 -5 97.37 100.02 3.19 o 6 8 -5 78.51 78.61 5.53 o 1 9 -5 161.50 169.90 5.21 o 3 9 -5 412.07 409.68 17.75 o 5 9 -5 76.70 67.36 2.90 o 0 10 -5 70.74 78.37 3.47 o 2 10 -5 31.90 35.35 2.57 o 4 10 -5 24.82 24.09 3.16 o 1 11 -5 50.26 56.94 3.39 o 3 11 -5 150.69 160.52 6.02 o 2 12 -5 14.61 12.51 2.57 o 2 0 -4 4303.89 4526.44 110.41 o 4 0 -4 1647.96 1651.21 42.38 o 3 1 -4 599.52 595.03 10.72 o 2 2 -4 18.15 23.23 1.40 o 4 2 -4 12.21 12.93 1.40 o 1 3 -4 36.25 38.48 1.42 o 3 3 -4 933.91 870.57 22.31 o 5 3 -4 16.84 17.16 1.94 o 7 3 -4 11.32 11.77 1.91 o 0 4 -4 3794.58 3756.61 84.71 o 2 4 -4 1685.29 1781.08 24.22 o 4 4 -4 857.41 855.20 15.06 o 6 4 -4 401.51 392.48 7.59 o 1 5 -4 199.29 181.77 3.25 o 3 5 -4 231.36 231.70 7.41 o 5 5 -4 23.20 31.91 1.71 o 7 5 -4 15.53 19.31 2.31 o 0 6 -4 300.14 307.19 7.58 o 2 6 -4 1692.44 1763.21 38.23 o 4 6 -4 1231.85 1261.28 24.52 o 6 6 -4 85.22 98.81 4.51 o 1 7 -4 318.37 340.19 8.36 o 3 7 -4 410.26 408.53 9.01 o 5 7 -4 62.50 52.29 2.38 o 7 7 -4 26.53 23.96 3.77 o 0 8 -4 284.43 270.25 7.06 o 2 8 -4 230.60 230.43 4.95 o 4 8 -4 95.85 94.63 2.99 o 6 8 -4 49.73 58.98 2.78 o 1 9 -4 246.62 251.50 4.94 o 3 9 -4 111.88 106.33 3.30 o 5 9 -4 102.61 110.04 7.08 o 0 10 -4 296.92 291.54 8.14 o 2 10 -4 272.75 306.00 8.34 o 4 10 -4 188.18 191.39 8.49 o 1 11 -4 24.88 26.31 2.48 o 3 11 -4 3.69 2.57 1.59 o 0 12 -4 23.13 22.52 2.59 o 2 12 -4 8.62 10.53 2.40 o 1 1 -3 3816.99 4293.39 100.81 o 3 1 -3 421.56 414.10 10.87 o 5 1 -3 504.69 486.54 13.13 o 2 2 -3 2066.63 2125.69 52.40 o 4 2 -3 692.27 667.86 17.19 o 6 2 -3 1294.43 1244.28 32.66 o 1 3 -3 612.73 642.53 11.02 o 3 3 -3 215.14 195.71 6.03 o 5 3 -3 52.15 47.05 2.87 o 7 3 -3 44.33 44.20 2.21 o 0 4 -3 574.92 597.53 12.96 o 2 4 -3 387.92 378.82 5.93 o 4 4 -3 219.02 197.85 4.29 o 6 4 -3 136.86 132.49 3.42 o 1 5 -3 1035.57 979.59 20.01 o 3 5 -3 36.18 30.08 1.71 o 5 5 -3 173.33 176.96 4.04 o 7 5 -3 104.34 106.49 3.43 o 0 6 -3 1256.98 1285.85 28.61 o 2 6 -3 268.17 270.24 4.14 o 4 6 -3 180.28 179.34 5.13 o 6 6 -3 134.21 132.94 3.73 o 1 7 -3 174.69 173.34 3.00 o 3 7 -3 135.89 127.12 3.12 o 5 7 -3 31.68 37.84 1.98 o 7 7 -3 12.64 13.05 1.88 o 0 8 -3 613.31 610.05 14.10 