#------------------------------------------------------------------------------ #$Date: 2013-02-22 12:27:16 +0200 (Fri, 22 Feb 2013) $ #$Revision: 74188 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/23/70/2237096.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2237096_Fobs loop_ _publ_author_name 'Davis, Wade L.' 'Muller, Alfred' _publ_section_title ; trans-Dichloridobis{tris[4-(trifluoromethyl)phenyl]phosphane-\kP}palladium(II) dichloromethane monosolvate ; _journal_coeditor_code ZQ2189 _journal_issue 12 _journal_name_full 'Acta Crystallographica Section E' _journal_page_first m1508 _journal_page_last m1509 _journal_volume 68 _journal_year 2012 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 72.764 _cell_angle_beta 78.362 _cell_angle_gamma 75.545 _cell_length_a 12.1491 _cell_length_b 14.0203 _cell_length_c 14.4334 _exptl_crystal_F_000 1180.00 _reflns_d_resolution_high 0.7494 _[local]_cod_data_source_file zq2189Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mo_12fm_wld11_0m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 269.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2.40 54.57 3.46 o 2 0 0 34158.65 33843.17 504.91 o 3 0 0 15523.05 16817.67 113.59 o 4 0 0 335.26 310.89 7.03 o 5 0 0 110.30 226.86 8.53 o 6 0 0 3528.86 3494.44 29.33 o 7 0 0 469.46 420.17 11.01 o 8 0 0 3176.88 3175.84 33.05 o 9 0 0 938.11 1122.04 21.10 o 10 0 0 746.42 642.36 17.50 o 11 0 0 573.74 509.85 21.50 o 12 0 0 50.49 42.10 13.10 o 13 0 0 49.89 64.99 13.32 o 14 0 0 1214.73 1188.03 65.26 o 15 0 0 30.41 48.20 15.02 o -15 1 0 39.14 53.14 16.21 o -14 1 0 1347.02 1427.90 43.89 o -13 1 0 466.09 435.64 24.17 o -12 1 0 24.18 -0.30 8.27 o -11 1 0 159.33 168.25 14.39 o -10 1 0 174.59 196.03 12.35 o -9 1 0 34.06 41.74 6.99 o -8 1 0 1949.20 1873.16 27.94 o -7 1 0 675.57 605.99 14.97 o -6 1 0 16114.64 16346.13 104.49 o -5 1 0 9989.38 10635.77 83.59 o -4 1 0 6042.84 6279.85 52.55 o -3 1 0 6689.01 6822.38 48.12 o -2 1 0 8.09 16.43 2.53 o -1 1 0 595.74 685.99 8.18 o 0 1 0 6655.32 6147.24 225.76 o 1 1 0 533.00 443.01 5.00 o 2 1 0 23214.89 23822.82 122.40 o 3 1 0 6674.96 7085.82 36.78 o 4 1 0 830.93 813.06 10.08 o 5 1 0 2091.27 2144.59 20.87 o 6 1 0 31.54 7.88 4.07 o 7 1 0 344.72 332.88 9.13 o 8 1 0 3858.43 3790.59 35.01 o 9 1 0 681.35 751.43 24.38 o 10 1 0 1771.73 1680.06 31.52 o 11 1 0 193.12 164.08 13.42 o 12 1 0 176.21 190.23 15.05 o 13 1 0 1252.27 1180.35 40.90 o 14 1 0 671.68 727.35 32.88 o 15 1 0 4.48 -2.75 11.59 o -15 2 0 32.62 56.14 22.73 o -14 2 0 378.93 423.58 29.34 o -13 2 0 248.10 284.34 21.12 o -12 2 0 407.03 393.12 22.87 o -11 2 0 538.50 574.51 25.61 o -10 2 0 32.66 30.97 10.94 o -9 2 0 2382.31 2259.73 34.28 o -8 2 0 186.61 215.15 12.07 o -7 2 0 125.59 170.97 10.27 o -6 2 0 1707.77 1561.15 21.67 o -5 2 0 1617.85 1602.48 21.10 o -4 2 0 8628.63 8788.17 70.66 o -3 2 0 4176.41 4262.02 40.50 o -2 2 0 55440.05 56263.41 531.46 o -1 2 0 209.89 154.34 6.29 o 0 2 0 6095.42 6278.81 61.45 o 1 2 0 2.60 8.86 1.86 o 2 2 0 1275.63 1170.29 10.70 o 3 2 0 10034.19 9912.83 49.93 o 4 2 0 5.49 13.52 4.73 o 5 2 0 1987.54 2161.66 19.88 o 6 2 0 92.58 51.71 7.26 o 7 2 0 194.31 203.42 9.16 o 8 2 0 5771.55 5440.10 50.14 o 9 2 0 22.88 29.28 6.30 o 10 2 0 397.29 390.08 22.43 o 11 2 0 193.84 254.19 15.44 o 12 2 0 984.99 971.84 31.36 o 13 2 0 66.30 64.59 13.32 o 14 2 0 439.44 437.76 27.32 o 15 2 0 33.85 2.70 25.12 o -14 3 0 262.55 310.12 23.25 o -13 3 0 174.42 201.78 18.99 o -12 3 0 621.16 648.77 31.43 o -11 3 0 291.44 285.34 17.50 o -10 3 0 1411.92 1489.27 31.09 o -9 3 0 35.96 38.45 8.35 o -8 3 0 308.51 297.56 21.63 o -7 3 0 4082.07 4103.81 50.26 o -6 3 0 310.23 301.81 11.63 o -5 3 0 1.25 -2.60 3.51 o -4 3 0 18534.10 17575.40 102.05 o -3 3 0 6411.98 6325.60 50.03 o -2 3 0 6274.56 6230.67 48.18 o -1 3 0 349.73 504.37 10.22 o 0 3 0 3785.04 3725.57 34.85 o 1 3 0 657.04 604.92 10.35 o 2 3 0 51634.95 51822.99 436.69 o 3 3 0 3161.55 3695.68 28.18 o 4 3 0 15151.54 15741.41 94.11 o 5 3 0 502.13 578.49 10.21 o 6 3 0 9108.54 9476.42 64.18 o 7 3 0 2344.00 2403.53 28.45 o 8 3 0 2397.63 2393.69 32.29 o 9 3 0 1492.33 1609.38 27.48 o 10 3 0 1606.33 1505.68 38.89 o 11 3 0 22.99 41.96 9.68 o 12 3 0 674.47 672.33 38.18 o 13 3 0 4.45 3.00 9.36 o 14 3 0 99.89 82.93 14.93 o 15 3 0 3.31 16.04 20.02 o -14 4 0 341.02 362.86 23.37 o -13 4 0 8.43 21.90 10.57 o -12 4 0 1027.27 999.34 29.90 o -11 4 0 35.77 12.88 8.92 o -10 4 0 753.33 749.37 22.19 o -9 4 0 103.86 104.77 11.87 o -8 4 0 1847.89 1844.60 29.74 o -7 4 0 720.95 688.10 16.21 o -6 4 0 1507.78 1529.74 22.89 o -5 4 0 3868.20 4007.97 38.24 o -4 4 0 1315.55 1028.07 17.00 o -3 4 0 9.81 -3.05 5.17 o -2 4 0 5245.88 5007.56 43.86 o -1 4 0 156.34 168.44 10.45 o 0 4 0 15404.86 15733.08 