o 2 8 -3 255.37 258.49 4.21 o 4 8 -3 158.87 162.68 4.12 o 6 8 -3 162.90 184.00 4.74 o 1 9 -3 661.73 671.48 11.19 o 3 9 -3 136.55 138.21 4.12 o 5 9 -3 189.58 202.05 5.06 o 0 10 -3 177.95 168.05 5.42 o 2 10 -3 204.32 195.37 5.73 o 4 10 -3 130.33 135.80 3.98 o 1 11 -3 438.53 437.49 10.04 o 3 11 -3 77.58 74.48 3.03 o 0 12 -3 163.70 163.14 5.73 o 2 12 -3 49.64 49.69 3.61 o 1 13 -3 10.12 10.10 2.49 o 2 0 -2 6830.64 6702.69 164.86 o 6 0 -2 87.16 79.48 3.56 o 1 1 -2 653.53 674.93 16.65 o 3 1 -2 653.92 711.03 11.74 o 5 1 -2 70.36 68.54 2.99 o 7 1 -2 49.05 48.47 3.35 o 0 2 -2 2325.04 2309.99 50.01 o 2 2 -2 1237.50 1233.63 19.75 o 4 2 -2 300.73 293.75 8.40 o 6 2 -2 186.72 180.37 6.26 o 1 3 -2 3616.30 3630.95 45.73 o 3 3 -2 2282.77 2303.37 24.94 o 5 3 -2 667.25 678.64 11.72 o 7 3 -2 147.61 156.87 8.50 o 0 4 -2 560.96 581.01 12.83 o 2 4 -2 846.45 925.56 13.17 o 4 4 -2 443.36 440.58 10.67 o 6 4 -2 14.21 12.71 1.27 o 8 4 -2 40.87 40.53 3.91 o 1 5 -2 180.61 181.41 6.18 o 3 5 -2 538.72 574.48 8.90 o 5 5 -2 16.62 21.08 1.38 o 7 5 -2 14.71 12.44 1.62 o 0 6 -2 1314.51 1304.20 28.10 o 2 6 -2 351.71 359.55 5.27 o 4 6 -2 176.35 152.21 3.57 o 6 6 -2 241.38 233.36 5.25 o 1 7 -2 1392.55 1450.84 19.36 o 3 7 -2 1982.52 2014.01 33.36 o 5 7 -2 494.09 470.40 8.99 o 7 7 -2 94.72 95.10 3.46 o 0 8 -2 262.30 267.76 6.98 o 2 8 -2 48.19 44.63 1.98 o 4 8 -2 27.55 26.35 1.57 o 6 8 -2 59.35 60.41 4.99 o 1 9 -2 16.21 13.03 0.94 o 3 9 -2 220.58 221.89 5.10 o 5 9 -2 5.97 6.11 1.44 o 0 10 -2 384.02 377.17 9.56 o 2 10 -2 7.38 8.69 1.03 o 4 10 -2 0.77 0.31 1.37 o 1 11 -2 1.75 1.83 1.17 o 3 11 -2 149.93 146.19 4.36 o 0 12 -2 98.97 99.20 4.38 o 2 12 -2 139.52 147.35 5.52 o 1 13 -2 72.62 81.57 3.19 o 1 1 -1 4358.20 4230.67 99.56 o 3 1 -1 418.37 446.32 7.32 o 5 1 -1 265.61 267.55 6.03 o 7 1 -1 145.60 154.92 16.81 o 0 2 -1 3193.76 3073.13 64.50 o 2 2 -1 6410.71 5651.49 80.44 o 4 2 -1 1922.15 2022.78 25.09 o 6 2 -1 277.41 285.87 5.63 o 8 2 -1 159.68 155.57 6.59 o 1 3 -1 3047.21 3000.44 93.94 o 3 3 -1 433.28 465.59 5.53 o 5 3 -1 241.95 223.95 4.57 o 7 3 -1 113.48 111.01 5.14 o 0 4 -1 707.27 645.97 16.93 o 2 4 -1 2014.65 2046.73 26.15 o 4 4 -1 907.00 975.16 12.76 o 6 4 -1 125.63 133.67 4.29 o 8 4 -1 96.28 100.84 5.62 o 1 5 -1 2996.02 2985.34 38.58 o 3 5 -1 2790.37 2815.28 36.06 o 5 5 -1 632.63 598.56 10.75 o 7 5 -1 163.38 168.16 4.29 o 0 6 -1 505.48 495.98 11.29 o 2 6 -1 198.16 203.91 4.08 o 4 6 -1 120.42 108.94 2.75 o 6 6 -1 42.27 42.73 2.11 o 1 7 -1 257.10 252.22 3.92 o 3 7 -1 479.86 454.22 8.41 o 5 7 -1 82.22 76.19 2.54 o 7 7 -1 26.31 27.48 2.21 o 0 8 -1 837.49 812.28 19.09 o 2 8 -1 618.75 613.90 8.61 o 4 8 -1 421.43 383.50 7.46 o 6 8 -1 141.33 143.03 4.06 o 1 9 -1 155.22 158.35 2.99 o 3 9 -1 231.25 225.45 6.50 o 5 9 -1 83.33 73.35 4.16 o 0 10 -1 234.42 223.22 6.51 o 2 10 -1 135.78 127.45 2.77 o 4 10 -1 109.82 101.70 3.39 o 1 11 -1 83.55 88.93 2.78 o 3 11 -1 126.45 132.61 4.22 o 0 12 -1 134.86 131.83 5.13 o 2 12 -1 68.34 70.74 2.35 o 1 13 -1 18.65 19.01 3.80 o 4 0 0 5486.00 5304.71 113.00 o 6 0 0 4838.82 5075.34 99.73 o 1 1 0 14.37 17.51 0.41 o 3 1 0 573.09 581.00 8.64 o 5 1 0 27.17 25.25 1.40 o 7 1 0 13.39 15.67 2.98 o 0 2 0 2398.75 2356.45 62.73 o 2 2 0 1434.87 1474.90 32.60 o 4 2 0 723.85 739.14 8.26 o 6 2 0 186.56 187.99 5.10 o 8 2 0 68.33 78.09 5.92 o 1 3 0 364.60 453.49 5.06 o 3 3 0 0.26 4.44 1.28 o 5 3 0 72.36 54.93 2.01 o 7 3 0 74.26 73.01 4.39 o 0 4 0 6034.15 5951.92 346.81 o 2 4 0 150.23 155.84 2.52 o 4 4 0 12.17 13.84 1.01 o 6 4 0 452.33 431.37 8.11 o 8 4 0 0.50 1.01 1.49 o 1 5 0 877.71 883.32 9.80 o 3 5 0 142.18 159.79 3.38 o 5 5 0 78.39 67.14 6.15 o 7 5 0 32.71 29.74 3.26 o 0 6 0 9.85 4.33 0.62 o 2 6 0 81.96 66.59 1.47 o 4 6 0 138.51 147.49 2.68 o 6 6 0 35.97 42.42 2.10 o 1 7 0 601.37 593.04 8.63 o 3 7 0 23.59 22.40 0.99 o 5 7 0 86.98 93.75 2.84 o 7 7 0 104.35 97.34 5.75 o 0 8 0 30.96 26.10 1.86 o 2 8 0 86.42 93.19 2.05 o 4 8 0 21.31 24.84 1.57 o 6 8 0 13.19 8.65 1.58 o 1 9 0 576.55 568.78 8.26 o 3 9 0 1.26 1.50 0.79 o 5 9 0 217.73 226.67 5.33 o 0 10 0 782.76 775.05 18.26 o 2 10 0 725.99 693.46 10.04 o 4 10 0 416.17 419.67 8.49 o 1 11 0 100.43 90.60 2.39 o 3 11 0 43.08 45.97 1.85 o 0 12 0 190.68 186.47 6.17 o 2 12 0 80.75 73.47 2.57 o 1 13 0 102.71 106.00 3.74 o 1 1 1 4472.68 4157.28 71.99 o 3 1 1 385.60 411.83 4.61 o 5 1 1 286.65 273.29 3.20 o 7 