115.23 o 1 4 0 120.29 135.44 6.77 o 2 4 0 4706.40 4645.54 42.44 o 3 4 0 8241.32 8511.91 56.69 o 4 4 0 10704.47 10387.32 67.47 o 5 4 0 7330.87 7259.30 51.01 o 6 4 0 13612.18 13459.36 92.99 o 7 4 0 175.05 146.11 9.98 o 8 4 0 1992.80 1984.18 31.45 o 9 4 0 853.33 891.31 24.80 o 10 4 0 747.51 718.89 19.33 o 11 4 0 325.21 304.63 28.55 o 12 4 0 1032.75 960.75 30.76 o 13 4 0 589.19 650.99 30.18 o 14 4 0 294.73 282.94 29.59 o 15 4 0 1.86 23.71 14.19 o -14 5 0 254.74 225.46 32.07 o -13 5 0 93.65 92.22 16.28 o -12 5 0 821.91 868.05 34.50 o -11 5 0 71.04 68.95 12.30 o -10 5 0 19.13 11.34 8.32 o -9 5 0 2.74 -6.86 6.86 o -8 5 0 1756.59 1650.05 35.16 o -7 5 0 6.59 9.13 5.70 o -6 5 0 4553.32 4571.52 58.55 o -5 5 0 193.75 119.54 8.28 o -4 5 0 1741.55 1649.57 23.46 o -3 5 0 2224.04 2612.05 38.98 o -2 5 0 23050.27 22913.48 151.83 o -1 5 0 93.88 153.54 8.31 o 0 5 0 34043.36 35445.34 243.07 o 1 5 0 151.47 175.06 8.46 o 2 5 0 5189.43 5080.92 48.58 o 3 5 0 85.96 99.72 9.98 o 4 5 0 11146.01 10061.11 67.98 o 5 5 0 209.33 263.56 8.99 o 6 5 0 51.37 53.10 4.82 o 7 5 0 426.57 391.47 11.51 o 8 5 0 2711.25 2673.50 37.84 o 9 5 0 46.13 33.92 7.61 o 10 5 0 408.63 317.14 18.80 o 11 5 0 17.10 20.73 8.89 o 12 5 0 1.11 -0.87 8.83 o 13 5 0 244.52 261.28 24.15 o 14 5 0 597.84 550.39 34.62 o 15 5 0 9.89 27.85 14.90 o -13 6 0 392.20 393.96 30.31 o -12 6 0 467.14 434.78 27.73 o -11 6 0 818.68 856.72 30.08 o -10 6 0 14.79 10.46 9.03 o -9 6 0 60.93 62.86 11.05 o -8 6 0 3922.23 3976.18 58.55 o -7 6 0 1524.12 1460.46 33.18 o -6 6 0 848.78 858.65 19.39 o -5 6 0 432.40 409.85 15.24 o -4 6 0 14.16 11.61 5.34 o -3 6 0 46.79 91.71 8.39 o -2 6 0 1646.28 1215.69 21.80 o -1 6 0 1713.65 1907.19 32.80 o 0 6 0 14719.79 14832.87 106.76 o 1 6 0 1352.19 1367.43 22.80 o 2 6 0 22660.51 23272.91 160.42 o 3 6 0 41.44 58.14 6.07 o 4 6 0 3770.78 3134.97 38.70 o 5 6 0 5308.80 5494.23 45.15 o 6 6 0 4206.30 4297.85 38.34 o 7 6 0 871.36 774.04 16.04 o 8 6 0 393.68 370.50 11.38 o 9 6 0 76.60 90.21 10.07 o 10 6 0 1249.68 1352.50 36.81 o 11 6 0 62.21 52.05 11.17 o 12 6 0 10.52 6.82 9.06 o 13 6 0 58.29 74.41 13.57 o 14 6 0 759.91 760.30 49.72 o 15 6 0 99.40 141.22 31.86 o -13 7 0 1.50 -1.99 14.64 o -12 7 0 17.90 10.63 12.30 o -11 7 0 18.30 17.50 10.74 o -10 7 0 1.33 1.16 8.91 o -9 7 0 1055.50 946.41 29.55 o -8 7 0 39.59 43.90 11.21 o -7 7 0 1427.04 1382.62 40.29 o -6 7 