1 1 156.37 170.95 4.83 o 0 2 1 3155.56 2994.84 62.83 o 2 2 1 6397.17 5787.46 157.09 o 4 2 1 1925.96 1987.54 26.51 o 6 2 1 271.81 282.01 6.79 o 8 2 1 159.15 177.22 11.37 o 1 3 1 3065.88 2950.56 30.67 o 3 3 1 427.98 457.80 5.28 o 5 3 1 245.11 230.59 3.62 o 7 3 1 114.89 118.04 7.10 o 0 4 1 726.92 683.97 8.64 o 2 4 1 1963.06 1968.78 21.66 o 4 4 1 880.61 925.44 12.23 o 6 4 1 127.61 135.17 5.51 o 8 4 1 93.85 105.67 3.43 o 1 5 1 3007.06 2968.53 38.11 o 3 5 1 2762.12 2741.59 30.02 o 5 5 1 636.13 594.89 15.18 o 7 5 1 164.59 169.84 4.13 o 0 6 1 491.34 484.07 6.55 o 2 6 1 191.44 195.51 2.58 o 4 6 1 115.70 103.06 2.14 o 6 6 1 39.97 36.99 1.98 o 1 7 1 251.85 249.49 3.96 o 3 7 1 490.91 472.93 6.79 o 5 7 1 80.29 83.08 2.89 o 7 7 1 25.27 23.44 3.51 o 0 8 1 873.45 859.49 16.85 o 2 8 1 600.31 593.18 9.50 o 4 8 1 407.59 372.44 5.82 o 6 8 1 149.49 146.62 4.02 o 1 9 1 161.78 159.89 3.62 o 3 9 1 234.85 230.05 8.37 o 5 9 1 86.99 80.60 4.01 o 0 10 1 237.97 234.37 6.74 o 2 10 1 138.26 134.15 4.06 o 4 10 1 112.59 102.86 2.62 o 1 11 1 92.06 95.98 2.57 o 3 11 1 131.74 133.98 3.43 o 0 12 1 141.74 141.01 5.17 o 2 12 1 65.33 68.46 2.28 o 1 13 1 17.92 18.45 1.89 o 0 0 2 1202.94 1162.93 17.02 o 2 0 2 6835.19 6700.74 123.42 o 4 0 2 2460.84 2441.42 29.39 o 6 0 2 76.37 75.31 2.66 o 1 1 2 622.90 666.82 5.22 o 3 1 2 670.12 721.31 6.86 o 5 1 2 65.18 59.58 1.15 o 7 1 2 46.08 47.36 2.50 o 0 2 2 2323.48 2338.86 25.30 o 2 2 2 1249.13 1217.12 10.37 o 4 2 2 306.03 299.95 3.49 o 6 2 2 185.29 183.32 2.50 o 8 2 2 44.66 49.63 5.45 o 1 3 2 3605.52 3507.64 30.21 o 3 3 2 2330.45 2326.03 25.13 o 5 3 2 665.30 668.76 7.60 o 7 3 2 144.88 163.77 4.50 o 0 4 2 547.10 572.55 8.72 o 2 4 2 854.42 910.96 12.37 o 4 4 2 447.20 439.31 5.19 o 6 4 2 13.10 11.19 1.20 o 8 4 2 41.99 45.43 3.10 o 1 5 2 185.30 182.49 2.40 o 3 5 2 537.80 563.18 6.54 o 5 5 2 17.63 22.61 1.93 o 7 5 2 15.17 12.69 1.46 o 0 6 2 1286.53 1269.48 16.38 o 2 6 2 364.08 364.73 5.81 o 4 6 2 187.26 159.79 3.60 o 6 6 2 237.11 237.74 5.03 o 1 7 2 1386.53 1461.86 14.18 o 3 7 2 1995.60 1990.76 29.42 o 5 7 2 492.15 474.38 7.10 o 7 7 2 93.33 89.82 3.11 o 0 8 2 263.78 266.98 4.09 o 2 8 2 48.45 45.67 1.47 o 4 8 2 27.73 31.38 1.43 o 6 8 2 59.84 62.79 4.55 o 1 9 2 11.89 9.82 0.94 o 3 9 2 219.41 231.57 4.00 o 5 9 2 4.29 5.16 1.46 o 0 10 2 363.85 358.45 9.68 o 2 10 2 5.38 4.37 0.92 o 4 10 2 0.67 0.17 1.00 o 1 11 2 1.63 1.96 0.98 o 3 11 2 150.08 147.51 3.29 o 0 12 2 96.62 102.27 4.57 o 2 12 2 138.81 142.07 3.68 o 1 13 2 71.35 80.39 4.37 o 1 1 3 3737.34 4025.18 41.79 o 3 1 3 407.58 412.95 4.10 o 5 1 3 489.77 483.05 5.49 o 7 1 3 225.74 244.28 3.28 o 0 2 3 17416.95 16344.74 202.36 o 2 2 3 2048.37 2127.32 16.42 o 4 2 3 681.97 646.04 6.34 o 6 2 3 1304.51 1271.00 13.54 o 8 2 3 99.06 96.23 5.68 o 1 3 3 605.58 642.00 5.47 o 3 3 3 220.04 213.79 3.75 o 5 3 3 50.53 48.45 1.08 o 7 3 3 43.30 43.40 2.25 o 0 4 3 562.63 575.71 6.36 o 2 4 3 410.46 393.44 3.63 o 4 4 3 230.60 215.60 3.12 o 6 4 3 136.74 129.19 2.62 o 1 5 3 1044.35 996.99 8.68 o 3 5 3 37.54 33.15 1.18 o 5 5 3 172.72 174.96 3.09 o 7 5 3 104.64 107.83 3.23 o 0 6 3 1276.70 1315.13 14.10 o 2 6 3 275.11 277.85 3.09 o 4 6 3 185.34 185.50 3.07 o 6 6 3 137.40 138.52 2.81 o 1 7 3 182.94 181.72 2.75 o 3 7 3 126.69 119.02 2.46 o 5 7 3 33.44 33.85 1.23 o 0 8 3 599.97 601.83 9.63 o 2 8 3 265.84 261.30 5.20 o 4 8 3 165.91 177.43 3.33 o 6 8 3 160.87 179.16 4.41 o 1 9 3 660.31 675.18 8.02 o 3 9 3 131.70 138.24 3.26 o 5 9 3 188.52 197.71 4.48 o 0 10 3 176.26 180.83 3.80 o 2 10 3 203.85 194.33 4.80 o 4 10 3 128.79 134.51 3.10 o 1 11 3 438.24 426.79 6.88 o 3 11 3 73.69 72.24 2.39 o 0 12 3 161.28 160.83 5.93 o 2 12 3 50.78 48.09 2.14 o 0 0 4 10703.54 11197.35 300.13 o 2 0 4 4369.63 4517.02 54.02 o 4 0 4 1674.27 1728.10 25.19 o 6 0 4 799.82 798.47 15.31 o 8 0 4 183.83 175.31 5.40 o 1 1 4 1039.86 1088.92 8.60 o 3 1 4 588.34 593.81 4.81 o 5 1 4 72.19 61.83 1.49 o 7 1 4 56.11 53.59 1.96 o 0 2 4 846.66 929.71 10.22 o 2 2 4 20.91 25.23 0.47 o 4 2 4 12.80 12.68 0.57 o 6 2 4 40.60 37.88 1.11 o 8 2 4 1.33 1.35 1.33 o 1 3 4 46.84 46.78 0.57 o 3 3 4 898.45 878.93 7.67 o 5 3 4 19.03 18.48 0.88 o 7 3 4 14.12 11.73 1.13 o 0 4 4 3775.93 4004.65 46.53 o 2 4 4 1675.90 1724.49 15.11 o 4 4 4 849.04 845.34 8.51 o 6 4 4 400.45 382.05 8.07 o 1 5 4 198.73 175.62 3.22 o 3 5 4 235.33 234.04 3.19 o 5 5 4 23.19 29.93 1.27 o 7 