0 1782.10 1846.43 36.34 o -5 7 0 14.19 15.39 6.25 o -4 7 0 5724.92 5998.83 56.22 o -3 7 0 133.37 118.18 10.97 o -2 7 0 4708.95 4717.49 50.19 o -1 7 0 2977.94 2970.64 37.30 o 0 7 0 13494.24 12405.16 96.12 o 1 7 0 1294.50 1286.66 36.16 o 2 7 0 4196.26 3817.86 45.35 o 3 7 0 2158.63 2420.27 34.40 o 4 7 0 150.36 138.11 8.71 o 5 7 0 1969.70 1842.48 26.32 o 6 7 0 2051.54 1984.27 31.26 o 7 7 0 239.34 175.59 8.94 o 8 7 0 656.44 618.87 15.73 o 9 7 0 618.85 618.16 23.99 o 10 7 0 20.69 31.55 8.72 o 11 7 0 14.04 2.92 8.46 o 12 7 0 7.12 11.65 9.88 o 13 7 0 337.49 323.56 27.51 o 14 7 0 973.95 1021.11 43.52 o 15 7 0 127.50 201.47 25.62 o -12 8 0 25.19 17.28 13.94 o -11 8 0 42.05 28.44 12.23 o -10 8 0 275.54 231.53 19.02 o -9 8 0 150.01 166.48 15.97 o -8 8 0 1536.66 1593.88 39.94 o -7 8 0 34.76 25.98 13.08 o -6 8 0 3062.64 2994.07 51.51 o -5 8 0 253.65 228.02 13.50 o -4 8 0 3663.64 3693.06 43.92 o -3 8 0 945.45 908.58 22.80 o -2 8 0 3925.66 4007.68 49.44 o -1 8 0 13.63 14.19 6.44 o 0 8 0 33912.01 34201.57 226.74 o 1 8 0 512.55 425.99 17.00 o 2 8 0 7022.28 6767.81 63.54 o 3 8 0 625.87 775.13 21.29 o 4 8 0 612.12 595.83 16.56 o 5 8 0 429.82 414.46 14.67 o 6 8 0 2010.48 1974.88 28.95 o 7 8 0 57.34 60.20 7.27 o 8 8 0 3309.65 3459.38 45.30 o 9 8 0 527.26 557.76 24.37 o 10 8 0 981.57 979.08 30.89 o 11 8 0 3.15 11.35 8.12 o 12 8 0 137.62 150.24 16.53 o 13 8 0 741.03 705.54 39.59 o 14 8 0 892.75 917.46 43.34 o 15 8 0 36.90 29.79 17.03 o -11 9 0 0.36 -10.71 10.71 o -10 9 0 174.08 201.44 19.40 o -9 9 0 467.97 440.16 24.94 o -8 9 0 1146.93 1171.43 43.15 o -7 9 0 677.12 566.33 36.14 o -6 9 0 6558.73 6432.66 133.92 o -5 9 0 995.29 917.53 26.25 o -4 9 0 1290.39 1275.52 32.89 o -3 9 0 613.34 614.12 32.41 o -2 9 0 6021.55 5965.75 82.58 o -1 9 0 27.82 42.24 8.07 o 0 9 0 5444.32 5437.98 58.91 o 1 9 0 23.05 18.10 6.80 o 2 9 0 6929.89 6924.59 67.49 o 3 9 0 816.45 757.13 22.21 o 4 9 0 4612.13 4885.34 52.69 o 5 9 0 274.43 287.22 14.08 o 6 9 0 1739.52 1813.82 29.57 o 7 9 0 1969.69 1869.13 33.06 o 8 9 0 4773.12 4594.34 71.57 o 9 9 0 493.22 596.52 25.45 o 10 9 0 1420.82 1373.71 36.61 o 11 9 0 180.67 159.13 14.68 o 12 9 0 1199.58 1192.86 43.13 o 13 9 0 57.10 44.43 25.57 o 14 9 0 343.19 313.73 29.24 o 15 9 0 8.53 -10.21 14.27 o -11 10 0 121.65 136.38 20.27 o -10 10 0 225.67 248.97 21.93 o -9 10 0 96.25 107.38 15.80 o -8 10 0 540.21 555.79 