5 4 15.22 19.59 2.55 o 0 6 4 306.76 313.04 3.73 o 2 6 4 1665.32 1693.66 14.90 o 4 6 4 1214.17 1231.85 12.23 o 6 6 4 87.03 98.13 3.22 o 1 7 4 314.27 323.96 3.46 o 3 7 4 395.84 396.12 4.37 o 5 7 4 61.57 51.13 1.76 o 0 8 4 285.52 268.74 4.18 o 2 8 4 231.43 229.65 2.53 o 4 8 4 96.55 98.62 1.96 o 6 8 4 49.88 57.21 2.10 o 1 9 4 251.78 260.40 3.18 o 3 9 4 116.63 111.13 2.47 o 5 9 4 104.83 109.16 2.67 o 0 10 4 314.57 307.12 9.41 o 2 10 4 272.94 275.59 4.86 o 4 10 4 187.10 181.34 3.08 o 1 11 4 25.27 23.91 2.81 o 3 11 4 3.91 2.13 1.26 o 0 12 4 24.52 18.85 2.69 o 2 12 4 8.15 9.69 1.76 o 1 1 5 735.58 720.13 5.80 o 3 1 5 210.02 192.87 1.95 o 5 1 5 180.27 176.23 2.47 o 7 1 5 52.30 55.56 1.48 o 0 2 5 2082.27 2273.44 28.70 o 2 2 5 2629.00 2691.17 20.80 o 4 2 5 1449.20 1447.48 15.30 o 6 2 5 289.39 279.69 3.65 o 8 2 5 119.28 117.62 5.02 o 1 3 5 980.25 1032.56 7.84 o 3 3 5 720.27 738.53 6.54 o 5 3 5 172.59 165.91 2.40 o 7 3 5 57.63 54.03 1.73 o 0 4 5 1378.42 1427.09 15.32 o 2 4 5 958.19 999.76 8.70 o 4 4 5 445.90 455.87 4.92 o 6 4 5 266.49 269.81 3.73 o 1 5 5 592.63 575.18 5.91 o 3 5 5 1076.31 1062.06 9.49 o 5 5 5 248.24 236.74 3.29 o 7 5 5 40.09 42.52 1.86 o 0 6 5 242.44 226.42 7.00 o 2 6 5 86.27 88.96 2.42 o 4 6 5 75.77 80.75 1.64 o 6 6 5 54.94 54.44 1.91 o 1 7 5 53.84 50.77 0.96 o 3 7 5 337.42 335.36 3.82 o 5 7 5 12.82 14.31 1.16 o 0 8 5 322.01 307.60 5.62 o 2 8 5 185.92 189.84 2.25 o 4 8 5 94.76 99.56 2.56 o 6 8 5 75.18 77.97 3.31 o 1 9 5 158.17 163.63 2.53 o 3 9 5 416.29 410.10 5.53 o 5 9 5 75.64 68.76 2.51 o 0 10 5 72.08 74.19 2.43 o 2 10 5 32.98 35.27 3.21 o 4 10 5 25.93 26.29 1.35 o 1 11 5 46.15 50.85 1.93 o 3 11 5 153.83 165.98 11.37 o 0 12 5 46.46 49.92 3.69 o 0 0 6 1357.17 1415.26 20.86 o 2 0 6 1311.96 1328.62 15.87 o 4 0 6 506.96 493.46 6.40 o 6 0 6 392.89 365.44 7.92 o 1 1 6 544.22 538.40 4.46 o 3 1 6 53.77 52.86 0.85 o 5 1 6 118.14 112.72 1.88 o 7 1 6 86.06 83.28 1.85 o 0 2 6 149.99 162.83 2.07 o 2 2 6 105.52 110.23 1.19 o 4 2 6 62.81 55.76 1.12 o 6 2 6 84.29 79.73 1.67 o 1 3 6 1148.77 1162.03 8.80 o 3 3 6 157.25 156.47 1.95 o 5 3 6 326.53 324.40 4.10 o 7 3 6 158.83 169.51 6.53 o 0 4 6 421.99 411.05 5.30 o 2 4 6 