30.39 o -7 10 0 7.57 11.92 10.68 o -6 10 0 173.74 180.29 17.46 o -5 10 0 21.96 26.24 9.38 o -4 10 0 1953.37 1982.15 39.96 o -3 10 0 678.75 591.47 21.11 o -2 10 0 3330.59 3449.97 48.66 o -1 10 0 44.41 59.64 9.17 o 0 10 0 1381.49 1499.37 30.38 o 1 10 0 49.95 45.29 8.18 o 2 10 0 6881.35 6680.32 73.69 o 3 10 0 115.92 134.26 12.67 o 4 10 0 4773.11 4928.46 55.50 o 5 10 0 475.38 423.23 17.81 o 6 10 0 2394.39 2419.13 44.32 o 7 10 0 2156.37 2005.30 37.98 o 8 10 0 2629.79 2584.08 60.48 o 9 10 0 155.88 133.99 18.20 o 10 10 0 128.15 180.57 20.99 o 11 10 0 315.83 295.23 30.33 o 12 10 0 485.29 511.76 29.27 o 13 10 0 5.85 6.14 13.91 o 14 10 0 45.67 28.14 18.78 o -10 11 0 500.24 609.03 33.04 o -9 11 0 45.94 24.49 12.65 o -8 11 0 458.23 455.69 29.12 o -7 11 0 573.23 482.77 28.52 o -6 11 0 1.69 2.03 9.98 o -5 11 0 94.33 65.41 19.35 o -4 11 0 1440.26 1442.19 34.20 o -3 11 0 472.99 480.41 20.74 o -2 11 0 4803.95 4960.49 62.86 o -1 11 0 473.90 497.74 27.92 o 0 11 0 1213.10 1160.78 28.58 o 1 11 0 163.11 181.80 14.21 o 2 11 0 5944.59 6246.68 68.78 o 3 11 0 333.24 313.87 19.20 o 4 11 0 1906.50 1729.91 32.73 o 5 11 0 19.42 22.10 7.66 o 6 11 0 4730.42 4487.21 60.12 o 7 11 0 1395.64 1317.04 53.62 o 8 11 0 32.90 43.01 11.39 o 9 11 0 1974.53 1971.10 75.95 o 10 11 0 1.50 6.39 15.19 o 11 11 0 158.65 178.86 22.81 o 12 11 0 303.69 297.65 50.11 o 13 11 0 264.37 279.91 41.82 o 14 11 0 244.56 283.66 61.42 o -9 12 0 89.81 102.43 17.28 o -8 12 0 274.63 272.20 25.00 o -7 12 0 79.48 77.25 15.82 o -6 12 0 692.76 599.65 31.82 o -5 12 0 24.42 28.89 11.89 o -4 12 0 312.02 348.94 21.36 o -3 12 0 750.42 654.48 30.61 o -2 12 0 2695.20 2607.73 53.69 o -1 12 0 216.62 161.93 15.12 o 0 12 0 4687.16 4580.91 61.15 o 1 12 0 193.79 181.05 14.96 o 2 12 0 5136.24 5222.72 64.42 o 3 12 0 609.18 609.19 26.29 o 4 12 0 3075.41 3146.59 52.43 o 5 12 0 0.02 -4.05 7.61 o 6 12 0 4718.37 4629.97 63.77 o 7 12 0 682.09 651.17 36.20 o 8 12 0 2820.07 2836.32 54.84 o 9 12 0 8.76 11.61 12.95 o 10 12 0 44.27 69.17 21.77 o 11 12 0 7.11 -15.75 15.75 o 12 12 0 133.54 197.47 38.06 o 13 12 0 384.17 467.94 45.79 o -8 13 0 250.28 283.58 28.69 o -7 13 0 350.14 313.78 26.50 o -6 13 0 1070.98 1111.54 41.17 o -5 13 0 43.50 85.59 15.77 o -4 13 0 287.17 294.54 28.30 o -3 13 0 158.72 198.50 20.28 o -2 13 0 1874.34 1840.50 36.55 o -1 13 0 429.72 456.63 22.96 o 0 13 0 6542.92 6813.26 