267.78 278.65 2.62 o 4 4 6 86.32 84.60 1.66 o 6 4 6 86.75 90.82 4.26 o 1 5 6 98.14 105.87 1.67 o 3 5 6 84.56 79.72 1.24 o 5 5 6 13.96 12.79 1.35 o 7 5 6 14.14 10.82 2.49 o 0 6 6 1119.58 1103.72 16.82 o 2 6 6 109.29 106.67 1.46 o 4 6 6 30.52 33.76 1.15 o 6 6 6 251.50 256.84 4.54 o 1 7 6 1107.91 1060.45 11.55 o 3 7 6 381.63 372.16 3.83 o 5 7 6 352.11 359.27 5.74 o 0 8 6 249.68 258.15 8.65 o 2 8 6 156.71 156.46 2.14 o 4 8 6 132.25 138.74 2.98 o 1 9 6 139.84 131.83 2.30 o 3 9 6 105.29 108.78 2.43 o 5 9 6 46.98 48.75 1.99 o 0 10 6 393.25 400.53 7.27 o 2 10 6 11.50 9.31 1.21 o 4 10 6 2.12 10.53 2.01 o 1 11 6 39.22 41.09 1.82 o 3 11 6 16.74 19.79 2.79 o 1 1 7 136.84 136.37 1.31 o 3 1 7 622.29 622.67 6.17 o 5 1 7 41.47 42.43 1.23 o 7 1 7 7.79 8.34 1.03 o 0 2 7 2745.75 2829.31 29.14 o 2 2 7 898.71 884.07 7.66 o 4 2 7 563.47 551.96 5.63 o 6 2 7 388.66 368.11 4.71 o 1 3 7 64.25 62.81 0.92 o 3 3 7 340.35 324.42 4.00 o 5 3 7 32.90 29.02 1.15 o 7 3 7 8.69 7.76 1.50 o 0 4 7 5.93 5.16 0.56 o 2 4 7 199.07 184.19 2.89 o 4 4 7 186.07 179.51 2.17 o 6 4 7 7.17 6.15 0.83 o 1 5 7 338.63 317.55 3.92 o 3 5 7 770.96 758.20 7.69 o 5 5 7 117.25 125.69 2.94 o 0 6 7 135.17 128.96 2.87 o 2 6 7 71.50 64.08 1.23 o 4 6 7 20.64 23.28 1.05 o 6 6 7 36.59 37.06 2.39 o 1 7 7 234.00 217.49 3.05 o 3 7 7 35.05 36.69 1.46 o 5 7 7 84.78 91.81 2.50 o 0 8 7 9.64 13.44 2.08 o 2 8 7 237.19 254.26 3.57 o 4 8 7 194.68 205.13 6.77 o 1 9 7 102.12 94.07 1.99 o 3 9 7 118.63 127.93 2.85 o 0 10 7 95.89 98.64 3.03 o 2 10 7 118.62 124.47 3.14 o 1 11 7 69.68 71.41 2.30 o 0 0 8 2128.61 2144.13 35.50 o 2 0 8 1303.20 1273.09 15.41 o 4 0 8 829.16 819.26 12.92 o 6 0 8 415.08 416.66 7.47 o 1 1 8 44.84 43.79 0.95 o 3 1 8 17.91 18.70 1.33 o 5 1 8 7.03 8.60 0.82 o 0 2 8 394.65 405.65 4.68 o 2 2 8 431.02 426.53 4.44 o 4 2 8 278.96 273.29 3.20 o 6 2 8 103.43 105.86 2.13 o 1 3 8 207.88 212.38 2.28 o 3 3 8 215.99 217.64 2.64 o 5 3 8 61.48 63.11 1.59 o 0 4 8 246.39 244.06 4.50 o 2 4 8 597.94 580.03 5.88 o 4 4 8 400.59 390.87 4.51 o 6 4 8 40.11 37.88 2.02 o 1 5 8 51.84 55.10 1.11 o 3 5 8 33.04 34.88 1.35 o 5 5 8 11.11 9.98 1.04 o 0 6 8 155.13 144.88 3.21 o 2 6 8 312.68 308.25 3.91 o 4 6 8 224.21 224.27 3.21 o 1 7 8 260.38 239.00 3.37 o 3 7 8 210.08 201.70 2.97 o 5 7 8 78.59 81.90 3.79 o 0 8 8 72.29 58.99 2.23 o 2 8 8 3.67 4.68 1.96 o 4 8 8 5.18 6.06 1.16 o 1 9 8 34.21 35.87 1.90 o 3 9 8 153.53 157.24 3.54 o 0 10 8 61.39 63.33 3.45 o 2 10 8 138.72 144.59 3.85 o 1 1 9 359.99 365.72 3.53 o 3 1 9 138.04 131.94 1.90 o 5 1 9 119.07 118.97 2.21 o 0 2 9 620.86 634.18 8.10 o 2 2 9 529.21 544.09 5.58 o 4 2 9 268.89 258.53 3.31 o 1 3 9 114.14 117.02 1.69 o 3 3 9 172.69 169.33 2.33 o 5 3 9 36.14 36.05 1.73 o 0 4 9 699.09 669.47 10.74 o 2 4 9 188.57 174.08 2.28 o 4 4 9 87.09 88.38 1.67 o 1 5 9 509.86 507.66 6.03 o 3 5 9 79.92 79.87 2.12 o 5 5 9 172.80 169.89 5.13 o 0 6 9 45.47 40.86 1.86 o 2 6 9 29.89 31.60 1.20 o 4 6 9 9.59 9.34 0.96 o 1 7 9 36.00 32.11 1.22 o 3 7 9 63.68 65.67 2.01 o 0 8 9 461.70 461.73 8.18 o 2 8 9 86.68 90.50 2.30 o 1 9 9 145.48 142.54 2.64 o 0 0 10 470.37 502.44 11.35 o 2 0 10 853.11 842.64 10.66 o 4 0 10 547.62 538.34 9.18 o 1 1 10 105.08 99.93 1.44 o 3 1 10 148.38 150.26 2.45 o 5 1 10 44.04 44.49 1.54 o 0 2 10 46.61 42.11 1.59 o 2 2 10 45.30 41.09 1.11 o 4 2 10 25.68 27.47 1.19 o 1 3 10 180.63 174.91 2.56 o 3 3 10 280.18 280.98 3.39 o 0 4 10 217.87 208.49 9.92 o 2 4 10 71.48 70.91 1.47 o 4 4 10 54.38 50.75 1.61 o 1 5 10 4.93 2.66 0.84 o 3 5 10 16.73 18.43 1.15 o 0 6 10 62.70 65.45 2.38 o 2 6 10 115.02 120.17 2.60 o 1 7 10 170.61 162.53 3.18 o 0 8 10 109.46 108.84 3.21 o 1 1 11 56.02 53.69 1.25 o 3 1 11 152.40 153.05 2.59 o 0 2 11 293.63 295.16 9.50 o 2 2 11 235.82 233.10 2.96 o 4 2 11 155.02 174.04 3.42 o 1 3 11 8.87 9.33 0.88 o 3 3 11 68.33 67.56 2.00 o 0 4 11 70.27 64.38 3.09 o 2 4 11 83.41 91.58 1.92 o 4 4 11 70.12 76.78 4.08 o 1 5 11 172.12 167.09 3.19 o 3 5 11 150.65 152.67 7.79 o 0 6 11 7.10 8.27 1.53 o 2 6 11 10.03 8.75 2.48 o 1 7 11 29.11 25.92 2.96 o 0 0 12 546.20 540.99 12.46 o 2 0 12 277.38 300.73 5.84 o 1 1 12 10.60 12.21 1.39 o 3 1 12 12.61 13.59 1.78 o 0 2 12 189.41 197.12 5.86 o 2 2 12 102.71 104.18 2.35 o 1 3 12 158.32 167.88 3.83 o 3 3 12 14.42 14.11 1.67 o 0 4 12 130.69 120.58 4.63 o 2 4 12 42.32 47.85 2.36 o 1 5 12 5.07 3.48 2.53 o 1 1 13 9.32 8.23 1.55 o