80.45 o 1 13 0 3.33 18.09 9.46 o 2 13 0 3671.42 3438.02 58.78 o 3 13 0 22.52 26.15 10.32 o 4 13 0 1367.51 1459.58 48.29 o 5 13 0 447.36 375.76 23.47 o 6 13 0 244.53 281.91 19.55 o 7 13 0 35.42 57.85 13.31 o 8 13 0 734.23 770.35 32.06 o 9 13 0 355.66 348.71 38.89 o 10 13 0 620.67 616.03 50.19 o 11 13 0 9.67 -4.37 18.09 o 12 13 0 13.06 12.31 19.85 o -7 14 0 9.88 -12.89 12.89 o -6 14 0 640.27 637.73 41.58 o -5 14 0 262.52 245.85 37.44 o -4 14 0 770.90 659.13 33.66 o -3 14 0 259.25 256.09 25.39 o -2 14 0 439.26 486.18 28.72 o -1 14 0 221.58 224.53 23.09 o 0 14 0 1986.11 1980.37 47.55 o 1 14 0 155.46 167.21 16.52 o 2 14 0 4621.70 4534.24 73.76 o 3 14 0 119.10 158.74 17.24 o 4 14 0 893.08 966.73 47.19 o 5 14 0 235.43 225.47 19.07 o 6 14 0 712.39 669.33 32.34 o 7 14 0 106.47 104.76 19.83 o 8 14 0 563.12 621.92 40.02 o 9 14 0 8.55 34.95 25.62 o 10 14 0 320.28 420.40 55.01 o 11 14 0 0.26 -17.03 17.03 o 12 14 0 113.76 114.98 56.52 o -5 15 0 17.30 -0.44 15.19 o -4 15 0 1829.16 1671.84 57.00 o -3 15 0 24.95 11.39 16.86 o -2 15 0 1416.16 1466.50 45.19 o -1 15 0 390.13 433.33 28.67 o 0 15 0 1203.41 1128.42 36.93 o 1 15 0 50.07 87.33 14.12 o 2 15 0 878.78 846.59 36.96 o 3 15 0 248.34 344.53 25.01 o 4 15 0 373.41 360.67 24.35 o 5 15 0 23.16 43.43 17.98 o 6 15 0 325.69 423.01 35.48 o 7 15 0 1.10 8.21 13.59 o 8 15 0 794.83 884.18 74.12 o 9 15 0 50.35 80.40 27.16 o 10 15 0 566.18 633.45 55.13 o 11 15 0 0.31 3.79 22.07 o -4 16 0 829.30 797.30 96.46 o -3 16 0 10.05 28.56 18.27 o -2 16 0 423.27 420.68 34.17 o -1 16 0 20.61 1.33 11.83 o 0 16 0 1157.71 1130.78 41.36 o 1 16 0 151.32 226.75 36.18 o 2 16 0 871.44 929.10 46.56 o 3 16 0 45.06 42.47 16.76 o 4 16 0 1477.31 1500.75 49.90 o 5 16 0 24.98 33.78 17.94 o 6 16 0 1476.62 1451.63 71.63 o 7 16 0 510.47 562.67 59.21 o 8 16 0 415.46 444.28 56.74 o 9 16 0 205.88 207.92 49.74 o -1 17 0 64.28 77.98 19.81 o 0 17 0 489.48 570.49 37.08 o 1 17 0 169.61 153.83 23.32 o 2 17 0 1432.28 1366.21 57.87 o 3 17 0 44.16 35.19 17.30 o 4 17 0 2436.20 2433.86 76.55 o 5 17 0 12.33 33.94 33.40 o 6 17 0 2284.68 2475.79 76.81 o 7 17 0 163.88 190.59 29.17 o -6 -17 1 9.41 5.87 17.26 o -5 -17 1 788.36 801.37 59.04 o -4 -17 1 485.38 435.41 39.89 o -3 -17 1 1012.91 1180.99 50.47 o -2 -17 1 13.36 0.05 15.02 o -1 -17 1 1198.04 1206.09 50.19 o 0 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